CN102283789B - Method for preparing collagen polypeptide nutrition washing-free conditioner composition and product thereof - Google Patents
Method for preparing collagen polypeptide nutrition washing-free conditioner composition and product thereof Download PDFInfo
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- CN102283789B CN102283789B CN 201010204462 CN201010204462A CN102283789B CN 102283789 B CN102283789 B CN 102283789B CN 201010204462 CN201010204462 CN 201010204462 CN 201010204462 A CN201010204462 A CN 201010204462A CN 102283789 B CN102283789 B CN 102283789B
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- hair
- collagen polypeptide
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- raw material
- feedstock composition
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Abstract
The invention discloses a method for preparing a collagen polypeptide nutrition washing-free conditioner composition. The method comprises the following steps of: preparing an A-phase raw material composition; preparing a B-phase raw material composition; preparing a C-phase raw material composition; preparing a D-phase raw material composition; slowing adding the B-phase raw material composition into the A-phase raw material composition while stirring, stirring, homogenizing and decreasing the temperature, and adding the C-phase raw material composition and the D-phase raw material composition; continuously stirring, decreasing the temperature to 35-38 DEG C, and discharging. The invention further discloses a product by adopting the method. The product comprises the following components according to percentage by weight: 0.3-12.0% of high-melting-point fat compound, 0.5-4.0% of emulsifier, 2.0-15.0% of emollient, 0.1-10.0% of humectant, 0.01-5% of collagen polypeptide, 0.0-10% of cationic conditioner, and the balance of deionized water. According to the method disclosed by the invention, the process is easy to control; the product has high-quality temperature; and the product is capable of transporting and supplying nutrition and melanin to hair so as to improve scalp cortex and prevent hair from becoming dry, yellow, forky, black and deciduous.
Description
Technical field
The present invention relates to Chemical Engineering Technology and goods field, particularly a kind of preparation method and goods thereof of collagen polypeptide nutrition washing-free hair care dairy compositions.
Background technology
Human is the distinctive rule of the Nature from the youth to the aging from growing into maturation, and who is also irresistible.Increasing the weight of along with environmental pollution in recent years, increasing discharge of poisonous waste is in atmosphere, the acidic materials that cause hair to decompose increase, add that uitraviolet intensity strengthens, people's life stress strengthens and dyes frequently, scald, blow, draw or physiological reason so that many people's hair geromorphism: look withered and yellow, dim, bleach, bifurcated, tarnish, even come off, being improved significantly in order to make the hair that is subject to heavy damage, people often use common nutritious hair conditioner to remove conditioning hair, but common hair conditioner all is washing-off type, a large amount of nutrient substance is not absorbed by hair but is gone by washing in washing process, has so both wasted resource, again contaminated environment.And the maximum advantage of the disposable nutrition hair care of collagen polypeptide breast is leave, and hair care Ruzhong nutrient substance collagen polypeptide can rest on hair surface and absorbed at leisure by hair in the use procedure.Collagen polypeptide can be absorbed by body rapidly in vivo, also can be absorbed by skin external, participate in the Cell regulate effect directly, strengthen the activity of cell, the main component of hair is keratoprotein, accounts for 97%, hair is made of the epithelial cell of keratinization, and the cell of epithelium all is subjected to the control of polypeptide, thinks in the past it only is that aminoacid forms, and the collagen polypeptide that really can improve rapidly hair quality is participating in the epithelial growth promoter of control.The insatiable hunger of collagen polypeptide: show transportation supply nutrition, melanin, absorption also promotes absorbing of trace element, and collagen polypeptide can synthesize rapidly collagen protein again and improve scalp cortex.Therefore can prevent that hair is withered, jaundice, bifurcated, bleach, come off.Domestic a lot of patent is applied to medical domain to active polypeptide, and the effect of polypeptide in medical domain also is obvious to all, although it is very extensive that polypeptide is used aspect medical science, but the application of polypeptide aspect cosmetics or very few, this is on the one hand because polypeptide is expensive, on the other hand because the active bad control of polypeptide.
