CN115501147A - Oil-control anti-dandruff non-antiseptic natural plant shampoo powder and preparation method thereof - Google Patents
Oil-control anti-dandruff non-antiseptic natural plant shampoo powder and preparation method thereof Download PDFInfo
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- 239000000843 powder Substances 0.000 title claims abstract description 58
- 239000002453 shampoo Substances 0.000 title claims abstract description 43
- 208000001840 Dandruff Diseases 0.000 title claims abstract description 35
- 230000002421 anti-septic effect Effects 0.000 title claims abstract description 11
- 238000002360 preparation method Methods 0.000 title claims description 25
- 239000000440 bentonite Substances 0.000 claims abstract description 50
- 229910000278 bentonite Inorganic materials 0.000 claims abstract description 50
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims abstract description 50
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 44
- 239000002041 carbon nanotube Substances 0.000 claims abstract description 44
- 229910021393 carbon nanotube Inorganic materials 0.000 claims abstract description 44
- 241000196324 Embryophyta Species 0.000 claims abstract description 40
- 239000000654 additive Substances 0.000 claims abstract description 40
- 230000000996 additive effect Effects 0.000 claims abstract description 38
- 238000000605 extraction Methods 0.000 claims abstract description 30
- 238000001035 drying Methods 0.000 claims abstract description 16
- 244000130592 Hibiscus syriacus Species 0.000 claims abstract description 15
- 235000018081 Hibiscus syriacus Nutrition 0.000 claims abstract description 15
- 239000002994 raw material Substances 0.000 claims abstract description 14
- 241001489091 Ganoderma sinense Species 0.000 claims abstract description 13
- 235000002789 Panax ginseng Nutrition 0.000 claims abstract description 11
- 241001289529 Fallopia multiflora Species 0.000 claims abstract description 10
- 240000003377 Shepherdia canadensis Species 0.000 claims abstract description 6
- 235000018324 Shepherdia canadensis Nutrition 0.000 claims abstract description 6
- 244000269722 Thea sinensis Species 0.000 claims abstract 4
- 238000003756 stirring Methods 0.000 claims description 55
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 27
- 238000002156 mixing Methods 0.000 claims description 24
- 238000005406 washing Methods 0.000 claims description 23
- 239000012747 synergistic agent Substances 0.000 claims description 22
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 21
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- 239000006087 Silane Coupling Agent Substances 0.000 claims description 20
- 239000003607 modifier Substances 0.000 claims description 15
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 14
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- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 14
- 239000002131 composite material Substances 0.000 claims description 14
- 235000010413 sodium alginate Nutrition 0.000 claims description 14
- 229940005550 sodium alginate Drugs 0.000 claims description 14
- 239000000661 sodium alginate Substances 0.000 claims description 14
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- 238000005260 corrosion Methods 0.000 claims description 11
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- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 7
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 7
- 238000001354 calcination Methods 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 7
- 239000008367 deionised water Substances 0.000 claims description 7
- 229910021641 deionized water Inorganic materials 0.000 claims description 7
- 235000008434 ginseng Nutrition 0.000 claims description 7
- VQEHIYWBGOJJDM-UHFFFAOYSA-H lanthanum(3+);trisulfate Chemical compound [La+3].[La+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O VQEHIYWBGOJJDM-UHFFFAOYSA-H 0.000 claims description 7
- 238000000643 oven drying Methods 0.000 claims description 7
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- 238000005536 corrosion prevention Methods 0.000 claims 2
- 244000284380 Hibiscus rosa sinensis Species 0.000 claims 1
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- 229940075285 dandruff control Drugs 0.000 claims 1
- 235000013399 edible fruits Nutrition 0.000 claims 1
- 239000012467 final product Substances 0.000 claims 1
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- 238000005516 engineering process Methods 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 2
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- 239000000853 adhesive Substances 0.000 description 2
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- A61K8/9783—Angiosperms [Magnoliophyta]
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Abstract
The invention discloses oil-control, anti-dandruff and non-antiseptic natural plant shampoo powder which comprises the following raw materials in parts by weight: 45-55 parts of gleditschia horrida, 10-20 parts of soapberry, 5-10 parts of shrubalthea, 3-6 parts of tea seed, 2-6 parts of cacumen biotae, 2-5 parts of polygonum multiflorum, 1-5 parts of ganoderma sinensis, 1-5 parts of red ginseng, 3-6 parts of carbon nano tube modified additive and 2-4 parts of bentonite synergist. The eight herbal plants are matched and combined according to the proportion, and then the natural plant shampoo powder is obtained through the extraction and drying technology, the advantages of no other chemical additives in the pure herbal plant raw materials, safety, naturalness and health are realized, the antifogging agent is not required to be added, the anti-dandruff and oil-control effects are realized, the powder shampoo product is more convenient to carry, and the anti-dandruff and oil-control effects of the shampoo powder are enhanced through the synergistic coordination and synergy of the carbon nano tube modified additive and the bentonite synergist.
