CN115645306A - Hair care product for enlarging, softening, fluffing and improving glossiness of hair and preparation method thereof - Google Patents
Hair care product for enlarging, softening, fluffing and improving glossiness of hair and preparation method thereof Download PDFInfo
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- 210000004209 hair Anatomy 0.000 title claims abstract description 100
- 238000002360 preparation method Methods 0.000 title description 33
- 240000004307 Citrus medica Species 0.000 claims abstract description 63
- 229920001661 Chitosan Polymers 0.000 claims abstract description 51
- 230000002195 synergetic effect Effects 0.000 claims abstract description 36
- 229940057070 sugarcane extract Drugs 0.000 claims abstract description 25
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 19
- VFKZECOCJCGZQK-UHFFFAOYSA-M 3-hydroxypropyl(trimethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCCO VFKZECOCJCGZQK-UHFFFAOYSA-M 0.000 claims abstract description 11
- 229920002907 Guar gum Polymers 0.000 claims abstract description 11
- 229920000688 Poly[(2-ethyldimethylammonioethyl methacrylate ethyl sulfate)-co-(1-vinylpyrrolidone)] Polymers 0.000 claims abstract description 11
- 239000004359 castor oil Substances 0.000 claims abstract description 11
- 235000019438 castor oil Nutrition 0.000 claims abstract description 11
- 229920001577 copolymer Polymers 0.000 claims abstract description 11
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims abstract description 11
- 235000010417 guar gum Nutrition 0.000 claims abstract description 11
- 239000000665 guar gum Substances 0.000 claims abstract description 11
- 229960002154 guar gum Drugs 0.000 claims abstract description 11
- CXMXRPHRNRROMY-UHFFFAOYSA-N n-Decanedioic acid Natural products OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229920002635 polyurethane Polymers 0.000 claims abstract description 11
- 239000004814 polyurethane Substances 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 38
- 238000003756 stirring Methods 0.000 claims description 35
- 238000002156 mixing Methods 0.000 claims description 34
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 28
- 108090000790 Enzymes Proteins 0.000 claims description 21
- 102000004190 Enzymes Human genes 0.000 claims description 21
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 21
- 229940088598 enzyme Drugs 0.000 claims description 21
- 238000001914 filtration Methods 0.000 claims description 21
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 17
- 239000008367 deionised water Substances 0.000 claims description 17
- 229910021641 deionized water Inorganic materials 0.000 claims description 17
- 235000010413 sodium alginate Nutrition 0.000 claims description 17
- 239000000661 sodium alginate Substances 0.000 claims description 17
- 229940005550 sodium alginate Drugs 0.000 claims description 17
- 240000000111 Saccharum officinarum Species 0.000 claims description 14
- 235000007201 Saccharum officinarum Nutrition 0.000 claims description 14
- 238000009210 therapy by ultrasound Methods 0.000 claims description 14
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 12
- 229910021389 graphene Inorganic materials 0.000 claims description 12
- 230000000694 effects Effects 0.000 claims description 8
- 125000002349 hydroxyamino group Chemical group [H]ON([H])[*] 0.000 claims description 8
- 108010059892 Cellulase Proteins 0.000 claims description 7
- 108010059820 Polygalacturonase Proteins 0.000 claims description 7
- 229940106157 cellulase Drugs 0.000 claims description 7
- 238000013329 compounding Methods 0.000 claims description 7
- 108010093305 exopolygalacturonase Proteins 0.000 claims description 7
- 230000000415 inactivating effect Effects 0.000 claims description 7
- 238000005360 mashing Methods 0.000 claims description 7
- 238000004537 pulping Methods 0.000 claims description 7
- 238000005406 washing Methods 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 4
- 239000003607 modifier Substances 0.000 claims description 3
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- 235000001938 Citrus medica Nutrition 0.000 claims 1
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- 244000303965 Cyamopsis psoralioides Species 0.000 abstract description 2
- 125000002091 cationic group Chemical group 0.000 abstract description 2
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- 230000003648 hair appearance Effects 0.000 description 1
- 230000037308 hair color Effects 0.000 description 1
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Abstract
The invention discloses a hair care product for enlarging, softening, fluffing and improving the brightness of hair, which comprises the following raw materials in parts by weight: 10-20 parts of polyquaternium-52, 5-10 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 3-5 parts of polyurethane, 2-6 parts of biogum, 1-4 parts of hydrogenated castor oil/sebacic acid copolymer, 1-3 parts of polyquaternium-11, 2-6 parts of sugarcane extract, 3-5 parts of citron fruit peel extract and 5-10 parts of chitosan synergistic improver. The cationic guar conditioning and repairing components deposit on the hair in a proper amount, the hair is not thick and heavy, is fluffy, is light in a formula technical system, has clear texture and light use feeling, forms a light wrapping layer on the hair, increases the diameter of the hair, enhances the fullness of the hair, can make the surface of the hair smooth and flat, and improves the brightness of the hair.