Application number is that 200810155593.3 Chinese invention patent application file has been put down in writing lip lipstick attapulgite clay, water solublity lanoline, peach kernel oil, Semen Sesami Nigrum oil, citric acid, collagen protein, glyceryl monostearate, methyl hydroxybenzoate, propylparaben and the deionized water of a kind of hair conditioner after marcelling after by modification and formed.Although mentioned therein the use collagen protein, its effect is not fully up to expectations.Simultaneously, hair care of the prior art breast preparation technology mostly exists all that complex technical process, working condition are not easy to control, the problem of unstable product quality.
Summary of the invention
In order to solve the problem of above-mentioned hair maintenance nursing, the purpose of this invention is to provide a kind of preparation method that contains collagen polypeptide nutrition washing-free hair care dairy compositions, be not easy to control to solve complex technical process, working condition in the prior art, the problem of unstable product quality;
The present invention also provide a kind of adopt said method preparation contain collagen polypeptide nutrition washing-free hair care dairy compositions, often use that goods provided by the invention can solve that hair is withered, dimness, jaundice, bifurcated, problem bleaches, comes off.
The objective of the invention is to adopt following technical scheme to realize:
A kind of preparation method of collagen polypeptide nutrition washing-free hair care dairy compositions, it is characterized in that: it comprises the steps:
1) preparation A phase feedstock composition: take by weighing respectively hard fat chemical compound, emollient, emulsifying agent, the antibacterial of preset proportion, add successively in the container warming while stirring to 90 ℃-95 ℃ to raw material and all dissolve;
2) preparation B phase feedstock composition: take by weighing respectively cation opsonizing agent, deionized water, the wetting agent of preset proportion, add successively in the container warming while stirring to 90 ℃-95 ℃ to raw material and all dissolve;
3) preparation C phase feedstock composition: the essence, the antibacterial that take by weighing respectively preset proportion;
4) preparation D phase feedstock composition: the collagen polypeptide that takes by weighing respectively preset proportion;
5) while stirring B phase feedstock composition is slowly added in the A phase feedstock composition, stirred 2-5 minute, homogenizing 3-8 minute, mixing speed was controlled at 20-30r/m, and homogenizing speed is 1400-2600r/m, and homogenizing temperature is controlled at 80-90 ℃;
6) stirring began cooling in 5 minutes behind the homogenizing;
Add C phase feedstock composition when 7) temperature is down to 45 ℃;
Add D phase feedstock composition when 8) temperature is down to 40 ℃,
9) continue to stir, cool to 35-38 ℃ of discharging, make collagen polypeptide nutrition washing-free hair care dairy compositions.
The preparation method of aforesaid collagen polypeptide nutrition washing-free hair care dairy compositions is characterized in that: its step 3) the C phase feedstock composition of preparation also comprises the antiseptic, the pearling agent that take by weighing preset proportion.
A kind of collagen polypeptide nutrition washing-free hair care dairy compositions that adopts the preceding method preparation, it is characterized in that: it comprises the component with following percentage by weight:
1). hard fat chemical compound 0.3-12.0%
2). emulsifying agent 0.5-4.0%
3). emollient 2.0-15.0%
4). wetting agent 0.1-10.0%
5). collagen polypeptide 0.05-5%
6). cation opsonizing agent 0.0-10%
7) antiseptic 0.0-0.5%
8) pearling agent 0.2-1%
7). the deionized water surplus.
The disposable hair care dairy compositions of aforesaid collagen polypeptide is characterized in that: in the end article that makes, collagen polypeptide content is 0.05%-5%..
The disposable hair care dairy compositions of aforesaid collagen polypeptide is characterized in that: described hard fat chemical compound is selected from one or more the mixture in aliphatic alcohol, fatty acid, fatty alcohol derivative, the derivative of fatty acid.
The disposable hair care dairy compositions of aforesaid collagen polypeptide is characterized in that: described emulsifying agent is nonionic emulsifier or anion emulsifier a kind of or their mixture of hydrophilic and oleophilic HLB value between 8-15.
The disposable hair care dairy compositions of aforesaid collagen polypeptide is characterized in that: used emollient is the mixing that is selected from one or both or they of following material:
1). Vegetable oil lipoprotein or hydrogenated vegetable fat;
2). polysiloxanes or methyl polysiloxane resin;
3). alkanes;
4). esters.
