CN106726756A - One kind repairs hair film and preparation method thereof - Google Patents
One kind repairs hair film and preparation method thereof Download PDFInfo
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- CN106726756A CN106726756A CN201611198160.7A CN201611198160A CN106726756A CN 106726756 A CN106726756 A CN 106726756A CN 201611198160 A CN201611198160 A CN 201611198160A CN 106726756 A CN106726756 A CN 106726756A
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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Abstract
The invention belongs to daily chemical product field, and in particular to one kind repairs hair film and preparation method thereof.The reparation hair film that the present invention is provided includes following components and its percentage by weight:APG 2 6%, behenyl base trimethyl ammonium chloride 8 18%, dimethyl silicone polymer 2 4%, menthol 1 2%, NMF 8 16%, care agent 14 24%, climbazole 1 3%, patchouli alcohol 1 5%, EDTA disodiums 0.1 0.3%, citric acid 0.1 0.3%, methyl hydroxybenzoate 0.1 0.3%, essence 0.1 0.3%, spermaceti ethylhydroxyethylcellulose 2 6% and water 14.8 60.6%.The reparation hair film that the present invention is provided can not only repair damaged hair, enhancing hair toughness, additionally it is possible to moisten scalp and hair-care, relieving itching and removing dandruff.Meanwhile, the reparation hair film that the present invention is provided is clearly comfortable, gentle to skin, non-stimulated.
Description
Technical field
The invention belongs to daily chemical product field, and in particular to one kind repairs hair film and preparation method thereof.
Background technology
Hair film can be entered as a kind of hair sealing compound, its nutriment for containing and moisture by the hair scale piece on hair
In hair, repairing fiber tissue is helped, fundamentally change hair quality, be particularly suitable for withered and damaged hair.On existing market
Hair film product it is numerous, but there is a problem of send out film in absorption of nutrient ingredients effect it is unsatisfactory, fail to be absorbed by hair
Nutriment be deposited on hair for a long time, the burden of hair is increased on the contrary, cause hair quality to be damaged, and other can be produced to ask
Topic.
Chinese patent application CN105232365A discloses a kind of hair treatment film and preparation method thereof, and its component is thickening
Agent, emulsifying agent, hair conditioner, preservative, essence, citric acid and colouring agent CI42090, balance deionized water is solvent, together
When additionally provide preparation method.The hair treatment film that the invention is provided has shield volume and moistening effect is good, hair is become submissive, rich
Glossiness advantage, but the invention is not obvious to the repairing effect of damaged hair.
Chinese patent application CN104116665A discloses a kind of deep layer and moistens reparation hair film, the parts by weight of its each component
For:Double -50 parts of aminopropyl dimethyl silicone polymer, 30-35 parts of behenyl base trimethyl ammonium chloride, glycerol stearate monoglyceride 10-
12 parts, cetanol 1-5 parts, glycerine 2-5 parts, propane diols 8-10 parts, dodecyldimethylammonium hydroxide inner salt 2-6 parts, fish pelargonium extraction
Liquid 15-35 parts, 15-35 parts, preservative 0.2-0.5 parts, NMF 3-11 parts and deionized water 25-35 parts of cactus extract.
The scalp for being removed grease is effectively repaired in the invention, and scalp deep layer is nourished, and protects scalp, recovers the internal system of scalp,
The purpose of removal dandruff is fundamentally reached, but the invention is not obvious to the repairing effect of damaged hair.
The content of the invention
In order to solve problems of the prior art, hair film and its preparation are repaired it is an object of the invention to provide one kind
Method.The reparation hair film that the present invention is provided can not only repair damaged hair, enhancing hair toughness, additionally it is possible to moisten scalp head
Hair, relieving itching and removing dandruff.The reparation hair film that the present invention is provided simultaneously is clearly comfortable, gentle to skin, non-stimulated.
