CN107296787A - A kind of deep layer repairs moisturizing hair film and preparation method thereof - Google Patents
A kind of deep layer repairs moisturizing hair film and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
Moisturizing hair film and preparation method thereof is repaired the present invention relates to a kind of deep layer, deep layer of the invention repairs the component that moisturizing hair film includes following weight percentage：Ginseng extract：5%~30%；Cation opsonizing agent：2.6%~9.5%；Thickener/emulsifier：0.7%~3%；Assign fat agent：1.8%~8%；Hair renovation agent：1.5%~11.5%；Anti-sensitizer：0.1%~1%；NMF：2%~10%；Preservative：0.015%~0.11%；PH adjusting agent：0.1%~0.5%；Essence：0.5%~1%, surplus is deionized water.Hydrolysis silk and silk gum with deep layer repair and the ethoxy urea and the composition of glycerine acted on efficient moisture-retention are with the addition of in the hair film that the present invention is provided, hair can be made to fully absorb nutrition and reach after can also make hair keep moistening smooth while deep layer repairs hair effect.
Description
Technical field
Film is sent out the present invention relates to one kind, more particularly to a kind of deep layer repairs moisturizing hair film and preparation method thereof.
Background technology
As environmental pollution is increasingly severe, hair dyeing and perm becomes more and more popular, the hair of people is impaired serious, adds and day
The life and work pressure all increased, causes dark hair to become withered crude, intensely dark, it is impossible to return to the state of healthy healthy hair, if
Handle not in time, not only hair root of hair can be made to damage completely, and individual also can produce worry because of hair, affect the life of people
Bioplasm amount.The appearance of the various hair diseases faced during these are daily, main cause be still we cleaning hair and scalp it
Afterwards, without being supplemented the nutrients in time to hair, washed just as daily after sheath skin to the sufficient nutrition of skin, we should discount
Hair and scalp fully absorb nutrition, and form protective layer outside hair simultaneously, protect it from damage, keep soft, glossy, richness
It is flexible.
It is a kind of moist hair treatment waxes to send out film, and it is the process that a deep layer conserves hair, sends out in film and contains after use
Some nutriment and moisture can enter in hair through the hair scale piece on hair, help repairing fiber tissue, make it recover to live
The hair quality for being difficult to arrange because impaired is nourished and repaired to power, depth, makes its reply health, soft glossy, be especially suitable for it is withered and
Damaged hair.But hair film in the market generally occurs within that the nourishing time is short, assimilation effect and moisturizing repairing effect are poor, therefore
Its composition further need to be improved to meet the market demand.
The A of Chinese patent CN 106551835 disclose a kind of ginseng rose profit hair hair film, and with the addition of that hair easily absorbs is all
Multi-nutrient：Ginseng root extract, Rosa Damascana, dexpanthenol etc. simply makes the hair scale piece of hair fully open, can
Hair is fully absorbed nutrition, and form protective layer outside hair simultaneously, prevent and treat it and be damaged again, keep soft, elasticity.But
Above-mentioned hair film does not add amino acid or protein-based hair maintenance agent, ginseng root extract, Rosa Damascana, dexpanthenol
Deng simply making the hair scale piece of hair fully open, extra nutrition will not be provided to hair, it is impossible to reach the reparation effect of profound level
Really, complete reparation state is reached.And NMF is not used, may be simply easily broken with rear hair, it is impossible to reach that moisturizing is moistened
The effect of hair.
The content of the invention
A kind of deep layer is provided and repairs moisturizing hair film it is an object of the invention to overcome the deficiencies in the prior art part, it is fitted
For withered and damaged hair, hair can be made to fully absorb nutrition after and reach that deep layer can be with while repair hair effect
Hair is set to keep moistening smooth.
To achieve the above object, the technical scheme taken of the present invention is：A kind of deep layer repairs moisturizing hair film, the hair film bag
Containing Ginseng extract, hair renovation agent and NMF, the hair renovation agent includes hydrolysis silk and silk collagen；It is described
NMF includes ethoxy urea and glycerine.
The deep layer that the present invention is provided repairs moisturizing hair film and contains Ginseng extract, hair maintenance agent and NMF.Wherein, people
Ginseng, which extracts liquid energy, makes the telangiectasis on head, improves the nutrition condition of hair, improves the tensile strength and extensibility of hair,
Make hair more compliant, it is easy to comb.Contain the plant hormone relevant with estrogen in ginseng simultaneously, the presence of these materials can
Improve skin of head blood circulation and regulation immunity, reach trichogenous effect and reduce growth period hair follicle cutin
Apoptosis and retrogression are formed, can prevent and reduce alopecia and disconnected hair, promote natural on-off cycles of hair growth development, repair impaired hair
Matter.In addition, Ginseng extract has preferable therapeutic effect to dermatitis, fungal infection, ginseng, ginseng extract etc. are added, no
But hair can be made more compliant, reduce dandruff, while preventing epilation, promoted the growth of new hair, can reach head beautiful
Effect of appearance.
The Main Ingredients and Appearance of hair is keratin, is the fibrous proteins that a class has connective and defencive function, containing many
Amino acid and several Ten microelements are planted, if iron deficiency and protein hair will turn yellow and bifurcated.And generally hair dries up and hair
Rough caused because keratin is lost in, and due to the loss of keratin, causes hair water shortage, this collagen like skin
It is lost in, the reason for causing scaly dry skin is the same.Therefore protein-based hair maintenance agent is added in hair film, so as to be hair supplement
The lac nutrition of loss, makes its glossy, healthy and strong.
Silk glue protein, is the natural polymer fibrin extracted from silk, content account for silk 70%~
80%, containing 18 kinds of amino acid, there is preferable affinity interaction to hair, can prevent in hair surface formation protectiveness transparent membrane
Only injury of the thioglycolate salt to hair, the various nutrients needed for supplement hair, improves the gloss and elasticity of hair, can be effective
Hair damage is prevented, makes hair distribute the gloss of ripples and the slim and graceful softness such as tiffany.Meanwhile, silk gum has to damaged hair
Obvious repairing effect.