The disposable hair care dairy compositions of aforesaid collagen polypeptide is characterized in that: wetting agent is selected from a kind of of polyhydric alcohol, hyaluronic acid or its sodium salt, ceramide or their mixing.
The disposable hair care dairy compositions of aforesaid collagen polypeptide is characterized in that: cation opsonizing agent is selected from one or more mixing in guar gum hydroxypropyl level trimethyl ammonium chloride, Polyquaternium-10, polyquaternary ammonium salt-47, the polyquaternary ammonium salt-7; Described collagen polypeptide is the eel collagen.
Method technical process of the present invention is easily controlled, the product property temperature, and its goods can transport supply nutrition, melanin to hair, improve scalp cortex, can prevent that hair is withered, jaundice, bifurcated, bleach, comes off; Can be used for the aqua products such as disposable hair care breast, hair nutrition water, cold cream frost, essence, emulsion.
Except the collagen polypeptide compositions, the percentage ratio of other raw material all refers to percentage by weight in the goods component of the present invention, and its ratio all is as the basis take the pure content of composition.
The present invention is applicable to disposable hair care breast, hair nutrition water, emulsion, cream frost, nutrition shampoo, Mian Zheng hairdressing gel etc.Collagen polypeptide contained among the present invention is slowly released on hair by liposome, is absorbed by hair gradually, help to solve that hair is withered, jaundice, bifurcated, problem bleaches, comes off.
The hard fat chemical compound can increase in the present invention the product denseness and increase the product conditioning effect, makes to do to send out wet all smoother of sending out, and softness, easily combing is difficult for dispersing.
The hard fat chemical compound is 0.3-12% in the use amount of the present composition, is preferably 1.0-9.0%, more preferably 3.0-6.0%.
Being best suited for hard fat chemical compound of the present invention is aliphatic alcohol, the fusing point of aliphatic alcohol is higher than 25 ℃, aliphatic alcohol of the present invention most preferably has 16 to the about aliphatic alcohol of 22 carbon atoms, and these aliphatic alcohol are saturated fatty alcohols, and can be straight or branched alcohol.The limiting examples of aliphatic alcohol comprises one or more the mixing in spermol, stearyl alcohol, the behenyl alcohol.
Be applicable to emulsifying agent of the present invention and be nonionic emulsifier or anion emulsifier a kind of or their mixing of hydrophilic and oleophilic HLB value between 8-15, most preferred emulsifying agent is nonionic emulsifier or anion emulsifier a kind of or their mixing of hydrophilic and oleophilic HLB value between 10-13.Emulsifying agent is selected from glucosides class, esters preferably.The glucosides class is selected from coco group glucoside, cetyl glucoside, eicosyl glucoside, C12-20 alkyl androstanediol.Esters is selected from C20-22 alkyl phosphate, tristerin, PEG-100 stearate, Sucrose Fatty Acid Ester.
Be applicable to emollient levels of the present invention and be 2.0 to approximately 15.0%, most preferably be 3.0-6.0%.Emollient has and moistens and the effect of soft skin and hair, can be in case trichoxerosis, and jag, withered and yellow, specifically can select following material:
1). Vegetable oil lipoprotein or hydrogenated vegetable fat (as: almond oil, Radix Oenotherae erythrosepalae oil, Semen pruni armeniacae oil, Rosehips oil, Jojoba oil, Semen Tritici aestivi germ oil, olive oil, carrot oil, Oleum Ricini, American Avocado Tree oil, Oleum Cocois, Petiolus Trachycarpi oil, cupu oil, cocoa butter, palm-kernel oil, soybean oil, Testa oryzae oil, aloe, mother-in-law sieve's fat, mowrah fat, Adeps Bovis seu Bubali resin, Oleum Arachidis hypogaeae semen, Semen Maydis oil, macadimia nut oil, candlenut oil, Oleum Hippophae, oleum lini, the Herba Passiflorae Caeruleae caul-fat, Flos Inulae, the Fructus Mangifera Indicae kernel oil, the Flos Rosae Multiflorae fruit oil);
2). polysiloxanes or methyl polysiloxane resin.The methyl phenyl silicone that comprises dimethyl siloxane and mixing; resin can effectively protect hair not to be subjected to the infringement of extraneous harmful chemical; and polysiloxanes or methyl polysiloxane resin are a kind of breathability oil; both can protect hair; can make again the hair eupnea and absorb nutrient substance, lubricated hair and water resistant effect can also be provided.
