CN105997553A - Liquid shampoo containing amino acid surfactant and preparation method thereof - Google Patents
Liquid shampoo containing amino acid surfactant and preparation method thereof Download PDFInfo
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- CN105997553A CN105997553A CN201610586803.9A CN201610586803A CN105997553A CN 105997553 A CN105997553 A CN 105997553A CN 201610586803 A CN201610586803 A CN 201610586803A CN 105997553 A CN105997553 A CN 105997553A
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- amino acid
- surfactant
- containing amino
- acid surfactant
- shampoo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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- Cosmetics (AREA)
Abstract
The invention discloses a liquid shampoo containing amino acid surfactant and a preparation method thereof. The liquid shampoo contains, by mass, an anionic surfactant 30%-60%, a cationic conditioner 0.05%-3%, a nonionic surfactant 1%-15% and the balance water. An amino acid surfactant used for the liquid shampoo serves as the main surfactant, one or more small molecule alcohols are added in a preparation process of the amino acid surfactant, and the solubility of lipid amino acids in the surfactants is improved. In addition, the amino acid surfactant can reduce the overall degreasing capability of the liquid shampoo, the durability of the combing property, softness, smoothness and smoothing feeling during hair cleaning with the liquid shampoo is improved, the liquid shampoo has unique moisturizing properties, soft feeling and oiling feeling, and the dandruff removing and oil control effects are improved.
Description
Technical field
The present invention relates to daily use chemicals product field, be specifically related to a kind of shampoo containing amino acid surfactant and preparation side thereof
Method.
Background technology
In recent years, people are more and more higher to the requirement of hair washing product, not only need to reach cleaning effect, more pay close attention to safety
With mildness, increasingly tend to select gentle, do not stimulate, natural product.Under constantly universal without silicone oil concept, without sulfur
Hydrochlorate shampoo causes the attention of masses the most simultaneously, and the advantage that mainly goes out without sulfate shampoo is exactly with thorn gentleer, low
The surfactant swashed substitutes traditional Sulfates surfactant, reduces the shampoo zest to scalp, it is to avoid draw
Send out the problem such as inflammation of sensitive scalp；Can be used for replacement sulfur Barbiturates anion surfactant mainly has aminoacid and Calculus Bovis
Barbiturates surfactant etc..Shampoo without sulfate is that primary raw material not only reduces surface work with amino acid surfactant
Property agent zest, some natural oils can be added to substitute the nursing role of silicone oil simultaneously, reach health care scalp with
Effect of hair.Amino acid surfactant is class shampoo raw material as mild as a dove, but still suffers from very in application process
The most unsolved difficult problem, such as difficult thickening, the hair conditioning problem such as not, corresponding shampoo then exists that cardability is poor, goes
The difficult problems such as bits poor effect.
Summary of the invention
In order to overcome the deficiencies in the prior art, first purpose of the present invention is to provide one containing amino acid surface activity
The shampoo of agent, is main surfactant with amino acid surfactant in shampoo, at amino acid surfactant
Preparation technology adds one or more small molecular alcohols, adds lipid aminoacid dissolubility in surfactant；
Amino acid surfactant can reduce the overall degreasing power of shampoo simultaneously, improves cardability when shampoo is had one's hair wash, softness
Degree, smoothness, the persistency of smooth feeling, bring the moisturizing power of uniqueness, soft feeling, glossy sense to hair, enhances anti-dandruff, control oil
Etc. effect.
Second object of the present invention is to provide for the preparation of a kind of above-mentioned shampoo containing amino acid surfactant
Method.
Realize the purpose of the present invention to reach by adopting the following technical scheme that:
A kind of shampoo containing amino acid surfactant, including following each component by mass percentage:
Described anion surfactant is made up of the following component calculated by weight percentage
Amino acid surfactant 30%～60%
Small molecular alcohol 1%～50%
Water surplus；
Preferably, also including the additive accounting for shampoo gross weight 0.0%～5%, described additive is viscosity-controlling agent, oil
At least one in fat, acid-base modifier, preservative, daily chemical essence.
Preferably, the pH of described shampoo is 5～8.
Preferably, selected viscosity modifier is methyl glucoside polyoxyethylene (120) ether dioleate, cetearyl alcohol
In alcohol polyethers-60 myristyl glycol, sodium chloride, potassium chloride, ammonium chloride, cellulose derivative, acrylic copolymer at least
A kind of；Described acid-base modifier is at least one in citric acid, phosphoric acid, sodium citrate；Described preservative is Kazon, benzene oxygen second
At least one in alcohol, chlorphenesin；Described oils and fats is Oleum Camelliae, Jojoba oil, house oil, Oleum Cocois, Oleum Vitis viniferae, heronsbill
One in oil.
