CN102836093A - Facial cream containing type I collagen - Google Patents
Facial cream containing type I collagen Download PDFInfo
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- CN102836093A CN102836093A CN2012103628136A CN201210362813A CN102836093A CN 102836093 A CN102836093 A CN 102836093A CN 2012103628136 A CN2012103628136 A CN 2012103628136A CN 201210362813 A CN201210362813 A CN 201210362813A CN 102836093 A CN102836093 A CN 102836093A
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Abstract
The invention discloses a facial cream containing type I collagen and a preparation method thereof. The facial cream consists of the following components in percentage by mass: 3-8 percent of glycerol, 0.01-0.05 percent of EDTA (Ethylene Diamine Tetraacetic Acid) Na2, 1-3 percent of fucose, 0.1-0.3 percent of methylparaben, 0.05-0.2 percent of propylben, 0.1-0.5 percent of allantoin, 0.5-2 percent of VC (Vitamin C) ethyl ether, 0.5-2 percent of vitamin B3, 0.5-1 percent of dipotassium glycyrrhizinate, 1-2 percent of M68, 1-10 percent of A165, 1-2 percent of 16-18 alcohol, 1-2 percent of DC200, 2-10 percent of GTCC (Caprylic/Capric Triglyceride), 1.5-10 percent of shea butter, 3-6 percent of cupuacu butter, 1-5 percent of 2EHP (Isooctyl Palmitate), 0.1-1 percent of vitamin A acetic ester, 0.4-1 percent of vitamin E acetic ester, 0.01-0.1 percent of piperine, 0.5-2 percent of type I collagen, 0.01-0.05 percent of essence, 0.1-0.5 percent of S-304, 1-5 percent of LS8740 and 50-75 percent of deionized water. The facial cream is prepared according to the method provided by the invention; and the facial cream contains type I collagen, has high absorptivity, can be used for deeply moistening and humidifying skin and replenishing water for skin, and has multiple skin-protecting and beautifying effects of nourishing skin, increasing skin elasticity, whitening, lightening speckles, reducing wrinkles and the like. As proved by test, the facial cream is very safe and has a good effect.
Description
Technical field:
The present invention relates to a kind of human body skin and repair articles for use, particularly a kind of proteic facial cream of type i collagen and manufacturing approach thereof of containing.
Background technology:
Collagen protein is a huge family, and is of a great variety, and high level of architectural complexity from molecular structure, supramolecular structure, arrives tissue distribution and function etc. again, has significant multiformity.They are present in the various tissues of human body, as, skin, bone, cornea, tendon, cartilage, vitreous body, Uterus wall, blood vessel wall, basement membrane, Placenta Hominis, endotheliocyte or the like.Type i collagen albumen is present in the skin, skeleton, blood vessel of human body etc. morely and plants in the tissue.Several factors all can cause the loss of various nutrition compositions; And the loss of collagen protein can cause supporting the collagen peptide bond and the elasticated net fracture of skin; Its spiral RF is destroyed immediately; Skin histology is oxidized, atrophy, subside, and drying, wrinkle appear in skin thus, aging phenomenon such as nonelastic relaxes.
Summary of the invention:
Based on above-mentioned cognition, the inventor has also designed the various type i collagen protein prescriptions that are added with, and in the hope of realize helping the maintenance skin, the reconstructed collagen albumin layer improves elasticity, the moisture of skin, so play skin whitening, the anti-ageing effect of preserving moisture.Through lot of test, it is simple that the inventor has developed a kind of preparation technology finally, and raw material is few but can reach the skin care item of above-mentioned many effects.
The purpose of this invention is to provide a kind of elasticity, moisture that improves skin, the Pear Power skin protection facial cream of anti-ageing effect and preparation method thereof of preserving moisture.
The object of the invention is realized through following technical proposals:
The mass percent of facial cream consists of: glycerol 3-8%, EDTA Na
20.01-0.05%, trehalose 1-3%, methyl hydroxybenzoate 0.1-0.3%, propylparaben 0.05-0.2%; Allantoin 0.1-0.5%, VC ethylether 0.5-2%, vitamin B3 0.5%-2%, glycyrrhizic acid dipotassium salt 0.5-1%; M68 1-2%, A 165 1-10%, 16-18 alcohol 1-2%, DC200 1-2%, GTCC 2-10%, shea butter 1.5-10%, simple and unsophisticated A Su fruit oil 3-6%, 2EHP 1-5%, vitamin A acetate 0.1-1%, Vitamin E acetate 0.4-1%; Piperine 0.01-0.1%, type i collagen albumen 0.5-2%, essence 0.01-0.05%; S-305 0.1-0.5%, LS8740 1-5%, deionized water 50-75%.
