CN105662910A - Fibroin hair conditioner and preparation method thereof - Google Patents
Fibroin hair conditioner and preparation method thereof Download PDFInfo
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- CN105662910A CN105662910A CN201610035623.1A CN201610035623A CN105662910A CN 105662910 A CN105662910 A CN 105662910A CN 201610035623 A CN201610035623 A CN 201610035623A CN 105662910 A CN105662910 A CN 105662910A
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- Prior art keywords
- fibroin
- hexadecanol
- hair conditioner
- panthenol
- hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to a hair conditioner, in particular to a fibroin hair conditioner and a preparation method thereof.The hair conditioner comprises, by weight percentage, 1-5% of fibroin, 3-8% of glycerin, 0.5-1% of vitamin E, 0.5-1% of lauryl trimethyl ammonium chloride, 1-5% of cetanol, 0.5-1% of hydroxy propyl cellulose, 0.1-0.5% of D-panthenol, 1-5% of dodecamethyl-cyclohexasiloxane, 0.1-0.5% of propylparaben, 0.1-0.5% of methylisothiazolinone, 0.8-3% of stearic triglyceride, 1-5% of Isoceteth-20 and the balance of deionized water.The fibroin hair conditioner has the advantages that the fibroin and the D-panthenol can nourish the scalp and hair and is contributive to the repair of the damaged hair and capable of enhancing hair elasticity; by the film-forming wrapping of the dodecamethyl-cyclohexasiloxan, the damaged hair can be well repaired and conditioned.
Description
[technical field]
The present invention relates to a kind of hair conditioner.
[background technology]
Hair conditioner, general and shampoo compositions uses, and is evenly spread upon on hair by appropriate hair conditioner, gently rubs in a moment, then use clear water rinsed clean after hair washing. Along with electricity is sent out, perms, had hair dyed more universal, the injury of hair is increasing, and the phenomenon such as dry hair, fracture generally exists, and the hair having submissive light is more by the personage that likes to be beautiful is craved for. At present, its application of Semen Maydis oil, mainly in the field such as food oils, protective foods, be not shown in the report about being applied in hair conditioner product by Semen Maydis oil.
[summary of the invention]
For the deficiencies in the prior art, it is an object of the invention to provide a kind of fibroin hair conditioner and its preparation method. It is made up of following compositions in weight percentage: fibroin 1~5%, glycerine 3~8%, vitamin-E 0.5~1%, lauryl trimethyl ammonium chloride 0.5~1%, hexadecanol 1~5%, hydroxypropylcellulose 0.5~1%, D-panthenol 0.1~0.5%, cyclohexasiloxane 1~5%, propylben 0.1~0.5%, methylisothiazolinone 0.1~0.5%, glycerol stearate three ester 0.8~3%, different hexadecanol polyethers-201~5%, deionized water surplus.
Further, it is made up of following compositions in weight percentage: fibroin hydrolyzate 2~4%, glycerine 5~7%, vitamin-E 0.6~0.9%, lauryl trimethyl ammonium chloride 0.6~0.9%, hexadecanol 2~4%, hydroxypropylcellulose 0.6~0.9%, D-panthenol 0.2~0.4%, cyclohexasiloxane 2~4%, propylben 0.2~0.4%, methylisothiazolinone 0.2~0.4%, glycerol stearate three ester 1~2%, different hexadecanol polyethers-202~4%, deionized water surplus.
Specifically, it is made up of following compositions in weight percentage: fibroin hydrolyzate 3%, glycerine 6%, vitamin-E 0.7%, lauryl trimethyl ammonium chloride 0.8%, hexadecanol 3%, hydroxypropylcellulose 0.7%, D-panthenol 0.3%, cyclohexasiloxane 3%, propylben 0.3%, methylisothiazolinone 0.3%, glycerol stearate three ester 1.5%, different hexadecanol polyethers-203%, deionized water surplus.