Silk molecular weight is hydrolyzed between 1000-2000Da, compared with other protein hydrolysate, the absorption of silk hair is hydrolyzed
Osmosis is relied primarily on, with substantivity, therefore is easily absorbed by hair, and silk concentration is improved, then hair is to silk egg
White uptake also accordingly increases, if the hair being damaged, and the absorption and adsorbance to the fibroin of low molecule amount are bigger,
Correspondingly reparation and protective effect of the fibroin to hair are more obvious.In addition fibroin is in hair surface formation some strength
β type crystalline films, so the film that fibroin is formed on hair is difficult to be flush with water, available for hairspray.
Ethoxy urea is a kind of brand-new, the NMF with outstanding advantage, and efficient moisture-retention effect can be provided to hair products
Fruit is while and the product without sticky feel.Ethoxy urea energy scattering and permeating is entered in the cuticula of hair, increases its water content
And aquation, alleviate drying, increase its toughness, with the extensive pH scope of applications.Compared with traditional NMF, ethoxy
Urine has more significant moistening effect, there is extraordinary coating sense, and smooth coating is felt, not tacky in hair products, no
Greasy, moist comfort, and a very wide range of applicability that itself nonionic is brought.And with expensive NMF phase
Than ethoxy urea can be with lower formulation cost, to reach identical effect；Even in based on glycerine, propane diols
In basic components, ethoxy urea can also be by the consumption (such as silicone oil) of the component for reducing other influences cream outward appearance, to reach
To more preferably moistening effect, more smooth coating is felt, identical even lower formulation cost.Even if under extreme conditions, hydroxyl
Ethyl urea can also prevent cuticula from being converted to solid crystalline phase, make softness to reach by forming liquid crystalline phase with hair cuticula
Purpose.Compared with other tested NMFs (such as PAC sodium, sorbierite, urea), ethoxy urea is in many aspects all more
Plus it is prominent.
The compatibility of hair renovation agent and NMF is used, the nutriment contained in hair film can be made through on hair
Hair scale piece enters in hair, helps repairing fiber tissue, it is rejuvenated, and depth is nourished and repaired and is difficult to arrange because impaired
Hair quality, make its reply health, it is soft glossy.
The preferred embodiment that film is sent out in moisturizing is repaired as deep layer of the present invention, the Ginseng extract is in the hair film
In weight/mass percentage composition be 5~30%；Weight/mass percentage composition of the hair renovation agent in the hair film for 1.5~
11.5%；Weight/mass percentage composition of the NMF in the hair film is 2~10%.
The preferred embodiment that film is sent out in moisturizing is repaired as deep layer of the present invention, the hydrolysis silk is in the hair film
Weight/mass percentage composition be 1~10%, weight/mass percentage composition of the silk collagen in the hair film for 0.5~
1.5%, weight/mass percentage composition of the ethoxy urea in the hair film is 1~5%, matter of the glycerine in the hair film
It is 1~5% to measure percentage composition.
The preferred embodiment that film is sent out in moisturizing is repaired as deep layer of the present invention, the Ginseng extract uses such as lower section
Method is prepared from：
(1) ginseng is cleaned up, ginseng, which is then put into grinder, is milled to 60-80 mesh；
(2) Extraction solvent is driven into tank by pump, heating extraction etoh solvent, the ratio of solvent and ginseng is 5:1
~10:1, it is ensured that Extraction solvent can rapidly be warming up to 40~60 DEG C；
(3) ground ginseng is put into tank body, opens ultrasonic system, ultrasonic power is opened to 150-200W, made
With time 30min~60min, material uniformly can be acted on by ultrasonic mechanical wave, the rapid dissolution of active ingredient is to carrying
Take in solvent；
(4) liquid is extracted out, be driven into fluid reservoir, terminate ultrasonic extraction process.
Compared with prior art, the Ginseng extract that the present invention is used uses ultrasonic extraction, and its advantage is to extract effect
Rate is high；Extraction time is short, and treating capacity is big；Extracting temperature is low, has protective effect to the active ingredient in plant；Extract impurity
Few, active ingredient is easily isolated, purified；Extraction process operating cost is low, and overall economic efficiency is significant；Operation is simple, if
Standby maintenance, easy maintenance.In addition, the Ginseng extract usage amount in the present invention is very big, nutrition and the toughness of hair can be increased, grown
Profit care scalp, reduces alopecia and delays the generation of white hair.
The present invention provides a kind of deep layer and repairs moisturizing hair film, and the hair film contains the component of following weight/mass percentage composition：People
Join extract solution：5%~30%；Cation opsonizing agent：2.6%~9.5%；Thickener/emulsifier：0.7%~3%；Assign fat agent：
1.8%~8%；Hair renovation agent：1.5%~11.5%；Anti-sensitizer：0.1%~1%；NMF：2%~10%；Anti-corrosion
Agent：0.015%~0.11%；PH adjusting agent：0.1%~0.5%；Essence：0.5%~1%, surplus is deionized water.
The preferred embodiment that film is sent out in moisturizing is repaired as deep layer of the present invention, the cation opsonizing agent includes behenyl
Base trimethyl ammonium chloride, cocoyl glucoside, cetrimonium chloride, polyquaternium -37；And the behenyl base trimethyl ammonium chloride is in institute
It is 0.5%~3% to state the weight/mass percentage composition in hair film, quality percentage of the cocoyl glucoside in the hair film
Content is 1%~3%, and weight/mass percentage composition of the polyquaternium -37 in the hair film is 0.1%~1%.
The preferred embodiment that film is sent out in moisturizing is repaired as deep layer of the present invention, the thickener/emulsifier includes ethoxy
Cellulose, PPG-1 tridecanols polyethers -6, trideceth -12；And quality of the hydroxyethyl cellulose in the hair film
Percentage composition is 0.5%~2%, weight/mass percentage composition of the PPG-1 tridecanols polyethers -60 in the hair film for 1%~
0.5%, weight/mass percentage composition of the trideceth -12 in the hair film is 0.1%~0.5%.
