CN105997735A - Natural hair washing and caring article and preparation method and application thereof - Google Patents
Natural hair washing and caring article and preparation method and application thereof Download PDFInfo
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- CN105997735A CN105997735A CN201610548516.9A CN201610548516A CN105997735A CN 105997735 A CN105997735 A CN 105997735A CN 201610548516 A CN201610548516 A CN 201610548516A CN 105997735 A CN105997735 A CN 105997735A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/14—Liposomes; Vesicles
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
Abstract
The invention discloses a natural hair washing and caring article and a preparation method and application thereof. The natural hair washing and caring article is prepared from lipidosome of pony seed oil and crambe maritime leave extract, hydrolysed fibroin and a surface active agent. The natural hair washing and caring article is prepared from natural ingredients, so that the hair cleaning and smoothing functions of common natural shampoos are achieved, the functions of nourishing hair and repairing damaged hair are further achieved, and meanwhile the solubility of the natural ingredients is greatly improved.
Description
Technical field
The present invention relates to hair-washing hair-care articles for use technical field, particularly to a kind of natural hair-washing hair-care articles for use and
Preparation method and application.
Background technology
Shampoo is main scalp and the hair compounding with surfactant for main body and forming, have cleaning people,
And keep the product of its beauty function, it is the commonly used daily chemical products of daily life.The component bag of shampoo
Include surfactant, stabilizer, functional additive, preservative and essence etc..Shampoo is a kind of
Hair cleaning agent, but also there is good nourishing scalp, anti-dandruff effect.
Existing shampoo is widely used the surfactant of chemosynthesis, and the most representative is
AES (laureth sulfuric acid), K12 (lauryl sulfate ester ammonium salt), CAB (dodecanamide propyl
Glycine betaine) etc..Surfactants of these synthesis, during chemosynthesis, generally require high temperature, strong
Acid, strong alkali environment, therefore inevitably result from various by-product, as produced two evils when producing AES
Alkane.In the surfactant of synthesis, harmful side product has a strong impact on Product Safety, healthy to human body
Impact.
Meanwhile, in addition to meeting cleaning function, shampoo also needs to meet the demand on consumer's functional effect,
Such as nourish scalp, repair damaged hair, anti-dandruff etc..These functional additives include organosilicon, change
The zinc compound etc. of work synthesis.Although there is certain effect at the additive initial stage of these chemosynthesis, but long
Phase uses and frequently can lead to scalp itch, destroys human embryo, the side effect being detrimental to health.Simultaneously this
A little synthetic additives are often also insoluble in water and surfactant, easy absorption on the scalp and hair of people,
Lasting to human body infringement, and easily cause the pollution to environment equally
And use natural product as raw material, both can reduce the risk introducing harmful substance, and can fit again
Consumer is desirable for the demand of " green, natural, environmental protection " product, is therefore the focus of attention in recent years.
Public announcement of a patent application CN103720637A discloses one and includes that plant extract, Oleum Cocois are derivative
Thing, activated water and the natural plant extract of auxiliary materials；
Public announcement of a patent application CN102716046A discloses a kind of containing virgin olive oil and derivant thereof
Shampoo and preparation method thereof.
Public announcement of a patent application CN103479539A discloses a kind of washing containing saponin and natural thickener
Flooding, wherein saponin includes sapindoside, theasaponin
Public announcement of a patent application CN104622732A discloses a kind of child containing natural plant preservative and washes
Flood.
Public announcement of a patent application CN104490644A discloses one and includes Fructus Sapindi Mukouossi extracting solution, saponin, flies
Raise the plant hair care composition of the grass composition such as extracting solution, Radix Sophorae Flavescentis extract.
Public announcement of a patent application CN104814895A discloses a kind of containing tea saponin, Camellia oil, Semen Vitis viniferae extraction
The natural shampoo of the compositions such as thing.
