CN102716046A - Liquid shampoo containing natural olive oil and derivative of natural olive oil and preparation method for liquid shampoo - Google Patents
Liquid shampoo containing natural olive oil and derivative of natural olive oil and preparation method for liquid shampoo Download PDFInfo
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- CN102716046A CN102716046A CN2012102304498A CN201210230449A CN102716046A CN 102716046 A CN102716046 A CN 102716046A CN 2012102304498 A CN2012102304498 A CN 2012102304498A CN 201210230449 A CN201210230449 A CN 201210230449A CN 102716046 A CN102716046 A CN 102716046A
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Abstract
The invention belongs to the field of cosmetics and discloses a liquid shampoo containing natural olive oil and a derivative of the natural olive oil and a preparation method for the liquid shampoo. The liquid shampoo comprises the following raw constituents: sodium polyethyleneglycol-7 (PEG-7) olive oil carboxylate, sodium 2-(2-dodecyloxyethoxy)ethyl sulphate, sodium olivoyl glutamate, olivamidopropyl betaine, glycol stearate, olive oil acylamide mono etobaccool amine (MEA), olive oil acyl hydrolyzed wheat protein, polydimethylsiloxane, PEG-7 olivate, sodium chloride, polyquaternium-10, citric acid, hydroxypropyl methyl cellulose, methylisothiazolinone, methyl chloride isothiazolinone, essence and the balance of deionized water. As the natural olive oil and the derivative thereof are adopted, the liquid shampoo disclosed by the invention is natural and mild, is low in stimulation and high in foam, can be used for a long time, not only can be used for repairing dry and damaged hair quality but also can be used for daily care and is better in smoothening and conditioning effect on the dry and damaged hair.
Description
Technical field
The invention belongs to cosmetic field, relate to a kind of shampoo that contains natural olive oil and derivant thereof and preparation method thereof.
Background technology
Extraneous factors such as environment, pollution, hair caring processing all can have influence on the health of hair.Climate change, ultraviolet all can cause damage to hair to the chemical constituent in the irradiation of hair, irrational carding method, the hair-washing hair-care product, and that the most serious damage generally occurs in is boiling hot to dying of hair, blow and send out etc. in the processing procedure.Withered, the jaundice of impaired hair lacks cordiality, and easy fracture is difficult to combing.This brings worry for people's life, even directly has influence on people's mental health.People hope through daily hair-washing hair-care processing impaired hair quality to be carried out maintenance and nursing.In recent years, the requirement of Along with people's growth in the living standard and back to nature, the hair-dressing and hair care product on the market more adopts natural component.
Hair care and nourishing is the popular research project of 21 century.In order constantly to satisfy the functional requirement of people to hair washing product, the research of natural plants nutrient substance more and more receives people's attention.
There is history in several thousand in coastwise contries to olive oil in Mediterranean, are described as " liquid golden ", and " vegetable oil queen ", " Mediterranean manna " has splendid health care and beauty functions.Olive oil is rich in vitamin A, D, E, K, F, multiple antioxidant and nutrient substance such as mineral, protein such as monobasic unsaturated fatty acid, polyphenol substance, Squalene.Therefore, olive oil can effectively reduce attack and the damage of radical pair cell membrane, protein, oils and fats, RNA and DNA, and great effect is arranged in beauty treatment, health care, health preserving.
It is fairly obvious that olive oil is used for the advantage of hair caring product.Olive oil has very strong permeability.Olive oil is spread upon on the scalp, can effectively moisten hair follicle, repair scalp cells, improve the scalp environment, make full of vitality, the stimulating hair growth of scalp.And olive oil contains abundant unsaturated fatty acid and vitamin E, can be moistened nutrition skin matter by skin absorbs, makes skin gloss exquisiteness and high resilience, blood circulation promoting and skin metabolism.Antioxidant content in the olive oil is hair nutrition supplementing more effectively, encourages hair, reduces dandruff and sends out fork, phalacrosis prevention and hair generation.
The shampoo product that does not also contain natural olive oil and derivant thereof in the market.
Summary of the invention
The purpose of this invention is to provide a kind of shampoo that contains olive oil and derivant thereof.
Another object of the present invention provides the method for preparing of above-mentioned shampoo.
The objective of the invention is to realize through following technical scheme:
A kind of shampoo that contains natural olive oil derivant, wherein the mass percent of each raw material components is:
All the other are deionized water.
The said shampoo that contains natural olive oil derivant, wherein the mass percent of each raw material components is:
All the other are deionized water.