Description
Technical Field
The invention relates to the technical field of hair washing, in particular to oil-control, anti-dandruff and non-antiseptic natural plant shampoo powder and a preparation method thereof.
Background
Hair, which refers to hair growing on the head. Hair is not an organ and therefore does not contain nerves and blood vessels, but contains cells. Hair is mainly used for protecting the head. The soft and fluffy hair has elasticity, can resist light collision and can help the evaporation of head sweat. Generally, about 10 ten thousand hairs of a person exist, and the length of the hairs is the longest among all hairs, especially for women who have long hairs. Some can be as long as 95 to 100cm, even 150cm, but generally can not exceed 200cm. The color of hair is generally determined by genes, and is usually black, golden, brown, red, and the like. As humans age, hair often becomes silvery white.
The existing shampoo powder has simple raw material composition and poor efficiency of removing dandruff and controlling oil, and needs further improvement and optimization treatment.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide natural plant shampoo powder for controlling oil, removing dandruff and preventing corrosion and a preparation method thereof, so as to solve the problems in the background technology.
The technical scheme adopted by the invention for solving the technical problems is as follows:
the invention provides oil-control, anti-dandruff and non-antiseptic natural plant shampoo powder which comprises the following raw materials in parts by weight:
45-55 parts of gleditsia sinensis, 10-20 parts of soapberry, 5-10 parts of hibiscus, 3-6 parts of tea seed, 2-6 parts of cacumen biotae, 2-5 parts of polygonum multiflorum, 1-5 parts of ganoderma sinense, 1-5 parts of red ginseng, 3-6 parts of carbon nano tube modified additive and 2-4 parts of bentonite synergistic agent.
Preferably, the shampoo powder comprises the following raw materials in parts by weight:
50 parts of Chinese honeylocust, 15 parts of Chinese soapberry, 7.5 parts of shrubalthea, 4.5 parts of tea seed, 4 parts of cacumen biotae, 3.5 parts of polygonum multiflorum, 3 parts of ganoderma sinense, 3 parts of red ginseng, 4.5 parts of carbon nanotube modified additive and 3 parts of bentonite synergistic agent.
Preferably, the preparation method of the carbon nanotube modified additive comprises the following steps:
s11: sending the carbon nano tube into 3-6 times of ethanol solvent, stirring and dispersing to form a suspending agent;
s12: adding 5-10 parts of sodium dodecyl sulfate into 20-30 parts of sodium alginate solution, then adding hydrochloric acid, adjusting the pH to 5.0, then adding 1-3 parts of silane coupling agent, and fully stirring and mixing to obtain a modifier;
s13: adding 10-20% of modifier into the suspending agent, stirring at 55-65 deg.C for 20-30min at a rotation speed of 100-300r/min, washing with water, and drying to obtain the modified additive.
Preferably, the mass fraction of the sodium alginate solution is 10-15%.
Preferably, the silane coupling agent is a silane coupling agent KH560.
Preferably, the preparation method of the bentonite synergistic agent comprises the following steps:
s21: calcining bentonite at 300-350 deg.C for 20-30min, and naturally cooling to room temperature;
s22: and (2) sending 10-15 parts of bentonite into 20-30 parts of chitosan solution, then adding 1-3 parts of tartaric acid and 0.2-0.5 part of lanthanum sulfate, stirring and dispersing uniformly, washing with water, and drying to obtain the bentonite synergist.
Preferably, the chitosan solution is prepared from chitosan, deionized water and acetic acid according to a weight ratio of 3.
