CN107280994A - One kind hydrolysis fibroin hair conditioner and preparation method thereof - Google Patents
One kind hydrolysis fibroin hair conditioner and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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Abstract
Fibroin hair conditioner is hydrolyzed the invention discloses one kind, raw material includes：NMF, cationic surfactant, assistant for emulsifying agent, oil, silicone oil, silicone oil emulsion, hydrolysis fibroin, preservative, essence, acidity regulator and water.The present invention discloses its preparation method.In hair conditioner formula of the present invention, due to mutual compatibility between each component, cooperate, cause hydrolysis fibroin to coat hair, occurs strong reciprocation with the keratoprotein in hair, the protein at damaged hair is filled, it is that hair supplements the nutrients to penetrate into inside hair, because fibroin is made up of 18 kinds of amino acid, therefore, damaged hair can be fundamentally repaired, hair is recovered to health status, can slide the hair more silk being equally made up of amino acid, submissive.
Description
The present invention relates to a kind of hair conditioner and preparation method thereof, and in particular to a kind of hair conditioner containing hydrolysis fibroin
And preparation method thereof, belong to household chemicals technical field.
Background technology
The impaired situation of the hair of modern is increasingly serious, and shampoo is difficult to meet to repair all required for damaged hair
Composition.Therefore consumer is more likely to select some quick-acting products, the reparation liquid for special nursing.Therefore hair conditioner produce
, it can close the epidermis scales of hair, make the smooth easy comb of healthy hair, and health is submissive, more can effectively be given than shampoo
Hair supplements the nutrients, and repairs damaged hair.
But, current hair conditioner product, can play makes hair submissive；Antistatic property, but hair will not move swiftly；Energy
Make hair smooth, protect hair surface, but can not fundamentally repair damaged hair.
The content of the invention
To solve the deficiencies in the prior art, the water of impaired hair can be effectively repaired it is an object of the invention to provide a kind of
Solve fibroin hair conditioner and preparation method thereof.
In order to realize above-mentioned target, the present invention is adopted the following technical scheme that：
One kind hydrolysis fibroin hair conditioner, includes per 100kg raw materials：
NMF：1-5kg；
Cationic surfactant：0.3-3kg；
Assistant for emulsifying agent：3-6kg；
Oil：2-5 kg；
Silicone oil：1-3kg,
Silicone oil emulsion：1-3kg；
Hydrolyze fibroin：0.01-0.5kg；
Preservative：0.05-0.1kg；
Essence：0.1-1.0kg；
Acidity regulator：Addition is that the pH value of regulation protein hydrolysate hair conditioner is 4.5-7.0；
Water：Surplus,
A phases, described assistant for emulsifying agent, oil and silicone oil are formed after described NMF, cationic surfactant and water mixing
B phases are formed after mixing, and described silicone oil emulsion, hydrolysis fibroin, preservative, essence and acidity regulator is classified as C phases.
Further preferably, above-mentioned hydrolysis fibroin hair conditioner, includes per 100kg raw materials：
NMF：4.0kg；
Cationic surfactant：2.0kg；
Assistant for emulsifying agent：3.0kg；
Oil：5.0kg；
Silicone oil：3.0kg,
Silicone oil emulsion：3.0kg；
Hydrolyze fibroin：0.5kg；
Preservative： 0.1kg；
Essence：0.3kg；
Acidity regulator：Addition is that the pH value of regulation protein hydrolysate hair conditioner is 4.5-7.0；
Water：Surplus,
A phases, described assistant for emulsifying agent, oil and silicone oil are formed after described NMF, cationic surfactant and water mixing
B phases are formed after mixing, and described silicone oil emulsion, hydrolysis fibroin, preservative, essence and acidity regulator is classified as C phases.
And above-mentioned NMF is glycerine, propane diols, butanediol, panthenol, D-sorbite, dipropylene glycol, hexylene glycol, isopropyl
At least one of alcohol, xylitol, trimethylglycine, polyethylene glycol.
Above-mentioned cationic surfactant is lauryl trimethyl ammonium chloride, cocotrimonium chloride, soya-bean oil fat
Base trimethyl ammonium chloride, hexadecyltrimethylammonium chloride, OTAC, behenyl base trimethyl ammonium chloride,
Butter aliphatic radical trimethyl ammonium chloride, octadecyl trimethyl sulfate methyl ammonium, cetearyl trimethyl ammonium chloride, cetearyl alcohol
Base alkyl dimethyl ammonium chloride, Varisoft 432PPG, h-tallow aliphatic radical octyldimethyl ammonium chloride, h-tallow fat
Base octyldimethyl Methylsulfate ammonium salt, stearic yl pyridines ammonium chloride, hard amide diallyidimethylammonium chloride, hard amide third
Base dimethylamine, PEG-5 stearyls ammonium chloride, lanolinamide ethyl trimethyl ethyl-sulfate ammonium salt, double h-tallow fat
Base alkyl dimethyl ammonium chloride, stearmide alcohol, stearylbenzyidimethylammonium ammonium chloride, acetamide propyltrimethylammonium chloride
At least one of ammonium.