The preferred embodiment that film is sent out in moisturizing is repaired as deep layer of the present invention, the thickener/emulsifier includes ethoxy
Cellulose, PPG-1 tridecanols polyethers -6, trideceth -12；And quality of the hydroxyethyl cellulose in the hair film
Percentage composition is 0.5%~2%, weight/mass percentage composition of the PPG-1 tridecanols polyethers -60 in the hair film for 1%~
0.5%, weight/mass percentage composition of the trideceth -12 in the hair film is 0.1%~0.5%.
The preferred embodiment of moisturizing hair film is repaired characterized in that, the tax fat agent is included as deep layer of the present invention
Hard ester-trimethyl ammonium chloride, glyceryl oleate, trihydroxy stearin, phytosterol Queensland nut oleate, propane diols two are pungent
Acid esters/dicaprate, and weight/mass percentage composition of the stearyl trimethyl ammonium chloride in the hair film is hard ester group front three
Ammonium chloride 1%~3%, weight/mass percentage composition of the glyceryl oleate in the hair film is 0.5%~2%, described three
Weight/mass percentage composition of the Oxystearin in the hair film is 0.1%~1%, and the phytosterol Queensland nut oleate exists
Weight/mass percentage composition in the hair film is 0.1%~1%, and the propylene/dicaprate is in the hair film
Weight/mass percentage composition be 0.1%~1%.
Allantoin, and institute are included as anti-sensitizer described in the preferred embodiment of deep layer of the present invention reparation moisturizing hair film
It is 0.1%~1% to state weight/mass percentage composition of the allantoin in the hair film；The pH adjusting agent includes citric acid, and described
Weight/mass percentage composition of the citric acid in the invention is 0.1%~0.5%；The preservative contain methylisothiazolinone and
Phenoxyethanol, and weight/mass percentage composition of the methylisothiazolinone in the hair film is 0.005%~0.01%.
The present invention provides a kind of deep layer and repairs the preparation method that film is sent out in moisturizing, comprises the following steps：
(1) all production apparatus are cleaned with water and carries out high-temperature disinfection treatment；
(2) deionized water is added by formula rate in emulsification pot, 85 DEG C is then heated to, according to the weight percent of raw material
Than weighing behenyl base trimethyl ammonium chloride, hydroxyethyl cellulose, trihydroxy stearin, trideceth -12, allantoin,
Matter stirs 5~10min to being uniformly dispersed, and is incubated 30min, starts cooling；
(3) when temperature is down to 40~45 DEG C, Ginseng extract, coconut palm are added in emulsification pot according to the percentage by weight of raw material
Oil base glucoside, PPG-1 tridecanols polyethers -6, cetrimonium chloride, polyquaternium -37, glyceryl oleate, the black alcohol Queensland nut of plant
Oleate, propylene/dicaprate, 10~15min of uniform stirring is uniform to being completely dispersed；
(4) temperature is down to less than 42 DEG C, emulsification pot in add hydrolytic collagen, silk glue protein, glycerine, ethoxy urea and
Preservative, 10~15min of stirring is uniform to being completely dispersed；
(5) with lemon acid for adjusting pH to inner quality standard 4.5-5.5；Viscosity is adjusted to inner quality standard 50000~80000；So
After stir, then sample censorship, it is qualified after discharge.
Compared with prior art, beneficial effects of the present invention are：The present invention deep layer repair moisturizing hair film, addition it is natural
Contain ginseng essential ingredient in Chinese herbal medicine Ginseng extract, panax ginseng extractum Huaneng Group improves the nutrition condition of hair, improve the anti-of hair
Tensile strength and extensibility, make hair more compliant, it is easy to comb, reachable also with preventing with reducing alopecia and the effect of disconnected hair
To effect of head beauty.Hair maintenance agent is used as using the composition of silk glue protein and hydrolysis silk so that hair and head
Skin not only obtains deep layer and nourishes but also obtain deep layer reparation, is that hair supplements the nutrients.Using ethoxy urea and glycerine compounding conduct
NMF, NMF used can be entered in the cuticula of hair with scattering and permeating so that not uninteresting after hair is dry, be remained in that
Hair is persistently moistened in the epidermis of wetting, lasting moisturizing.Hair film of the present invention, using Ginseng extract, silk glue protein, hydrolysis silkworm
Silk, ethoxy urea and glycerine carry out compounded combination so that the hair film has the effect of deep layer reparation moisturizing.
Embodiment
For the object, technical solutions and advantages of the present invention are better described, below in conjunction with specific embodiment to the present invention
It is described further.
Embodiment 1
Deep layer of the present invention repairs a kind of embodiment that film is sent out in moisturizing, deep layer described in the present embodiment repair moisturizing hair film include with
The component of lower weight/mass percentage composition：Ginseng extract 30%；Cation opsonizing agent 6.3% (behenyl base trimethyl ammonium chloride 2%,
Cocoyl glucoside 2.5%, cetrimonium chloride 1.5%, polyquaternium -37 are 0.3%)；(the hydroxy ethyl fiber of thickener/emulsifier 2.0%
Element 1.5%, PPG-1 tridecanols polyethers -60.2%, trideceth -120.3%)；Assign (the hard ester-trimethyl of fat agent 3.9%
Ammonium chloride 2%, glyceryl oleate 0.8%, trihydroxy stearin 0.3%, phytosterol Queensland nut oleate 0.5%, the third two
Alcohol dicaprylate/dicaprate 0.3%)；Hair renovation agent 2.3% (silk glue protein 0.8%, hydrolysis silk 1.5%)；Antiallergic
Agent (allantoin) 0.5%；NMF 6% (glycerine 3%, ethoxy urea 3%)；(the methylisothiazolinone of preservative 0.088%
0.008%th, Phenoxyethanol 0.08%)；PH adjusting agent (citric acid) 0.3%；Remaining is water.