The said shampoo method for preparing that contains natural olive oil derivant, this method comprises the following steps:
(1) takes by weighing raw material by formulation weight percentage ratio;
(2) deionized water is heated to 70 ℃~90 ℃ in the water pot, get polyquaternary ammonium salt-10, hydroxypropyl emthylcellulose together in pot stirring and dissolving even; Successively PEG-7 olive oil carboxylic acid sodium, sodium laureth sulfate, Fructus Canarii albi oleoyl sodium glutamate, olive oil amido propyl betaine, olive oil acyl hydrolase wheat protein are added dissolving, then in the suction vacuum emulsification pot; With ethylene glycol stearate, olive oil amide MEA, polydimethylsiloxane add in the vacuum kettle, stirring and dissolving is even, insulation 20min;
(3) start vacuum equipment, homogenizing 5 ~ 10min under vacuum state; Stir cooling;
When (4) cooling to 45 ℃, the cancellation vacuum adds PEG-7 olive oil acid esters, sodium chloride, Methylisothiazolinone, methylchloroisothiazandnone, essence, stirs;
(5) get final product to 6.0-7.5 with citric acid adjustment pH value at last.
Essence can be selected different odor types according to product type.
Beneficial effect of the present invention:
Prescription of the present invention is exactly that surfactant, conditioner, wetting agent etc. are from natural olive oil derivant composition with the maximum different of conventional formulation; Natural, gentle, low stimulation, high foam; Can life-time service, both can make the usefulness of dry impaired hair quality maintenance, also can be used as the usefulness of daily nursing.Dry damaged hair there is submissive preferably conditioning effect.
The cardability of hair is an important indicator of check shampoo or hair products nursing efficacy.The cardability of hair typically refers to the resistance size that runs into during through hair when comb.Carding force is more little, explains that the cardability of hair is good more, and the nursing efficacy of hair product is good more.
Cardability method of testing commonly used cardability method of testing commonly used has sense organ assessment method and instrument test method.
The sensory evaluation method is mainly by prescription teacher impression in person, half a head experiment and 3 links completion of market survey of competing product; Assess through formulating marking system, to doing, wet Hair setting property evaluation score value, full marks were in 5 minutes; 5 are divided into hair is prone to combing; Effect was the poorest in 1 minute, and it is serious to tangle during combing, hair coarse, dry and astringent.Use the back to estimate by filling in the unified questionnaire of formulating, this is practical and can reflects the evaluation methodology of market effect.
Instrumental measurement mainly is that the correct Comb rational faculty compares test, divides wet comb method and dried comb method.The improvement degree of the correct dry wet cardability of shampoo or hair products can utilize instron tensile strength tester to measure.
The effect evaluation of shampoo of the present invention, we mainly adopt the test of Hair setting power and crowd's half a head to test and estimate.
The test of Hair setting power:
Instron tensile strength tester can be used to measure the rational effect of the correct Comb of hair products, the resistance opposite with the comb direction of motion that produces when leading to pigtail through the continuous record comb.The resistance that to be comb produce in the pigtail length combing effect process of the determination data that obtains reflection.The mensuration of Hair setting property is exactly under hair dry state and hygrometric state two states, and the resistance that in the combing hair process, is run into through instron tensile strength tester machinery comb and the situation of change of resistance are judged the quality of Hair setting performance.Carding force is more little, explains that the cardability of hair is good more.
The test of hair washing product crowd half a head:
Be divided into left and right sides two parts to experimenter's hair from the centre, two parts use shampoo of the present invention and common shampoo to help the experimenter to clean hair respectively, gently rub left and right sides two parts hair respectively, and the denseness and the spreadability of assessment shampoo; Water is rinsed well, the compliance of sensation hair when bath, the washability of shampoo; Pinch the most of moisture of decaptitating on sending out; After the flushing, smoothness, the flexibility of sensation the right and left hair; And with two identical comb combing simultaneously both sides hairs, assessment is prone to cardability.Blow to eighty per cant with the hair dryer hair and to do, assess the performance of compliance, glossiness and the combing of both sides hair once more.Investigate the situation that 30 experimenters use product of the present invention and common shampoo (like Herba leucadis ciliatae
shampoo, down together).Various aspects of performance is given a mark, and 5 are divided into effect significantly (best result), and 1 is divided into not obvious (minimum branch), and 2 ~ 4 are divided into effectively, and synthetic data is averaged, and at last data is compiled statistics, analyzes.