Above-mentioned assistant for emulsifying agent is：At least one of fatty alcohol, wax, stearate, and the described preferred 16- of fatty alcohol
18 alcohol.
Above-mentioned oil is：In vegetable oil, glyceryl ester, branched fatty alcohol, branched chain fatty acid, dimethicone at least
One kind, and the described preferred ethoxylated vegetable oil of vegetable oil.
Above-mentioned preservative is parabens, Kathon CG, Sensiva SC50, Phenoxyethanol, IPBC, benzoic acid
At least one of sodium, phenmethylol.
Above-mentioned essence is odorant.
And above-mentioned acidity regulator is then citric acid or lactic acid.
In addition, a kind of preparation method of above-mentioned hydrolysis fibroin hair conditioner, comprises the following steps：
S1：A phases each component is added into kettle according to quality proportioning first, B phases each component is added into oil cauldron according to quality proportioning mixes
Close uniform, and be heated separately to 80-85 DEG C；
S2：The 15-20% of A phases in kettle is drawn into emulsification pot, then the B phases in oil cauldron are sucked into emulsification pot, is then carried out
5-10min's homogenizes, in Homogenization, the clout for the A phases that substep is added in kettle, then keeps being stirred under vacuum 20min；
S3：Mixture after step S2 is stirred under vacuum is cooled to less than 40 DEG C, and C phases are then sequentially added in the state of stirring
In silicone oil emulsion, hydrolysis fibroin, preservative, essence and acidity regulator, after being uniformly mixed, be cooled to room temperature,
Discharging obtains protein hydrolysate hair conditioner after detection is qualified, and the pH value of protein hydrolysate hair conditioner is measured as at 25 DEG C using dilution method
4.5-7.0。
The present invention is advantageous in that：In hair conditioner formula of the present invention, due to mutual compatibility, phase between each component
Strong reciprocation occurs for mutually cooperation, the keratoprotein that hydrolysis fibroin can be coated in hair, with hair, fills damaged hair
The protein at place, it is that hair supplements the nutrients to penetrate into inside hair, and because fibroin is made up of 18 kinds of amino acid, because
This, can fundamentally repair damaged hair, hair is recovered to health status, can make the hair being equally made up of amino acid more
Plus silk slide, it is submissive.
Brief description of the drawings
Fig. 1 is that hair conditioner hair drying comb manages power test result figure.
Embodiment
Make specific introduce to the present invention below in conjunction with specific embodiment.
In the present invention, the formula for hydrolyzing fibroin hair conditioner is as shown in the table：
Wherein, NMF selects glycerine, and cationic surfactant selects OTAC, and assistant for emulsifying agent is selected
16-18 alcohol, oil is odorant from 2EHP, essence.
Certainly, NMF is alternatively selection propane diols, butanediol, panthenol, D-sorbite, dipropylene glycol, hexylene glycol, isopropyl
At least one of alcohol, xylitol, trimethylglycine, polyethylene glycol.
Cationic surfactant is alternatively lauryl trimethyl ammonium chloride, cocotrimonium chloride, soya-bean oil aliphatic radical
Trimethyl ammonium chloride, hexadecyltrimethylammonium chloride, behenyl base trimethyl ammonium chloride, butter aliphatic radical trimethyl ammonium chloride, ten
Eight alkyl trimethyl sulfate methyl ammoniums, cetearyl trimethyl ammonium chloride, cetearyl alkyl dimethyl ammonium chloride, double hexadecanes
Base alkyl dimethyl ammonium chloride, h-tallow aliphatic radical octyldimethyl ammonium chloride, h-tallow aliphatic radical octyldimethyl sulfate methyl ammonium
Salt, stearic yl pyridines ammonium chloride, hard amide diallyidimethylammonium chloride, hard amide diemethylamine, PEG-5 stearyl chlorides
Change ammonium, lanolinamide ethyl trimethyl ethyl-sulfate ammonium salt, double h-tallow aliphatic radical alkyl dimethyl ammonium chlorides, stearmide
At least one of alcohol, stearylbenzyidimethylammonium ammonium chloride, acetamide hydroxypropyltrimonium chloride.
Assistant for emulsifying agent can also be other fatty alcohols, wax, stearate etc..
And oil can also be then other plant oil, glyceryl ester, branched fatty alcohol, branched chain fatty acid, dimethicone
Deng.