Description
Technical Field
The invention relates to the technical field of hair care, in particular to a hair care product for plump, thin and soft hair, fluffy hair and improving glossiness and a preparation method thereof.
Background
Hair, which refers to hair growing on the head. Hair is not an organ and therefore does not contain nerves and blood vessels, but contains cells. Hair is mainly used for protecting the head. The soft and fluffy hair has elasticity, can resist light collision and can help the evaporation of sweat on the head. Generally, there are about 10 ten thousand hairs of a human, and the length of the hair is the longest in all hairs, especially in women who leave their hair. Some can be as long as 95 to 100cm, even 150cm, but generally can not exceed 200cm.
The existing hair care product can not improve the brightness of hair, has poor flexibility and softness effect, and needs further improvement treatment, so that the invention provides the hair care product with the functions of photothermal protection and hair color protection.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a hair care product for plumping, thinning and softening hair, relaxing hair and improving the brightness and a preparation method thereof so as to solve the problems in the background technology.
The technical scheme adopted by the invention for solving the technical problems is as follows:
the invention provides a hair care product for plumping, softening and fluffing hair and improving glossiness, which comprises the following raw materials in parts by weight:
10-20 parts of polyquaternium-52, 5-10 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 3-5 parts of polyurethane, 2-6 parts of biogum, 1-4 parts of hydrogenated castor oil/sebacic acid copolymer, 1-3 parts of polyquaternium-11, 2-6 parts of sugarcane extract, 3-5 parts of citron fruit peel extract, 5-10 parts of chitosan synergistic improver and 5-10 parts of deionized water.
Preferably, the hair care product comprises the following raw materials in parts by weight:
the composition comprises, by weight, 52 parts of polyquaternium-52 parts, 7.5 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 4 parts of polyurethane, 2 parts of biogum-2 parts, 2.5 parts of hydrogenated castor oil/sebacic acid copolymer, 2 parts of polyquaternium-11 parts, 4 parts of sugarcane extract, 4 parts of citron fruit peel extract, 7.5 parts of chitosan synergistic improver and 7.5 parts of deionized water.
Preferably, the preparation method of the sugarcane extract comprises the following steps:
s01: adding sugarcane into 2-3 times of water, mixing, pulping, adding complex enzyme 5-10% of the total amount of sugarcane, performing enzymolysis at 30-32 deg.C for 20-30 hr, and finishing enzymolysis;
s02: inactivating enzyme, adding into 3-6 times of water, extracting with slow fire for 1-2 hr, and filtering to obtain caulis Sacchari sinensis extract.
Preferably, the complex enzyme is prepared by compounding cellulase and pectinase according to the weight ratio of 3:1.
Preferably, the preparation method of the citron fruit peel extract comprises the following steps:
mashing citron pericarp, adding the mashed citron pericarp into sodium alginate solution of which the amount is 2-5 times that of the citron pericarp, stirring uniformly, adding 2-5% of hydroxy amino acid of the total amount of the citron pericarp, continuously stirring and mixing fully, washing with water, filtering to obtain filter residue, placing the filter residue into ethanol solution for ultrasonic treatment, finally decocting with slow fire for 1-2 hours, and filtering to obtain the citron pericarp extract.
Preferably, the mass fraction of the sodium alginate solution is 10-15%.
Preferably, the mass fraction of the ethanol solution is 90-95%.
Preferably, the power of the ultrasonic treatment is 100-500W, and the ultrasonic time is 20-30min.
