CN108485848A - A kind of hair soap and preparation method thereof of aqueous gel phase particle - Google Patents
A kind of hair soap and preparation method thereof of aqueous gel phase particle Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/045—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on non-ionic surface-active compounds and soap
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Abstract
The invention discloses a kind of hair soaps and preparation method thereof of aqueous gel phase particle; contain hydrogel particle and plant soap base rich in active skull cap components in hair soap; hydrogel can be made to have protective effect to ginger oil, angelica extract, Flos Bombacis Malabarici extract by physical action; and reach slow release effect when using hair soap, and then give full play to anti-dandruff, the antipruritic effect of active constituent；The aerogel dressing of the present invention has significant antiinflammatory and bacteriostatic functions, can promote the healing for damaging skin, in conjunction with active constituent nutrition scalp, improves scalp environment, can effectively prevent alopecia；The hair soap ingredient of the present invention is mild, safe and non-toxic, environmentally protective, can not only clean, is anti-dandruff, is antipruritic, moreover it is possible to the problem of being effectively improved withered and yellowish hairs, short-tempered, bifurcated.
Description
Technical field
The present invention relates to cosmetic fields, and in particular to a kind of hair soap and preparation method thereof of aqueous gel phase particle.
Background technology
The epidermal cell of usual human body scalp is constantly released to epidermis as final nothing since matrix cells are constantly bred
The cuticula of life and fall off, when scalp is problematic, epidermis cannot be ripe very well, and peels off and form dandruff, normal condition
Lower dandruff amount is seldom, but since modern life pressure is big, rhythm of life is fast, environmental pollution, does not focus on the reasons such as health,
So that dandruff increases, it is accompanied by itching of the scalp, seriously affects personal image.Dandruff can substantially be divided into two classes：It is a kind of
The problems such as being drying property, being fallen off by dry scalp, scalp, causes；One is oil, by using the cortex of scalp as nutrition
Bacteria breed and cause to generate.The approach of existing anti-dandruff is generally：Deoil, appropriate moisturizing or inhibit fungi.Therefore, it washes
Product is sent out into indispensable daily necessities in for people's lives.
China Patent No. CN104146892A discloses antidandruff and antipruritic shampoo, including cassia twig, Radix Polygoni Multiflori, asarum and radix rehmanniae preparata
Bulk pharmaceutical chemicals ingredient so that shampoo have anti-dandruff and itching-relieving, restraining and sterilizing bacteria, the effect of recuperating qi-blood.China Patent No.
CN1543925 discloses a kind of shampoo cream and preparation method thereof containing eclipta, and the wherein amount of Yeradetajo extract is gross weight
Remover, builder, moisturizer, preservative and pearling agent etc. are also contained in the 40~70% of amount, have pitch-black hair, reduce head
The advantageous effect of scurf.
As the improvement of people's living standards, increasingly paying attention to health, not only require hair washing product that there is good wash
Hair, hair care, anti-dandruff, antipruritic, Anti-hair loss and other effects, also require hair washing product environmentally protective, safe.Currently, selling on the market
Although the hair washing product sold has certain anti-dandruff effect, but it is many it is anti-dandruff be not thorough, itching of the scalp is easy recurrent exerbation, use
Afterwards withered and yellowish hairs, short-tempered cannot improve.
Invention content
The purpose of the present invention is to provide a kind of hair soap and preparation method thereof of aqueous gel phase particle, mild, peace
It is Atoxic, environmentally protective, it can not only anti-dandruff and itching-relieving, moreover it is possible to the problem of being effectively improved withered and yellowish hairs, short-tempered, bifurcated.
To achieve the above object, the present invention provides the following technical solution：
A kind of hair soap of aqueous gel phase particle include mass percent be 25~75% plant soap bases and 20~
35% hydrogel phase particle.
Further, the plant soap base is prepared by vegetable oil, soapberry extract, Tea Saponin and caustic alkali
It arrives.
Further, the hydrogel phase particle includes mainly the water obtained by star polyethylene glycol and heparin derivatives
Gel dressing also includes ginger oil, angelica extract, Flos Bombacis Malabarici extract.