Preservative is parabens, Kathon CG, Sensiva SC50, Phenoxyethanol, IPBC, sodium benzoate, benzene
At least one of methanol.
Acidity regulator can also be lactic acid.In the present invention, the pH value of the protein hydrolysate hair conditioner finally adjusted is
4.5-7.0。
Form A phases after described NMF, cationic surfactant and water mixing, described assistant for emulsifying agent, oil and
B phases are formed after silicone oil mixing, and described silicone oil emulsion, hydrolysis fibroin, preservative, essence and acidity regulator is classified as
C phases.
。
Above-mentioned 16-18 alcohol is cetostearyl alcohol.
The preparation method of hair conditioner described in above example is：
A phases are formed after glycerine, OTAC and water mixing, B is formed after 16-18 alcohol, 2EHP, silicone oil mixing
Phase, and silicone oil emulsion, hydrolysis fibroin, preservative, essence and citric acid are referred to C phases.
Concretely comprise the following steps：
S1：A phases each component is added into kettle according to quality proportioning first, B phases each component is added into oil cauldron according to quality proportioning mixes
Close uniform, and be heated separately to 80-85 DEG C；
S2：The 15-20% of A phases in kettle is drawn into emulsification pot, then the B phases in oil cauldron are sucked into emulsification pot, is then carried out
5-10min's homogenizes, in Homogenization, the clout for the A phases that substep is added in kettle, then keeps being stirred under vacuum 20min；
S3：Mixture after step S2 is stirred under vacuum is cooled to less than 40 DEG C, and silicon is then sequentially added in the state of stirring
Fat liquor, hydrolysis fibroin, preservative, essence and citric acid, after being uniformly mixed, are cooled to room temperature, after detection is qualified
Discharging obtains protein hydrolysate hair conditioner.
According to《Hair care product efficacy assessments》In evaluation method, used instrument test method and sensory testing's method.
The dry cardability of hair conditioner is tested with the tensiometer of Instron 3365, it is as shown in Figure 1 that half a head hair care compares test result.
As shown in Figure 1：The hair conditioner of hydrolysis fibroin is with the addition of, Hair setting power is smaller in dry comb, thus may be used
Know, addition hydrolysis fibroin can substantially reduce Hair setting power.
12 women are chosen to carry out true man's half a head experiment, age 20-45 Sui, hair average length：5 inches, hair class
Type：It is smooth to arrive coarse Asia human hair.
Half is using the hair conditioner described in embodiment 4, and half carries out double-blind using the hair conditioner described in comparative example,
By professional test, group performs.Specific test result is as shown in table 1：
Table 1：
。
As shown in Table 1：Hair conditioner its test result containing hydrolysis fibroin have two it is important the characteristics of：Dry hair easily comb
Reason and smooth feeling are good.And the hair conditioner of the fibroin containing hydrolysis, arrange this point in hair and be substantially better than other products, allow and do hair
Glittering degree/gloss more preferably, and dry hair and wet hair process smooth feeling are more preferable.
The basic principles, principal features and advantages of the present invention have been shown and described above.The technical staff of the industry should
Understand, the invention is not limited in any way for above-described embodiment, it is all to be obtained by the way of equivalent substitution or equivalent transformation
Technical scheme, all falls within protection scope of the present invention.
Claims (10)
1. one kind hydrolysis fibroin hair conditioner, it is characterised in that include per 100kg raw materials：
NMF：1-5kg；
Cationic surfactant：0.3-3kg；
Assistant for emulsifying agent：3-6kg；
Oil：2-5 kg；
Silicone oil：1-5kg,
Silicone oil emulsion：1-3kg；
Hydrolyze fibroin：0.01-0.5kg；
Preservative：0.05-0.1kg；
Essence：0.1-1.0kg；
Acidity regulator：Addition is that the pH value of regulation protein hydrolysate hair conditioner is 4.5-7.0；
Water：Surplus,
A phases, described assistant for emulsifying agent, oil and silicone oil are formed after described NMF, cationic surfactant and water mixing
B phases are formed after mixing, and described silicone oil emulsion, hydrolysis fibroin, preservative, essence and acidity regulator is classified as C phases.
2. a kind of hydrolysis fibroin hair conditioner according to claim 1, it is characterised in that include per 100kg raw materials：
NMF：4.0kg；
Cationic surfactant：2.0kg；
Assistant for emulsifying agent：3.0kg；
Oil：5.0kg；
Silicone oil：3.0kg,
Silicone oil emulsion：3.0kg；
Hydrolyze fibroin：0.5kg；
Preservative： 0.1kg；
Essence：0.3kg；
Acidity regulator：Addition is that the pH value of regulation protein hydrolysate hair conditioner is 4.5-7.0；
Water：Surplus,
A phases, described assistant for emulsifying agent, oil and silicone oil are formed after described NMF, cationic surfactant and water mixing
B phases are formed after mixing, and described silicone oil emulsion, hydrolysis fibroin, preservative, essence and acidity regulator is classified as C phases.