Preferably, the preparation method of the chitosan synergistic improver comprises the following steps: adding chitosan into deionized water according to a weight ratio of 1:5, then adding citric acid, adjusting the pH to 5.0, then adding graphene accounting for 5-10% of the total amount of the chitosan, and fully stirring and mixing to obtain the chitosan synergistic improver.
The inventor finds that the product of the invention is not added with citron fruit peel extract and sugarcane extract, the glossiness and the elasticity rate of the product have the trend of deterioration, and the chitosan synergistic effect improver is not added, so that the performance of the product is more remarkably deteriorated, and meanwhile, the citron fruit peel extract and the sugarcane extract in the product can be synergistically combined with the chitosan synergistic effect improver to jointly improve and optimize the performance of the product;
in addition, the inventor of the invention also finds that the performance of the product is poor because no hydroxy amino acid is added and no sodium alginate solution is adopted for treatment in the preparation of the citron fruit peel extract, the performance of the product is improved most obviously only because the chitosan synergistic improver prepared by the method of the invention is adopted, in addition, no graphene is added in the preparation of the chitosan synergistic improver, the performance of the product is obviously poor, and the addition of the graphene has an obvious effect on the hair improving effect of the product.
The invention also provides a preparation method of the hair care product for enlarging, softening, fluffing and relaxing the hair and improving the brightness, which comprises the following steps: sequentially adding the raw materials into a stirrer, stirring and mixing for 30-50min at a mixing speed of 650-750r/min, and finishing stirring to obtain the hair care product.
Compared with the prior art, the invention has the following beneficial effects:
the cationic guar conditioning and repairing ingredients deposit on the hairline in a proper amount, the hairline is not thick and heavy, the hair is more fluffy, the hairline is light, the texture is clear, the use feeling is light, a light wrapping layer is formed on the hairline, the diameter of the hairline is increased, the fullness of the hairline is enhanced, the surface of the hairline is smooth and flat, the brightness of the hair is improved, the fullness of the hairline of the product is improved by the cooperation of the sugarcane extract and the citron fruit peel extract, and meanwhile, the cooperation effect between the sugarcane extract and the citron fruit peel extract is enhanced by the cooperation of the chitosan cooperation effect-improving agent, so that the combination effect between the raw materials is improved, and the brightness of the hair and the quality of the hairline are obviously improved.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below with reference to specific embodiments, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The hair care product for enlarging, softening and fluffing hair and improving glossiness of the hair comprises the following raw materials in parts by weight:
10-20 parts of polyquaternium-52, 5-10 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 3-5 parts of polyurethane, 2-6 parts of biogum-2, 1-4 parts of hydrogenated castor oil/sebacic acid copolymer, 1-3 parts of polyquaternium-11, 2-6 parts of sugarcane extract, 3-5 parts of citron fruit peel extract, 5-10 parts of chitosan synergistic improver and 5-10 parts of deionized water.
The hair care product comprises the following raw materials in parts by weight:
the composition comprises, by weight, 52 parts of polyquaternium-52 parts, 7.5 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 4 parts of polyurethane, 2 parts of biogum-2 parts, 2.5 parts of hydrogenated castor oil/sebacic acid copolymer, 2 parts of polyquaternium-11 parts, 4 parts of sugarcane extract, 4 parts of citron fruit peel extract, 7.5 parts of chitosan synergistic improver and 7.5 parts of deionized water.
The preparation method of the sugarcane extract comprises the following steps:
s01: adding sugarcane into 2-3 times of water, mixing, pulping, adding complex enzyme 5-10% of the total amount of sugarcane, performing enzymolysis at 30-32 deg.C for 20-30 hr, and finishing enzymolysis;
s02: inactivating enzyme, adding into 3-6 times of water, extracting with slow fire for 1-2 hr, and filtering to obtain caulis Sacchari sinensis extract.
The complex enzyme of the embodiment is prepared by compounding cellulase and pectinase according to the weight ratio of 3:1.
The preparation steps of the citron pericarp extract of this example are:
mashing citron pericarp, then adding the mashed citron pericarp into sodium alginate solution 2-5 times of the mashed citron pericarp, stirring uniformly, then adding 2-5% of hydroxy amino acid of the total weight of the citron pericarp, continuously stirring and mixing fully, finally washing with water, filtering to obtain filter residue, placing the filter residue into ethanol solution for ultrasonic treatment, finally decocting with slow fire for 1-2h, and filtering to obtain the citron pericarp extract.