Preferably, described amino acid surfactant is N-acyl amino hydrochlorate；Described N-acyl amino hydrochlorate is N-acyl
One or more in base sarcosinate, N-acyl glutamate, N-acylalaninies salt, N-acylaspartic acid salt；Institute
Stating N-acyl amino hydrochlorate is N-acyl amino acid alkali metal salt, N-acyl amino acid ammonium salt, N-acyl amino amine acid salt, N-acyl
Base amino amino ethylate.
Preferably, a length of 8～18 carbon atoms of the alkyl group carbochain in described amino acid surfactant.
Preferably, described small molecular alcohol be dipropylene glycol, ethanol, ethylene glycol, propanol, propylene glycol, butanol, 1,3-fourth two
At least one in alcohol, Polyethylene Glycol-M (0 < M < 800), polypropylene glycol-N (0 < N < 70).
Preferably, described cation opsonizing agent is guar hydroxypropyltrimonium ammonium chloride, polyquaternary ammonium salt-7, polyquaternary amine
One or more in salt-10, Polyquaternium-67, palmitamide hydroxypropyltrimonium chloride.
Preferably, described nonionic surfactant is alkyl-glucoside.
The present invention also provides for the preparation method of a kind of shampoo containing amino acid surfactant, it is characterised in that include as
Lower step:
(1) add water in a kettle., add cation opsonizing agent polymer, be slowly stirred, be uniformly dispersed, be heated to 70
～90 DEG C；
(2) according to recipe requirements be separately added into anion surfactant, nonionic surfactant, viscosity modifier,
Treat that these materials are completely dissolved, and lower the temperature after being uniformly dispersed；Temperature is down to 40～50 DEG C, adds preservative, daily chemical essence continuation
Stirring, mix homogeneously；
(3) adding acid-base modifier, the pH value of regulation product is to 5～8.
Compared to existing technology, the beneficial effects of the present invention is:
1, shampoo of the present invention is main surfactant with amino acid surfactant, in amino acid surface activity
The preparation technology of agent adds one or more small molecular alcohols, adds the dissolving in surfactant of the lipid aminoacid
Property；Lipid aminoacid is the compound that aminoacid and fatty acid response obtain during purification amino acid surfactant, contains
There is hydrophilic and oleophilic structure, skin is had good affinity.And alcohol and the amino acid whose mixed dissolution of lipid, change lipid ammonia
The hydrophile-lipophile balance of base acid itself, becomes more hydrophilic, it is easier to absorption, at hair and skin surface, improves hair washing washing
Cardability when sending out, pliability, smoothness, the persistency of smooth feeling, bring the effects such as unique anti-dandruff, control oil to hair.
2, shampoo provided by the present invention has well solubilising effect to various plants oils and fats, animal oil with synthetic ester oil
Really, reduce the degreasing power of shampoo, zest simultaneously, improve shampoo to hair hair conditioning and the oily anti-dandruff effect of control.
Detailed description of the invention
Below, in conjunction with detailed description of the invention, the present invention is described further:
Embodiment 1:
A kind of shampoo containing amino acid surfactant, including following each component by mass percentage:
Described anion surfactant include accounting for the amino acid surfactant of surfactant gross weight 30%, 25%
Small molecular alcohol, the water of surplus；Described amino acid surfactant is sodium lauroyl sarcosine；Described small molecular alcohol is double third sweet
Alcohol；Described cation opsonizing agent is guar hydroxypropyltrimonium ammonium chloride；Described nonionic surfactant is alkyl Fructus Vitis viniferae
Glucosides；Described oils and fats is Oleum Camelliae；Described preservative is Kazon.
Embodiment 2:
A kind of shampoo containing amino acid surfactant, including following each component by mass percentage:
Described anion surfactant include accounting for the amino acid surfactant of surfactant gross weight 42%, 1%
Small molecular alcohol, the water of surplus；Described amino acid surfactant is cocoamido sodium propionate；Described small molecular alcohol is the third two
Alcohol；Described cation opsonizing agent is polyquaternary ammonium salt-7；Described nonionic surfactant is alkyl-glucoside；Described oils and fats is
Oleum Camelliae；Described preservative is chlorphenesin；Described acid-base modifier is citric acid.
Embodiment 3:
A kind of shampoo containing amino acid surfactant, including following each component by mass percentage:
Described surfactant includes accounting for the amino acid surfactant of surfactant gross weight 60%, the little molecule of 20%
Alcohol, the water of surplus；Described amino acid surfactant is cocoamido sodium propionate；Described small molecular alcohol is ethanol；Described sun
Ion conditioner is Polyquaternium-10；Described nonionic surfactant is alkyl-glucoside；Described oils and fats is Oleum Camelliae；
Described preservative is chlorphenesin；Described acid-base modifier is citric acid；Described viscosity modifier is methyl glucoside polyoxy
Ethylene (120) ether dioleate；Described daily chemical essence is rose scent daily chemical essence.
