CN107550795A - Nourish reparation, black hair anticreep camellia oleifera fruit shampoo and preparation method thereof - Google Patents
Nourish reparation, black hair anticreep camellia oleifera fruit shampoo and preparation method thereof Download PDFInfo
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Abstract
One kind nourishes reparation, black hair anticreep camellia oleifera fruit shampoo, consists of the following composition:Deionized water 5, sodium lauroyl glutamate, Cocoamidopropyl betaine, ammonium lauryl sulfate, APG, fresh squeezing tea fruit emulsion, guar hydroxypropyltrimonium ammonium chloride, acrylamido propyl trimethyl ammonium chloride/acrylamide copolymer, the Octyl Ethers of PPG 3, water-soluble jojoba oil, glycerine, EGDS, disodium ethylene diamine tetraacetate, radix-polygoni multiflori extract, Semen Sesami Nigrum extract, Rhizoma Chuanxiong extract, glossy privet fruit extract, prepared rehmannia root extract, Cacumen Platycladi extract, Fructus Gleditsia extract, salt, essence, Kathon CG.The nourishing reparation, black hair anticreep camellia oleifera fruit shampoo use raw material based on fresh tea fruit pulp, and rich in materials such as camellia oil, Tea Saponin, tea polysaccharide, tea albumen, flavones, being re-dubbed shampoo, there is extraordinary nourish to repair and the effect of black hair anticreep.
Description
Technical field
It is particularly a kind of to nourish reparation, black hair anticreep camellia oleifera fruit shampoo the present invention relates to a kind of shampoo.
Background technology
Squeezed the juice using fresh tea fruit and extract tea oil and tea fruit juice in tea fruit, retain Tea Saponin, tea polysaccharide, tea egg in tea fruit
In vain, the material such as flavones, this stability is high, the high emulsion of nutritional ingredient, in the exploitation applied to all kinds of cosmetics, have non-
Often good skin and hair nursing effect.
The content of the invention
It is an object of the invention to wash camellia oleifera fruit latex composite compounding into a kind of camellia oleifera fruit with nourishing reparation, black hair anticreep
Lotion.
The technical scheme is that：
One kind nourishes reparation, black hair anticreep camellia oleifera fruit shampoo, according to mass fraction meter, is made up of following component:Deionized water
50-60 parts, sodium lauroyl glutamate 10-15 parts, Cocoamidopropyl betaine 5-10 parts, alkylsurfuric acid ammonium 5-8 parts, alkyl sugar
Glycosides 2-4 parts, camellia oleifera fruit emulsion 20-35 parts, guar hydroxypropyltrimonium ammonium chloride 0.1-0.3 parts, acrylamide propyl front three
Ammonium chloride/0.2 part of acrylamide copolymer 0.1-, PPG-3 Octyl Ether 0.1-0.5 parts, water-soluble jojoba oil 0.5-1 parts,
Glycerine 1-2 parts, EGDS 0.8-1.2 parts, disodium ethylene diamine tetraacetate 0.05-0.1 parts, radix-polygoni multiflori extract 2-
4 parts, Semen Sesami Nigrum extract 3-5 parts, Rhizoma Chuanxiong extract 1-3 parts, glossy privet fruit extract 2-4 parts, prepared rehmannia root extract 1-3 parts, side
CedarLeaves extract 2-4 parts, Fructus Gleditsia extract 1-3 parts, salt 1-2 parts, essence 0.1-0.5 parts, Kathon CG 0.05-0.1 parts.
The wherein described preferred ammonium lauryl sulfate of alkylsurfuric acid ammonium.
The preferred APG0810 of wherein described APG.