In addition, the present invention also provides the preparation method of hair soap, this approach includes the following steps：
(1) caustic alkali is dissolved in Tea Saponin and soapberry extract, is mixed with vegetable oil, stirred evenly, in 45~85
30~60min of saponification is carried out at DEG C, obtains plant soap base；
(2) ginger oil, Radix Angelicae Sinensis is added after star polyethylene glycol and heparin derivatives crosslinking 40min being obtained aerogel dressing
Extract, Flos Bombacis Malabarici extract object and deionized water form aquagel liquid solution gel；
(3) aquagel liquid solution gel is added in plant soap base, deionized water is added, stirring forms dispersion
Hydrogel phase particle in plant soap base；
(4) it pours into various molds, cooling 3~5d is stood at aeration-drying and can be obtained hair soap.
Caustic alkali in above-mentioned steps (1) is sodium hydroxide or potassium hydroxide；Vegetable oil is camellia oil, Avocado Oil, castor-oil plant
It is one or more in oil, wheat-germ oil, coconut oil, apricot kernel oil.And the caustic alkali accounts for the 1~5% of plant weight of oil,
Tea Saponin accounts for the 10~25% of plant weight of oil, and soapberry extract accounts for 15~30%.
In above-mentioned steps (2), heparin derivatives are more vulcanization heparin, and are 1 with ratio when star polyethylene glycol crosslinked:
2~10；Aerogel dressing accounts for the 35~50% of aquagel liquid solution gel；Ginger oil account for aquagel liquid solution gel 1~
5%；Angelica extract accounts for aquagel liquid solution gel 1~3%；Flos Bombacis Malabarici extract account for aquagel liquid solution gel 2~
8%.
It is larger that hydrogel sheet is smashed when aquagel liquid solution gel mixes in soap base in step (3) described above
Formation is smaller to obtain hydrogel phase particle.
Following introduce is made to the fractions of the present invention：
Soapberry extract beneficial substance of more human bodies containing there are many, such as：Reduced sugar, aliphatic acid, grease, oleic acid, class are recklessly
Radish element, riboflavin, protein, vitamin and amino acid, the sapindoside contained contain abundant glucosides substance, main
Will be based on Triterpene saponins, sapindoside or a kind of natural mild nonionic surfactant, modern research shows that
It can act on the effect of human skin realizes antibacterial, anti-inflammatory and anti-dandruff and itching-relieving.
Angelica extract is warm-natured, nontoxic, can expand capillary of skin, accelerates blood circulation, containing abundant micro
Element, energy nutrition scalp, improves scalp environment, prevents hair loss.
Ginger oil can improve oiliness scalp environment, can go intermittent headache, control headache, and promote hair growth.
Tea Saponin obtains foaming power with very strong, and being that one kind is good obtains natural surfactant, must not influenced, be gone by the water hardness
Dirty power is good, and for that hair can not only be made soft glossy after washing hair in hair soap, feel is good, and green non-poisonous, safe to use,
With hair care skin-care effect, and can anti-inflammatory anti-itch, anti-dandruff equal pharmacological functions.
Flos Bombacis Malabarici extract contains lupenone, the triterpenes chemical combination such as lupeol and feather fan -20 (29)-dilute -3 ketone
Object, polysaccharide and 7 flavone compounds, there is a heat-clearing, dispelling wind and eliminating dampness, activating blood circulation and reducing swelling, and pharmacological activity mainly has antibacterial, anti-inflammatory, anti-
Tumour and Hepatocyte protection, Flos Bombacis Malabarici extract and tea oil, Tea Saponin can complement each other, and play good that anti-dandruff and itching-relieving is imitated
Fruit.
Compared with prior art, the device have the advantages that it is as follows：The hydrogel phase that hair soap of the present invention contains
Grain, can make hydrogel have protective effect to ginger oil, angelica extract, Flos Bombacis Malabarici extract, and using by physical action
Reach slow release effect when hair soap, and then gives full play to anti-dandruff, the antipruritic effect of active constituent；The aerogel dressing tool of the present invention
There are significant antiinflammatory and bacteriostatic functions, the healing for damaging skin can be promoted, in conjunction with active constituent nutrition scalp, improves scalp environment,
It can effectively prevent alopecia；The hair soap ingredient of the present invention is mild, safe and non-toxic, environmentally protective, can not only clean, is anti-dandruff, is antipruritic,
The problem of also can effectively improve withered and yellowish hairs, short-tempered, bifurcated.