The method of the fibroin hair conditioner of the present invention comprises the following steps:
(1). take raw material by claims 1 to 3 any one formula;
(2). deionized water, glycerine, hydroxypropylcellulose, fibroin hydrolyzate and lauryl trimethyl ammonium chloride are heated to 60~80 DEG C in aqueous phase pot, stir evenly, in suction vacuum emulsification pot;
(3). hexadecanol, D-panthenol, cyclohexasiloxane, propylben, glycerol stearate three ester and different hexadecanol polyethers-20 are added oil phase pot is heated to 60~80 DEG C, stir evenly, in suction vacuum emulsification pot;
(4). start vacuum unit, under vacuum conditions homogeneous 5~10min, stir borehole cooling;
(5). add vitamin-E and methylisothiazolinone when vacuum emulsification pot is cooled to 40~50 DEG C, stir evenly;
(6). continue to be cooled to room temperature, discharging.
Further, the preparation method of described fibroin hydrolyzate is: after being extracted out from silk cocoon by silk, is immersed in 80~90 DEG C of water, hydro-oxidation sodium adjust ph to 10~11, stirs 1~3h, is cooled to room temperature, to obtain final product after elimination insolubles.
In sum, it is an advantage of the invention that: fibroin and D-panthenol can nourish scalp and hair, contribute to repairing damaged hair, strengthen hair elasticity. Wrapped up by the film forming of cyclohexasiloxane, it is possible to make damaged hair obtain good restoration care. Can life-time service, both can do the nursing of dryness, damaged hair, it is also possible to as the use of daily nursing. After using, hair is submissive, smooth, glossy, head is not itched.
[embodiment]
The following examples can help the technician of this area more fully to understand the present invention, but cannot limit the present invention by any way.
Embodiment 1
Fibroin hair conditioner each composition of raw materials amount: fibroin 1g, glycerine 3g, vitamin-E 0.5g, lauryl trimethyl ammonium chloride 0.5g, hexadecanol 1g, hydroxypropylcellulose 0.5g, D-panthenol 0.1g, cyclohexasiloxane 1g, propylben 0.1g, methylisothiazolinone 0.1g, glycerol stearate three ester 0.8g, different hexadecanol polyethers-201g, deionized water 90.4g.
Preparation method: after being extracted out from silk cocoon by silk, is immersed in 80 DEG C of water, hydro-oxidation sodium adjust ph to 11, stirs 1h, is cooled to room temperature, obtains fibroin hydrolyzate after elimination insolubles. Raw material is taken by formula; Deionized water, glycerine, hydroxypropylcellulose, fibroin hydrolyzate and lauryl trimethyl ammonium chloride are heated to 80 DEG C in aqueous phase pot, stir evenly, in suction vacuum emulsification pot; Hexadecanol, D-panthenol, cyclohexasiloxane, propylben, glycerol stearate three ester and different hexadecanol polyethers-20 are added oil phase pot is heated to 80 DEG C, stir evenly, in suction vacuum emulsification pot; Start vacuum unit, under vacuum conditions homogeneous 5min, stir borehole cooling; Vacuum emulsification pot adds vitamin-E and methylisothiazolinone when being cooled to 40 DEG C, stir evenly; Continue to be cooled to room temperature, discharging.
Embodiment 2
Fibroin hair conditioner each composition of raw materials amount: fibroin 5g, glycerine 8g, vitamin e1 g, lauryl trimethyl ammonium chloride 1g, hexadecanol 5g, hydroxypropylcellulose 1g, D-panthenol 0.5g, cyclohexasiloxane 5g, propylben 0.5g, methylisothiazolinone 0.5g, glycerol stearate three ester 3g, different hexadecanol polyethers-205g, deionized water 64.5g.