Preferably, described camellia oleifera fruit emulsion preparation technology is：
（1）Selection：Selection just harvesting, fresh full camellia oleifera fruit machinery peel off, and remove shell, cleaning obtains fresh tea seed；
（2）Crush：By step（1）Gained tea seed puts into pulverizer, obtains tea seed particle（Particle is less than 1 millimeter）, moisture
Content 40-60%；
（3）Split-phase：By step（2）Gained tea seed particle puts into juice extractor, and extruding obtains solid fiber powder and serum；
（4）Purification：By step（3）Gained serum is transported in retort, and PH is adjusted to 2.5-4, adds acid protease, water-bath
It is heated to 50-60 DEG C, after 20-30min, adds decolorising agent, described decolorising agent is activated carbon and/or atlapulgite, adsorbs ratio
- the 1500m of surface area 10002/ g, 20 DEG C -40 DEG C of temperature, mixing time are 20-30 minutes, and mixing speed is 20-60 revs/min
Clock, addition serum weight 1-6% super-cell, is filtered by leaf-type filter, is obtained and is clarified fresh camellia oleifera fruit emulsion；
The present invention is combined by activated carbon and atlapulgite under specific decolorization adsorption aperture, can effectively coordinate protease
Remove sensitizer and pigment, and retentive activity thing very well.
Preferably, step（2）Described crusher sifting aperture 2-10 millimeters, pulverized particles are less than 1 millimeter, moisture
40%-60%；Squeeze the juice well.
Preferably, step（3）Described juice extractor squeezes 0.1 millimeter ~ 1 millimeter of gap, carries out separation of solid and liquid well.
Preferably, step（4）Described acid protease and the weight ratio of serum are（0.1-4）：1000.
Preferably, described acid protease is that the excellent Aspergillus usamii of seed selection is made through depth fermentation..
Preferably, step（4）Described decolorising agent and the weight ratio of serum are（2-5）：100.
The present invention nourishes reparation, the preparation method of black hair anticreep camellia oleifera fruit shampoo, and its preparation technology is：
（1）It is prewired：Fresh oil tea emulsion is heated to 50-80 DEG C, is proportionally added into sodium lauroyl glutamate, cocamidopropyl propyl amide
Glycine betaine, ammonium lauryl sulfate, APG, guar hydroxypropyltrimonium ammonium chloride, acrylamido propyl trimethyl chlorine
Change ammonium/acrylamide copolymer, PPG-3 Octyl Ethers, water-soluble jojoba oil, glycerine, EGDS, ethylenediamine tetraacetic
Acetic acid disodium, heating stirring, mixing time are 20-30 minutes, and mixing speed is 20-60 revs/min, obtains fusions；
（2）Emulsification：In step（1）In, in proportion plus radix-polygoni multiflori extract, Semen Sesami Nigrum extract, Rhizoma Chuanxiong extract, the fruit of glossy privet carry
Thing, prepared rehmannia root extract, Cacumen Platycladi extract, Fructus Gleditsia extract ionized water are taken, is stirred, mixing time is 20-30 minutes, stirring
Speed is 50-80 revs/min, obtains primary emulsifying thing；
（3）Shaping：In step（2）The primary emulsifying thing of gained squeezes into homogenizer, perfuming essence, Kathon CG, salt, homogeneous 10-30 minutes,
Obtain nourishing reparation, black hair anticreep camellia oleifera fruit shampoo.
The beneficial effects of the present invention are：
（1）This method processing step is simple, effectively desensitization, the characteristics of warm camellia oleifera fruit and other components, forms stabilising system
Technology；
（2）Gained nourishes reparation, black hair anticreep camellia oleifera fruit shampoo is to use raw material based on fresh tea fruit pulp, rich in camellia
The materials such as oil, Tea Saponin, tea polysaccharide, tea albumen, flavones, being re-dubbed shampoo, there is extraordinary nourish to repair and black hair anticreep
Effect.