Deep layer described in the present embodiment repairs the preparation method that film is sent out in moisturizing, comprises the following steps：
(1) all production apparatus are cleaned with water and carries out high-temperature disinfection treatment；
(2) deionized water is added by formula rate in emulsification pot, 85 DEG C is then heated to, according to the weight percent of raw material
Than weighing behenyl base trimethyl ammonium chloride, hydroxyethyl cellulose, trihydroxy stearin, trideceth -12, allantoin,
Matter stirs 5~10min to being uniformly dispersed, and is incubated 30min, starts cooling；
(3) when temperature is down to 40~45 DEG C, Ginseng extract, coconut palm are added in emulsification pot according to the percentage by weight of raw material
Oil base glucoside, PPG-1 tridecanols polyethers -6, cetrimonium chloride, polyquaternium -37, glyceryl oleate, the black alcohol Queensland nut of plant
Oleate, propylene/dicaprate, 10~15min of uniform stirring is uniform to being completely dispersed；
(4) temperature is down to less than 42 DEG C, emulsification pot in add hydrolytic collagen, silk glue protein, glycerine, ethoxy urea and
Preservative, 10~15min of stirring is uniform to being completely dispersed；
(5) with lemon acid for adjusting pH to inner quality standard 4.5-5.5；Viscosity is adjusted to inner quality standard 50000~80000；So
After stir, then sample censorship, it is qualified after discharge.Ginseng extract used can be made by oneself or directly buy in city in the present embodiment
, it is preferable that the Ginseng extract is adopted to be prepared from the following method：
(1) ginseng is cleaned up, ginseng, which is then put into grinder, is milled to 60-80 mesh；
(2) Extraction solvent is driven into tank by pump, heating extraction etoh solvent, the ratio of solvent and ginseng is 5:1
~10:1, it is ensured that Extraction solvent can rapidly be warming up to 40~60 DEG C；
(3) ground ginseng is put into tank body, opens ultrasonic system, ultrasonic power is opened to 150-200W, made
With time 30min~60min, material uniformly can be acted on by ultrasonic mechanical wave, the rapid dissolution of active ingredient is to carrying
Take in solvent；
(4) liquid is extracted out, be driven into fluid reservoir, terminate ultrasonic extraction process
Embodiment 2
Deep layer of the present invention repairs a kind of embodiment that film is sent out in moisturizing, deep layer described in the present embodiment repair moisturizing hair film include with
The component of lower weight/mass percentage composition：Ginseng extract 20%；Cation opsonizing agent 6.3% (behenyl base trimethyl ammonium chloride 2%,
Cocoyl glucoside 2.5%, cetrimonium chloride 1.5%, polyquaternium -37 are 0.3%)；(the hydroxy ethyl fiber of thickener/emulsifier 2.0%
Element 1.5%, PPG-1 tridecanols polyethers -60.2%, trideceth -12：0.3%)；Assign (the hard ester group front three of fat agent 3.9%
Ammonium chloride 2%, glyceryl oleate 0.8%, trihydroxy stearin 0.3%, phytosterol Queensland nut oleate 0.5%, third
Glycol dicaprylate/dicaprate 0.3%)；Hair renovation agent 2.3% (silk glue protein 0.8%, hydrolysis silk 1.5%)；It is anti-
Quick dose of (allantoin) 0.5%；NMF 6% (glycerine 3%, ethoxy urea 3%)；(the methylisothiazolinone of preservative 0.088%
0.008%th, Phenoxyethanol 0.08%)；PH adjusting agent (citric acid) 0.3%；Remaining is water.
Deep layer described in the present embodiment repairs the preparation method that film is sent out in moisturizing, as described in Example 1.
Embodiment 3
Deep layer of the present invention repairs a kind of embodiment that film is sent out in moisturizing, deep layer described in the present embodiment repair moisturizing hair film include with
The component of lower weight/mass percentage composition：Ginseng extract 10%；Cation opsonizing agent 6.3% (behenyl base trimethyl ammonium chloride 2%,
Cocoyl glucoside 2.5%, cetrimonium chloride 1.5%, polyquaternium -37 are 0.3%)；(the hydroxy ethyl fiber of thickener/emulsifier 2.0%
Element 1.5%, PPG-1 tridecanols polyethers -60.2%, trideceth -120.3%)；Assign (the hard ester-trimethyl of fat agent 3.9%
Ammonium chloride 2%, glyceryl oleate 0.8%, trihydroxy stearin 0.3%, phytosterol Queensland nut oleate 0.5%, the third two
Alcohol dicaprylate/dicaprate 0.3%)；Hair renovation agent 2.3% (silk glue protein 0.8%, hydrolysis silk 1.5%)；Antiallergic
Agent (allantoin) 0.5%；NMF 6% (glycerine 3%, ethoxy urea 3%)；(the methylisothiazolinone of preservative 0.088%
0.008%th, Phenoxyethanol 0.08%)；PH adjusting agent (citric acid) 0.3%；Remaining is water.
Deep layer described in the present embodiment repairs the preparation method that film is sent out in moisturizing, as described in Example 1.
Embodiment 4
Deep layer of the present invention repairs a kind of embodiment that film is sent out in moisturizing, deep layer described in the present embodiment repair moisturizing hair film include with
The component of lower weight/mass percentage composition：Ginseng extract 20%；Cation opsonizing agent 6.3% (behenyl base trimethyl ammonium chloride 2%,
Cocoyl glucoside 2.5%, cetrimonium chloride 1.5%, polyquaternium -37 are 0.3%)；(the hydroxy ethyl fiber of thickener/emulsifier 2.0%
Element 1.5%, PPG-1 tridecanols polyethers -6,0.2%；Trideceth -12 is 0.3%)；Assign (the hard ester group front three of fat agent 3.9%
Ammonium chloride 2%, glyceryl oleate 0.8%, trihydroxy stearin 0.3%, phytosterol Queensland nut oleate 0.5%, third
Glycol dicaprylate/dicaprate 0.3%)；Hair renovation agent 1.3% (silk glue protein 0.8%, hydrolysis silk 0.5%)；It is anti-
Quick dose of (allantoin) 0.5%；NMF 6% (glycerine 3%, ethoxy urea 3%)；(the methylisothiazolinone of preservative 0.088%
0.008%th, Phenoxyethanol 0.08%)；PH adjusting agent (citric acid) 0.3%；Remaining is water.