The present invention is a kind of to repair hair film, including following components and its percentage by weight:
APG 2-6%, behenyl base trimethyl ammonium chloride 8-18%, dimethyl silicone polymer 2-4%, menthol 1-
2%th, NMF 8-16%, care agent 14-24%, climbazole 1-3%, patchouli alcohol 1-5%, EDTA- disodium 0.1-0.3%,
Citric acid 0.1-0.3%, methyl hydroxybenzoate 0.1-0.3%, essence 0.1-0.3%, spermaceti ethylhydroxyethylcellulose 2-6% and water
14.8-60.6%.APG is purchased from Guangzhou Jian Chuan bio tech ltd, dimethyl silicone polymer CAS NO:9006-
65-9, spermaceti ethylhydroxyethylcellulose is purchased from Guangzhou Shi Sheng Chemical Co., Ltd.s.
The reasonable science of compatibility of the present invention, each component interphase interaction, cooperateed with reparation damaged hair, enhancing hair toughness,
Moisten effect of scalp and hair-care and relieving itching and removing dandruff.
Further, described reparation hair film is made up of following components and its percentage by weight:
APG 4%, behenyl base trimethyl ammonium chloride 13%, dimethyl silicone polymer 3%, menthol 1.5%, moisturizing
Agent 12%, care agent 19%, climbazole 2%, patchouli alcohol 3%, EDTA- disodiums 0.2%, citric acid 0.2%, methyl hydroxybenzoate
0.2%th, essence 0.2%, spermaceti ethylhydroxyethylcellulose 4% and water 37.7%.
Further, the NMF constitutes 2 by weight by Sodium Hyaluronate, cetostearyl alcohol and glycerine:2:1.
Further, the care agent is by hydrolyzed wheat protein, lecithin and lanolin by weight 3:1:1 composition.
Meanwhile, present invention also offers a kind of preparation method for repairing hair film, comprise the following steps:
S1 is added water in container, is heated to 70~80 DEG C, and APG, behenyl base trimethyl chlorine are added while stirring
Change ammonium and dimethyl silicone polymer, stir to being completely dissolved, obtain solution A;
Step S1 resulting solutions A is cooled to 65~75 DEG C by S2, and EDTA- disodiums and methyl hydroxybenzoate are added while stirring, is stirred
Mix uniform, obtain solution B;
Step S2 resulting solutions B is cooled to 50~60 DEG C by S3, and menthol, NMF, care agent, sweet is added while stirring
Precious element and patchouli alcohol, stir to being completely dissolved, and obtain solution C;
Step S3 resulting solutions C is cooled to 30~40 DEG C by S4, adds essence, while with lemon acid for adjusting pH value to 5.5-
6.5, it is eventually adding coconut oleoyl amine MEA and adjusts viscosity to 4000-5000, stir, obtain final product.
Further, pH is 6.1 in the step S4, and viscosity is 4200.
The reparation hair film that the present invention is provided, by the order and its temperature that control raw material to add, makes its each component more preferable
Interact, maximum its synergy of performance so that damaged hair is being repaired in the invention for preparing, and strengthens hair toughness,
Scalp and hair-care and relieving itching and removing dandruff aspect effect are moistened substantially, while beneficial to the absorption of hair.
Compared with prior art, the reparation hair film that the present invention is provided has the advantage that:
1) the reparation hair film that the present invention is provided, can repair damaged hair, strengthen hair toughness, moisten scalp and hair-care;
2) the reparation hair film that the present invention is provided, can be salubrious comfortable with relieving itching and removing dandruff;
3) the reparation hair film that the present invention is provided, it is non-stimulated to skin safe, it is easy to absorb.
Specific embodiment
Below by specific embodiment, the present invention is described in further detail, and following examples are only limitted to the mesh of illustration
, it is not intended to limit protection scope of the present invention.
Embodiment 1 is a kind of to repair hair film
Described reparation hair film is made up of following components and its percentage by weight:
APG 2%, behenyl base trimethyl ammonium chloride 8%, dimethyl silicone polymer 2%, menthol 1%, hyalomitome
Sour sodium 3.2%, cetostearyl alcohol 3.2%, glycerine 1.6%, hydrolyzed wheat protein 8.4%, lecithin 2.8%, lanolin
2.8%th, climbazole 1%, patchouli alcohol 1%, EDTA- disodiums 0.1%, citric acid 0.1%, methyl hydroxybenzoate 0.1%, essence
0.1%th, spermaceti ethylhydroxyethylcellulose 2% and water 60.6%.