Primary raw material used in the present invention is described as follows：
Camellia oleifera fruit：It is the fruit of tea oil tree.Tea oil tree is the main woody oleiferous plants tree in China, is described as " east tree ", belongs to camellia
Section's Camellia evergreen dungarunga, it is the distinctive woody vegetable oil resource in China.3-6 meters of the height of tree, the diameter of a cross-section of a tree trunk 1.3 meters above the ground is up to 24-30 lis
Rice, smooth bark is taupe；Tea oil tree list leaf alternate, flower are both sexes white, and October, Post flowering was until fruit between October next year
Can be ripe, therefore, tea oil tree has rare flowers and fruits homophyletic phenomenon；Fruit is capsule, is mostly ellipse, has fine, soft fur.Seed
Mostly yellowish-brown, glossy, triangular shape.Tea oil tree is grown in remote mountains, inhales natural nutrient to the greatest extent, evergreen longevity, the age of tree was up to 200 years
More than；It is untouched to retain fresh tea fruit nutritional ingredient using fresh tea fruit cold pressing, rich in unsaturated oils, protein, starch,
Tea Saponin, flavones, polyphenol, VE etc., have moisturizing, moisten, antibacterial, anti-inflammatory and other effects, for taking care of hair, can prevent favus of the scalp, dandruff,
Alopecia and black hair and other effects.
Sodium lauroyl glutamate：Gentle anion surfactant, no anaphylaxis, it is applicable to various sensitiveness fleshes
Skin and baby products etc., blackhead or hoary hair, resistance to hard water are not led to, there is high biological degradability.
Cocoamidopropyl betaine:It is a kind of zwitterionic surfactant, is respectively provided with acid and alkalescence condition
Excellent stability, cation and anion characteristic is presented respectively under the conditions of acid-base property, often with anions and canons and nonionic table
Face activating agent is used in combination, and its compatibility is good, and excitant is small, and soluble in water, foam is more, strong detergency, has excellent thickening
Property, flexibility, bactericidal properties, antistatic behaviour, hard water resistance property, can significantly improve washing class product softness, conditioning and low-temperature stabilization
Property.
Ammonium lauryl sulfate：Anion surfactant, it is soluble in water, compounded with anion, amphion, nonionic
5 property are good, have good emulsification, foaming, infiltration, decontamination and dispersive property, can increase hair soft for shampoo.
APG：Synthesized by renewable resource natural fat alcohol and glucose, be that a kind of performance is more comprehensively new
Nonionic surfactant, have the characteristic of conventional nonionic and anion surfactant concurrently, with high surface, well
Ecological security and intermiscibility, it is internationally recognized preferred " green " functional surfactant.
Guar hydroxypropyltrimonium ammonium chloride：It polymerize with superior water-soluble and adsorption capacity cationic cellulose
Thing, can be compatible with anion, cation, nonionic and zwitterionic surfactant, and excitant is low, its unique cationic
Impaired hair protein matrix can be repaired, keeps hair to moisten, assigns the superior carding property of hair and glossy smooth sense
Feel.
Acrylamido propyl trimethyl ammonium chloride/acrylamide copolymer：Water-soluble cationic polymer, can be obvious
Improve hair washing, hair products bath and wet comb smooth feeling
PPG-3 Octyl Ethers：For in shampoo, hair gloss can be significantly improved, make hair is smooth to be easier to arrange, can be effective
Entanglement when hair rinses is removed, effectively prevents that hair is short-tempered.
Water-soluble jojoba oil：Water-soluble assignment agent, shampoo flushing, wet comb, the smoothness of dry comb are can effectively improve, is prevented
Only hair winding, knotting.
Disodium ethylene diamine tetraacetate：A kind of important complexing agent, complex compound easily is formed with reference to calcium ions and magnesium ions in water, prevents calcium
Magnesium ion and surfactant fluid, so that it is guaranteed that the cleaning of surfactant, foaming effect.
Glycerine：A kind of polyalcohol NMF, hair washing process surfactant is avoided to remain, while it is steady to improve shampoo low temperature
It is qualitative.
EGDS：Pearling agent and tax ester agent, there is provided product is pleasing.
Radix-polygoni multiflori extract：Containing nutritions such as phosphatide, energy hairy root nourishing and hair follicle, improve scalp ecology, promote head
Nigrescence pigment generates, and makes hair pitch-black.