Shampoo result of use statistical table of the present invention
The specific embodiment
Below through embodiment the present invention is done further elaboration.
Embodiment 1
The mass percent that contains each raw material components of shampoo of natural olive oil derivant: PEG-7 olive oil carboxylic acid sodium 10%; Sodium laureth sulfate 2%; Fructus Canarii albi oleoyl sodium glutamate 4%; Olive oil amido propyl betaine 4%; Ethylene glycol stearate 1%; Olive oil amide MEA 2%; Olive oil acyl hydrolase wheat protein 0.5%; Polydimethylsiloxane 0.5%; PEG-7 olive oil acid esters 1%; Sodium chloride 0.5%; Polyquaternary ammonium salt-100.5%; Citric acid 0.05%; Hydroxypropyl emthylcellulose 0.05%; Methylisothiazolinone 0.05%; Methylchloroisothiazandnone 0.05%; Essence 0.5%; All the other are deionized water, and each constituent content sum is 100%.
Method for preparing: take by weighing raw material by prescription quality percentage ratio; Deionized water is heated to 80 ℃ in the water pot, get polyquaternary ammonium salt-10, hydroxypropyl emthylcellulose together in pot stirring and dissolving even; Successively PEG-7 olive oil carboxylic acid sodium, sodium laureth sulfate, Fructus Canarii albi oleoyl sodium glutamate, olive oil amido propyl betaine are added dissolving, then in the suction vacuum emulsification pot; With ethylene glycol stearate, olive oil amide MEA, polydimethylsiloxane add in the vacuum kettle, stirring and dissolving is even, insulation 20min; Start vacuum equipment, homogenizing 5min under vacuum state; Stir cooling; When cooling to 45 ℃, the cancellation vacuum adds PEG-7 olive oil acid esters, sodium chloride, Methylisothiazolinone, methylchloroisothiazandnone, essence, stirs; With citric acid adjustment pH value to 7.0, get finished product at last.
The carding property test: product of the present invention is through test, and dried comb power is compared with common shampoo and descended 13.3%, and wet comb power is compared and descended 8.6%, and effect is remarkable.
The crowd tests investigation: shampoo of the present invention is compared with common shampoo, sliminess, smear degree and be prone to the flushing performance better.Relatively going up along the slippage degree, no matter when being bath, during wet sending out, still doing when sending out, product of the present invention all obviously is superior to common shampoo; After using product of the present invention, hair is easier to combing, and is more soft.After dried the sending out, the glossiness and the elasticity of hair improve greatly.
Embodiment 2
The mass percent that contains each raw material components of shampoo of natural olive oil derivant: PEG-7 olive oil carboxylic acid sodium 15%; Sodium laureth sulfate 4%; Fructus Canarii albi oleoyl sodium glutamate 7%; Olive oil amido propyl betaine 7%; Ethylene glycol stearate 1.5%; Olive oil amide MEA4%; Olive oil acyl hydrolase wheat protein 1%; Polydimethylsiloxane 2%; PEG-7 olive oil acid esters 3%; Sodium chloride 0.5%; Polyquaternary ammonium salt-100.5%; Citric acid 0.05%; Hydroxypropyl emthylcellulose 0.05%; Methylisothiazolinone 0.05%; Methylchloroisothiazandnone 0.05%; Essence 0.5%; All the other are deionized water, and each constituent content sum is 100%.
Method for preparing: take by weighing raw material by prescription quality percentage ratio; Deionized water is heated to 80 ℃ in the water pot, get polyquaternary ammonium salt-10, hydroxypropyl emthylcellulose together in pot stirring and dissolving even; Successively PEG-7 olive oil carboxylic acid sodium, sodium laureth sulfate, Fructus Canarii albi oleoyl sodium glutamate, olive oil amido propyl betaine are added dissolving, then in the suction vacuum emulsification pot; With ethylene glycol stearate, olive oil amide MEA, polydimethylsiloxane add in the vacuum kettle, stirring and dissolving is even, insulation 20min; Start vacuum equipment, homogenizing 10min under vacuum state; Stir cooling; When cooling to 45 ℃, the cancellation vacuum adds PEG-7 olive oil acid esters, sodium chloride, Methylisothiazolinone, methylchloroisothiazandnone, essence, stirs; Get finished product with citric acid adjustment pH value to 6.8 at last.
The carding property test: product of the present invention is through test, and dried comb power is compared with common shampoo and descended 10.4%, and wet comb power is compared and descended 9%, and effect is remarkable.