Embodiment 4:
A kind of shampoo containing amino acid surfactant, including following each component by mass percentage:
Described anion surfactant include accounting for the amino acid surfactant of surfactant gross weight 35%, 50%
Small molecular alcohol, the water of surplus；Described amino acid surfactant is sodium lauroyl glutamate；Described small molecular alcohol is poly-second two
Alcohol-M (0 < M < 800)；Described cation opsonizing agent is palmitamide hydroxypropyltrimonium chloride；Described nonionic surfactant
For alkyl-glucoside；Described oils and fats is Jojoba oil；Described preservative is Kazon；Described acid-base modifier is phosphoric acid；Described
Viscosity modifier is ceteareth-60 myristyl glycol；Described daily chemical essence is orchid odor type daily chemical essence.
Each component and the content of the shampoo containing amino acid surfactant of embodiment 5～8 are as shown in table 1 below
Table 1
Embodiment 9
According to the formula of any one embodiment of embodiment 1～8, prepare washing containing amino acid surfactant as follows
Flood；
(1) add water in a kettle., add cation opsonizing agent polymer, be slowly stirred, be uniformly dispersed, be heated to 70
～90 DEG C；
(2) it is separately added into anion surfactant, cation opsonizing agent, non-ionic surface active according to recipe requirements
Agent, viscosity modifier, treat that these materials are completely dissolved, and lower the temperature after being uniformly dispersed；Temperature is down to 40～50 DEG C, adds anticorrosion
Agent, essence continue stirring, mix homogeneously；
(3) adding pH adjusting agent, the pH value of regulation product is to 5～8.
Each component and the content of the shampoo containing amino acid surfactant of embodiment 10～13 are as shown in table 2 below
Table 2
Checking embodiment
Embodiment efficacy assessments is used sensory evaluation method, and detailed description of the invention is as follows:
By the shampoo described in the embodiment 5 of preparation～8 and embodiment 10～13, it is respectively issued to 100 ages at 18-
The volunteer of 40 years old tests use.Wherein 50 male of volunteer, 50 women, according to phase when volunteer uses shampoo sample
The hair washing of method together, every kind of shampoo was distinguished continuously with two weeks, marked shampoo according to the sensation of oneself, and scoring is adopted
By 5 points of systems, 1 is divided into worst, and 3 points moderate, and 5 are divided into best, and the highest effect of score is the best.Various using effects evaluate average mark knot
Fruit is listed in the table below 3.
Table 3
For a person skilled in the art, can technical scheme as described above and design, make other each
Plant corresponding change and deformation, and all these changes and deforms the protection model that all should belong to the claims in the present invention
Within enclosing.
Claims (10)
1. the shampoo containing amino acid surfactant, it is characterised in that include each group the most by mass percentage
Point:
Described anion surfactant is made up of the following component calculated by weight percentage
Amino acid surfactant 30%～60%
Small molecular alcohol 1%～50%
Water surplus.
Shampoo containing amino acid surfactant the most according to claim 1, it is characterised in that: also include accounting for shampoo
The additive of gross weight 0%～5%, described additive is in viscosity-controlling agent, oils and fats, acid-base modifier, preservative, daily chemical essence
At least one.
Shampoo containing amino acid surfactant the most according to claim 2, it is characterised in that: the pH of described shampoo
It is 5～8.
Shampoo containing amino acid surfactant the most according to claim 2, it is characterised in that: selected viscosity adjustment
Agent be methyl glucoside polyoxyethylene (120) ether dioleate, ceteareth-60 myristyl glycol, sodium chloride,
At least one in potassium chloride, ammonium chloride, cellulose derivative, acrylic copolymer；Described acid-base modifier is citric acid, phosphorus
At least one in acid, sodium citrate；Described preservative is at least one in Kazon, phenoxyethanol, chlorphenesin；Described oil
Fat is the one in Oleum Camelliae, Jojoba oil, house oil, Oleum Cocois, Oleum Vitis viniferae, sun caul-fat.
Shampoo containing amino acid surfactant the most according to claim 1, it is characterised in that: described amino acid surface
Activating agent is N-acyl amino hydrochlorate；Described N-acyl amino hydrochlorate is N-acyl sarcosinates, N-acyl glutamate, N-acyl
One or more in base alanine salt, N-acylaspartic acid salt；Described N-acyl amino hydrochlorate is N-acylamino acid
Alkali metal salt, N-acyl amino acid ammonium salt, N-acyl amino amine acid salt, N-acylamino acid ethylaminoethanol salt.
Shampoo containing amino acid surfactant the most according to claim 1, it is characterised in that: described amino acid surface
A length of 8～18 carbon atoms of the alkyl group carbochain in activating agent.