For the safety issue existing for the shampoo of chemistry, each producer also increases natural shampoo
Exploitation.Natural plant extracts is often big than complex functionality composition in minimal effective concentration, and dissolubility is not
Height, which also limits natural plant extracts application in natural shampoo, the skill of existing natural shampoo
Art often focuses in the research of natural surfactant, but due to natural surfactant solubilizing effect relatively
Weak, it is impossible to some water-fast oil or natural plant extracts of solubilising completely, also cause institute the most on the market
The main efficacy results of development concentrates on cleaning and submissive hair aspect, causes natural shampoo functional side
Face is not enough, such as, nourish scalp, safeguard scalp health aspect, and existing natural shampoo then effect is more weak.
Summary of the invention
Based on this, the present invention provides a kind of natural hair-washing hair-care articles for use and its preparation method and application.The present invention
For the shampoo of existing chemical composition in the problem of secure context, and existing natural shampoo is in function side
The not enough problem in face, develops a natural function shampoo.This shampoo prepared by natural component and
Become, not only there is the effect cleaning submissive hair of common natural shampoo, have more nourishing hair, reparation
The function of damaged hair, dissolubility is improved significantly simultaneously.
The invention provides a kind of natural hair-washing hair-care articles for use.
A kind of natural hair-washing hair-care articles for use, including peony seed oil and the liposome of Crambe abyssinica leaf extract, hydrolysis silkworm
Fibroin and surfactant.
Further, described natural hair-washing hair-care articles for use also include conditioner, preservative, acid-base modifier, perfume (or spice)
Material and deionized water, the percetage by weight of each composition is:
Preferably, described liposome is to adopt to prepare with the following method:
Step one, peony seed oil is mixed homogeneously with Crambe abyssinica leaf extract, obtain mixture；Wherein, male
Red seed oil is 1:1～5:1 with the mass ratio of Crambe abyssinica leaf extract；
Step 2, phospholipid is mixed homogeneously with cholesterol after as matrix material, both mass ratioes be 1:1～
5:1；
Step 3, by the mixture of matrix material Yu step one, be dissolved in the dehydrated alcohol of 3～6 times of quality,
Decompression boils off solvent on the rotary evaporator；
Step 4, addition phosphate buffer, ultrasonic disperse, obtain milky liposome turbid liquor.
The pH value of described phosphate buffer is 6.5～8.0；
Described surfactant be soapberry extract, thea saponin extracting solution, coconut oil diethanol amide or
More than one in empgen BB.Particularly preferably, described surfactant is soapberry extract.
The separating and extracting process of described hydrolyzed silkworm silk albumen is the deionization adding 2～5 times of weight in silkworm silk
Water, is heated to 80～95 DEG C；Regulation pH value is 11～13, makes silkworm silk hydrolyze 2～5 hours, decolours, removes
Miscellaneous, sucking filtration and get final product.
The extracting method of described peony seed oil is: sorting of being peeled off by seed of Flos Moutan, at 100～120 DEG C, fry 50～
70 minutes, then parch material is sent into oil press squeezing and obtains coarse wool oil, be filtrated to get clear crude oil, will be clear
Crude oil, after alkali refining aquation, adds water degumming precipitation, then decolours and get final product.
The preparation technology of described Crambe abyssinica leaf extract, for weighing Crambe abyssinica leaf, adds the ethanol of 2～5 times of weight,
It is heated to 50～60 DEG C, extracts 0.5～2 hour, filter, filtrate is concentrated, add volume phase to concentrated solution
When in concentrated solution volume 1～the water of 2 times, stirring, left at room temperature 12～filtration after 24 hours, obtain filtrate；
Concentrate drying and get final product.
On the other hand, present invention also offers the preparation method of described a kind of natural hair-washing hair-care articles for use, bag
Include following steps:
(1) heating water to 75～80 DEG C, stirring condition adds surfactant and conditioner to being completely dissolved；
(2) it is cooled to less than 45 DEG C, adds hydrolyzed silkworm silk albumen, peony seed oil and Crambe abyssinica leaf extract
Liposome and preservative, stirring is to being completely dissolved
(3) adding acid-base modifier, regulation pH value is 5.5～6.5；
(4) add spice, stir 20～60 minutes, to obtain final product.