3). alkanes.As: the isomery dodecane, the isomery tetradecane, the isomery hexadecane, squalane, hydrogenation gathers certain herbaceous plants with big flowers alkene, etc.
4). esters.As: isopropyl palmitate, iso-octyl palmitate, isopropyl myristate, isononyl isononanoate, butyl stearate, IPIS, three benzenetricarboxylic acids, 13 esters, trimerized linoleic acid three isopropyl esters, the propylene glycol isostearate, propylene glycol dicaprate, propylene glycol dicaprylate, pentaerythritol stearic acid ester 2, isostearic acid butyl ester, carbonic acid dibutyl ester etc.
Be applicable to wetting agent of the present invention and be selected from a kind of of polyhydric alcohol, hyaluronic acid or its sodium salt, ceramide or their mixing.Its polyhydric alcohol consumption is between 1.0-10.0%, and preferable amount is between 2-8%, and most preferred quantities is between 3-7%.The consumption of hyaluronic acid and sodium salt thereof and ceramide is at 0.1-10%, and most preferably weight is between 0.1-2%.These materials can absorb airborne moisture and play moisture-keeping function under certain condition.
Wetting agent can keep moisture, when being coated onto on the skin and the skin close contact, and can be with moisture transmission to epidermis.Polyhydric alcohol is such as propylene glycol, sorbitol, and glycerol, 1.3 butanediols, dipropylene glycol, methyl propanediol, molecular weight is at the Polyethylene Glycol below 2000, polyglycereol, maltose alcohol, xylitol etc.Hyaluronic acid or its sodium salt are 1% aqueous solutions.
Being applicable to cation opsonizing agent of the present invention is selected from: one or more mixing in guar gum hydroxypropyl-trimethyl ammonium chloride, Polyquaternium-10, polyquaternary ammonium salt-47, the polyquaternary ammonium salt-7. and its consumption is between 0.0-10%, preferred percent is at 0.1-8%, and most preferably percentage ratio is between 0.2-4%.
Be applicable to collagen polypeptide and be selected from the eel collagen, its consumption is between 0.05-5%, and preferred weight is between 0.05-3%, and most preferably weight is between 0.05-1.This collagen polypeptide is to utilize bright japanese eel skin, and active bio extracts and keeps primary peptide.The concentrated intrinsic nutrition elite of fresh water eel fish skin.The collagen polypeptide compositions that forms with liposome again.
People's vital movement is that the body the people carries out, and planting in people's body has a kind of very important material also not to be familiar with by people so far, and he is called " bone in the bone, the meat in the meat, the skin in the skin " by medical science and biologist.This is being at the developed countries such as America and Europe fashionable " collagen protein " just.Collagen protein (Collagen) is a kind of extracellular protein, and it is to twist into spiral fibrous proteins by three peptide chains.Collagen protein is the rich in protein of people's in-vivo content, it is rich in the aminoacid such as glycine (Glycine), proline (Proline), hydroxyproline (Hydroxyproline) of needed by human, accounts for 1/3rd of human body protein total amount.
Collagen protein is macro-molecular protein, can not be directly absorbed by the body.Collagen polypeptide is the enzymatic hydrolysate of collagen protein, and molecular weight contains the whole aminoacid of collagen protein below 10,000 D, and its good absorbability, dissolubility, water absorption, moisture retention etc. are that collagen protein is incomparable.Get up with liposome again, be applied on hair and the skin and can slowly release, provide nutrition for skin and hair endlessly.The health that keeps hair and skin.