Semen Sesami Nigrum extract：Skin care, blacking hair and nourishing face.
Rhizoma Chuanxiong extract：The promoting flow of qi and blood circulation, black hair strengthen the hair.
Glossy privet fruit extract：Improving eyesight black hair, strengthen the hair anticreep.
Prepared rehmannia root extract：Black hair, black palpus.
Cacumen Platycladi extract：Promoting blood circulation, black beard and hair.
Fructus Gleditsia extract：Anti-dandruff, black hair, anticreep.
Deionized water：Eliminate in the pure water after ionic species impurity, produced using the method for RO counter-infiltrations, using ion
The anion and cation that exchanger resin is gone in water removal, make solvent and carrier.
Salt：Main component is NaCl, and the viscosity of liquid is matched somebody with somebody in increase.
Essence：The smell of finished product is adjusted, is allowed to pleasant comfortable.
Kathon CG：The aqueous solution is light amber transparency liquid, and smell is gentle, is mainly used in cosmetics anti-corrosion, toxicity is low, antibacterial
Sphere of action is wide, effect is strong and cosmetic material compatibility is good.
Embodiment
Alkylsurfuric acid ammonium is ammonium lauryl sulfate in embodiment；APG is APG0810.
Camellia oleifera fruit emulsion preparation technology is：
（1）Selection：Selection just harvesting, fresh full camellia oleifera fruit machinery peel off, and remove shell, cleaning obtains fresh tea seed；
（2）Crush：By step（1）Gained tea seed puts into pulverizer（5 millimeters of crusher sifting aperture）, obtain plant material particle
（Particle is less than 1 millimeter）, moisture 50%；
（3）Split-phase：By step（2）Gained tea seed feed particles put into juice extractor（Squeeze 0.4 millimeter of gap）, extrude and consolidated
Body fiber powder and serum；
（4）Purification：By step（3）Gained serum is transported in retort, and pH value is adjusted to 3.5, adds acid protease as choosing
Educate excellent Aspergillus usamii to be made through depth fermentation, the weight ratio with serum is 3：1000；Heating water bath is to 55 DEG C, after 25min,
The weight ratio of addition bleaching agent activated carbon, dosage and serum is 3:100,30 DEG C of temperature, mixing time is 25 minutes, mixing speed
For 40 revs/min, 3% super-cell of serum weight is added, is filtered by leaf-type filter, obtained and clarify fresh oil tea
Fruit emulsion.
Embodiment 1
The nourishing reparation of embodiment 1, black hair anticreep camellia oleifera fruit shampoo, are made up of following processing step：
（1）It is prewired：Fresh oil tea emulsion is heated to 60 DEG C, is proportionally added into sodium lauroyl glutamate, cocamidopropyl propyl amide sweet tea
Dish alkali, ammonium lauryl sulfate, APG, guar hydroxypropyltrimonium ammonium chloride, acrylamido propyl trimethyl chlorination
Ammonium/acrylamide copolymer, PPG-3 Octyl Ethers, water-soluble jojoba oil, glycerine, EGDS, ethylenediamine tetrem
Acid disodium, heating stirring, mixing time are 20 minutes, and mixing speed is 40 revs/min, obtains fusions；
（2）Emulsification：In step（1）In, in proportion plus radix-polygoni multiflori extract, Semen Sesami Nigrum extract, Rhizoma Chuanxiong extract, the fruit of glossy privet carry
Thing, prepared rehmannia root extract, Cacumen Platycladi extract, Fructus Gleditsia extract, ionized water are taken, is stirred, mixing time is 20-30 minutes, is stirred
Speed is mixed as 60 revs/min, obtains primary emulsifying thing；
（3）Shaping：In step（2）The primary emulsifying thing of gained squeezes into homogenizer, perfuming essence, Kathon CG, salt, homogeneous 20 minutes, obtains
Nourish reparation, black hair anticreep camellia oleifera fruit shampoo.