Specific embodiment
Below with specific embodiment, the present invention is further elaborated：
Embodiment 1
A kind of preparation method of the hair soap of aqueous gel phase particle is as follows：0.56g sodium hydroxides are dissolved in 5.6g tea soaps
It in element and 8.4g soapberry extracts, mixes, stirs evenly with 56g camellia oils, saponification 30min is carried out at 45 DEG C, is obtained
Plant soap base；It is 1 by ratio:2 star polyethylene glycol and heparin derivatives crosslinking 40min is added after obtaining aerogel dressing
0.2g ginger oil, 0.2g angelica extracts, 0.4g Flos Bombacis Malabarici extracts and 3g deionized waters form aquagel liquid solution glue
It is solidifying；20g aquagel liquid solution gels are added in 75g plant soap bases, 5g deionized waters are added, stirring forms dispersion
Hydrogel phase particle in plant soap base；It pours into various molds, cooling 3d is stood at aeration-drying and can be obtained hair washing
Soap.
Embodiment 2
A kind of preparation method of the hair soap of aqueous gel phase particle is as follows：By 0.2g potassium hydroxide be dissolved in 2g Tea Saponins and
It in 3g soapberry extracts, mixes, stirs evenly with 20g wheat-germ oils, saponification 60min is carried out at 85 DEG C, must be planted
Physical property soap base；It is 1 by ratio:2 star polyethylene glycol and heparin derivatives crosslinking 40min is added after obtaining aerogel dressing
1.75g ginger oil, 1.05g angelica extracts, 2.8g Flos Bombacis Malabarici extracts and 5g deionized waters form aquagel liquid solution glue
It is solidifying；35g aquagel liquid solution gels are added in 25g plant soap bases, 35g deionized waters are added, stirring forms dispersion
Hydrogel phase particle in plant soap base；It pours into various molds, cooling 5d is stood at aeration-drying and can be obtained hair washing
Soap.
Embodiment 3
A kind of preparation method of the hair soap of aqueous gel phase particle is as follows：0.03g sodium hydroxides are dissolved in 7.8g tea soaps
It in element and 9.4g soapberry extracts, mixes, stirs evenly with 31.25g apricot kernel oils, saponification 45min is carried out at 65 DEG C,
Obtain plant soap base；It is 1 by ratio:2 star polyethylene glycol and heparin derivatives crosslinking 40min adds after obtaining aerogel dressing
Enter 0.75g ginger oil, 0.5g angelica extracts, 1.25g Flos Bombacis Malabarici extracts and 5g deionized waters, forms gel aqueous fluid liquid solution
Gelling；25g aquagel liquid solution gels are added in 50g plant soap bases, 20g deionized waters are added, stirring forms and divides
The hydrogel phase particle being dispersed in plant soap base；It pours into various molds, the cooling 4d of standing, which can be obtained, at aeration-drying washes
Send out soap.
Comparative example 1
A kind of preparation method of the hair soap of aqueous gel phase particle is as follows：By 0.3g sodium hydroxides be dissolved in 4g Tea Saponins and
It in 5g soapberry extracts, mixes, stirs evenly with 30g camellia oils, saponification 30min is carried out at 45 DEG C, obtains vegetalitas
Soap base；It is 1 by ratio:0.42g is added after obtaining aerogel dressing in 3 star polyethylene glycol and heparin derivatives crosslinking 40min
Ginger oil, 0.40g angelica extracts, 0.74g Flos Bombacis Malabarici extracts and 10g deionized waters form aquagel liquid solution gel；
42g aquagel liquid solution gels are added in 30g plant soap bases, 18g deionized waters, stirring is added, formation is dispersed in
Hydrogel phase particle in plant soap base；It pours into various molds, cooling 3d is stood at aeration-drying and can be obtained hair soap.
Comparative example 2
0.3g sodium hydroxides are dissolved in 4g Tea Saponins, 5g soapberry extracts, 0.42g ginger oil, the extraction of 0.40g Radix Angelicae Sinensis
It in object, 0.74g Flos Bombacis Malabarici extracts and 10g deionized waters, mixes, stirs evenly with 30g camellia oils, saponification is carried out at 45 DEG C
30min is reacted, is poured into various molds, cooling 3d is stood at aeration-drying and can be obtained hair soap.
Compliance test result
Foam performance is tested：
Foaming method is Ross-Mile test methods (IS0696-1975 or GB7462-87), soap concentration 0.5g/L, water
Hardness 150ppm, technical field of soaps obtain technical staff generally receive viewpoint is, foam performance (foam volume/cm) represents soap
Item obtains cleaning properties, and control group is commercially available hair soap.Test obtain result see the table below 1.
Table 1
The hair soap of the present invention has good cleaning capacity known to the test result of table 1.
Present invention employs the methods of normal individual trial evaluation test to evaluate each index of hair soap.