Further, present invention also offers described one natural hair-washing hair-care articles for use shampoo, conditioner with
And the application in bath gel.
It is functional additive that natural shampoo involved in the present invention with the addition of peony seed oil, has nourishing head
Send out, the effect of removing scurf and relieving itching.
Natural shampoo involved in the present invention with the addition of Crambe abyssinica leaf extract as softener, has smooth
Hair, but not there is the effect of greasy feeling.
It is functional additive that natural shampoo involved in the present invention with the addition of hydrolyzed silkworm silk albumen, has and repaiies
Multiple damaged hair, repairs effect sending out tail of jag.Described hydrolyzed silkworm silk albumen percent mass in formula
Ratio is 0.1～3%, and best proportion is 0.5～2%；
Further, described conditioner include guar hydroxypropyltrimonium chloride, polyquaternary ammonium salt-43, third
More than one in olefin(e) acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer；
Further, during described preservative includes Cortex Magnoliae Officinalis extract, Aloe extract, Cortex Mori extract
More than one；
Further, described acid-base modifier is citric acid；
Further, more than one during described essence includes natural lemon quintessence oil or natural orchid compound.
The present invention is relative to prior art have the advantage that and beneficial effect.
(1) present invention uses natural extract to be surfactant, it is to avoid synthetic surfactant is remained
The impurity harm to health；Present invention discover that when surfactant is soapberry extract, active component
The dissolubility of (peony seed oil and Crambe abyssinica leaf extract) is improved, simultaneously peony seed oil and Crambe abyssinica leaf
The activity of extract also can improve.
(2) hair care product involved in the present invention with the addition of natural peony seed oil is functional additive,
There is nourishing hair, the effect of removing scurf and relieving itching, the natural safety of this composition.
(3) shampoo involved in the present invention with the addition of hydrolyzed silkworm silk albumen is functional additive, has and repaiies
Multiple damaged hair, repairs effect sending out tail of jag.
(4) natural shampoo involved in the present invention with the addition of Crambe abyssinica leaf extract as softener, has
Smooth hair, but not there is the effect of greasy feeling.
(5) for improving peony seed oil and the dissolubility of Crambe abyssinica leaf extract and bioavailability, system of the present invention
For containing peony seed oil and the liposome of Crambe abyssinica leaf extract, active component (peony seed oil and Crambe abyssinica leaf
Extract) dissolubility be greatly increased, the problem solving the solubilizing effect difference of surfactant, simultaneously can
To utilize the advantage that liposome is identical with cell membrane component, improve peony seed oil and Crambe abyssinica leaf extract
Absorbability, substantially increases hair care effect.
(6) natural shampoo of the present invention is compared with traditional chemical shampoo, has safe and harmless effect,
With the addition of again multiple natural function composition simultaneously, possessing outside the function that common shampoo is conventional, having more taste
Support hair, removing scurf and relieving itching and the effect of reparation damaged hair.
Detailed description of the invention
In order to make the purpose of the present invention, technical scheme and advantage clearer, below in conjunction with embodiment,
The present invention is further elaborated.Should be appreciated that specific embodiment described herein only in order to
Explain the present invention, be not intended to limit the present invention.
Embodiment 1-embodiment 4:
The separating and extracting process of described hydrolyzed silkworm silk albumen is the deionized water adding 4 times of weight in silkworm silk,
It is heated to 80 DEG C；Regulation pH value is 11, makes silkworm silk hydrolyze 4 hours, decolouring, remove impurity, sucking filtration and get final product.
The extracting method of described peony seed oil is: sorting of being peeled off by seed of Flos Moutan, at 100 DEG C, fries 60 minutes,
Then parch material is sent into oil press squeezing and obtains coarse wool oil, be filtrated to get clear crude oil, clear crude oil is passed through
After alkali refining aquation, add water degumming precipitation, then decolour and get final product.