Embodiment 2-7
Embodiment 2-7 nourishing reparation, black hair anticreep camellia oleifera fruit shampoo, its preparation process condition with embodiment 1, are substantially
The condition such as reaction raw materials and proportion scale, temperature, time is slightly different, specifically as listed in table 1.
The embodiment 1-6 of table 1 nourishing reparation, black hair anticreep camellia oleifera fruit shampoo preparation process condition
。
The formula of comparative example 1 is consistent with embodiment 6, and difference is that the preparation method of camellia oleifera fruit emulsion is different, comparative example 1
Using neutral proteinase --- subtilopeptidase A.
Comparative example 2
The formula of comparative example 2 is consistent with embodiment 6, and difference is that the preparation method of camellia oleifera fruit emulsion is different, and comparative example 2 uses
Alkali protease --- serine protease.
Comparative example 3
Camellia oleifera fruit emulsion dosage is 50 parts in the formula of comparative example 3, other consistent with embodiment 6.
It is cold-resistant resistance to that nourishing reparation obtained by embodiment 1-6, comparative example 1-3, black hair anticreep camellia oleifera fruit shampoo are tested it
Heat endurance, scalp anaphylaxis, moisten moisturizing, cleaning, black hair, alopecia.
The embodiment 1-6 of table 2, its functional attributes test result of comparative example 1-3 shampoos
。
Nourishing obtained by embodiment 1-6, comparative example 1-3 is repaired, its functional attributes of black hair anticreep camellia oleifera fruit shampoo and
The used method of testing of physical and chemical index test is as follows.
（1）Cold-resistant heat-resistant stability
Carried out according to 6.2.1 in GB/T 29680 and 6.2.2.
（2）Degree of allergic reaction is tested
Step 1：The gauze of four thickness is cut into a diameter of 1cm circle with scissors, totally 8, had one's hair wash with 1 gram of camellia oleifera fruit of steel bale-out
Liquid, is coated on circular gauze, and blank is done with deionized water；
Step 2：The gripping of gauze tweezers is placed at the anteflexion arm of subject, fixed with adhesive tape, starts timing；
Step 3：Torn after 48h adhesive tape, and observe the reaction of skin at gauze covering immediately；Observe result.
（3）Cleanliness testing, specific method are as follows：
Embodiment 1-6, comparative example 1-3, the nourishing reparation of gained, black hair anticreep camellia oleifera fruit shampoo are uniformly applied to three days not
Make on the hair cleaned, finger, which is grabbed, to be rubbed 10 minutes, will be white of dry towel after two minutes when all hairs are all in uniform white
Bits are wiped clean；With white oil-Absorbing Sheets, rubbing head is sent out again, checks oil-Absorbing Sheets；Contrast does not carry out the hair of any cleaning.
（4）The method of testing for moistening maintenance performance of keeping humidity is tested for head, and specific method is as follows：
Nourishing reparation obtained by embodiment 1-6, black hair anticreep camellia oleifera fruit shampoo are uniformly applied to coarse, dry by the lost head
Hair, experience and moisten moistening effect and repair situation, and record（- expression almost do not have ,+represents, ++ represent it is fine, +++ table
It is very good to show）, moisture preserving time is recorded, untill no moisture feeling.Contrast coarse, dry damaged hair.
（5）Black hair, the method for testing of anticreep performance are tested for head, and specific method is as follows：
By the nourishing reparation obtained by embodiment 1-6, comparative example 1-3, black hair anticreep camellia oleifera fruit shampoo be uniformly applied to white hair and
On the hair of alopecia crowd, finger, which is grabbed, rubs hair and massaging scalp, is used continuously 3 months, record（- expression does not almost have ,+table
Express friendship, ++ represent very well, +++ represent it is very good）Contrast uses front heat condition.
From table 2, the present invention nourishes reparation, black hair anticreep camellia oleifera fruit shampoo uses original based on fresh tea fruit pulp
Material, rich in materials such as camellia oil, Tea Saponin, tea polysaccharide, tea albumen, flavones, compound decontamination, maintenance composition, can deep enough hair,
Hair care moisturizing, the hair tip, cleaning black hair anticreep and other effects are repaired, and without anaphylaxis.