Tester：Every group of 10 physically and mentally healthy female volunteers, 18~35 years old age, it is emphasized that：It is on probation
The volunteer for the hair soap that embodiment 3 is prepared is with scalp irritation, the symptom of itch.
Test product：The hair soap that Examples 1 to 3 and comparative example 1~2 are prepared.
Testing time and method：Corresponding product is used per group membership 1 month, use, used once in one day every other day, and
And other hair care products, each volunteer cannot be used to be fully completed entire test item during using hair soap
Mesh.
Test result：By the way of sense organ self-appraisal, the work(of breaking of hair is measured using the survey of MTT175 hairs test result
Instrument is tried to measure.Organoleptic indicator measures and is shown in Table 2.
Table 2
| Group | Foam degree | Wet and slippery degree | Irritation | It is anti-inflammatory | Glossiness | Anti- head is itched |
| Embodiment 1 | + | + | + | + | + | + |
| Embodiment 2 | + | + | + | + | + | + |
| Embodiment 3 | + | + | + | + | + | + |
| Comparative example 1 | - | + | + | - | - | - |
| Comparative example 2 | - | + | + | - | - | - |
Index parsing in table 2：Foam multilist shows that the cleaning capacity of hair soap is strong, and the ability of degreasing is also strong.+ indicate bubble
Foam is abundant ,-indicate low foam；Hair will not mutually be wound when wet and slippery degree is hair bath.+ indicate not wind ,-indicate that hair twines
Around；Irritation refer to during use and use after to the comfort level of scalp, face, hair.+ indicate stimulation ,-indicate not pierce
Swash；Anti-inflammatory refers to using after hair soap, and scalp inflammation takes an evident turn for the better.+ indicate that antiphlogistic effects are good ,-indicate invalid to inflammation；Light
Damp degree refers to that hair surface forms layer protecting film after hair washing, and hair gloss can be made beautiful.+ indicate that nature is glossy ,-indicate
It is withered and yellow, it dries or without significant change；It refers to that head is not itched in three days after washing hair that anti-head, which is itched,.+ indicate that head is not itched ,-indicate that head is itched.
And the result shows that there is the hair soap of the present invention good inflammation-resisting itch-stopping effect, hydrogel particle can make active constituent
Sustained release osmotic, nutrition scalp keep hair quality more healthy.
Hair breaks work(test：
Hair is one kind most full of elasticity in natural fiber, and the tensile property of hair depends on the a- keratin of cortex, a-
The telescopicing performance of keratin is fine, and hair is allow to elongate twice of original length.After hair elongates to a certain extent, α-
Spiral is destroyed, and is changed into β-conformation, loss of elasticity.Healthy hair cortex has certain elasticity and toughness, and the fur being destroyed
Matter, elasticity and toughness decline, and are easily broken off.
Select MTT175 hair testers, German Dio-stron companies production.Hair to be tested first in 25 DEG C of temperature,
It is balanced for 24 hours in the environment of relative humidity 50%.Due to longitudinal three positions of hair：The tensile property presence of root, middle part, taper
Nuance, therefore remove root and taper, surplus middle part about 10cm are tested, by hair be fixed on instrument two copper sheets it
Between, clamp distance 30cm, tensile speed 12.5mm/min carry out breaking test, and record breaks the data such as work(.Every group takes 20
Hair is tested.
Five groups of hairs are sampled, parallel determination is averaged three times, is as a result indicated with breaking work(, unit：Joule (J) is drawn
Breaking, work(is smaller to illustrate that hair damage is more serious, as a result see the table below 3.
Table 3
| Test | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 |
| Break work((J) | 0.014 | 0.014 | 0.015 | 0.011 | 0.009 |
By the data of table 3 it is found that the hair soap of the present invention can effective nutrition scalp, improve hair quality, so that hair is anti-
Extraneous ability increases.
Above example only illustrates embodiment of the present invention, and there is no have limitation in any form to the present invention；Appoint
What is engaged in professional and technical personnel, all has the ability to make some changes or modification using the technology contents disclosed, becomes equivalent
The equivalent embodiment of variation carries out simple modification, equivalent change and modification to the present invention, belongs to according to the technology of the present invention essence
In the range of technical solution of the present invention.
Claims (10)
1. a kind of hair soap of aqueous gel phase particle, which is characterized in that including mass percent be 25~75% vegetalitas soaps
Base and 20~35% hydrogel phase particles.
2. hair soap according to claim 1, which is characterized in that the plant soap base is carried by vegetable oil, soapberry
Object, Tea Saponin and caustic alkali is taken to be prepared.