The mass fraction of the sodium alginate solution in the embodiment is 10-15%.
The mass fraction of the ethanol solution in this example is 90-95%.
The ultrasonic treatment power of the embodiment is 100-500W, and the ultrasonic time is 20-30min.
The preparation method of the chitosan synergistic improver comprises the following steps: adding chitosan into deionized water according to a weight ratio of 1:5, then adding citric acid, adjusting the pH to 5.0, then adding graphene accounting for 5-10% of the total amount of the chitosan, and fully stirring and mixing to obtain the chitosan synergistic improver.
The preparation method of the hair care product for increasing the brightness of voluminous, thin, soft and fluffy hair of the hair comprises the following steps: sequentially adding the raw materials into a stirrer, stirring and mixing for 30-50min at a mixing speed of 650-750r/min, and finishing stirring to obtain the hair care product.
Example 1.
The hair care product for increasing the brightness of voluminous, thin, soft and fluffy hair comprises the following raw materials in parts by weight:
the bio-sugar-free chitosan synergistic modifier comprises, by weight, 52 parts of polyquaternium-52 parts, 5 parts of guar gum hydroxypropyl trimethylammonium chloride, 3 parts of polyurethane, 2 parts of biogum-2 parts, 1 part of hydrogenated castor oil/sebacic acid copolymer, 1 part of polyquaternium-11 parts, 2 parts of sugarcane extract, 3 parts of citron fruit peel extract, 5 parts of chitosan synergistic modifier and 5 parts of deionized water.
The preparation method of the sugarcane extract comprises the following steps:
s01: adding sugarcane into 2 times of water, mixing, pulping, adding a complex enzyme accounting for 5% of the total weight of the sugarcane, performing enzymolysis at 30 ℃ for 20h, and finishing enzymolysis;
s02: inactivating enzyme, adding into 3 times of water, extracting with slow fire for 1 hr, and filtering to obtain caulis Sacchari sinensis extract.
The complex enzyme of the embodiment is prepared by compounding cellulase and pectinase according to the weight ratio of 3:1.
The preparation steps of the citron pericarp extract of this example are:
mashing citron pericarp, adding the mashed citron pericarp into a sodium alginate solution of which the weight is 2 times that of the citron pericarp, stirring uniformly, adding 2% of hydroxy amino acid of the total weight of the citron pericarp, continuously stirring and mixing fully, washing with water, filtering to obtain filter residue, placing the filter residue into an ethanol solution for ultrasonic treatment, decocting with slow fire for 1h, and filtering after the decoction is finished to obtain the citron pericarp extract.
The mass fraction of the sodium alginate solution in this example was 10%.
The mass fraction of the ethanol solution in this example was 90%.
The power of the ultrasonic treatment in this example was 100W, and the ultrasonic time was 20min.
The preparation method of the chitosan synergistic improver comprises the following steps: adding chitosan into deionized water according to a weight ratio of 1:5, then adding citric acid, adjusting the pH to 5.0, then adding graphene accounting for 5% of the total amount of the chitosan, and fully stirring and mixing to obtain the chitosan synergistic improver.
The preparation method of the hair care product for increasing the brightness of voluminous, thin, soft and fluffy hair of the hair comprises the following steps: sequentially adding the raw materials into a stirrer, stirring and mixing for 30min at the rotation speed of 650r/min, and finishing stirring to obtain the hair care product.
Example 2.
The hair care product for increasing the brightness of voluminous, thin, soft and fluffy hair comprises the following raw materials in parts by weight:
20 parts of polyquaternium-52 parts, 10 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 5 parts of polyurethane, 2 parts of biogum, 4 parts of hydrogenated castor oil/sebacic acid copolymer, 3 parts of polyquaternium-11 parts, 6 parts of sugarcane extract, 5 parts of citron fruit peel extract, 10 parts of chitosan synergistic improver and 10 parts of deionized water.
The preparation method of the sugarcane extract comprises the following steps:
s01: adding sugarcane into 3 times of water, mixing, pulping, adding 10% of compound enzyme of the total amount of the sugarcane, performing enzymolysis at 32 ℃ for 30h, and finishing enzymolysis;
s02: inactivating enzyme, adding 6 times of water, extracting with slow fire for 2 hr, and filtering to obtain caulis Sacchari sinensis extract.