Preparation method: after being extracted out from silk cocoon by silk, is immersed in 90 DEG C of water, hydro-oxidation sodium adjust ph to 10, stirs 1h, is cooled to room temperature, obtains fibroin hydrolyzate after elimination insolubles. Raw material is taken by formula; Deionized water, glycerine, hydroxypropylcellulose, fibroin hydrolyzate and lauryl trimethyl ammonium chloride are heated to 60 DEG C in aqueous phase pot, stir evenly, in suction vacuum emulsification pot;Hexadecanol, D-panthenol, cyclohexasiloxane, propylben, glycerol stearate three ester and different hexadecanol polyethers-20 are added oil phase pot is heated to 60 DEG C, stir evenly, in suction vacuum emulsification pot; Start vacuum unit, under vacuum conditions homogeneous 10min, stir borehole cooling; Vacuum emulsification pot adds vitamin-E and methylisothiazolinone when being cooled to 50 DEG C, stir evenly; Continue to be cooled to room temperature, discharging.
Embodiment 3
Fibroin hair conditioner each composition of raw materials amount: fibroin hydrolyzate 2g, glycerine 5g, vitamin-E 0.6g, lauryl trimethyl ammonium chloride 0.6g, hexadecanol 2g, hydroxypropylcellulose 0.6g, D-panthenol 0.2g, cyclohexasiloxane 2g, propylben 0.2g, methylisothiazolinone 0.2g, glycerol stearate three ester 1g, different hexadecanol polyethers-202g, deionized water 83.6g.
Preparation method: after being extracted out from silk cocoon by silk, is immersed in 85 DEG C of water, hydro-oxidation sodium adjust ph to 10.5, stirs 2h, is cooled to room temperature, obtains fibroin hydrolyzate after elimination insolubles. Raw material is taken by formula; Deionized water, glycerine, hydroxypropylcellulose, fibroin hydrolyzate and lauryl trimethyl ammonium chloride are heated to 70 DEG C in aqueous phase pot, stir evenly, in suction vacuum emulsification pot; Hexadecanol, D-panthenol, cyclohexasiloxane, propylben, glycerol stearate three ester and different hexadecanol polyethers-20 are added oil phase pot is heated to 70 DEG C, stir evenly, in suction vacuum emulsification pot; Start vacuum unit, under vacuum conditions homogeneous 6min, stir borehole cooling; Vacuum emulsification pot adds vitamin-E and methylisothiazolinone when being cooled to 45 DEG C, stir evenly; Continue to be cooled to room temperature, discharging.
Embodiment 4
Fibroin hair conditioner each composition of raw materials amount: fibroin hydrolyzate 4g, glycerine 7g, vitamin-E 0.9g, lauryl trimethyl ammonium chloride 0.9g, hexadecanol 4g, hydroxypropylcellulose 0.9g, D-panthenol 0.4g, cyclohexasiloxane 4g, propylben 0.4g, methylisothiazolinone 0.4g, glycerol stearate three ester 2g, different hexadecanol polyethers-204g, deionized water 71.1g.
Preparation method: after being extracted out from silk cocoon by silk, is immersed in 85 DEG C of water, hydro-oxidation sodium adjust ph to 10.5, stirs 2h, is cooled to room temperature, obtains fibroin hydrolyzate after elimination insolubles. Raw material is taken by formula; Deionized water, glycerine, hydroxypropylcellulose, fibroin hydrolyzate and lauryl trimethyl ammonium chloride are heated to 70 DEG C in aqueous phase pot, stir evenly, in suction vacuum emulsification pot; Hexadecanol, D-panthenol, cyclohexasiloxane, propylben, glycerol stearate three ester and different hexadecanol polyethers-20 are added oil phase pot is heated to 70 DEG C, stir evenly, in suction vacuum emulsification pot; Start vacuum unit, under vacuum conditions homogeneous 8min, stir borehole cooling; Vacuum emulsification pot adds vitamin-E and methylisothiazolinone when being cooled to 45 DEG C, stir evenly; Continue to be cooled to room temperature, discharging.
Embodiment 5
Fibroin hair conditioner each composition of raw materials amount: fibroin hydrolyzate 3g, glycerine 6g, vitamin-E 0.7g, lauryl trimethyl ammonium chloride 0.8g, hexadecanol 3g, hydroxypropylcellulose 0.7g, D-panthenol 0.3g, cyclohexasiloxane 3g, propylben 0.3g, methylisothiazolinone 0.3g, glycerol stearate three ester 1.5g, different hexadecanol polyethers-203g, deionized water 77.4g.