The invention also provides a preparation method of the natural plant shampoo powder for controlling oil, removing dandruff and preventing corrosion, which comprises the following steps:
the method comprises the following steps: washing fructus Gleditsiae Abnormalis, fructus Sapindi Mukouossi, hibiscus syriacus, semen Camelliae sinensis, folium Platycladi, polygoni Multiflori radix, ganoderma, and Ginseng radix Rubri with water, draining, extracting in an extraction tank to obtain extractive solution, and oven drying to obtain composite powder;
step two: and fully stirring and mixing the composite powder particles, the carbon nano tube modified additive and the bentonite synergistic agent to obtain the natural plant shampoo powder.
Preferably, in the extraction treatment, the extraction temperature is 100-105 ℃, and the extraction time is 1-2h.
Preferably, the rotating speed for fully stirring and mixing is 1000-1500r/min, and the stirring time is 20-30min.
Compared with the prior art, the invention has the following beneficial effects:
the natural plant shampoo powder is prepared by matching and combining eight kinds of herbaceous plants according to the proportion and then processing the herbaceous plants through an extraction and drying technology, has the advantages that the pure herbaceous plant raw materials are free of other chemical additives, safe, natural and healthy, an antifogging agent is not required to be added, the effect of removing dandruff and controlling oil is achieved, powder shampoo products are convenient to carry, and the dandruff removing and controlling effect of the shampoo powder is enhanced through synergistic coordination and synergy of the carbon nano tube modified additive and the bentonite synergist.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below with reference to specific embodiments, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The oil-controlling, dandruff-removing and corrosion-preventing natural plant shampoo powder comprises the following raw materials in parts by weight:
45-55 parts of gleditsia sinensis, 10-20 parts of soapberry, 5-10 parts of hibiscus, 3-6 parts of tea seed, 2-6 parts of cacumen biotae, 2-5 parts of polygonum multiflorum, 1-5 parts of ganoderma sinense, 1-5 parts of red ginseng, 3-6 parts of carbon nano tube modified additive and 2-4 parts of bentonite synergistic agent.
The shampoo powder comprises the following raw materials in parts by weight:
50 parts of Chinese honeylocust, 15 parts of Chinese soapberry, 7.5 parts of shrubalthea, 4.5 parts of tea seed, 4 parts of cacumen biotae, 3.5 parts of polygonum multiflorum, 3 parts of ganoderma sinense, 3 parts of red ginseng, 4.5 parts of carbon nanotube modified additive and 3 parts of bentonite synergistic agent.
The preparation method of the carbon nanotube modified additive of the embodiment comprises the following steps:
s11: sending the carbon nano tube into 3-6 times of ethanol solvent, stirring and dispersing to form a suspending agent;
s12: adding 5-10 parts of sodium dodecyl sulfate into 20-30 parts of sodium alginate solution, then adding hydrochloric acid, adjusting the pH to 5.0, then adding 1-3 parts of silane coupling agent, and stirring and mixing fully to obtain a modifier;
s13: adding 10-20% of modifier into the suspending agent, stirring at 55-65 deg.C for 20-30min at a rotation speed of 100-300r/min, washing with water, and drying to obtain the modified additive.
The mass fraction of the sodium alginate solution in the embodiment is 10-15%.
The silane coupling agent of the present example is a silane coupling agent KH560.
The preparation method of the bentonite blending agent in the embodiment comprises the following steps:
s21: calcining bentonite at 300-350 deg.C for 20-30min, and naturally cooling to room temperature;
s22: and (2) sending 10-15 parts of bentonite into 20-30 parts of chitosan solution, then adding 1-3 parts of tartaric acid and 0.2-0.5 part of lanthanum sulfate, stirring and dispersing uniformly, washing with water, and drying to obtain the bentonite synergist.
The chitosan solution of the embodiment is prepared from chitosan, deionized water and acetic acid according to the weight ratio of 3.
The preparation method of the natural plant shampoo powder capable of controlling oil, removing dandruff and preventing corrosion comprises the following steps:
the method comprises the following steps: washing fructus Gleditsiae Abnormalis, fructus Sapindi Mukouossi, hibiscus syriacus, semen Camelliae sinensis, folium Platycladi, polygoni Multiflori radix, ganoderma, and Ginseng radix Rubri with water, draining, extracting in an extraction tank to obtain extractive solution, and oven drying to obtain composite powder;
step two: and fully stirring and mixing the composite powder particles, the carbon nano tube modified additive and the bentonite synergistic agent to obtain the natural plant shampoo powder.