In addition, by the nourishing reparation obtained by embodiment 1-6, black hair anticreep camellia oleifera fruit shampoo, by examining microorganism to refer to
Mark, sanitary index《Cosmetics safety technical specification》（Version in 2015）, obtain the testing result shown in table 3 below.
Reparation, black hair anticreep camellia oleifera fruit shampoo microorganism, sanitary index are nourished obtained by the embodiment 1-6 of table 3
。
The present invention nourishes reparation, black hair anticreep camellia oleifera fruit shampoo toxicology test：Skin irritation test（Multiple skin
Irritation test）
Test objective：Observe rabbit intact skin long-time multiple-contact tested material（The shampoo of embodiments of the invention）Afterwards
Caused skin irritation reaction, peace is provided for the nourishing reparation of embodiments of the invention, black hair anticreep camellia oleifera fruit shampoo
Full property foundation.
Test basis：《Cosmetics safety technical specification》Version in 2015；Test method：From white New Zealand rabbits 8, with
Machine is divided into 2 groups, every group 4；A groups:Experimental group, B groups:Deionized water control group.24h is by family's rabbit back backbone both sides before experiment
Hair is cut, and skin surface is not damaged in cropping, and unhairing scope is 3cm × 3cm, and application area is 2.5cm × 2.5cm, tested
Nourishing reparation of the thing group to various embodiments of the present invention, black hair anticreep camellia oleifera fruit shampoo, take tested material 0.5ml to be coated directly on the back of the body
The side of portion's backbone, opposite side apply 0.5ml control group deionized waters, smear 1 time daily, continuously smear 14d；Opened from second day
Begin, cropping when smearing every time, residual tested material is removed with deionized water；Result is observed after one hour, according to《Cosmetics safety
Technical specification》（Version in 2015）Skin irritation test table scoring, check plot and trial zone are equally handled.
Evaluation of result：Every rabbit average integral daily is calculated according to the following formula, is pierced by specification list deciding rabbit skin
Swash intensity, and observe other toxic actions in addition to excitant.
。
Result of the test：Tested material was carried out in the multiple skin irritation test observation period, gave various embodiments of the present invention
Nourishing reparation, after black hair anticreep camellia oleifera fruit shampoo, rabbit has no erythema, oedema；Have no systemic toxicity profiles performance and dead feelings
Condition, the weight of animals increase, on breathing, circulating, central nervous system, four limbs activity etc. is without influence.
Conclusion (of pressure testing)：The nourishing reparations of various embodiments of the present invention, black hair anticreep camellia oleifera fruit shampoo are to white New Zealand
Rabbit intact skin is nonirritant.
Claims (7)
1. one kind nourishes reparation, black hair anticreep camellia oleifera fruit shampoo, according to mass fraction meter, it is made up of following component:Go from
Sub- water 50-60 parts, sodium lauroyl glutamate 10-15 parts, Cocoamidopropyl betaine 5-10 parts, ammonium lauryl sulfate 5-8
Part, APG 2-4 parts, camellia oleifera fruit emulsion 20-35 parts, guar hydroxypropyltrimonium ammonium chloride 0.1-0.3 parts, acrylamide
Hydroxypropyltrimonium chloride/0.2 part of acrylamide copolymer 0.1-, PPG-3 Octyl Ether 0.1-0.5 parts, water-soluble jojoba oil
0.5-1 parts, glycerine 1-2 parts, EGDS 0.8-1.2 parts, disodium ethylene diamine tetraacetate 0.05-0.1 parts, the fleece-flower root
Extract 2-4 parts, Semen Sesami Nigrum extract 3-5 parts, Rhizoma Chuanxiong extract 1-3 parts, glossy privet fruit extract 2-4 parts, prepared rehmannia root extract
1-3 parts, Cacumen Platycladi extract 2-4 parts, Fructus Gleditsia extract 1-3 parts, salt 1-2 parts, essence 0.1-0.5 parts, Kathon CG 0.05-0.1
Part.