Preparation method: after being extracted out from silk cocoon by silk, is immersed in 85 DEG C of water, hydro-oxidation sodium adjust ph to 10.5, stirs 2h, is cooled to room temperature, obtains fibroin hydrolyzate after elimination insolubles. Raw material is taken by formula; Deionized water, glycerine, hydroxypropylcellulose, fibroin hydrolyzate and lauryl trimethyl ammonium chloride are heated to 70 DEG C in aqueous phase pot, stir evenly, in suction vacuum emulsification pot; Hexadecanol, D-panthenol, cyclohexasiloxane, propylben, glycerol stearate three ester and different hexadecanol polyethers-20 are added oil phase pot is heated to 70 DEG C, stir evenly, in suction vacuum emulsification pot; Start vacuum unit, under vacuum conditions homogeneous 7min, stir borehole cooling; Vacuum emulsification pot adds vitamin-E and methylisothiazolinone when being cooled to 45 DEG C, stir evenly; Continue to be cooled to room temperature, discharging.
Aesthetic effect is tested
Compare with the product obtained by embodiment 1~5 and certain commercially available product. Experimenter is the women of routine use hair care product. 60 experimenters being divided into 6 groups at random, every index is provided 0~10 point, 10 points of representatives are the most satisfied, and 0 point represents dissatisfied. Result is as shown in table 1. Can drawing, hair is had better repairing effect by the fibroin hair conditioner of the present invention.
Table 1:
Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Commercially available product | |
Slipping after top | 8.7 | 8.3 | 8.6 | 8.1 | 8.9 | 7.3 |
Smoothness during bath | 8.0 | 8.5 | 8.0 | 8.7 | 8.8 | 8.0 |
Antistatic | 8.9 | 8.7 | 8.2 | 8.0 | 8.5 | 7.9 |
A dry elasticity | 8.4 | 8.3 | 8.5 | 8.1 | 8.0 | 7.8 |
Although, above the present invention is described in detail with a general description of the specific embodiments, but on basis of the present invention, it is possible to it being made some modifications or improvements, this will be apparent to those skilled in the art. Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, all belong to the scope of protection of present invention.
Claims (5)
1. a fibroin hair conditioner, it is characterized in that, it is made up of following compositions in weight percentage: fibroin 1~5%, glycerine 3~8%, vitamin-E 0.5~1%, lauryl trimethyl ammonium chloride 0.5~1%, hexadecanol 1~5%, hydroxypropylcellulose 0.5~1%, D-panthenol 0.1~0.5%, cyclohexasiloxane 1~5%, propylben 0.1~0.5%, methylisothiazolinone 0.1~0.5%, glycerol stearate three ester 0.8~3%, different hexadecanol polyethers-201~5%, deionized water surplus.
2. fibroin hair conditioner according to claim 1, it is characterized in that, it is made up of following compositions in weight percentage: fibroin hydrolyzate 2~4%, glycerine 5~7%, vitamin-E 0.6~0.9%, lauryl trimethyl ammonium chloride 0.6~0.9%, hexadecanol 2~4%, hydroxypropylcellulose 0.6~0.9%, D-panthenol 0.2~0.4%, cyclohexasiloxane 2~4%, propylben 0.2~0.4%, methylisothiazolinone 0.2~0.4%, glycerol stearate three ester 1~2%, different hexadecanol polyethers-202~4%, deionized water surplus.
3. fibroin hair conditioner according to claim 2, it is characterized in that, it is made up of following compositions in weight percentage: fibroin hydrolyzate 3%, glycerine 6%, vitamin-E 0.7%, lauryl trimethyl ammonium chloride 0.8%, hexadecanol 3%, hydroxypropylcellulose 0.7%, D-panthenol 0.3%, cyclohexasiloxane 3%, propylben 0.3%, methylisothiazolinone 0.3%, glycerol stearate three ester 1.5%, different hexadecanol polyethers-203%, deionized water surplus.