In the extraction treatment of this example, the extraction temperature is 100-105 deg.C, and the extraction time is 1-2h.
The rotating speed for stirring and mixing fully in the embodiment is 1000-1500r/min, and the stirring time is 20-30min.
Example 1.
The oil-control, anti-dandruff and non-antiseptic natural plant shampoo powder comprises the following raw materials in parts by weight:
45 parts of gleditschia horrida, 10 parts of soapberry, 5 parts of shrubalthea, 3 parts of tea seed, 2 parts of cacumen biotae, 2 parts of polygonum multiflorum, 1 part of ganoderma sinense, 1 part of red ginseng, 3 parts of carbon nano tube modified additive and 2 parts of bentonite synergist.
The preparation method of the carbon nanotube modified additive of the embodiment comprises the following steps:
s11: sending the carbon nano tube into 3 times of ethanol solvent, stirring and dispersing to form a suspending agent;
s12: adding 5 parts of sodium dodecyl sulfate into 20 parts of sodium alginate solution, then adding hydrochloric acid, adjusting the pH to 5.0, then adding 1 part of silane coupling agent, and fully stirring and mixing to obtain a modifier;
s13: adding 10 percent of modifier into the suspending agent, stirring at 55 ℃ for 20min at the stirring speed of 100r/min, washing with water, and drying to obtain the carbon nano tube modified additive.
The mass fraction of the sodium alginate solution in this example was 10%.
The silane coupling agent of the present example is a silane coupling agent KH560.
The preparation method of the bentonite synergist in the embodiment comprises the following steps:
s21: calcining bentonite at 300 deg.C for 20min, and naturally cooling to room temperature;
s22: and (3) sending 10 parts of bentonite into 20 parts of chitosan solution, then adding 1 part of tartaric acid and 0.2 part of lanthanum sulfate, stirring and dispersing uniformly, washing with water, and drying to obtain the bentonite synergist.
The chitosan solution of the embodiment is prepared from chitosan, deionized water and acetic acid according to a weight ratio of 3.
The preparation method of the natural plant shampoo powder capable of controlling oil, removing dandruff and preventing corrosion comprises the following steps:
the method comprises the following steps: washing fructus Gleditsiae Abnormalis, fructus Sapindi Mukouossi, hibiscus syriacus, semen Camelliae sinensis, folium Platycladi, polygoni Multiflori radix, ganoderma, and Ginseng radix Rubri with water, draining, extracting in an extraction tank to obtain extractive solution, and oven drying to obtain composite powder;
step two: and fully stirring and mixing the composite powder particles, the carbon nano tube modified additive and the bentonite synergistic agent to obtain the natural plant shampoo powder.
In the extraction treatment of this example, the extraction temperature was 100 ℃ and the extraction time was 1 hour.
The rotating speed for stirring and mixing fully in the embodiment is 1000r/min, and the stirring time is 20min.
Example 2.
The oil-control, anti-dandruff and non-antiseptic natural plant shampoo powder comprises the following raw materials in parts by weight:
55 parts of Chinese honeylocust, 20 parts of Chinese soapberry, 10 parts of shrubalthea, 6 parts of tea seeds, 6 parts of cacumen biotae, 5 parts of polygonum multiflorum, 5 parts of ganoderma sinense, 5 parts of red ginseng, 6 parts of carbon nano tube modified additive and 4 parts of bentonite synergistic agent.
The preparation method of the carbon nanotube modified additive of the embodiment comprises the following steps:
s11: sending the carbon nano tube into 6 times of ethanol solvent, stirring and dispersing to form a suspending agent;
s12: adding 10 parts of sodium dodecyl sulfate into 30 parts of sodium alginate solution, then adding hydrochloric acid, adjusting the pH value to 5.0, then adding 3 parts of silane coupling agent, and fully stirring and mixing to obtain a modifier;
s13: and adding a modifier accounting for 20 percent of the total amount into the suspending agent, stirring at 65 ℃ for 30min at the stirring speed of 300r/min, washing with water after the stirring is finished, and drying to obtain the carbon nano tube modified additive.
The mass fraction of the sodium alginate solution in this example was 15%.
The silane coupling agent of the present example is a silane coupling agent KH560.