Preparation method:
S1 is added water in container, is heated to 75 DEG C, and APG, behenyl base trimethyl ammonium chloride are added while stirring
And dimethyl silicone polymer, stir to being completely dissolved, obtain solution A;
Step S1 resulting solutions A is cooled to 70 DEG C by S2, and EDTA- disodiums and methyl hydroxybenzoate are added while stirring, and stirring is equal
It is even, obtain solution B;
Step S2 resulting solutions B is cooled to 55 DEG C by S3, and menthol, Sodium Hyaluronate, cetearyl alcohol are added while stirring
Alcohol, glycerine, hydrolyzed wheat protein, lecithin, lanolin, climbazole and patchouli alcohol, stir to being completely dissolved, and obtain solution C;
Step S3 resulting solutions C is cooled to 35 DEG C by S4, adds essence, while be 6.1 with lemon acid for adjusting pH value, finally
It is 4200 to add coconut oleoyl amine MEA regulation viscosity, is stirred, and is obtained final product.
Embodiment 2 is a kind of to repair hair film
Described reparation hair film is made up of following components and its percentage by weight:
It is APG 4%, behenyl base trimethyl ammonium chloride 13%, dimethyl silicone polymer 3%, menthol 1.5%, transparent
Matter acid sodium 4.8%, cetostearyl alcohol 4.8%, glycerine 2.4%, hydrolyzed wheat protein 11.4%, lecithin 3.8%, lanolin
3.8%th, climbazole 2%, patchouli alcohol 3%, EDTA- disodiums 0.2%, citric acid 0.2%, methyl hydroxybenzoate 0.2%, essence
0.2%th, spermaceti ethylhydroxyethylcellulose 4% and water 37.7%.
Preparation method is similar to Example 1.
Embodiment 3 is a kind of to repair hair film
Described reparation hair film is made up of following components and its percentage by weight:
APG 6%, behenyl base trimethyl ammonium chloride 18%, dimethyl silicone polymer 4%, menthol 2%, hyalomitome
Sour sodium 6.4%, cetostearyl alcohol 6.4%, glycerine 3.2%, hydrolyzed wheat protein 14.4%, lecithin 4.8%, lanolin
4.8%th, climbazole 3%, patchouli alcohol 5%, EDTA- disodiums 0.3%, citric acid 0.3%, methyl hydroxybenzoate 0.3%, essence
0.3%th, spermaceti ethylhydroxyethylcellulose 6% and water 14.8%.
Preparation method is similar to Example 1.
Comparative example 1 is a kind of to repair hair film
Described reparation hair film is made up of following components and its percentage by weight:
It is APG 4%, behenyl base trimethyl ammonium chloride 13%, dimethyl silicone polymer 3%, menthol 1.5%, transparent
It is matter acid sodium 4%, cetostearyl alcohol 4%, glycerine 4%, hydrolyzed wheat protein 11.4%, lecithin 3.8%, lanolin 3.8%, sweet
Precious element 2%, patchouli alcohol 3%, EDTA- disodiums 0.2%, citric acid 0.2%, methyl hydroxybenzoate 0.2%, essence 0.2%, cetyl
Hydroxyethyl cellulose 4% and water 37.7%.
Preparation method is similar to Example 1.
Difference with embodiment 2 is that the weight of Sodium Hyaluronate, cetostearyl alcohol and glycerine is compared into 2:2:1 replaces with
1:1:1。
Comparative example 2 is a kind of to repair hair film
Described reparation hair film is made up of following components and its percentage by weight:
It is APG 4%, behenyl base trimethyl ammonium chloride 13%, dimethyl silicone polymer 3%, menthol 1.5%, transparent
Matter acid sodium 4.8%, cetostearyl alcohol 4.8%, glycerine 2.4%, hydrolyzed wheat protein 6.33%, lecithin 6.33%, lanolin
6.34%th, climbazole 2%, patchouli alcohol 3%, EDTA- disodiums 0.2%, citric acid 0.2%, methyl hydroxybenzoate 0.2%, essence
0.2%th, spermaceti ethylhydroxyethylcellulose 4% and water 37.7%.