The preparation technology of described Crambe abyssinica leaf extract, for weighing Crambe abyssinica leaf, adds the ethanol of 5 times of weight,
It is heated to 50 DEG C, extracts 1 hour, filter, filtrate is concentrated, add volume to concentrated solution and be equivalent to concentrate
Liquid amasss the water of 2 times, and stirring, left at room temperature filters after 15 hours, obtains filtrate；Concentrate drying and get final product.
The preparation method employing following steps of the shampoo of embodiment of the present invention 1-4:
(1) according to form formula, heating water to 75 DEG C, stirring condition adds surfactant and conditioner
To being completely dissolved；
(2) it is cooled to 43 DEG C, adds hydrolyzed silkworm silk albumen, peony seed oil and the lipid of Crambe abyssinica leaf extract
Body and preservative, stirring is to being completely dissolved
(3) adding acid-base modifier, regulation pH value is 5.5；
(4) add spice, stir 30 minutes, to obtain final product.
Described liposome is to adopt to prepare with the following method:
Step one, peony seed oil is mixed homogeneously with Crambe abyssinica leaf extract, obtain mixture；Wherein, male
Red seed oil is 5:3 with the mass ratio of Crambe abyssinica leaf extract；
Step 2, phospholipid is mixed homogeneously with cholesterol after as matrix material, both mass ratioes are 3:1；
Step 3, by the mixture of matrix material Yu step one, be dissolved in the dehydrated alcohol of 5 times of quality,
Decompression boils off solvent on the rotary evaporator；
Step 4, addition pH value are the phosphate buffer of 7.4, and ultrasonic disperse obtains milky liposome
Suspension.
Embodiment 5 (reference examples): the parts by weight of each composition are:
According to formula, heating water to 75 DEG C, stirring condition adds surfactant and conditioner to the most molten
Solve；It is cooled to 43 DEG C, adds hydrolyzed silkworm silk albumen, peony seed oil, Crambe abyssinica leaf extract and preservative,
Stirring is to being completely dissolved；Adding acid-base modifier, regulation pH value is 5.5；Add spice, stir 30 minutes,
Obtain.
Contrast experiment 1: what the shampoo of embodiment 1 added is the liposome of peony seed oil/Crambe abyssinica leaf extract
(drug loading 80%)；What the shampoo of embodiment 5 added is peony seed oil and the mixing of Crambe abyssinica leaf extract
Thing；Centrifugal mode is used to contrast the stability of both emulsification systems the shampoo of embodiment 1 and embodiment 5.
Take two kinds of shampoos of identical weight, under the rotating speed that 4000rpm/ divides, after centrifugal 8 hours, pour color comparison tube into
Middle standing 10 minutes, observes two kinds of person's states.The shampoo of embodiment 1, after centrifugal 8 hours, is still protected
Holding uniformly, and the shampoo of embodiment 5 is after 8 hours centrifugal, liquid upper strata has lamination to occur.
After this explanation adds with liposomal form, the dissolubility of peony seed oil and Crambe abyssinica leaf extract is improved.
Contrast test 2: the shampoo interpolation taking the embodiment of the present invention 1 is peony seed oil/Crambe abyssinica leaf extract
Liposome (drug loading 80%)；What the shampoo of embodiment 5 added is peony seed oil and the extraction of Crambe abyssinica leaf
The mixture of thing carries out clinical research, and occupation mode is once a day, uses 14 days, and experimenter is to using effect
Fruit is given a mark, and result is as shown in the table:
| Detection project | Experiment number | Embodiment 1 | Embodiment 5 |
| Head pruritus degree (20 points) | 30 | 18 | 14 |
| Dandruff degree (20 points) | 30 | 18 | 11 |
| Hair compliance (20 points) | 30 | 19 | 13 |
| Cleaning effect (20 points) | 30 | 18 | 15 |
| Hair quality degree of improvement (20 points) | 30 | 17 | 14 |
| Total score | 90 | 67 |
After comparing result explanation adds with liposomal form, peony seed oil and the active of Crambe abyssinica leaf extract obtain
Arrive raising.