The preparation method of the bentonite blending agent in the embodiment comprises the following steps:
s21: calcining bentonite at 350 deg.C for 30min, and naturally cooling to room temperature;
s22: and (2) feeding 15 parts of bentonite into 30 parts of chitosan solution, then adding 3 parts of tartaric acid and 0.5 part of lanthanum sulfate, stirring and dispersing uniformly, washing with water, and drying to obtain the bentonite synergistic agent.
The chitosan solution of the embodiment is prepared from chitosan, deionized water and acetic acid according to the weight ratio of 3.
The preparation method of the natural plant shampoo powder capable of controlling oil, removing dandruff and preventing corrosion comprises the following steps:
the method comprises the following steps: washing fructus Gleditsiae Abnormalis, fructus Sapindi Mukouossi, hibiscus syriacus, semen Camelliae sinensis, folium Platycladi, polygoni Multiflori radix, ganoderma, and Ginseng radix Rubri with water, draining, extracting in an extraction tank to obtain extractive solution, and oven drying to obtain composite powder;
step two: and fully stirring and mixing the composite powder particles, the carbon nano tube modified additive and the bentonite synergistic agent to obtain the natural plant shampoo powder.
In the extraction treatment of this example, the extraction temperature was 105 ℃ and the extraction time was 2 hours.
The rotating speed for sufficient stirring and mixing in the embodiment is 1500r/min, and the stirring time is 30min.
Example 3.
The oil-controlling, dandruff-removing and corrosion-preventing natural plant shampoo powder comprises the following raw materials in parts by weight:
50 parts of Chinese honeylocust, 15 parts of Chinese soapberry, 7.5 parts of shrubalthea, 4.5 parts of tea seed, 4 parts of cacumen biotae, 3.5 parts of polygonum multiflorum, 3 parts of ganoderma sinense, 3 parts of red ginseng, 4.5 parts of carbon nanotube modified additive and 3 parts of bentonite synergistic agent.
The preparation method of the carbon nanotube modified additive of the embodiment comprises the following steps:
s11: sending the carbon nano tube into 4.5 times of ethanol solvent, stirring and dispersing to form a suspending agent;
s12: adding 7.5 parts of sodium dodecyl sulfate into 25 parts of sodium alginate solution, then adding hydrochloric acid, adjusting the pH to 5.0, then adding 2 parts of silane coupling agent, and fully stirring and mixing to obtain a modifier;
s13: adding a modifier accounting for 15% of the total amount into the suspending agent, stirring at 60 ℃ for 25min at the stirring speed of 200r/min, washing with water, and drying to obtain the carbon nano tube modified additive.
The mass fraction of the sodium alginate solution in this example was 12.5%.
The silane coupling agent of the present example is a silane coupling agent KH560.
The preparation method of the bentonite synergist in the embodiment comprises the following steps:
s21: calcining bentonite at 325 deg.C for 25min, and naturally cooling to room temperature;
s22: and (2) feeding 12.5 parts of bentonite into 25 parts of chitosan solution, then adding 2 parts of tartaric acid and 0.35 part of lanthanum sulfate, stirring and dispersing uniformly, washing with water, and drying to obtain the bentonite synergistic agent.
The chitosan solution of the embodiment is prepared from chitosan, deionized water and acetic acid according to the weight ratio of 3.
The preparation method of the natural plant shampoo powder for controlling oil, removing dandruff and having no corrosion resistance comprises the following steps:
the method comprises the following steps: washing fructus Gleditsiae Abnormalis, fructus Sapindi Mukouossi, hibiscus syriacus, tea seed, folium Platycladi, polygoni Multiflori radix, ganoderma, and Ginseng radix Rubri with water, draining, extracting in an extraction tank to obtain extractive solution, and oven drying to obtain composite powder;
step two: and fully stirring and mixing the composite powder particles, the carbon nano tube modified additive and the bentonite synergistic agent to obtain the natural plant shampoo powder.
In the extraction treatment of this example, the extraction temperature was 102.5 ℃ and the extraction time was 1.5 hours.
In the embodiment, the rotation speed for sufficient stirring and mixing is 1250r/min, and the stirring time is 25min.
Example 4.
The oil-controlling, dandruff-removing and corrosion-preventing natural plant shampoo powder comprises the following raw materials in parts by weight:
47 parts of Chinese honeylocust, 12 parts of Chinese soapberry, 6 parts of shrubalthea, 4 parts of tea seeds, 3 parts of cacumen biotae, 3 parts of polygonum multiflorum, 2 parts of ganoderma sinense, 2 parts of red ginseng, 4 parts of carbon nano tube modified additive and 3 parts of bentonite synergistic agent.