Preparation method is similar to Example 1.
Difference with embodiment 2 is that the weight of hydrolyzed wheat protein, lecithin and lanolin is compared into 3:1:1 replaces with
1:1:1。
Test example one, irritation test/toxicology test
1. test material:Reparation hair film prepared by embodiment 1-3.
2. subjects:Choose healthy rabbit 60, body weight 180-220g, male and female half and half.
3. content of the test:
Rabbit is randomly divided into 3 groups, every group 20, embodiment 1-3 groups is denoted as.24h before experiment, cuts off experiment white rabbit back
The hair of backbone both sides, it is respectively 3cm × 3cm not damage epidermis, unhairing scope or so.Reparation hair film prepared by Example 1-3 is each
0.5g is added on 4 layers of gauze of 2.5cm × 2.5cm, is affixed on side skin, another with immobilization with adhesive tape after being covered with one layer of oilpaper
Side is blank.Gauze is removed after closing 4h, and is cleaned with clear water, this observes recipient site local skin after 1,24,48h
Reaction, presses《Cosmetics health specification》(version in 2007) skin irritation/corrosion test carries out dermoreaction scoring, with tested
The average value of animal integration carries out overall merit, and observes other side effects effect in addition to excitant.
4. result of the test:
Each observing time point top average < 0.5 in experiment, belongs to nonirritant.That is, skin irritation test result
For:It is nonirritant.Acute ocular irritation test result is:It is nonirritant.Therefore the reparation that the present invention is provided sends out film to skin temperature
With it is nontoxic non-stimulated.
Test example two, sensory evaluation is tested
1. test material:Reparation hair film prepared by embodiment 1-3 and comparative example 1-2.
2. subjects:The people of crowd 100 on probation, at 20-40 Sui, women, hair generally occurs in that hair is done for age distribution
Phenomenon that is withered, following the string with flexibility, may not influence the other diseases of this result of the test.
3. content of the test:
Crowd on probation is divided into 5 groups, every group of 20 people, i.e. embodiment 1-3 groups and comparative example 1-2 groups, respectively to embodiment 1-3
And reparation hair film sensory evaluation test prepared by comparative example 1-2, each sampling January, tester according to oneself feel into
Row scoring.Standards of grading:Ten point system is taken, 1 point worst, 10 points best, and fraction more high effect is better.
4. result of the test:Various reparation hair film using effect evaluation results are as shown in table 1.
Table 1 repairs hair film sensory evaluation effect
As shown in Table 1, preferably, i.e., the reparation hair film that prepared by the present invention is or not the sensory evaluation of the reparation hair film that prepared by the present invention
Damaged hair, enhancing hair toughness can only be repaired, additionally it is possible to moisten scalp and hair-care, relieving itching and removing dandruff.And prepared by comparative example 1-2
The sensory evaluation for repairing hair film is relatively of the invention poor, illustrate that compatibility of the present invention is reasonable, science, and each component has mutually cooperateed with reparation
Damaged hair, strengthens hair toughness, moistens scalp and hair-care, the effect of relieving itching and removing dandruff.Meanwhile, the reparation hair film that the present invention is provided makes
With it is rear substantially feel it is salubrious, comfortable, without greasy feeling.
Claims (6)
1. it is a kind of to repair hair film, it is characterised in that including following components and its percentage by weight:
APG 2-6%, behenyl base trimethyl ammonium chloride 8-18%, dimethyl silicone polymer 2-4%, menthol 1-2%, guarantor
Humectant 8-16%, care agent 14-24%, climbazole 1-3%, patchouli alcohol 1-5%, EDTA- disodium 0.1-0.3%, citric acid
0.1-0.3%, methyl hydroxybenzoate 0.1-0.3%, essence 0.1-0.3%, spermaceti ethylhydroxyethylcellulose 2-6% and water 14.8-
60.6%.