3. hair soap according to claim 1, which is characterized in that the hydrogel phase particle includes mainly to be gathered by star
The aerogel dressing that ethylene glycol and heparin derivatives obtain also includes ginger oil, angelica extract, Flos Bombacis Malabarici extract.
4. a kind of preparation method such as claims 1 to 3 any one of them hair soap, which is characterized in that this method include with
Lower step：
(1) caustic alkali is dissolved in Tea Saponin and soapberry extract, is mixed with vegetable oil, stirred evenly, at 45~85 DEG C
30~60min of saponification is carried out, plant soap base is obtained；
(2) ginger oil, Radix Angelicae Sinensis extraction is added after star polyethylene glycol and heparin derivatives crosslinking 40min being obtained aerogel dressing
Object, Flos Bombacis Malabarici extract object and deionized water form aquagel liquid solution gel；
(3) aquagel liquid solution gel is added in plant soap base, deionized water, stirring is added, formation is dispersed in plant
Hydrogel phase particle in object soap base；
(4) it pours into various molds, cooling 3~5d is stood at aeration-drying and can be obtained hair soap.
5. the preparation method of hair soap according to claim 4, which is characterized in that the caustic alkali in the step (1) is
Sodium hydroxide or potassium hydroxide.
6. the preparation method of hair soap according to claim 4, which is characterized in that the vegetable oil in the step (1) is
It is one or more in camellia oil, Avocado Oil, castor oil, wheat-germ oil, coconut oil, apricot kernel oil.
7. the preparation method of hair soap according to claim 4, which is characterized in that in the step (1), caustic alkali accounts for plant
The 1~5% of object weight of oil, Tea Saponin account for the 10~25% of plant weight of oil, and soapberry extract accounts for 15~30%.
8. the preparation method of hair soap according to claim 4, which is characterized in that in the step (2), heparin derivatives
To vulcanize heparin, and it is 1 with ratio when star polyethylene glycol crosslinked more:2~10.
9. the preparation method of hair soap according to claim 4, which is characterized in that in the step (2), aerogel dressing
Account for the 35~50% of aquagel liquid solution gel；Ginger oil accounts for aquagel liquid solution gel 1~5%；Angelica extract accounts for
Aquagel liquid solution gel 1~3%；Flos Bombacis Malabarici extract accounts for aquagel liquid solution gel 2~8%.
10. the preparation method of hair soap according to claim 4, which is characterized in that in the step (3), gel aqueous fluid
Liquid solution gelling is in soap base when mixing, and larger hydrogel sheet is smashed to form smaller hydrogel phase particle.
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| CN201810198479.2A CN108485848A (en) | 2018-03-09 | 2018-03-09 | A kind of hair soap and preparation method thereof of aqueous gel phase particle |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109793681A (en) * | 2018-12-26 | 2019-05-24 | 拉芳家化股份有限公司 | It is a kind of containing educating the shampoo composite for sending out hair loss composite reactive Essence anti- |
| CN110055141A (en) * | 2019-04-09 | 2019-07-26 | 嘉兴市爵拓科技有限公司 | The purposes of common bombax flower water extraction object |
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| CN102961292A (en) * | 2012-12-10 | 2013-03-13 | 大连创达技术交易市场有限公司 | Pure plant essential oil shampoo soap |
| CN107034050A (en) * | 2017-05-08 | 2017-08-11 | 北京联合大学 | One kind contains gleditsia sinensis and the two-in-one hair soap of semen armeniacae amarae and preparation method thereof |
| CN107034051A (en) * | 2017-05-08 | 2017-08-11 | 北京联合大学 | One kind is containing amygdalate hair soap and preparation method thereof |
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2018
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| CN102961292A (en) * | 2012-12-10 | 2013-03-13 | 大连创达技术交易市场有限公司 | Pure plant essential oil shampoo soap |
| CN107034050A (en) * | 2017-05-08 | 2017-08-11 | 北京联合大学 | One kind contains gleditsia sinensis and the two-in-one hair soap of semen armeniacae amarae and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109793681A (en) * | 2018-12-26 | 2019-05-24 | 拉芳家化股份有限公司 | It is a kind of containing educating the shampoo composite for sending out hair loss composite reactive Essence anti- |
| CN110055141A (en) * | 2019-04-09 | 2019-07-26 | 嘉兴市爵拓科技有限公司 | The purposes of common bombax flower water extraction object |
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Application publication date: 20180904 |