4. the preparation method of a fibroin hair conditioner, it is characterised in that, comprise step:
(1). take raw material by claims 1 to 3 any one formula;
(2). deionized water, glycerine, hydroxypropylcellulose, fibroin hydrolyzate and lauryl trimethyl ammonium chloride are heated to 60~80 DEG C in aqueous phase pot, stir evenly, in suction vacuum emulsification pot;
(3). hexadecanol, D-panthenol, cyclohexasiloxane, propylben, glycerol stearate three ester and different hexadecanol polyethers-20 are added oil phase pot is heated to 60~80 DEG C, stir evenly, in suction vacuum emulsification pot;
(4). start vacuum unit, under vacuum conditions homogeneous 5~10min, stir borehole cooling;
(5). add vitamin-E and methylisothiazolinone when vacuum emulsification pot is cooled to 40~50 DEG C, stir evenly;
(6). continue to be cooled to room temperature, discharging.
5. the preparation method of fibroin hair conditioner according to claim 4, it is characterized in that, the preparation method of described fibroin hydrolyzate is: after being extracted out from silk cocoon by silk, it is immersed in 80~90 DEG C of water, hydro-oxidation sodium adjust ph to 10~11, stir 1~3h, it is cooled to room temperature after elimination insolubles, to obtain final product.
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106580842A (en) * | 2016-11-24 | 2017-04-26 | 江苏爱西施科技服务咨询股份有限公司 | Silk fibroin composite hydrogel for hair care and preparation method thereof |
CN106619172A (en) * | 2016-11-25 | 2017-05-10 | 江苏爱西施科技服务咨询股份有限公司 | Preparation method of hair care article containing fine silk protein powder |
CN107280994A (en) * | 2017-05-04 | 2017-10-24 | 上海章华保健化妆品有限公司 | One kind hydrolysis fibroin hair conditioner and preparation method thereof |
CN107970142A (en) * | 2018-01-05 | 2018-05-01 | 湖北瑞晟生物有限责任公司 | A kind of fragrant profit hair conditioner and preparation method thereof |
CN111195220A (en) * | 2020-02-12 | 2020-05-26 | 中国热带农业科学院海口实验站 | Hair conditioner with repairing function and preparation method and application thereof |
CN112190501A (en) * | 2020-09-10 | 2021-01-08 | 泉后(广州)生物科技研究院有限公司 | Silk essence capable of protecting hair and hands simultaneously and preparation method thereof |
CN114617793A (en) * | 2021-11-30 | 2022-06-14 | 天津师范大学 | Mulberry leaf protein hair conditioner and preparation method thereof |
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106580842A (en) * | 2016-11-24 | 2017-04-26 | 江苏爱西施科技服务咨询股份有限公司 | Silk fibroin composite hydrogel for hair care and preparation method thereof |
CN106619172A (en) * | 2016-11-25 | 2017-05-10 | 江苏爱西施科技服务咨询股份有限公司 | Preparation method of hair care article containing fine silk protein powder |
CN107280994A (en) * | 2017-05-04 | 2017-10-24 | 上海章华保健化妆品有限公司 | One kind hydrolysis fibroin hair conditioner and preparation method thereof |
CN107970142A (en) * | 2018-01-05 | 2018-05-01 | 湖北瑞晟生物有限责任公司 | A kind of fragrant profit hair conditioner and preparation method thereof |
CN111195220A (en) * | 2020-02-12 | 2020-05-26 | 中国热带农业科学院海口实验站 | Hair conditioner with repairing function and preparation method and application thereof |
CN112190501A (en) * | 2020-09-10 | 2021-01-08 | 泉后(广州)生物科技研究院有限公司 | Silk essence capable of protecting hair and hands simultaneously and preparation method thereof |
CN114617793A (en) * | 2021-11-30 | 2022-06-14 | 天津师范大学 | Mulberry leaf protein hair conditioner and preparation method thereof |
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