Except mentioned component, also may contain other used in compositions composition in the recipe ingredient of the present invention, such as additive, antiseptic, pearling agent, spice, pigment.Add content generally at 0.0-5%, can select plant extraction liquid, animal extracting solution.The mixing of one or more in the biochemical product.As: Aloe, arnica montana, fragrant honeybee leaf, bigarabe, Flos Chrysanthemi, Cortex Cinnamomi, Radix Notoginseng, Radix Ginseng, Fructus Gleditsia, Ganoderma, Fructus Arctii, lavandula angustifolia, Fructus Cucumidis sativi, Sargassum, Herba Rosmarini Officinalis etc. plant extraction liquid, a kind of or its mixing of placenta extracting liquid, RHEGF, hydrolyzed silkworm silk, Lac regis apis, propolis, vitamin e acetate, vitamin A palmitate, nicotiamide, vitamin B6 etc.The consumption of antiseptic is between 0.2-1.0%, such as a kind of or its mixing of methyl hydroxybenzoate, this propyl ester of hydroxyl, ethyl hydroxybenzoate, butyl hydroxybenzoate, oxybenzene isobutyl ester, imidazolidinyl urea, chlormethylisothiazo,ine ketone, Methylisothiazolinone, iodo propinyl carbamate (IPBC), DMDM Hydantoin, sodium benzoate, potassium sorbate.Raw materials used and pigment and perfume ingredient all are the regulations that meets China 2007 editions " cosmetics health standard " in the prescription.
Deionized water used in the present invention is by reverse osmosis and twice purification of ion exchange resin, the pure water that makes by ultraviolet disinfection again, and its electrical conductivity is lower than 2.0.
The specific embodiment
The interior various embodiments of the scope of the invention are further set forth and illustrated to following example, the example of giving only is for illustrative, be not used for limiting the present invention, because in the situation that do not deviate from the spirit and scope of the present invention, can carry out multiple change to the present invention.Unless stated otherwise.The following raw materials according title is all write by material name or its trade name of INCI name.
Embodiment 1
Referring to table 1, it is the concrete component prescription of the disposable hair care breast that provides of the embodiment of the invention.
A kind of preparation method of collagen polypeptide nutrition washing-free hair care dairy compositions, according to table 1, it comprises the steps:
1) preparation A phase feedstock composition: take by weighing respectively hard fat chemical compound, emollient, emulsifying agent, the antibacterial of preset proportion, add successively in the container warming while stirring to 90 ℃-95 ℃ to raw material and all dissolve;
2) preparation B phase feedstock composition: take by weighing respectively cation opsonizing agent, deionized water, the wetting agent of preset proportion, add successively in the container warming while stirring to 90 ℃-95 ℃ to raw material and all dissolve;
3) preparation C phase feedstock composition: the essence, antibacterial, pearling agent, the antiseptic that take by weighing respectively preset proportion;
4) preparation D phase feedstock composition: the collagen polypeptide, vitamin e acetate, the Aloe extraction solution that take by weighing respectively preset proportion;
5) while stirring B phase feedstock composition is slowly added in the A phase feedstock composition, stirred 2-5 minute, homogenizing 3-8 minute, mixing speed was controlled at 20-30r/m, and homogenizing speed is 1400-2600r/m, and homogenizing temperature is controlled at 80-90 ℃;
6) stirring began cooling in 5 minutes behind the homogenizing;
Add C phase feedstock composition when 7) temperature is down to 45 ℃;
Add D phase feedstock composition when 8) temperature is down to 40 ℃,
9) continue to stir, cool to 35-38 ℃ of discharging, make collagen polypeptide nutrition washing-free hair care dairy compositions.
A kind of collagen polypeptide nutrition washing-free hair care dairy compositions that adopts the preceding method preparation, it is characterized in that: it comprises the component with following percentage by weight:
1). hard fat chemical compound 0.3-12.0%
2). emulsifying agent 0.5-4.0%
3). emollient 2.0-15.0%
4). wetting agent 0.1-10.0%
5). collagen polypeptide 0.05-5%
6). cation opsonizing agent 0.0-10%
7) antiseptic 0.0-0.5%
8) pearling agent 0.2-1%
9). the deionized water surplus.
The disposable hair care dairy compositions of aforesaid collagen polypeptide is characterized in that: in the end article that makes, collagen polypeptide content is 0.05%-5%.
And other adjuvants, such as essence, antibacterial, chelating agent, nutrient.The percentage ratio of raw material all refers to percentage by weight, and its ratio all is as the basis take the pure content of composition.