The crowd tests investigation: shampoo of the present invention is compared with common shampoo, sliminess, smear degree and be prone to the flushing performance better.Relatively going up along the slippage degree, no matter when being bath, during wet sending out, still doing when sending out, product of the present invention all obviously is superior to common shampoo; After using product of the present invention, hair is easier to combing, and is more soft.After dried the sending out, the glossiness and the elasticity of hair improve greatly.
Claims (3)
3. according to the said shampoo method for preparing that contains natural olive oil derivant of claim 1 or 2, it is characterized in that this method comprises the following step:
(1) takes by weighing raw material by formulation weight percentage ratio;
(2) deionized water is heated to 70 ℃~90 ℃ in the water pot, get polyquaternary ammonium salt-10, hydroxypropyl emthylcellulose together in pot stirring and dissolving even; Successively PEG-7 olive oil carboxylic acid sodium, sodium laureth sulfate, Fructus Canarii albi oleoyl sodium glutamate, olive oil amido propyl betaine, olive oil acyl hydrolase wheat protein are added dissolving, then in the suction vacuum emulsification pot; With ethylene glycol stearate, olive oil amide MEA, polydimethylsiloxane add in the vacuum kettle, stirring and dissolving is even, insulation 20min;
(3) start vacuum equipment, homogenizing 5 ~ 10min under vacuum state; Stir cooling;
When (4) cooling to 45 ℃, the cancellation vacuum adds PEG-7 olive oil acid esters, sodium chloride, Methylisothiazolinone, methylchloroisothiazandnone, essence, stirs;
(5) get final product to 6.0-7.5 with citric acid adjustment pH value at last.
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Cited By (6)
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CN103599006A (en) * | 2013-11-13 | 2014-02-26 | 钟准 | Formula of shampoo for promoting hair growth |
CN106924131A (en) * | 2015-12-28 | 2017-07-07 | 广州市优品化妆品科技有限公司 | A kind of preparation method of ginger shampoo |
CN107349143A (en) * | 2016-05-10 | 2017-11-17 | 广州市优品化妆品科技有限公司 | A kind of tealeaves tea seed extract shampoo and preparation method thereof |
EP3536383A1 (en) * | 2018-03-06 | 2019-09-11 | Richli, Remo | Cleaning and disinfecting preparations comprising a polyoxyalkylene carboxylate |
EP3744819A1 (en) * | 2019-05-26 | 2020-12-02 | Fama Holding AG | Composition with alkoxylated fatty acids |
CN115463057A (en) * | 2021-06-11 | 2022-12-13 | 广州辰沐生物科技有限公司 | Olive amino acid cleansing foam and preparation method thereof |
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103599006A (en) * | 2013-11-13 | 2014-02-26 | 钟准 | Formula of shampoo for promoting hair growth |
CN103599006B (en) * | 2013-11-13 | 2016-12-07 | 钟准 | A kind of formula promoting natural on-off cycles of hair growth shampoo |
CN106924131A (en) * | 2015-12-28 | 2017-07-07 | 广州市优品化妆品科技有限公司 | A kind of preparation method of ginger shampoo |
CN107349143A (en) * | 2016-05-10 | 2017-11-17 | 广州市优品化妆品科技有限公司 | A kind of tealeaves tea seed extract shampoo and preparation method thereof |
EP3536383A1 (en) * | 2018-03-06 | 2019-09-11 | Richli, Remo | Cleaning and disinfecting preparations comprising a polyoxyalkylene carboxylate |
EP3744819A1 (en) * | 2019-05-26 | 2020-12-02 | Fama Holding AG | Composition with alkoxylated fatty acids |
CN115463057A (en) * | 2021-06-11 | 2022-12-13 | 广州辰沐生物科技有限公司 | Olive amino acid cleansing foam and preparation method thereof |
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Effective date of registration: 20210728 Address after: No.7, Jiangyun Road, Jiangning District, Nanjing, Jiangsu Province, 210000 Patentee after: NANJING INST OF COMPREHENSIVE UTILIZATION OF WILD PLANT CHINA COOP Address before: 515821 southeast of Xiushui Road, Laimei Industrial Zone, Chenghai District, Shantou City, Guangdong Province Patentee before: Guangdong Yawei Biotechnology Co.,Ltd. Patentee before: NANJING INST OF COMPREHENSIVE UTILIZATION OF WILD PLANT CHINA COOP |
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