The preparation method of the carbon nanotube modified additive of the embodiment comprises the following steps:
s11: sending the carbon nano tube into 4 times of ethanol solvent, stirring and dispersing to form a suspending agent;
s12: adding 6 parts of sodium dodecyl sulfate into 22 parts of sodium alginate solution, then adding hydrochloric acid, adjusting the pH to 5.0, then adding 2 parts of silane coupling agent, and fully stirring and mixing to obtain a modifier;
s13: adding 12 percent of modifier into the suspending agent, stirring for 22min at 57 ℃, wherein the stirring speed is 120r/min, and after the stirring, washing and drying to obtain the carbon nano tube modified additive.
The mass fraction of the sodium alginate solution in this example was 12%.
The silane coupling agent of the present example is a silane coupling agent KH560.
The preparation method of the bentonite blending agent in the embodiment comprises the following steps:
s21: calcining bentonite at 310 deg.C for 22min, and naturally cooling to room temperature;
s22: and (3) sending 12 parts of bentonite into 22 parts of chitosan solution, then adding 2 parts of tartaric acid and 0.3 part of lanthanum sulfate, stirring and dispersing uniformly, washing with water, and drying to obtain the bentonite synergist.
The chitosan solution of the embodiment is prepared from chitosan, deionized water and acetic acid according to a weight ratio of 3.
The preparation method of the natural plant shampoo powder capable of controlling oil, removing dandruff and preventing corrosion comprises the following steps:
the method comprises the following steps: washing fructus Gleditsiae Abnormalis, fructus Sapindi Mukouossi, hibiscus syriacus, semen Camelliae sinensis, folium Platycladi, polygoni Multiflori radix, ganoderma, and Ginseng radix Rubri with water, draining, extracting in an extraction tank to obtain extractive solution, and oven drying to obtain composite powder;
step two: and fully stirring and mixing the composite powder particles, the carbon nano tube modified additive and the bentonite synergistic agent to obtain the natural plant shampoo powder.
In the extraction treatment of this example, the extraction temperature was 102 ℃ and the extraction time was 1.2 hours.
The rotation speed for sufficient stirring and mixing in the embodiment is 1100r/min, and the stirring time is 22min.
Comparative example 1.
Unlike example 3, no tea seeds were added.
Comparative example 2.
Different from the example 3, the ganoderma sinensis is not added.
Comparative example 3.
Unlike example 3, no carbon nanotube modifying additive was added.
Comparative example 4.
The difference from example 3 is that the carbon nanotube modifying additive is replaced with carbon nanotubes.
Comparative example 5.
Unlike example 3, the method for preparing the carbon nanotube modification additive was different, and no modifier was added.
Comparative example 6.
In contrast to example 3, no bentonite synergist was added.
The ten-grade rating method of adhesive dandruff is adopted. The age of the tested population is 18-45 years, the male and female halves have scalp problems with different degrees, the dandruff score is 5-10 grade, the double-blind method is adopted, and a hairdresser of a beauty salon uses a blank sample, an application sample and a comparative sample (double-blind half-head washing test) on the hair of each tested person for 14 days and washes the hair every other day; the dandruff condition of the human subjects was evaluated on day 0 and 14, respectively. The calculation efficiency is high.
Ten-stage rating method for adhesive scurf
The products of examples 1-3 and comparative examples 1-6 tested the properties of the hair as follows:
as can be seen from comparative examples 1-6, examples 1-3;
the product of the invention is not added with tea seeds and ganoderma sinense, the effective rate of the product has a trend of changing, meanwhile, the effective rate of the product is obviously reduced because no carbon nano tube modified additive and no bentonite synergistic agent are added, and the performance of the product is different because the preparation methods of the carbon nano tube modified additive are different.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Furthermore, it should be understood that although the present specification describes embodiments, not every embodiment includes only a single embodiment, and such description is for clarity purposes only, and it is to be understood that all embodiments may be combined as appropriate by one of ordinary skill in the art to form other embodiments as will be apparent to those of skill in the art from the description herein.