Wherein the hard fat chemical compound is hexadecanol (spermol), octadecanol (stearyl alcohol); Emulsifying agent is PEG-100 stearate and tristerin
Emollient is polydimethylsiloxane, carbonic acid dibutyl ester, Jojoba oil; Wetting agent is glycerol; Cation opsonizing agent is Polyquaternium-10, and collagen polypeptide is eel collagen polypeptide, and anticorrosion and bactericidal agent is methyl hydroxybenzoate, propyl hydroxybenzoate, Methylisothiazolinone; Nutrient is vitamin e acetate, Aloe extraction solution.
Table 1
Hair caring laboratory tests test behind the Nutritional Nursing Care hair:
It is that sample among reference product and the embodiment compares that hair caring chamber when test adopted the commercially available famous brand name G of China.Do not contain collagen protein among this brand G, all the other raw materials are similar, and content has certain difference.Experimenter (long hair women) adopts double-blind trial-half a head test method, and half hair uses the G product, half hair uses the sample in the embodiment product, the experimenter is totally 30 people, one group of per five people, totally six groups are used respectively six products among the embodiment, product and G product used 15 days continuously, continue again to follow the tracks of 5 days, (full marks are 10 minutes, and hair is smooth to every experimenter's hair being estimated marking by 20 professional hairdressers before using every day, light, pitch-black, flexible, 0 is divided into the hair that is badly damaged, and hair is withered, dim, jaundice, bifurcated, bleach), every group average is as the fractional value of hair on the same day.Can use the microscopic examination hair condition in the test process in case of necessity, the result gathers such as table 2.
Table 2
Find out that from the experimental data of table 2 respectively use contained the disposable hair care breast of 0.05%, 0.1%, 0.2%, 0.5%, 0.8%, 1.0% collagen polypeptide after 15 days, hair quality has improvement in various degree.And the state after hair quality can continue to keep repairing after stopping using, and commercially available famous brand G hair conditioner is unsatisfactory to the improvement of hair quality, and hair is very fast after stopping using gets back to again original state, and this explanation contains the disposable hair care breast of collagen polypeptide the maintenance of hair obviously is better than commercially available common hair conditioner.In addition, from table 2, it can also be seen that the raising along with collagen polypeptide content, the hair care breast to the reparation power of hair also in remarkable enhancing, when collagen polypeptide reaches 0.8% at hair care Ruzhong content from 0.5%, the hair care breast reaches the strongest to the reparation power of hair, and when continuing to increase the content of collagen polypeptide, the hair care breast that the improvement of hair quality is contained in 0.8% collagen polypeptide does not relatively have great change, so the use amount of suggestion collagen polypeptide is controlled at 0.8% for best in prescription, has added on the contrary waste.This perhaps fall to send out what scalp relevant to the absorbability of nutrient substance.
The elastic mensuration of hair
Hair elasticity determines the situation of scalp cortex; The soft also high resilience of good hair quality.For elasticity is tested, get a hair, stretch with thumb and forefinger, healthy hair can redraw on former long basis approximately 1/3 length, and can recover former length.Impaired or poor hair quality can not recover former length, and dry or easily broken hair quality then can be broken when applying tension force.
The test first day is got a hair from position, 30 experimenter crowns in the hair caring chamber, be cut into 15 centimetres of the same length, be placed on constant temperature (25 ℃), take out after 3 hours in the calorstat of constant humidity (65%), elasticity is tested, concrete grammar is with thumb and the forefinger hair that stretches at leisure, until fracture, measures the length of hair after stretching.Get a hair from the same position of experimenter again in Ahau, be cut into 15 centimetres of length, be put into constant temperature (25 ℃), take out after 3 hours in the calorstat of constant humidity (65%), elasticity is tested, concrete grammar be with thumb and forefinger at leisure stretching head be dealt into fracture or move to and get final product when length is 20 centimetres, record the average length when breaking, whether seeing of not breaking can recover the original length.
Table 3
Find out to use from the experimental data of table 3 and contain that the elasticity of hair has increase behind collagen polypeptide and the disposable hair care breast, when the content of collagen protein in the product reaches 0.8% when above, it is maximum that the elasticity of hair reaches, namely elongate original 1/3 and can not rupture, and just can recover the original length after two hours.Commercially available G hair conditioner is then substantially not obvious to the elastic effect that increases hair.