Facial cream of the present invention preferably is prepared as follows method, comprises step:
1) gets glycerol 3-8% by quality, EDTA Na
20.01-0.05%, trehalose 1-3%, methyl hydroxybenzoate 0.1-0.3%, propylparaben 0.05-0.2%; Allantoin 0.1-0.5%, VC ethylether 0.5-2%, vitamin B3 0.5%-2%, glycyrrhizic acid dipotassium salt 0.5-1%; M68 1-2%, A 165 1-10%, 16-18 alcohol 1-2%, DC200 1-2%, GTCC 2-10%, shea butter 1.5-10%, simple and unsophisticated A Su fruit oil 3-6%, 2EHP 1-5%, vitamin A acetate 0.1-1%, Vitamin E acetate 0.4-1%; Piperine 0.01-0.1%, type i collagen albumen 0.5-2%, essence 0.01-0.05%; S-305 0.1-0.5%, LS8740 1-5%, deionized water 50-75%.
2) preparing A phase: with deionized water, glycerol, EDTA Na
2, trehalose, allantoin, VC ethylether, vitamin B3, glycyrrhizic acid dipotassium salt and the methyl hydroxybenzoate of the amount of getting 1/2 put into container successively, be heated to 80 ℃ under stirring.
3) preparation B phase: in the time of the preparing A phase; With M68, A 165,16-18 alcohol, DC200, GTCC, shea butter, simple and unsophisticated A Su fruit oil, 2EHP; Vitamin A acetate; Vitamin E acetate, piperine, propylparaben and the methyl hydroxybenzoate that remains 1/2 amount are put into another container successively, are heated to 80 ℃ under stirring.
4) with A be added to B mutually in, stir to homogenizing with 5000-12000rpm; Naturally cool to 60 ℃.
5) S-305 is joined in the step 4) gained uniform homogeneous blend, stir to homogenizing, naturally cool to 40 ℃ with 5000-12000rpm.
6) type i collagen albumen is added in the step 5) gained uniform homogeneous blend, stirs with 800-1500rpm.
7) LS8740, essence are joined in the step 6) gained mixture, with the 800-1500rpm stirring and evenly mixing.
8) fill, decals, be up to the standards, the packing.
Following implication is represented in writing a Chinese character in simplified form of being adopted among the present invention:
EDTA Na
2: disodiumedetate;
VC ethylether: vitamin C ethylether;
M68: cetyl glucoside
A 165: glyceryl monostearate
DC200: dimethicone DC-200;
GTCC: caprylic/capric triglyceride;
2EHP: iso-octyl palmitate;
S-305: match Bick SEPIGEL 305 emulsifying agents;
LS8740: the LS of Kening Co.,Ltd active additive serial model No.: LS8740
16-18 alcohol: 16 octadecanol, C16:C18=3:7
The main effect of various compositions is among the present invention:
1. hexadeca-octadecyl alcohol glucoside, self emulsifying glyceryl monostearate, S-305 are emulsifying agent.
2. sad capric acid triglyceride and iso-octyl palmitate are isostearyl glyceryl pentaerythrityl ether.
3. vitamin A acetate is to regulate the growth of epithelial tissue cell and the healthy necessary factor, makes coarse aging skin surface attenuation, promotes cell metabolism normalization, and the wrinkle removal effect is obvious.
4. a kind of novel microcirculation activator of vitamin E Nicotinate can directly act on blood vessel wall, the diastole peripheral vessels; Promote blood circulation of skin, improve skin elasticity, delaying skin wears out and has certain effect; And can reduce the content because of the aged pigment of age increase, Pear Power effect.
5. α-bisabolol has the scytitis of reduction effect, and can reduce product simultaneously stimulates, and improves the irritation ability of skin.
6. the ethoxy phosphoamide has hygroscopicity and the function that keeps moisture content.
7. allantoin has lucifuge, sterilization and anticorrosion, pain relieving, antioxidation, can make skin keep moisture content, and is moist and soft.
8.I collagen type gets into skin corium and helps the maintenance skin, the reconstructed collagen albumin layer improves elasticity, the moisture of skin, and then skin whitening, plays the anti-ageing effect of preserving moisture.
9. the nicotiamide external can reduce the generation of fatty acid and triglyceride in the sebum, thereby receives the fine, soft fur hole and reduce acne the order of severity when taking place.