2. according to the nourishing reparation described in claim 1, black hair anticreep camellia oleifera fruit shampoo, it is characterised in that：Described alkane
Base ammonium sulfate is ammonium lauryl sulfate.
3. according to the nourishing reparation described in claim 1, black hair anticreep camellia oleifera fruit shampoo, it is characterised in that：It is wherein described
APG be APG0810.
4. according to the nourishing reparation described in claim 1, black hair anticreep camellia oleifera fruit shampoo, it is characterised in that：
Described camellia oleifera fruit emulsion preparation technology is：
（1）Selection：Selection just harvesting, fresh full camellia oleifera fruit machinery peel off, and remove shell, cleaning obtains fresh tea seed；
（2）Crush：By step（1）Gained tea seed puts into pulverizer, obtains tea seed particle；
（3）Split-phase：By step（2）Gained tea seed particle puts into juice extractor, and extruding obtains solid fiber powder and serum；
（4）Purification：By step（3）Gained serum is transported in retort, and pH value is adjusted to 2.5-4, adds acid protease, water
Bath is heated to 50-60 DEG C, after 20-30min, adds bleaching agent activated carbon and atlapulgite, 20 DEG C -40 DEG C of temperature, mixing time
For 20-30 minutes, mixing speed is 20-60 revs/min, addition serum weight 1-6% super-cell, passes through blade mistake
Filter filters, and obtains camellia oleifera fruit emulsion；
It is according to claim 4 to nourish reparation, black hair anticreep camellia oleifera fruit shampoo, it is characterised in that step（4）Described in
Acid protease and the weight ratio of serum be（0.1-4）：1000.
5. according to claim 4 nourish reparation, black hair anticreep camellia oleifera fruit shampoo, it is characterised in that step（4）Middle institute
The acid protease stated is that the excellent Aspergillus usamii of seed selection is made through depth fermentation.
6. according to the nourishing reparation described in claim 4, black hair anticreep camellia oleifera fruit shampoo, it is characterised in that step（4）In
Described decolorising agent is activated carbon and/or carclazyte, and the weight ratio of decolorising agent and serum is（2-5）：100, adsorption specific surface area
1000 -1500m2/g。
7. according to claim 1 nourishing repair, the preparation method of black hair anticreep camellia oleifera fruit shampoo, its preparation technology is：
（1）It is prewired：Fresh oil tea emulsion is heated to 50-80 DEG C, is proportionally added into sodium lauroyl glutamate 10-15 parts, cocounut oil
Amido propyl betaine 5-10 parts, ammonium lauryl sulfate 5-8 parts, APG, guar hydroxypropyltrimonium ammonium chloride, third
Acrylamide hydroxypropyltrimonium chloride/acrylamide copolymer, PPG-3 Octyl Ethers, water-soluble jojoba oil, glycerine, ethylene glycol
Double stearates, disodium ethylene diamine tetraacetate, heating stirring, mixing time are 20-30 minutes, and mixing speed is 20-60 revs/min
Clock, obtain fusions；
（2）Emulsification：In step（1）In fusions, add radix-polygoni multiflori extract, Semen Sesami Nigrum extract, Rhizoma Chuanxiong extract, female in proportion
Loyal seed extract, prepared rehmannia root extract, Cacumen Platycladi extract, Fructus Gleditsia extract, ionized water, stirring, mixing time are 20-30 points
Clock, mixing speed are 50-80 revs/min, obtain primary emulsifying thing；
（3）Shaping：In step（2）The primary emulsifying thing of gained squeezes into homogenizer, perfuming essence, Kathon CG, salt, homogeneous 10-30 minutes,
Obtain nourishing reparation, black hair anticreep camellia oleifera fruit shampoo.