The complex enzyme of the embodiment is prepared by compounding cellulase and pectinase according to the weight ratio of 3:1.
The preparation steps of the citron pericarp extract of this example are:
mashing citron pericarp, then adding the mashed citron pericarp into 5 times of sodium alginate solution, stirring uniformly, then adding 5% of hydroxyl amino acid of the citron pericarp total amount, continuing stirring and mixing fully, finally washing with water, filtering to obtain filter residue, placing the filter residue into ethanol solution for ultrasonic treatment, finally decocting with slow fire for 2 hours, and after the decoction, filtering to obtain the citron pericarp extract.
The mass fraction of the sodium alginate solution in this example was 15%.
The mass fraction of the ethanol solution in this example was 95%.
The power of the ultrasonic treatment in this embodiment is 500W, and the ultrasonic time is 30min.
The preparation method of the chitosan synergistic improver comprises the following steps: adding chitosan into deionized water according to a weight ratio of 1:5, then adding citric acid, adjusting the pH to 5.0, then adding graphene accounting for 10% of the total amount of the chitosan, and fully stirring and mixing to obtain the chitosan synergistic improver.
The preparation method of the hair care product for increasing the brightness of voluminous, thin, soft and fluffy hair of the hair comprises the following steps: and sequentially adding the raw materials into a stirrer, stirring and mixing for 50min at the mixing speed of 750r/min, and finishing stirring to obtain the hair care product.
Example 3.
The hair care product for increasing the brightness of voluminous, thin, soft and fluffy hair comprises the following raw materials in parts by weight:
the composition comprises, by weight, 52 parts of polyquaternium-52 parts, 7.5 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 4 parts of polyurethane, 2 parts of biogum-2 parts, 2.5 parts of hydrogenated castor oil/sebacic acid copolymer, 2 parts of polyquaternium-11 parts, 4 parts of sugarcane extract, 4 parts of citron fruit peel extract, 7.5 parts of chitosan synergistic improver and 7.5 parts of deionized water.
The preparation method of the sugarcane extract comprises the following steps:
s01: adding sugarcane into 2.5 times of water, mixing, pulping, adding complex enzyme accounting for 7.5% of the total amount of the sugarcane, performing enzymolysis at 31 ℃ for 25h, and finishing enzymolysis;
s02: inactivating enzyme, adding into 4.5 times of water, extracting with slow fire for 1.5 hr, and filtering to obtain caulis Sacchari sinensis extract.
The complex enzyme of the embodiment is prepared by compounding cellulase and pectinase according to the weight ratio of 3:1.
The preparation steps of the citron pericarp extract of this example are:
mashing citron pericarp, adding the mashed citron pericarp into a sodium alginate solution with the weight being 3.5 times that of the citron pericarp, stirring uniformly, adding hydroxy amino acid accounting for 3.5 percent of the total weight of the citron pericarp, continuously stirring and mixing fully, washing with water, filtering to obtain filter residue, placing the filter residue into an ethanol solution for ultrasonic treatment, finally decocting with slow fire for 1.5h, and filtering to obtain the citron pericarp extract.
The mass fraction of the sodium alginate solution in this example was 12.5%.
The mass fraction of the ethanol solution in this example was 92.5%.
The power of the ultrasonic treatment in this example was 300W, and the ultrasonic time was 25min.
The preparation method of the chitosan synergistic improver comprises the following steps: adding chitosan into deionized water according to a weight ratio of 1:5, then adding citric acid, adjusting the pH to 5.0, then adding graphene accounting for 7.5% of the total amount of the chitosan, and fully stirring and mixing to obtain the chitosan synergistic improver.
The preparation method of the hair care product for plumping, softening and fluffing hair and improving glossiness of the hair provided by the embodiment comprises the following steps of: and sequentially adding the raw materials into a stirrer, stirring and mixing for 40min at the mixing speed of 700r/min, and finishing stirring to obtain the hair care product.
Example 4.