Advantage of the present invention and characteristics are:
1. adding type i collagen albumen among the present invention is the medical grade collagen protein that from the Mus tail of specific pathogen free, extracts, and pure natural extracts the high-tech biological product through the biotechnology preparation, and is safe.
2. these article absorbability is good, can get into dermal tissue reparation fracture, aged elastic fibrous web, thereby increases the skin compactness, reduces deep wrinkle, the microgroove that calms down, and makes skin-tightening and high resilience.
3. these article can be accelerated the cell renewal speed.Improve skin elasticity from deep layer, moisten, preserve moisture, anti-ageing effect is obvious.
4. these article combine LS8740 active additive, multivitamin, shea butter and simple and unsophisticated A Su fruit oil, improve further that it moistens, preserves moisture, reparation, anti-ageing effect, reach many efficacy effects.
The specific embodiment
In order to understand the present invention better, below in conjunction with embodiment the present invention is described further, but does not limit the present invention.
Embodiment 1
Get glycerol 5% by mass percentage, EDTA Na
20.03%, trehalose 1%, methyl hydroxybenzoate 0.2%, propylparaben 0.05%, allantoin 0.3%; VC ethylether 2%, vitamin B3 1%, glycyrrhizic acid dipotassium salt 0.5%, M682%, A 1652%, 16-18 alcohol 2%, DC200 1.5%, GTCC 4%, shea butter 2%, simple and unsophisticated A Su fruit oil 3%, 2EHP 5%; Vitamin A acetate 0.5%, Vitamin E acetate 0.5%, piperine 0.05%, type i collagen albumen 1%; Essence 0.02%, S-305 0.3%, and LS8740 2%, deionized water 64.05%.
With deionized water, glycerol, EDTA Na
2, trehalose, allantoin, VC ethylether, vitamin B3, glycyrrhizic acid dipotassium salt and 0.1% methyl hydroxybenzoate put into container A successively, is heated to 80 ℃ under stirring; While is extracting container B in addition; Successively with M68, A 165,16-18 alcohol, DC200, GTCC, shea butter, simple and unsophisticated A Su fruit oil, 2EHP, vitamin A acetate, Vitamin E acetate; Piperine, propylparaben and 0.1% methyl hydroxybenzoate are put into, and are heated to 80 ℃ under stirring; Then the mixture in the A container is joined in the B container, and stir to homogenizing with 5000-12000rpm; Naturally cool to 60 ℃; To wherein adding S-305, stir to homogenizing again, naturally cool to 40 ℃ with 5000-12000rpm; To wherein adding type i collagen albumen, stir again with 800-1500rpm.At last to wherein adding LS8740, essence, with the 800-1500rpm stirring and evenly mixing; Fill, decals, be up to the standards, must contain the facial cream of I collagen type.
Embodiment 2
Get glycerol 6% by mass percentage, EDTA Na
20.03%, trehalose 2%, methyl hydroxybenzoate 0.2%, propylparaben 0.05%, allantoin 0.4%; VC ethylether 2%, vitamin B3 0.5%, glycyrrhizic acid dipotassium salt 0.5%, M68 2%, A 165 3%, 16-18 alcohol 2%, DC2002%, GTCC 6%, shea butter 3%, simple and unsophisticated A Su fruit oil 3%, 2EHP 4%; Vitamin A acetate 1%, Vitamin E acetate 1%, piperine 0.01%, type i collagen albumen 0.5%; Essence 0.01%, S-305 0.3%, and LS8740 2%, deionized water 58.5%;
Press the method operation of embodiment, must contain the facial cream of I collagen type.
Embodiment 3
Get glycerol 7% by mass percentage, EDTA Na
20.03%, trehalose 3%, methyl hydroxybenzoate 0.2%, propylparaben 0.05%, allantoin 0.2%; VC ethylether 1%, vitamin B3 1.5%, glycyrrhizic acid dipotassium salt 0.5%, M68 2%, A 1654%, 16-18 alcohol 2%, DC200 2%, GTCC 8%, shea butter 4%, simple and unsophisticated A Su fruit oil 3%, 2EHP 3%; Vitamin A acetate 0.5%, Vitamin E acetate 0.5%, piperine 0.05%, type i collagen albumen 2%; Essence 0.01%, S-305 0.3%, LS87403%, deionized water 52.16%.
Press the method operation of embodiment, must contain the facial cream of I collagen type.
Test Example
Experimental subject: 42 routine triers, wherein male 13 examples, women's 29 examples.Year mean age (30.3 ± 8.4).