Contrast test 3: with the addition of soapberry extract in surfactant in the shampoo of embodiment 1-3；Implement
The shampoo of example 4 does not add soapberry extract, enforcement 2, embodiment 3 are centrifuged with embodiment 4
Stability test and Comparison of clinical effect are as follows:
| Detection project | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Dewatering ability is tested | Without layering | Without layering | Slight layering |
| Head pruritus degree (20 points) | 17 | 16 | 16 |
| Dandruff degree (20 points) | 16 | 14 | 14 |
| Hair compliance (20 points) | 18 | 15 | 14 |
| Cleaning effect (20 points) | 18 | 15 | 15 |
| Hair quality degree of improvement (20 points) | 16 | 14 | 13 |
| Total score | 85 | 74 | 72 |
Comparing result explanation surfactant with the addition of soapberry extract, peony seed oil and Crambe abyssinica leaf carry
The dissolubility and the activity that take thing are improved.
The shampoo of the present invention safety when ensureing use, while life-time service is harmless, adds
The natural function compositions such as peony seed oil, hydrolyzed silkworm silk albumen, Crambe abyssinica leaf extract, have nourishing head
Send out, removing scurf and relieving itching and repair damaged hair effect.Invention is by peony seed oil and Crambe abyssinica leaf extract system
Standby one-tenth liposome, improves dissolubility and bioavailability.
Embodiment described above only have expressed the several embodiments of the present invention, it is impossible to is interpreted as the present invention special
The restriction of profit scope.It should be pointed out that, for the person of ordinary skill of the art, without departing from this
On the premise of inventive concept, it is also possible to make some deformation and improvement, these broadly fall into the protection model of the present invention
Enclose.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (10)
1. natural hair-washing hair-care articles for use, it is characterised in that include peony seed oil and Crambe abyssinica leaf extract
Liposome, hydrolyzed silkworm silk albumen and surfactant.
One the most according to claim 1 natural hair-washing hair-care articles for use, it is characterised in that also include adjusting
Reason agent, preservative, acid-base modifier, spice and deionized water, the percetage by weight of each composition is:
One the most according to claim 1 and 2 natural hair-washing hair-care articles for use, it is characterised in that described fat
Plastid is to adopt to prepare with the following method:
Step one, peony seed oil is mixed homogeneously with Crambe abyssinica leaf extract, obtain mixture；Wherein, male
Red seed oil is 1:1～5:1 with the mass ratio of Crambe abyssinica leaf extract；
Step 2, phospholipid is mixed homogeneously with cholesterol after as matrix material, both mass ratioes be 1:1～
5:1；
Step 3, by the mixture of matrix material Yu step one, be dissolved in the dehydrated alcohol of 3～6 times of quality,
Decompression boils off solvent on the rotary evaporator；
Step 4, addition phosphate buffer, ultrasonic disperse, obtain milky liposome turbid liquor.
One the most according to claim 3 natural hair-washing hair-care articles for use, it is characterised in that described seed of Flos Moutan
The extracting method of oil is: sorting of being peeled off by seed of Flos Moutan, at 100～120 DEG C, fries 50～70 minutes, then
Parch material is sent into oil press squeezing and obtains coarse wool oil, be filtrated to get clear crude oil, by clear crude oil through alkali refining
After aquation, add water degumming precipitation, then decolour and get final product.
One the most according to claim 3 natural hair-washing hair-care articles for use, it is characterised in that described Crambe abyssinica
The preparation technology of leaf extract for weighing Crambe abyssinica leaf, add 2～5 times of weight ethanol, be heated to 50～
60 DEG C, extract 0.5～2 hour, filter, filtrate is concentrated, add volume to concentrated solution and be equivalent to concentrated solution
Volume 1～the water of 2 times, stirring, left at room temperature 12～filtration after 24 hours, obtain filtrate；Concentrate drying
Obtain.