Shampoo containing amino acid surfactant the most according to claim 1, it is characterised in that: described small molecular alcohol is
Dipropylene glycol, ethanol, ethylene glycol, propanol, propylene glycol, butanol, 1,3 butylene glycol, Polyethylene Glycol-M (0 < M < 800), poly-the third two
At least one in alcohol-N (0 < N < 70).
Shampoo containing amino acid surfactant the most according to claim 1, it is characterised in that: described cationic conditioning
Agent is guar hydroxypropyltrimonium ammonium chloride, polyquaternary ammonium salt-7, Polyquaternium-10, Polyquaternium-67, palmitamide propyl group
One or more in trimethyl ammonium chloride.
Shampoo containing amino acid surfactant the most according to claim 1, it is characterised in that: described non-ionic surface
Activating agent is alkyl-glucoside.
10. the preparation method of the shampoo containing amino acid surfactant as claimed in claim 2, it is characterised in that bag
Include following steps:
(1) add water in a kettle., add cation opsonizing agent polymer, be slowly stirred, be uniformly dispersed, be heated to 70～
90℃；
(2) it is separately added into anion surfactant, nonionic surfactant, viscosity modifier according to recipe requirements, treats this
A little materials are completely dissolved, and lower the temperature after being uniformly dispersed；Temperature is down to 40～50 DEG C, adds preservative, daily chemical essence continuation stirring,
Mix homogeneously；
(3) adding acid-base modifier, the pH value of regulation product is to 5～8.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610586803.9A CN105997553A (en) | 2016-07-22 | 2016-07-22 | Liquid shampoo containing amino acid surfactant and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610586803.9A CN105997553A (en) | 2016-07-22 | 2016-07-22 | Liquid shampoo containing amino acid surfactant and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106473958A (en) * | 2016-11-04 | 2017-03-08 | 深圳市婴缘健康有限公司 | A kind of two-in-one hair washing bath oil of infant |
| CN107375028A (en) * | 2017-07-31 | 2017-11-24 | 广州道明研究院有限公司 | A kind of non-stimulated no silicon shampoo and preparation method thereof |
| CN108379117A (en) * | 2018-02-01 | 2018-08-10 | 广州百孚润化工有限公司 | A kind of compound surfactant and a kind of cleaning compositions |
| CN108403461A (en) * | 2018-02-01 | 2018-08-17 | 广州百孚润化工有限公司 | A kind of conditioner composition and its application |
| CN108653027A (en) * | 2018-07-03 | 2018-10-16 | 广州仲思生物科技有限公司 | A kind of amino acid transparent hair shampoo and preparation method without dioxane and silica |
| CN110721108A (en) * | 2019-09-26 | 2020-01-24 | 广州妮趣化妆品有限公司 | Thickening composition of cocoyl alanine salt and application thereof |
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| CN102895151A (en) * | 2012-10-22 | 2013-01-30 | 广州立白企业集团有限公司 | Sulfate-free hair cleanser and preparation method thereof |
| CN103251523A (en) * | 2013-05-21 | 2013-08-21 | 纳爱斯集团有限公司 | Oil-control shampoo composite |
| CN104224575A (en) * | 2014-09-12 | 2014-12-24 | 广州市天吻娇颜化妆品有限公司 | Transparent silicone-oil-free hairdressing composition and preparation method thereof |
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| CN102824279A (en) * | 2012-09-13 | 2012-12-19 | 纳爱斯集团有限公司 | Low-accumulation mild type shampoo composition |
| CN102895151A (en) * | 2012-10-22 | 2013-01-30 | 广州立白企业集团有限公司 | Sulfate-free hair cleanser and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106473958A (en) * | 2016-11-04 | 2017-03-08 | 深圳市婴缘健康有限公司 | A kind of two-in-one hair washing bath oil of infant |
| CN107375028A (en) * | 2017-07-31 | 2017-11-24 | 广州道明研究院有限公司 | A kind of non-stimulated no silicon shampoo and preparation method thereof |
| CN108379117A (en) * | 2018-02-01 | 2018-08-10 | 广州百孚润化工有限公司 | A kind of compound surfactant and a kind of cleaning compositions |
| CN108403461A (en) * | 2018-02-01 | 2018-08-17 | 广州百孚润化工有限公司 | A kind of conditioner composition and its application |
| CN108653027A (en) * | 2018-07-03 | 2018-10-16 | 广州仲思生物科技有限公司 | A kind of amino acid transparent hair shampoo and preparation method without dioxane and silica |
| CN110721108A (en) * | 2019-09-26 | 2020-01-24 | 广州妮趣化妆品有限公司 | Thickening composition of cocoyl alanine salt and application thereof |
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Application publication date: 20161012 |