3. a kind of described hydrolysis fibroin hair conditioner according to claim 1 or 2, it is characterised in that described guarantor
Humectant is that glycerine, propane diols, butanediol, panthenol, D-sorbite, dipropylene glycol, hexylene glycol, isopropanol, xylitol, trimethyl are sweet
At least one of propylhomoserin, polyethylene glycol.
4. a kind of described hydrolysis fibroin hair conditioner according to claim 1 or 2, it is characterised in that described sun
Ionic surface active agent is lauryl trimethyl ammonium chloride, cocotrimonium chloride, soya-bean oil aliphatic radical trimethyl ammonium chloride, ten
Six alkyl trimethyl ammonium chlorides, OTAC, behenyl base trimethyl ammonium chloride, butter aliphatic radical trimethyl ammonia chloride
It is ammonium, octadecyl trimethyl sulfate methyl ammonium, cetearyl trimethyl ammonium chloride, cetearyl alkyl dimethyl ammonium chloride, double
Hexadecyldimethyl benzyl ammonium ammonium chloride, h-tallow aliphatic radical octyldimethyl ammonium chloride, h-tallow aliphatic radical octyldimethyl sulfuric acid
Methyl esters ammonium salt, stearic yl pyridines ammonium chloride, hard amide diallyidimethylammonium chloride, hard amide diemethylamine, PEG-5 are hard
It is aliphatic radical ammonium chloride, lanolinamide ethyl trimethyl ethyl-sulfate ammonium salt, double h-tallow aliphatic radical alkyl dimethyl ammonium chlorides, hard
At least one of acyl amine alcohol, stearylbenzyidimethylammonium ammonium chloride, acetamide hydroxypropyltrimonium chloride.
5. described a kind of hydrolysis fibroin hair conditioner according to claim 1 or 2, it is characterised in that described helps
Emulsifying agent is：At least one of fatty alcohol, wax, stearate, and the described preferred 16-18 alcohol of fatty alcohol.
6. a kind of described hydrolysis fibroin hair conditioner according to claim 1 or 2, it is characterised in that described oil
It is divided into：At least one of vegetable oil, glyceryl ester, branched fatty alcohol, branched chain fatty acid, dimethicone, and described plant
Thing oil preferably ethoxylated vegetable oil.
7. described a kind of hydrolysis fibroin hair conditioner according to claim 1 or 2, it is characterised in that described is anti-
Rotten agent be parabens, Kathon CG, Sensiva SC50, Phenoxyethanol, IPBC, sodium benzoate, phenmethylol in extremely
Few one kind.
8. a kind of described hydrolysis fibroin hair conditioner according to claim 1 or 2, it is characterised in that described perfume (or spice)
Essence is odorant.
9. a kind of described hydrolysis fibroin hair conditioner according to claim 1 or 2, it is characterised in that described acid
It is citric acid or lactic acid to spend conditioning agent.
10. the preparation method of the hydrolysis fibroin hair conditioner described in a kind of claim 1 or 2, it is characterised in that including following
Step：
S1：A phases each component is added into kettle according to quality proportioning first, B phases each component is added into oil cauldron according to quality proportioning mixes
Close uniform, and be heated separately to 80-85 DEG C；
S2：The 15-20% of A phases in kettle is drawn into emulsification pot, then the B phases in oil cauldron are sucked into emulsification pot, is then carried out
5-10min's homogenizes, in Homogenization, the clout for the A phases that substep is added in kettle, then keeps being stirred under vacuum 20min；
S3：Mixture after step S2 is stirred under vacuum is cooled to less than 40 DEG C, and C phases are then sequentially added in the state of stirring
In silicone oil emulsion, hydrolysis fibroin, preservative, essence and acidity regulator, after being uniformly mixed, be cooled to room temperature,
Discharging obtains protein hydrolysate hair conditioner after detection is qualified, and the pH value of protein hydrolysate hair conditioner is measured as at 25 DEG C using dilution method
4.5-7.0。
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| CN107822927A (en) * | 2017-12-06 | 2018-03-23 | 湖北工程学院 | Hair conditioner and preparation method thereof |
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| CN113842333A (en) * | 2021-08-09 | 2021-12-28 | 善颜互联网科技(上海)有限公司 | Water-oil two-phase accurate hair care nourishing liquid |
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Application publication date: 20171024 |