In sum, the present composition can transport supply nutrition, melanin to hair, and absorption and promotion hair absorb trace element, and collagen polypeptide can synthesize rapidly collagen protein again and improve scalp cortex.Therefore often use this product that impaired hair quality is improved significantly.
Embodiment group 2:
Referring to table 4, preparation method and the goods of the collagen polypeptide nutrition washing-free hair care dairy compositions that the present embodiment provides, substantially the same manner as Example 1, its difference is each component and content difference in its prescription.
Table 4
Wherein the hard fat chemical compound is 22 alcohol (behenyl alcohol); Emulsifying agent is selected from glucosides class, esters.
Emollient is Vegetable oil lipoprotein or hydrogenated vegetable fat, alkanes.Such as isomery dodecane, the isomery tetradecane, isomery hexadecane, squalane, a kind of in the poly-certain herbaceous plants with big flowers alkene of hydrogenation. esters.As: isopropyl palmitate, iso-octyl palmitate, isopropyl myristate, isononyl isononanoate, butyl stearate, IPIS, three benzenetricarboxylic acids, 13 esters, trimerized linoleic acid three isopropyl esters, the propylene glycol isostearate, propylene glycol dicaprate, propylene glycol dicaprylate, pentaerythritol stearic acid ester 2, isostearic acid butyl ester, carbonic acid dibutyl ester etc., Jojoba oil; Wetting agent is propylene glycol, sorbitol, 1.3 butanediols, dipropylene glycol, arbitrary in the methyl propanediol; Cation opsonizing agent is a kind of in guar gum hydroxypropyl-trimethyl ammonium chloride, polyquaternary ammonium salt-47, the polyquaternary ammonium salt-7, and collagen polypeptide is eel collagen polypeptide, and antiseptic or antibacterial are a kind of in methyl hydroxybenzoate, propyl hydroxybenzoate, the Methylisothiazolinone; Nutrient is vitamin e acetate, Aloe extraction solution.
Hair caring laboratory tests test behind the Nutritional Nursing Care hair
It is that sample in reference product X and the embodiment group 2 compares that hair caring chamber when test adopted background technology institute record scheme.Experimenter (long hair women) adopts double-blind trial-half a head test method, and half hair uses the X product, half hair uses the sample in embodiment group 2 products, the experimenter is totally 30 people, one group of per five people, totally six groups are used respectively six products among the embodiment, product and G product used 15 days continuously, continue again to follow the tracks of 5 days, (full marks are 10 minutes, and hair is smooth to every experimenter's hair being estimated marking by 20 professional hairdressers before using every day, light, pitch-black, flexible, 0 is divided into the hair that is badly damaged, and hair is withered, dim, jaundice, bifurcated, bleach), every group average is as the fractional value of hair on the same day.Can use the microscopic examination hair condition in the test process in case of necessity, the result gathers such as table 5.
Table 5
Find out that from the experimental data of table 5 respectively use contained the disposable hair care breast of 0.8%-1.0% collagen polypeptide after 15 days, hair quality and comparison X ratio have obvious progress.
The elastic mensuration of hair:
Hair elasticity determines the soft also high resilience of the hair quality in order of scalp cortex.For elasticity is tested, get a hair, stretch with thumb and forefinger, healthy hair can redraw on former long basis approximately 1/3 length, and can recover former length.Impaired or poor hair quality can not recover former length, and dry or easily broken hair quality then can be broken when applying tension force.
The test first day is got a hair from position, 30 experimenter crowns in the hair caring chamber, be cut into 15 centimetres of the same length, be placed on constant temperature (25 ℃), take out after 3 hours in the calorstat of constant humidity (65%), elasticity is tested, concrete grammar is with thumb and the forefinger hair that stretches at leisure, until fracture, measures the length of hair after stretching.Get a hair from the same position of experimenter again in Ahau, be cut into 15 centimetres of length, be put into constant temperature (25 ℃), take out after 3 hours in the calorstat of constant humidity (65%), elasticity is tested, concrete grammar be with thumb and forefinger at leisure stretching head be dealt into fracture or move to and get final product when length is 20 centimetres, record the average length when breaking, whether seeing of not breaking can recover the original length, its cohersive and integrated data sees Table 6.