Deep layer described in the present embodiment repairs the preparation method that film is sent out in moisturizing, as described in Example 1.
Embodiment 5
Deep layer of the present invention repairs a kind of embodiment that film is sent out in moisturizing, deep layer described in the present embodiment repair moisturizing hair film include with
The component of lower weight/mass percentage composition：Ginseng extract 20%；Cation opsonizing agent 6.3% (behenyl base trimethyl ammonium chloride 2%,
Cocoyl glucoside 2.5%, cetrimonium chloride 1.5%, polyquaternium -37 are 0.3%)；(the hydroxy ethyl fiber of thickener/emulsifier 2.0%
Element：1.5%；PPG-1 tridecanols polyethers -6：0.2%；Trideceth -12：0.3%)；Assign (the hard ester group three of fat agent 3.9%
Ammonio methacrylate 2%, glyceryl oleate 0.8%, trihydroxy stearin 0.3%, phytosterol Queensland nut oleate 0.5%,
Propylene/dicaprate 0.3%)；Hair renovation agent 2.3% (silk glue protein 0.8%, hydrolysis silk 1.5%)；
Anti-sensitizer (allantoin) 0.5%；NMF 4% (glycerine 3%, ethoxy urea 1%)；(the methylisothiozoline of preservative 0.088%
Ketone 0.008%, Phenoxyethanol 0.08%)；PH adjusting agent (citric acid) 0.3%；Remaining is water.
Deep layer described in the present embodiment repairs the preparation method that film is sent out in moisturizing, as described in Example 1.
Embodiment 6
Deep layer of the present invention repairs a kind of embodiment that film is sent out in moisturizing, deep layer described in the present embodiment repair moisturizing hair film include with
The component of lower weight/mass percentage composition：Ginseng extract 5%；Cation opsonizing agent 2.6% (behenyl base trimethyl ammonium chloride 0.5%,
Cocoyl glucoside 1%, cetrimonium chloride 1%, polyquaternium -37 are 0.1%)；(the hydroxyethyl cellulose of thickener/emulsifier 0.7%
0.5%th, PPG-1 tridecanols polyethers -6 0.1%, trideceth -12 be 0.1%)；Assign (the hard ester-trimethyl of fat agent 1.8%
Ammonium chloride 1%, glyceryl oleate 0.5%, trihydroxy stearin 0.1%, phytosterol Queensland nut oleate 0.1%, the third two
Alcohol dicaprylate/dicaprate 0.1%)；Hair renovation agent 1.5% (silk glue protein 0.5%, hydrolysis silk 1%)；Anti-sensitizer
(allantoin) 0.1%；NMF 2% (glycerine 1%, ethoxy urea 1%)；(the methylisothiazolinone of preservative 0.015%
0.005%th, Phenoxyethanol 0.01%)；PH adjusting agent (citric acid) 0.1%；Remaining is water.
Deep layer described in the present embodiment repairs the preparation method that film is sent out in moisturizing, as described in Example 1.
Embodiment 7
Deep layer of the present invention repairs a kind of embodiment that film is sent out in moisturizing, deep layer described in the present embodiment repair moisturizing hair film include with
The component of lower weight/mass percentage composition：Ginseng extract 30%；Cation opsonizing agent 9.5% (behenyl base trimethyl ammonium chloride 3%,
Cocoyl glucoside 3%, cetrimonium chloride 2.5%, polyquaternium -37 are 1%)；(the hydroxyethyl cellulose of thickener/emulsifier 2.0%
3%th, PPG-1 tridecanols polyethers -6 0.5%, trideceth -12 be 0.5%)；Assign (the hard ester-trimethyl chlorination of fat agent 8%
Ammonium 3%, glyceryl oleate 2%, trihydroxy stearin 1%, phytosterol Queensland nut oleate 1%, propylene/
Dicaprate 1%)；(the silk glue protein 1.5% of hair renovation agent 11.5%；Hydrolyze silk 10%)；Anti-sensitizer (allantoin)
1%；NMF 10% (glycerine 5%, ethoxy urea 5%)；Preservative 0.015% (methylisothiazolinone 0.01%, benzene oxygen second
Alcohol 1%)；PH adjusting agent (citric acid) 0.5%；Remaining is water.
Deep layer described in the present embodiment repairs the preparation method that film is sent out in moisturizing, as described in Example 1.
Embodiment 8
Physico-chemical tests are carried out to present invention hair film, gained Testing index is as follows
(1) character is detected
This product is that viscosity is suitable, is had good stability, fragrant is charming, silk profit is smooth, fine and smooth uniform milky hair
Film
(2) pH value is detected
This product is sampled, and is determined with pH meter, and it is 4.5~5.5 to measure pH value
(3) viscosity number is detected
This product is sampled, and is determined with viscosimeter, is measured viscosity number ＞ 100000
(4) Detection of Stability
This product is sampled, and is encapsulated in transparence cosmetic bottle, be respectively placed in quartz lamp illumination, -15 DEG C, 5 DEG C, 25 DEG C,
Under 48 DEG C of experiment conditions, the continuance test of 3 months by a definite date, observation are carried out to outward appearance, fragrance, pH value, viscosity and sundry item
Whether the bad phenomenons such as bleed, layering, separation, precipitation, discoloration, peculiar smell, demulsification is occurred, testing result shows, the bad knot of the above
Fruit is not appeared in test process, illustrates that it has good stability.