2. it is as claimed in claim 1 to repair hair film, it is characterised in that to be made up of following components and its percentage by weight:Alkyl
Glucosides 4%, behenyl base trimethyl ammonium chloride 13%, dimethyl silicone polymer 3%, menthol 1.5%, NMF 12%, nursing
Agent 19%, climbazole 2%, patchouli alcohol 3%, EDTA- disodiums 0.2%, citric acid 0.2%, methyl hydroxybenzoate 0.2%, essence
0.2%th, spermaceti ethylhydroxyethylcellulose 4% and water 37.7%.
3. it is as claimed in claim 1 or 2 to repair hair film, it is characterised in that the NMF is by Sodium Hyaluronate, cetearyl alcohol
Alcohol and glycerine are by weight 2:2:1 composition.
4. it is as claimed in claim 1 or 2 to repair hair film, it is characterised in that the care agent is by hydrolyzed wheat protein, lecithin
With lanolin by weight 3:1:1 composition.
5. the preparation method of film is sent out in the reparation as described in claim 1-4 is any, it is characterised in that comprise the following steps:
S1 is added water in container, is heated to 70~80 DEG C, and APG, behenyl base trimethyl ammonium chloride are added while stirring
And dimethyl silicone polymer, stir to being completely dissolved, obtain solution A;
Step S1 resulting solutions A is cooled to 65~75 DEG C by S2, and EDTA- disodiums and methyl hydroxybenzoate are added while stirring, and stirring is equal
It is even, obtain solution B;
Step S2 resulting solutions B is cooled to 50~60 DEG C by S3, and menthol, NMF, care agent, climbazole are added while stirring
And patchouli alcohol, stir to being completely dissolved, obtain solution C;
Step S3 resulting solutions C is cooled to 30~40 DEG C by S4, adds essence, while with lemon acid for adjusting pH value to 5.5-6.5,
It is eventually adding coconut oleoyl amine MEA and adjusts viscosity to 4000-5000, stir, obtains final product.
6. it is as claimed in claim 5 to repair the preparation method for sending out film, it is characterised in that pH is 6.1, viscosity in the step S4
It is 4200.
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Cited By (3)
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CN107296787A (en) * | 2017-08-01 | 2017-10-27 | 曾万祥 | A kind of deep layer repairs moisturizing hair film and preparation method thereof |
CN107789212A (en) * | 2017-09-30 | 2018-03-13 | 朱耀灯 | A kind of water moistens glossy Haircare composition |
CN111631983A (en) * | 2019-03-01 | 2020-09-08 | 广州旭妆生物科技有限公司 | Softening and repairing hair care composition and application thereof |
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CN104116665A (en) * | 2013-04-28 | 2014-10-29 | 刘梅 | Deep moisturizing and repairing hair mask |
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CN102258443A (en) * | 2011-07-19 | 2011-11-30 | 高志亮 | Nutrient hair mask |
CN104116665A (en) * | 2013-04-28 | 2014-10-29 | 刘梅 | Deep moisturizing and repairing hair mask |
CN103565677A (en) * | 2013-11-12 | 2014-02-12 | 上海方木精细化工有限公司 | Refreshing lemon liquid soap |
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CN107296787A (en) * | 2017-08-01 | 2017-10-27 | 曾万祥 | A kind of deep layer repairs moisturizing hair film and preparation method thereof |
CN107789212A (en) * | 2017-09-30 | 2018-03-13 | 朱耀灯 | A kind of water moistens glossy Haircare composition |
CN111631983A (en) * | 2019-03-01 | 2020-09-08 | 广州旭妆生物科技有限公司 | Softening and repairing hair care composition and application thereof |
CN111631983B (en) * | 2019-03-01 | 2023-02-03 | 广州旭妆生物科技有限公司 | Softening and repairing hair care composition and application thereof |
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Application publication date: 20170531 |