Test method:
1. divide into groups: contrast group on probation (A group), the present invention's group on probation (B group), matched group is the commodity facial cream that is marked with identical effect
2. the trier sooner or later evenly is applied in face with facial cream after clean, and the right faces of all triers are smeared similar commodity facial cream (A group), and left face is smeared facial cream of the present invention (B group), and in lasting 8 weeks, all trier faces do not use other skincare products in the trial employment period.
3. the position that cheekbone is the highest is as the test position; Center probe aligning test position adopts skinanalysis apparatus (Cutometer MPA 580) to test position portion elasticity number, melanin value, moisture content value about 8 weeks back detection experimenters before trying out and after trying out.Adopt German CK image analyzer photographic analysis.The each detection tested by same people, same instrument.
4. calculate the score value that improves that every trier uses test position, back portion elasticity number, moisture content value, computational methods: (back on probation test value-Pretesting value on probation)/Pretesting value on probation * 100%; Melanin value is improved the branch value calculating method: (Pretesting value on probation-back on probation test value)/Pretesting value on probation * 100%.Calculate each class value and improve score value, 20-40%, the number in>=40% three interval≤20%.
5. the result adopts SPSS 16.0 statistical analysis softwares to carry out X 2 test.P＜0.05 difference has statistical significance, and P >=0.05 difference does not have statistical significance.
6. result
On probation 8 week back trier face part of detecting be that the score value that improves of elasticity, melanin, moisture carries out statistical analysis in different interval numbers and finds; These article are in elasticity and the moisture effect of having clear improvement; And the more similar commodity of the situation of improving the aspect are good, and difference has statistical significance (P＜0.05).These article are to the black effect of having clear improvement, and the more similar commodity of data show improvement are good, but difference does not have statistical significance (P >=0.05).Result of the test is seen table 1.In the trial employment period, ill symptomses such as allergy appear in none example of all triers.
The score value that improves that table 1 is tried out 8 all backs elasticity, melanin, moisture compares in different interval numbers
Claims (2)
1. a facial cream that contains the I collagen type is characterized in that its mass percent consists of: glycerol 3-8%, EDTA Na
20.01-0.05%, trehalose 1-3%, methyl hydroxybenzoate 0.1-0.3%, propylparaben 0.05-0.2%; Allantoin 0.1-0.5%, VC ethylether 0.5-2%, vitamin B3 0.5%-2%, glycyrrhizic acid dipotassium salt 0.5-1%; M68 1-2%, A 165 1-10%, 16-18 alcohol 1-2%, DC200 1-2%, GTCC 2-10%, shea butter 1.5-10%, simple and unsophisticated A Su fruit oil 3-6%, 2EHP1-5%, vitamin A acetate 0.1-1%, Vitamin E acetate 0.4-1%; Piperine 0.01-0.1%, type i collagen albumen 0.5-2%, essence 0.01-0.05%; S-305 0.1-0.5%, LS8740 1-5%, deionized water 50-75%.
2. a kind of method for preparing that contains the facial cream of I collagen type according to claim 1 is characterized in that comprising step:
1) gets glycerol 3-8% by quality, EDTA Na
20.01-0.05%, trehalose 1-3%, methyl hydroxybenzoate 0.1-0.3%, propylparaben 0.05-0.2%; Allantoin 0.1-0.5%, VC ethylether 0.5-2%, vitamin B3 0.5%-2%, glycyrrhizic acid dipotassium salt 0.5-1%; M681-2%, A 165 1-10%, 16-18 alcohol 1-2%, DC200 1-2%, GTCC 2-10%, shea butter 1.5-10%, simple and unsophisticated A Su fruit oil 3-6%, 2EHP 1-5%, vitamin A acetate 0.1-1%, Vitamin E acetate 0.4-1%; Piperine 0.01-0.1%, type i collagen albumen 0.5-2%, essence 0.01-0.05%; S-305 0.1-0.5%, LS8740 1-5%, deionized water 50-75%;
2) preparing A phase: with deionized water, glycerol, EDTA Na
2, trehalose, allantoin, VC ethylether, vitamin B3, glycyrrhizic acid dipotassium salt and the methyl hydroxybenzoate of the amount of getting 1/2 put into container successively, be heated to 80 ℃ under stirring;
3) preparation B phase: in the time of the preparing A phase; With M68, A 165,16-18 alcohol, DC200, GTCC, shea butter, simple and unsophisticated A Su fruit oil, 2EHP; Vitamin A acetate; Vitamin E acetate, piperine, propylparaben and the methyl hydroxybenzoate that remains 1/2 amount are put into another container successively, are heated to 80 ℃ under stirring;