(5) centrifugation detection
This product is sampled, and is encapsulated in centrifuge tube and is centrifuged 30min under 3000r/min, sees whether occur not disperseing
Composition, testing result shows not dispersion component do not occur, illustrates that its Combination is good.
(6) anaphylaxis is stimulated to detect
This product is sampled, and it is applied in right amount on volunteer (18-58 Sui, 30 people) the back of the hand and is observed 30min, sees whether it occurs
The phenomenons such as redness, dermexanthesis, foaming, observation indicate that, ill symptomses do not occur, and illustrate that this product will not produce stimulation to skin
And allergy sex chromosome mosaicism.
(7) hair film resultant effect detection
Control group and test group are set, and control group is divided into 6 groups, and test group is divided into 7 groups.
6 groups of control group difference are as follows：
Control group 1：One kind hair film, the hair film is free of Ginseng extract, includes the component of following weight/mass percentage composition：Sun
Ion conditioner 6.3% (behenyl base trimethyl ammonium chloride 2%, cocoyl glucoside 2.5%, cetrimonium chloride 1.5%, polyquaternary amine
Salt -37 is 0.3%)；Thickener/emulsifier 2.0% (hydroxyethyl cellulose 1.5%, PPG-1 tridecanols polyethers -60.2%, tridecane
Alcohol polyethers -120.3%)；Assigning fat agent 3.9%, (hard ester-trimethyl ammonium chloride 2%, glyceryl oleate 0.8%, trihydroxy are stearic
Essence 0.3%, phytosterol Queensland nut oleate 0.5%, propylene/dicaprate 0.3%)；Hair renovation agent
2.3% (silk glue protein 0.8%, hydrolysis silk 1.5%)；Anti-sensitizer (allantoin) 0.5%；NMF 6% (glycerine 3%, hydroxyl
Ethyl carbamide 3%)；Preservative 0.088% (methylisothiazolinone 0.008%, Phenoxyethanol 0.08%)；PH adjusting agent (lemon
Acid) 0.3%；Remaining is water.
Control group 2：One kind hair film, the hair film is free of hair renovation agent, includes the component of following weight/mass percentage composition：People
Join extract solution 30%；Cation opsonizing agent 6.3% (behenyl base trimethyl ammonium chloride 2%, cocoyl glucoside 2.5%, the bent chlorine in west
Ammonium 1.5%, polyquaternium -37 are 0.3%)；Thickener/emulsifier 2.0% (hydroxyethyl cellulose 1.5%, PPG-1 tridecanols polyethers-
60.2%th, trideceth -120.3%)；Assign fat agent 3.9% (hard ester-trimethyl ammonium chloride 2%, glyceryl oleate
0.8%th, trihydroxy stearin 0.3%, phytosterol Queensland nut oleate 0.5%, propylene/dicaprate
0.3%)；Anti-sensitizer (allantoin) 0.5%；NMF 6% (glycerine 3%, ethoxy urea 3%)；(the methyl of preservative 0.088%
OIT 0.008%, Phenoxyethanol 0.08%)；PH adjusting agent (citric acid) 0.3%；Remaining is water.
Control group 3：One kind hair film, the hair film is free of NMF, includes the component of following weight/mass percentage composition：Ginseng is carried
Take liquid 30%；Cation opsonizing agent 6.3% (behenyl base trimethyl ammonium chloride 2%, cocoyl glucoside 2.5%, cetrimonium chloride
1.5%th, polyquaternium -37 is 0.3%)；Thickener/emulsifier 2.0% (hydroxyethyl cellulose 1.5%, PPG-1 tridecanols polyethers-
60.2%th, trideceth -120.3%)；Assign fat agent 3.9% (hard ester-trimethyl ammonium chloride 2%, glyceryl oleate
0.8%th, trihydroxy stearin 0.3%, phytosterol Queensland nut oleate 0.5%, propylene/dicaprate
0.3%)；Hair renovation agent 2.3% (silk glue protein 0.8%, hydrolysis silk 1.5%)；Anti-sensitizer (allantoin) 0.5%；It is anti-
Rotten agent 0.088% (methylisothiazolinone 0.008%, Phenoxyethanol 0.08%)；PH adjusting agent (citric acid) 0.3%；Remaining
For water.
Control group 4：One kind hair film, the hair film is free of ginseng and hair renovation agent, includes following weight/mass percentage composition
Component：Cation opsonizing agent 6.3% (behenyl base trimethyl ammonium chloride 2%, cocoyl glucoside 2.5%, cetrimonium chloride 1.5%,
Polyquaternium -37 is 0.3%)；Thickener/emulsifier 2.0% (hydroxyethyl cellulose 1.5%, PPG-1 tridecanols polyethers -60.2%,
Trideceth -120.3%)；Assign fat agent 3.9% (hard ester-trimethyl ammonium chloride 2%, glyceryl oleate 0.8%, three hydroxyls
Base stearin 0.3%, phytosterol Queensland nut oleate 0.5%, propylene/dicaprate 0.3%)；Antiallergic
Agent (allantoin) 0.5%；NMF 6% (glycerine 3%, ethoxy urea 3%)；(the methylisothiazolinone of preservative 0.088%
0.008%th, Phenoxyethanol 0.08%)；PH adjusting agent (citric acid) 0.3%；Remaining is water.
Control group 5：One kind hair film, the hair film is free of ginseng and NMF, includes the component of following weight/mass percentage composition：
Cation opsonizing agent 6.3% (behenyl base trimethyl ammonium chloride 2%, cocoyl glucoside 2.5%, cetrimonium chloride 1.5%, poly- season
Ammonium salt -37 is 0.3%)；Thickener/emulsifier 2.0% (hydroxyethyl cellulose 1.5%, PPG-1 tridecanols polyethers -6 0.2%, 13
Alkanol polyethers -12 is 0.3%)；Assigning fat agent 3.9%, (hard ester-trimethyl ammonium chloride 2%, glyceryl oleate 0.8%, trihydroxy are hard
Fat essence 0.3%, phytosterol Queensland nut oleate 0.5%, propylene/dicaprate 0.3%)；Hair is repaired
Agent 2.3% (silk glue protein 0.8%, hydrolysis silk 1.5%)；Anti-sensitizer (allantoin) 0.5%；(the methyl of preservative 0.088%
OIT 0.008%, Phenoxyethanol 0.08%) pH adjusting agent；(citric acid) 0.3%；Remaining is water.