The hair care product for increasing the brightness of voluminous, thin, soft and fluffy hair comprises the following raw materials in parts by weight:
52 parts of polyquaternium-52 parts, 6 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 3 parts of polyurethane, 2 parts of biogum carbohydrate gum, 2 parts of hydrogenated castor oil/sebacic acid copolymer, 2 parts of polyquaternium-11 parts, 3 parts of sugarcane extract, 4 parts of citron fruit peel extract, 6 parts of chitosan synergistic improver and 6 parts of deionized water.
The preparation method of the sugarcane extract comprises the following steps:
s01: adding sugarcane into 2 times of water, mixing and pulping, then adding complex enzyme accounting for 6% of the total amount of the sugarcane to perform enzymolysis treatment, wherein the enzymolysis temperature is 31 ℃, the enzymolysis time is 22 hours, and the enzymolysis is finished;
s02: inactivating enzyme, adding into 4 times of water, extracting with slow fire for 1.2 hr, and filtering to obtain caulis Sacchari sinensis extract.
The complex enzyme of the embodiment is prepared by compounding cellulase and pectinase according to the weight ratio of 3:1.
The preparation steps of the citron pericarp extract of this example are:
mashing citron pericarp, then adding the mashed citron pericarp into a sodium alginate solution in an amount which is 3 times that of the mashed citron pericarp, stirring uniformly, then adding 3% of hydroxy amino acid of the citron pericarp total amount, continuously stirring and mixing fully, finally washing with water, filtering to obtain filter residue, placing the filter residue into an ethanol solution for ultrasonic treatment, finally decocting with slow fire for 1.2h, and filtering after the decoction is finished to obtain the citron pericarp extract.
The mass fraction of the sodium alginate solution in this example was 12%.
The mass fraction of the ethanol solution in this example was 92%.
The power of the ultrasonic treatment in this example was 200W, and the ultrasonic time was 22min.
The preparation method of the chitosan synergistic improver comprises the following steps: adding chitosan into deionized water according to a weight ratio of 1:5, then adding citric acid, adjusting the pH to 5.0, then adding graphene accounting for 6% of the total amount of the chitosan, and fully stirring and mixing to obtain the chitosan synergistic improver.
The preparation method of the hair care product for plumping, softening and fluffing hair and improving glossiness of the hair provided by the embodiment comprises the following steps of: and sequentially adding the raw materials into a stirrer, stirring and mixing for 35min at the mixing speed of 660r/min, and finishing stirring to obtain the hair care product.
Comparative example 1.
Unlike example 3, citron pericarp extract was not added.
Comparative example 2.
In contrast to example 3, no sugar cane extract was added.
Comparative example 3.
Different from example 3, the citron pericarp extract was prepared without adding hydroxy amino acid.
Comparative example 4.
Unlike example 3, the citron pericarp extract was prepared without treatment with sodium alginate solution.
Comparative example 5.
The difference from the example 3 is that no chitosan synergistic improver is added.
Comparative example 6.
The difference from the example 3 is that no graphene is added in the preparation of the chitosan synergistic improver.
Taking female volunteers which are healthy, have the same hair quality and are 30-40 years old, wherein the hair lengths of the female volunteers are within the range of 20-25CM, randomly dividing the volunteers into 9 groups, carrying out hair care treatment on the 9 groups of volunteers by using the hair care products prepared in the examples 1-3 and the comparative examples 1-6 according to the numbering sequence, testing the glossiness and the elasticity rate of the hair care products 1 time per night after 7 days, and measuring the glossiness data by using a glossmeter through an incident angle of 85 degrees, wherein the results are as follows;
the performance of the products of examples 1-3 and comparative examples 1-6 was tested as follows:
as can be seen from comparative examples 1-6 and examples 1-3;
the product of the invention is not added with citron fruit peel extract and sugarcane extract, the glossiness and the elasticity rate of the product have the trend of deterioration, and simultaneously, chitosan synergistic improver is not added, the performance deterioration of the product is more obvious, and the citron fruit peel extract and the sugarcane extract in the product can be synergistically combined with the chitosan synergistic improver to jointly improve and optimize the performance of the product;
in addition, hydroxyl amino acid is not added in the preparation of the citron fruit peel extract, sodium alginate solution is not adopted for treatment, the performance of the product is poor, only the chitosan synergistic improver prepared by the method is most obviously improved on the performance of the product, in addition, graphene is not added in the preparation of the chitosan synergistic improver, the performance of the product is obviously deteriorated, and the addition of the graphene has an obvious effect on the hair improving effect of the product.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
Claims (10)
1. A hair care product for plumping, softening, fluffing and improving the brightness of hair is characterized by comprising the following raw materials in parts by weight:
10-20 parts of polyquaternium-52, 5-10 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 3-5 parts of polyurethane, 2-6 parts of biogum, 1-4 parts of hydrogenated castor oil/sebacic acid copolymer, 1-3 parts of polyquaternium-11, 2-6 parts of sugarcane extract, 3-5 parts of citron fruit peel extract, 5-10 parts of chitosan synergistic improver and 5-10 parts of deionized water.