Claims (10)
1. The oil-control anti-dandruff non-antiseptic natural plant shampoo powder is characterized by comprising the following raw materials in parts by weight:
45-55 parts of gleditsia sinensis, 10-20 parts of soapberry, 5-10 parts of hibiscus, 3-6 parts of tea seed, 2-6 parts of cacumen biotae, 2-5 parts of polygonum multiflorum, 1-5 parts of ganoderma sinense, 1-5 parts of red ginseng, 3-6 parts of carbon nano tube modified additive and 2-4 parts of bentonite synergistic agent.
2. The natural plant shampoo powder for controlling oil, removing dandruff and preventing corrosion according to claim 1, wherein the shampoo powder comprises the following raw materials in parts by weight:
50 parts of Chinese honeylocust fruit, 15 parts of soapberry, 7.5 parts of shrubalthea, 4.5 parts of tea seed, 4 parts of cacumen biotae, 3.5 parts of fleece-flower root, 3 parts of ganoderma sinense, 3 parts of red ginseng, 4.5 parts of carbon nano tube modified additive and 3 parts of bentonite synergistic agent.
3. The natural plant shampoo powder for controlling oil, removing dandruff and preventing corrosion according to claim 1, wherein the preparation method of the carbon nanotube modified additive comprises the following steps:
s11: sending the carbon nano tube into 3-6 times of ethanol solvent, stirring and dispersing to form a suspending agent;
s12: adding 5-10 parts of sodium dodecyl sulfate into 20-30 parts of sodium alginate solution, then adding hydrochloric acid, adjusting the pH to 5.0, then adding 1-3 parts of silane coupling agent, and fully stirring and mixing to obtain a modifier;
s13: adding 10-20% of modifier into the suspending agent, stirring at 55-65 deg.C for 20-30min at a rotation speed of 100-300r/min, washing with water, and drying to obtain the final product.
4. The natural plant shampoo powder with the functions of controlling oil, removing dandruff and no corrosion prevention as claimed in claim 3, wherein the mass fraction of the sodium alginate solution is 10-15%.
5. The natural plant shampoo powder for controlling oil, removing dandruff and preventing corrosion according to claim 3, wherein the silane coupling agent is KH560.
6. The natural plant shampoo powder for controlling oil, removing dandruff and having no antiseptic property of claim 1, wherein the preparation method of the bentonite synergistic agent comprises the following steps:
s21: calcining bentonite at 300-350 deg.C for 20-30min, and naturally cooling to room temperature;
s22: and (2) sending 10-15 parts of bentonite into 20-30 parts of chitosan solution, then adding 1-3 parts of tartaric acid and 0.2-0.5 part of lanthanum sulfate, stirring and dispersing uniformly, washing with water, and drying to obtain the bentonite synergistic agent.
7. The natural plant shampoo powder for controlling oil, removing dandruff and preventing corrosion according to claim 6, wherein the chitosan solution is prepared from chitosan, deionized water and acetic acid according to a weight ratio of 3.
8. A process for preparing the natural plant shampoo powder for controlling oil, removing dandruff and having no antiseptic property as claimed in any one of claims 1 to 7, comprising the steps of:
the method comprises the following steps: washing fructus Gleditsiae Abnormalis, fructus Sapindi Mukouossi, hibiscus syriacus, tea seed, folium Platycladi, polygoni Multiflori radix, ganoderma, and Ginseng radix Rubri with water, draining, extracting in an extraction tank to obtain extractive solution, and oven drying to obtain composite powder;
step two: and fully stirring and mixing the composite powder particles, the carbon nano tube modified additive and the bentonite synergistic agent to obtain the natural plant shampoo powder.
9. The method for preparing the natural plant shampoo powder for controlling oil, removing dandruff and having no antiseptic property as claimed in claim 8, wherein the extraction temperature is 100-105 ℃ in the extraction treatment, and the extraction is performed for 1-2h.
10. The method for preparing the natural plant shampoo powder with oil control, dandruff control and no corrosion prevention according to claim 8, wherein the rotation speed for sufficient stirring and mixing is 1000-1500r/min, and the stirring time is 20-30min.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN116407483A (en) * | 2023-06-06 | 2023-07-11 | 广东时尚女孩生物科技有限公司 | Formula and preparation method of oil-control moisturizing facial cleanser |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN116407483A (en) * | 2023-06-06 | 2023-07-11 | 广东时尚女孩生物科技有限公司 | Formula and preparation method of oil-control moisturizing facial cleanser |
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Application publication date: 20221223 |