Control group 6：One kind hair film, the hair film is free of hair renovation agent and NMF, includes following weight/mass percentage composition
Component：
Ginseng extract 30%；Cation opsonizing agent 6.3% (behenyl base trimethyl ammonium chloride 2%, cocoyl glucoside
2.5%th, cetrimonium chloride 1.5%, polyquaternium -37 be 0.3%)；Thickener/emulsifier 2.0% (hydroxyethyl cellulose 1.5%, PPG-
1 tridecanol polyethers -60 0.2%, trideceth -12 are 0.3%)；Assign (the hard ester-trimethyl ammonium chloride of fat agent 3.9%
2%th, glyceryl oleate 0.8%, trihydroxy stearin 0.3%, phytosterol Queensland nut oleate 0.5%, propane diols two are pungent
Acid esters/dicaprate 0.3%)；Anti-sensitizer (allantoin) 0.5%；Preservative 0.088% (methylisothiazolinone 0.008%,
Phenoxyethanol 0.08%)；PH adjusting agent (citric acid) 0.3%；Remaining is water.
The preparation method of hair film described in 6 groups of control groups, as described in Example 1.
The hair film that embodiment 1~7 is prepared is respectively adopted in 7 groups of test groups.
Using opinion poll point system, by asking volunteer to try out this product and filling in table on probation come overall merit this product.Point
Not Xuan Qu different age group volunteer (18-38,50 people；38-58,50 people) as object on probation, hair washing in every two days once, connects
It is continuous to use three months, fill in table on probation after trying out and scored.Every using effect total score is 5 points in grade form：5 points are highests
Point, represent very satisfied；4 points are preferable, are relatively satisfied with；3 points are to receive；Less than the 3 points models for that cannot receive
Enclose.The following is every using effect average situation：
Table 1：The grade form on probation of experimental group and control group
| Using effect | Compliance | It is alimentary | Moisture retention | It is nonirritant |
| Test group 1 | 4.95 | 4.94 | 4.94 | 5.00 |
| Test group 2 | 4.90 | 4.89 | 4.94 | 5.00 |
| Test group 3 | 4.89 | 4.82 | 4.92 | 5.00 |
| Test group 4 | 4.91 | 4.80 | 4.93 | 5.00 |
| Test group 5 | 4.94 | 4.92 | 4.84 | 5.00 |
| Test group 6 | 4.85 | 4.75 | 4.80 | 5.00 |
| Test group 7 | 4.92 | 4.92 | 4.93 | 5.00 |
| Control group 1 | 4.89 | 2.36 | 4.72 | 5.00 |
| Control group 2 | 2.25 | 4.73 | 4.80 | 5.00 |
| Control group 3 | 4.82 | 4.83 | 2.86 | 5.00 |
| Control group 4 | 2.16 | 2.27 | 4.85 | 5.00 |
| Control group 5 | 4.82 | 2.35 | 2.78 | 5.00 |
| Control group 6 | 2.20 | 4.80 | 2.76 | 5.00 |
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than the present invention is protected
The limitation of scope is protected, although being explained in detail with reference to preferred embodiment to the present invention, one of ordinary skill in the art should
Understand, technical scheme can be modified or equivalent substitution, without departing from the essence of technical solution of the present invention
And scope.
Claims (10)
1. a kind of deep layer repairs moisturizing hair film, it is characterised in that described comprising Ginseng extract, hair renovation agent and NMF
Hair renovation agent includes hydrolysis silk and silk collagen；The NMF includes ethoxy urea and glycerine.
2. deep layer as claimed in claim 1 repairs moisturizing hair film, it is characterised in that the Ginseng extract is in the hair film
Weight/mass percentage composition be 5~30%；Weight/mass percentage composition of the hair renovation agent in the hair film for 1.5~
11.5%；Weight/mass percentage composition of the NMF in the hair film is 2~10%.
3. deep layer as claimed in claim 2 repairs moisturizing hair film, it is characterised in that the hydrolysis silk is in the hair film
Weight/mass percentage composition is 1~10%, and weight/mass percentage composition of the silk collagen in the hair film is 0.5~1.5%,
Weight/mass percentage composition of the ethoxy urea in the hair film is 1~5%, quality percentage of the glycerine in the hair film
Content is 1~5%.
4. deep layer as claimed in claim 1 repairs moisturizing hair film, it is characterised in that the Ginseng extract is adopted with the following method
It is prepared from：
(1) ginseng is cleaned up, ginseng, which is then put into grinder, is milled to 60-80 mesh；
(2) Extraction solvent is driven into tank by pump, heating extraction etoh solvent, the ratio of solvent and ginseng is 5:1~10:
1, it is ensured that Extraction solvent can rapidly be warming up to 40~60 DEG C；
(3) ground ginseng is put into tank body, opens ultrasonic system, ultrasonic power is opened to 150-200W, during effect
Between 30min~60min, material uniformly can be acted on by ultrasonic mechanical wave, the rapid dissolution of active ingredient to extract it is molten
In agent；
(4) liquid is extracted out, be driven into fluid reservoir, terminate ultrasonic extraction process.