Table 6
Find out to use from the experimental data of table 6 and contain that the elasticity of hair has increase behind collagen polypeptide and the disposable hair care breast, it is maximum that the elasticity of hair reaches, and namely elongates original 1/3 and can not rupture, and just can recover the original length after two hours.X hair conditioner then has certain effect to the elasticity that increases hair, but not obvious.
The present invention is not limited to above-described embodiment, as described in the above embodiment of the present invention, adopts the method identical or approximate with it or component and the collagen polypeptide nutrition washing-free hair care dairy compositions preparation method and the goods thereof that obtain, all in protection domain of the present invention.
Claims (2)
1. the preparation method of a collagen polypeptide nutrition washing-free hair care dairy compositions, it is characterized in that: it comprises the steps:
1) preparation A phase feedstock composition: take by weighing respectively hard fat chemical compound, emollient, emulsifying agent, the antibacterial of preset proportion, add successively in the container warming while stirring to 90 ℃-95 ℃ to raw material and all dissolve;
2) preparation B phase feedstock composition: take by weighing respectively cation opsonizing agent, deionized water, wetting agent and the EDETATE SODIUM of preset proportion, add successively in the container warming while stirring to 90 ℃-95 ℃ to raw material and all dissolve;
3) preparation C phase feedstock composition: the essence, antibacterial, the pearling agent that take by weighing respectively preset proportion;
4) preparation D phase feedstock composition: the collagen polypeptide, vitamin e acetate, the Aloe extraction solution that take by weighing respectively preset proportion;
5) while stirring B phase feedstock composition is slowly added in the A phase feedstock composition, stirred 2-5 minute, homogenizing 3-8 minute, mixing speed was controlled at 20-30r/m, and homogenizing speed is 1400-2600r/m, and homogenizing temperature is controlled at 80-90 ℃;
6) stirring began cooling in 5 minutes behind the homogenizing;
Add C phase feedstock composition when 7) temperature is down to 45 ℃;
Add D phase feedstock composition when 8) temperature is down to 40 ℃,
9) continue to stir, cool to 35-38 ℃ of discharging, make collagen polypeptide nutrition washing-free hair care dairy compositions; The component prescription of above-mentioned hair care dairy compositions is:
A phase: hexadecanol 3%, octadecanol 1.5%, PEG-100 stearate and tristerin 3%, Jojoba oil 2%, polydimethylsiloxane 1.5%, dicaprylyl carbonate 1%, methyl hydroxybenzoate 0.15%, propyl hydroxybenzoate 0.05%;
C phase: essence 0.3%, Methylisothiazolinone 0.0006%, pearling agent 0.5%;
D phase: eel collagen polypeptide 0.1%, vitamin e acetate 0.1%, Aloe extraction solution 0.8%;
B phase: EDETATE SODIUM 0.05%, Polyquaternium-10 0.2%, glycerol 4%, deionized water surplus;
Above percentage ratio all is weight percentage.
2. collagen polypeptide nutrition washing-free hair care dairy compositions, it prepares according to the described method of claim 1.
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| CN105662910A (en) * | 2016-01-20 | 2016-06-15 | 广西南岜仔科技有限公司 | Fibroin hair conditioner and preparation method thereof |
| CN108815020A (en) * | 2018-06-27 | 2018-11-16 | 跨越生物科技（滁州）有限公司 | A kind of disposable nutrition profit hair-cream preparation method of water conservation |
| CN111956521A (en) * | 2020-09-16 | 2020-11-20 | 上海海盈通感光材料有限公司 | Hair care composition and application thereof, hair conditioner and scalp essence adopting composition and preparation method thereof |
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| CN101427986A (en) * | 2008-12-17 | 2009-05-13 | 广东名臣有限公司 | Cleaning-free hair conditioner and method of producing the same |
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| CN101427986A (en) * | 2008-12-17 | 2009-05-13 | 广东名臣有限公司 | Cleaning-free hair conditioner and method of producing the same |
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