4) with A be added to B mutually in, stir to homogenizing with 5000-12000rpm; Naturally cool to 60 ℃;
5) S-305 is joined in the step 4) gained uniform homogeneous blend, stir to homogenizing, naturally cool to 40 ℃ with 5000-12000rpm;
6) type i collagen albumen is added in the step 5) gained uniform homogeneous blend, stirs with 800-1500rpm;
7) LS8740, essence are joined in the step 6) gained mixture, with the 800-1500rpm stirring and evenly mixing;
8) fill, decals, be up to the standards, the packing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN 201210362813 CN102836093B (en) | 2012-09-26 | 2012-09-26 | Facial cream containing type I collagen |
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| Application Number | Priority Date | Filing Date | Title |
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| CN 201210362813 CN102836093B (en) | 2012-09-26 | 2012-09-26 | Facial cream containing type I collagen |
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| CN102836093B CN102836093B (en) | 2013-06-12 |
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| CN 201210362813 Expired - Fee Related CN102836093B (en) | 2012-09-26 | 2012-09-26 | Facial cream containing type I collagen |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103800401A (en) * | 2014-02-25 | 2014-05-21 | 苗相臣 | Granulation promoting and healing ointment |
| CN105407866A (en) * | 2013-05-31 | 2016-03-16 | 纽特瑞科斯科技公司 | Combination of active agents for treating skin aging |
| CN107375032A (en) * | 2017-08-11 | 2017-11-24 | 天津嘉氏堂科技有限公司 | A kind of composition and preparation method for repairing skin barrier |
| CN108619018A (en) * | 2018-05-14 | 2018-10-09 | 杨森 | A kind of skin barrier repair cream and preparation method thereof |
| CN110327080A (en) * | 2019-07-05 | 2019-10-15 | 上海应用技术大学 | The skin hypersensitivity detection method and application of gold bergamot essential oil and/or hydrosol |
| CN112107504A (en) * | 2020-09-24 | 2020-12-22 | 成都维德医疗器械有限责任公司 | Preparation method of modified type I collagen gel |
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| CN102018632A (en) * | 2010-12-15 | 2011-04-20 | 广州潮徽化工科技有限公司 | High-efficiency moisturizing composition and preparation method and application thereof in cosmetics |
| CN102048666A (en) * | 2010-11-26 | 2011-05-11 | 新时代健康产业（集团）有限公司 | Skin care composition with wrinkle removing and resisting function and preparation and preparation method thereof |
| CN102085168A (en) * | 2011-01-26 | 2011-06-08 | 珠海市时代经典化妆品有限公司 | Anti-aging cosmetic |
| CN102178617A (en) * | 2011-05-09 | 2011-09-14 | 刘佩华 | Protein skin care products having function of skin repair and care |
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2012
- 2012-09-26 CN CN 201210362813 patent/CN102836093B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102048666A (en) * | 2010-11-26 | 2011-05-11 | 新时代健康产业（集团）有限公司 | Skin care composition with wrinkle removing and resisting function and preparation and preparation method thereof |
| CN102018632A (en) * | 2010-12-15 | 2011-04-20 | 广州潮徽化工科技有限公司 | High-efficiency moisturizing composition and preparation method and application thereof in cosmetics |
| CN102085168A (en) * | 2011-01-26 | 2011-06-08 | 珠海市时代经典化妆品有限公司 | Anti-aging cosmetic |
| CN102178617A (en) * | 2011-05-09 | 2011-09-14 | 刘佩华 | Protein skin care products having function of skin repair and care |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105407866A (en) * | 2013-05-31 | 2016-03-16 | 纽特瑞科斯科技公司 | Combination of active agents for treating skin aging |
| CN103800401A (en) * | 2014-02-25 | 2014-05-21 | 苗相臣 | Granulation promoting and healing ointment |
| CN107375032A (en) * | 2017-08-11 | 2017-11-24 | 天津嘉氏堂科技有限公司 | A kind of composition and preparation method for repairing skin barrier |
| CN108619018A (en) * | 2018-05-14 | 2018-10-09 | 杨森 | A kind of skin barrier repair cream and preparation method thereof |
| CN110327080A (en) * | 2019-07-05 | 2019-10-15 | 上海应用技术大学 | The skin hypersensitivity detection method and application of gold bergamot essential oil and/or hydrosol |
| CN112107504A (en) * | 2020-09-24 | 2020-12-22 | 成都维德医疗器械有限责任公司 | Preparation method of modified type I collagen gel |
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| CN102836093B (en) | 2013-06-12 |
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