5. the deep layer as described in any one of Claims 1 to 4 repairs moisturizing hair film, it is characterised in that the hair film contains as follows
The component of weight/mass percentage composition：Ginseng extract：5%~30%；Cation opsonizing agent：2.6%~9.5%；Thickener/emulsifier：
0.7%~3%；Assign fat agent：1.8%~8%；Hair renovation agent：1.5%~11.5%；Anti-sensitizer：0.1%~1%；Moisturizing
Agent：2%~10%；Preservative：0.015%~0.11%；PH adjusting agent：0.1%~0.5%；Essence：0.5%~1%, it is remaining
Measure as deionized water.
6. deep layer as claimed in claim 5 repairs moisturizing hair film, it is characterised in that the cation opsonizing agent includes behenyl base
Trimethyl ammonium chloride, cocoyl glucoside, cetrimonium chloride, polyquaternium -37；And the behenyl base trimethyl ammonium chloride is described
It is 0.5%~3% to send out the weight/mass percentage composition in film, and quality percentage of the cocoyl glucoside in the hair film contains
Measure as 1%~3%, weight/mass percentage composition of the cetrimonium chloride in the hair film is 1%~2.5%, the polyquaternium-
37 weight/mass percentage composition in the hair film is 0.1%~1%.
7. deep layer as claimed in claim 5 repairs moisturizing hair film, it is characterised in that the thickener/emulsifier is fine comprising ethoxy
Tie up element, PPG-1 tridecanols polyethers -6, trideceth -12；And quality hundred of the hydroxyethyl cellulose in the hair film
Point content is 0.5%~2%, weight/mass percentage composition of the PPG-1 tridecanols polyethers -60 in the hair film for 1%~
0.5%, weight/mass percentage composition of the trideceth -12 in the hair film is 0.1%~0.5%.
8. deep layer as claimed in claim 5 repairs moisturizing hair film, it is characterised in that the tax fat agent includes hard ester-trimethyl
The capric acid of ammonium chloride, glyceryl oleate, trihydroxy stearin, phytosterol Queensland nut oleate, propylene/bis-
Ester, and weight/mass percentage composition of the stearyl trimethyl ammonium chloride in the hair film is hard ester-trimethyl ammonium chloride 1%
~3%, weight/mass percentage composition of the glyceryl oleate in the hair film is 0.5%~2%, and the trihydroxy stearin exists
Weight/mass percentage composition in the hair film is 0.1%~1%, and the phytosterol Queensland nut oleate is in the hair film
Weight/mass percentage composition is 0.1%~1%, and quality percentage of the propylene/dicaprate in the hair film contains
Measure as 0.1%~1%.
9. deep layer as claimed in claim 5 repairs moisturizing hair film, it is characterised in that the anti-sensitizer includes allantoin, and institute
It is 0.1%~1% to state weight/mass percentage composition of the allantoin in the hair film；The pH adjusting agent includes citric acid, and described
Weight/mass percentage composition of the citric acid in the invention is 0.1%~0.5%；The preservative contain methylisothiazolinone and
Phenoxyethanol, and weight/mass percentage composition of the methylisothiazolinone in the hair film is 0.005%~0.01%.
10. such as a kind of preparation method of deep layer reparation moisturizing hair film of any one of claim 1~9, comprise the following steps：
(1) all production apparatus are cleaned with water and carries out high-temperature disinfection treatment；
(2) deionized water is added by formula rate in emulsification pot, then heats to 85 DEG C, claim according to the percentage by weight of raw material
Behenyl base trimethyl ammonium chloride is taken, hydroxyethyl cellulose, trihydroxy stearin, trideceth -12, allantoin, homogeneous is stirred
5~10min is mixed to being uniformly dispersed, 30min is incubated, starts cooling；
(3) when temperature is down to 40~45 DEG C, Ginseng extract, cocoyl are added in emulsification pot according to the percentage by weight of raw material
Glucoside, PPG-1 tridecanols polyethers -6, cetrimonium chloride, polyquaternium -37, glyceryl oleate, the black alcohol Queensland nut oleic acid of plant
Ester, propylene/dicaprate, 10~15min of uniform stirring is uniform to being completely dispersed；
(4) temperature is down to less than 42 DEG C, and hydrolytic collagen, silk glue protein, glycerine, ethoxy urea and anti-corrosion are added in emulsification pot
Agent, 10~15min of stirring is uniform to being completely dispersed；
(5) with lemon acid for adjusting pH to inner quality standard 4.5-5.5；Viscosity is adjusted to inner quality standard 50000~80000；Then stir
Mix uniform, then sample censorship, qualified rear discharging.
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Cited By (5)
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| CN107982091A (en) * | 2017-12-14 | 2018-05-04 | 广州市博贤化妆品有限公司 | A kind of ferment is good for hair profit and supports smooth hair film |
| CN108451890A (en) * | 2018-06-21 | 2018-08-28 | 佛山市三水区嘉华化学研究院（普通合伙） | A kind of deep layer repairs moisturizing hair film and preparation method thereof |
| CN111388344A (en) * | 2020-04-08 | 2020-07-10 | 广州骐源生物科技有限公司 | Hair care and nourishing composition containing fibroin and preparation method thereof |
| CN111821220A (en) * | 2020-07-29 | 2020-10-27 | 广东领秀首美生物科技有限公司 | Hair care composition, repairing hair film and preparation method thereof |
| CN114191370A (en) * | 2021-12-31 | 2022-03-18 | 广东柏俐臣生物科技有限公司 | Hair-care gel and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107982091A (en) * | 2017-12-14 | 2018-05-04 | 广州市博贤化妆品有限公司 | A kind of ferment is good for hair profit and supports smooth hair film |
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| CN111388344A (en) * | 2020-04-08 | 2020-07-10 | 广州骐源生物科技有限公司 | Hair care and nourishing composition containing fibroin and preparation method thereof |
| CN111821220A (en) * | 2020-07-29 | 2020-10-27 | 广东领秀首美生物科技有限公司 | Hair care composition, repairing hair film and preparation method thereof |
| CN114191370A (en) * | 2021-12-31 | 2022-03-18 | 广东柏俐臣生物科技有限公司 | Hair-care gel and preparation method thereof |
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