2. The hair care product for achieving the effects of enlarging, softening and relaxing hair and improving the glossiness according to claim 1, wherein the hair care product comprises the following raw materials in parts by weight:
the composition comprises, by weight, 52 parts of polyquaternium-52 parts, 7.5 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 4 parts of polyurethane, 2 parts of biogum-2 parts, 2.5 parts of hydrogenated castor oil/sebacic acid copolymer, 2 parts of polyquaternium-11 parts, 4 parts of sugarcane extract, 4 parts of citron fruit peel extract, 7.5 parts of chitosan synergistic improver and 7.5 parts of deionized water.
3. The hair care product for enhancing the brightness of voluminous, thin, soft and fluffy hair according to claim 1, wherein the sugar cane extract is prepared by:
s01: adding sugarcane into 2-3 times of water, mixing, pulping, adding complex enzyme accounting for 5-10% of the total weight of the sugarcane, performing enzymolysis at 30-32 deg.C for 20-30h, and finishing enzymolysis;
s02: inactivating enzyme, adding into 3-6 times of water, extracting with slow fire for 1-2 hr, and filtering to obtain caulis Sacchari sinensis extract.
4. The hair care product for improving the brightness of the voluminous, thin, soft and fluffy hair according to claim 3, wherein the complex enzyme is prepared by compounding cellulase and pectinase according to a weight ratio of 3:1.
5. The hair care product of claim 1, wherein the citrus medica pericarp extract is prepared by the steps of:
mashing citron pericarp, adding the mashed citron pericarp into sodium alginate solution of which the amount is 2-5 times that of the citron pericarp, stirring uniformly, adding 2-5% of hydroxy amino acid of the total amount of the citron pericarp, continuously stirring and mixing fully, washing with water, filtering to obtain filter residue, placing the filter residue into ethanol solution for ultrasonic treatment, finally decocting with slow fire for 1-2 hours, and filtering to obtain the citron pericarp extract.
6. The hair care product for enhancing the brightness of the voluminous, thin, soft and fluffy hair according to claim 5, wherein the mass fraction of the sodium alginate solution is 10-15%.
7. A hair care product for providing volume, fineness, softness, and volume to the hair, and improving shine according to claim 5, wherein the ethanol solution is present in an amount of 90-95% by weight.
8. A hair care product for providing volume, fineness, softness, and volume to the hair, and improving shine according to claim 5, wherein the power of the ultrasonic treatment is 100-500W, and the ultrasonic time is 20-30min.
9. The hair care product for enhancing the brightness of the voluminous, thin, soft and fluffy hair according to claim 1, wherein the chitosan synergistic effect modifier is prepared by: adding chitosan into deionized water according to a weight ratio of 1:5, then adding citric acid, adjusting the pH to 5.0, then adding graphene accounting for 5-10% of the total amount of the chitosan, and fully stirring and mixing to obtain the chitosan synergistic improver.
10. A process for preparing a hair care product for providing enhanced shine to voluminous, thin, soft, fluffy hair according to any of claims 1-9, comprising the steps of: sequentially adding the raw materials into a stirrer, stirring and mixing for 30-50min at a mixing speed of 650-750r/min, and finishing stirring to obtain the hair care product.
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| Application Number | Priority Date | Filing Date | Title |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116135201A (en) * | 2023-04-04 | 2023-05-19 | 广州美思生物技术有限公司 | Washing and caring product for improving hair drying speed and fluffiness after washing and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116135201A (en) * | 2023-04-04 | 2023-05-19 | 广州美思生物技术有限公司 | Washing and caring product for improving hair drying speed and fluffiness after washing and preparation method thereof |
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Application publication date: 20230131 |