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| CN108531301A (en) * | 2018-06-08 | 2018-09-14 | 海南侯臣生物科技有限公司 | A kind of natural neutral vegetables and fruits cleaning agent and preparation method thereof |
| CN111632016A (en) * | 2020-07-15 | 2020-09-08 | 云南柏莎健康产业有限公司 | Rose-fragrance-type bioactive hair-washing and hair-protecting antibacterial liquid |
| CN111956587A (en) * | 2020-09-16 | 2020-11-20 | 陈媛婷 | Black-hair and bright-hair shampoo and preparation method thereof |
| CN112516043A (en) * | 2020-12-11 | 2021-03-19 | 贵州理工学院 | A Chinese medicinal shampoo with effects of blackening hair, promoting hair growth, relieving itching and removing dandruff |
| CN112587434A (en) * | 2021-01-05 | 2021-04-02 | 石远琳 | Hair blackening agent, preparation method of hair blackening agent and washing and caring liquid |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104188869A (en) * | 2014-09-14 | 2014-12-10 | 吴世阔 | Liquid shampoo and preparation method thereof |
| CN104473823A (en) * | 2014-12-03 | 2015-04-01 | 刘三猫 | Traditional Chinese medicine healthcare hair shampoo |
| CN103550072B (en) * | 2013-11-13 | 2016-03-16 | 长沙昊瑞生物科技有限公司 | A kind of Application way of aqueous extraction Oleum Camelliae technique waste water and shampoo prescription |
| CN106309175A (en) * | 2015-06-19 | 2017-01-11 | 焦爱军 | Traditional Chinese medicine shampoo for stopping alopecia and regenerating hair as well as preparation method thereof |
| CN106667837A (en) * | 2016-12-29 | 2017-05-17 | 长沙昊瑞生物科技有限公司 | Camellia oleifera component based body lotion and preparation method thereof |
-
2017
- 2017-10-18 CN CN201710972965.0A patent/CN107550795A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103550072B (en) * | 2013-11-13 | 2016-03-16 | 长沙昊瑞生物科技有限公司 | A kind of Application way of aqueous extraction Oleum Camelliae technique waste water and shampoo prescription |
| CN104188869A (en) * | 2014-09-14 | 2014-12-10 | 吴世阔 | Liquid shampoo and preparation method thereof |
| CN104473823A (en) * | 2014-12-03 | 2015-04-01 | 刘三猫 | Traditional Chinese medicine healthcare hair shampoo |
| CN106309175A (en) * | 2015-06-19 | 2017-01-11 | 焦爱军 | Traditional Chinese medicine shampoo for stopping alopecia and regenerating hair as well as preparation method thereof |
| CN106667837A (en) * | 2016-12-29 | 2017-05-17 | 长沙昊瑞生物科技有限公司 | Camellia oleifera component based body lotion and preparation method thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108042438A (en) * | 2018-02-08 | 2018-05-18 | 陕西莹润生物医药科技有限公司 | Anticreep shampoo for ladies only and preparation method thereof |
| CN108531301A (en) * | 2018-06-08 | 2018-09-14 | 海南侯臣生物科技有限公司 | A kind of natural neutral vegetables and fruits cleaning agent and preparation method thereof |
| CN111632016A (en) * | 2020-07-15 | 2020-09-08 | 云南柏莎健康产业有限公司 | Rose-fragrance-type bioactive hair-washing and hair-protecting antibacterial liquid |
| CN111956587A (en) * | 2020-09-16 | 2020-11-20 | 陈媛婷 | Black-hair and bright-hair shampoo and preparation method thereof |
| CN112516043A (en) * | 2020-12-11 | 2021-03-19 | 贵州理工学院 | A Chinese medicinal shampoo with effects of blackening hair, promoting hair growth, relieving itching and removing dandruff |
| CN112587434A (en) * | 2021-01-05 | 2021-04-02 | 石远琳 | Hair blackening agent, preparation method of hair blackening agent and washing and caring liquid |
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Application publication date: 20180109 |