One the most according to claim 1 and 2 natural hair-washing hair-care articles for use, it is characterised in that described table
Face activating agent is that soapberry extract, thea saponin extracting solution, coconut oil diethanol amide or dodecyl are sweet
More than one in dish alkali.
One the most according to claim 6 natural hair-washing hair-care articles for use, it is characterised in that live in described surface
Property agent is soapberry extract.
8. want the natural hair-washing hair-care articles for use of the one described in 1 or 2 according to right, it is characterised in that described hydrolysis
The separating and extracting process of fibroin be in silkworm silk add 2～5 times of weight deionized water, be heated to 80～
95℃；Regulation pH value is 11～13, makes silkworm silk hydrolyze 2～5 hours, decolouring, remove impurity, sucking filtration and get final product.
9. the preparation method of a kind of natural hair-washing hair-care articles for use that one of claim 1～8 is described, its feature exists
In, comprise the following steps:
(1) heating water to 75～80 DEG C, stirring condition adds surfactant and conditioner to being completely dissolved；
(2) it is cooled to less than 45 DEG C, adds hydrolyzed silkworm silk albumen, peony seed oil and Crambe abyssinica leaf extract
Liposome and preservative, stirring is to being completely dissolved
(3) adding acid-base modifier, regulation pH value is 5.5～6.5；
(4) add spice, stir 20～60 minutes, to obtain final product.
10. the one natural hair-washing hair-care articles for use that one of claim 1～8 is described shampoo, conditioner and
Application in bath gel.
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| CN201610548516.9A CN105997735B (en) | 2016-07-13 | 2016-07-13 | A kind of natural hair-washing hair-care articles and its preparation method and application |
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| CN106691970A (en) * | 2017-01-22 | 2017-05-24 | 李忠泽 | Soapberry silk protein shampoo |
| CN107280994A (en) * | 2017-05-04 | 2017-10-24 | 上海章华保健化妆品有限公司 | One kind hydrolysis fibroin hair conditioner and preparation method thereof |
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| CN108066222A (en) * | 2018-01-23 | 2018-05-25 | 广州市经典伊秀化妆品有限公司 | A kind of scalp care hair shampoo of the extract of bran containing tea and preparation method thereof |
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| CN109925250A (en) * | 2019-05-08 | 2019-06-25 | 西藏农牧学院 | A kind of Tibetan medicine plant extracts shampoo and preparation method thereof |
| CN110075019A (en) * | 2019-04-25 | 2019-08-02 | 南京康之源农业科技发展有限公司 | A kind of tree peony shampoo and preparation method thereof |
| CN110664674A (en) * | 2019-08-15 | 2020-01-10 | 广州欧盛化妆品有限公司 | Beard care oil |
| CN110946787A (en) * | 2018-09-26 | 2020-04-03 | 台山美环健芦荟制品有限公司 | Non-irritating aloe hair conditioner |
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| CN109512744A (en) * | 2018-12-29 | 2019-03-26 | 广州博科健康科技集团有限公司 | A kind of eyelashes growth-promoting media and preparation method thereof |
| CN110075019A (en) * | 2019-04-25 | 2019-08-02 | 南京康之源农业科技发展有限公司 | A kind of tree peony shampoo and preparation method thereof |
| CN109925250A (en) * | 2019-05-08 | 2019-06-25 | 西藏农牧学院 | A kind of Tibetan medicine plant extracts shampoo and preparation method thereof |
| CN110664674A (en) * | 2019-08-15 | 2020-01-10 | 广州欧盛化妆品有限公司 | Beard care oil |
| CN112933014A (en) * | 2021-03-09 | 2021-06-11 | 重庆拓道农业发展有限公司 | Natural shampoo product with rose flower and fruit stock solution formula and preparation method thereof |
| CN114533647A (en) * | 2022-03-31 | 2022-05-27 | 广州旭妆生物科技有限公司 | Silicon oil-free anti-dandruff shampoo composition and preparation method thereof |
| CN115317397A (en) * | 2022-09-23 | 2022-11-11 | 广西和桂集团有限公司 | Polypeptide-containing shampoo and preparation method thereof |
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