CN107550796B - Desensitized itching-relieving, dandruff-removing and hair-loss-preventing tea seed shampoo and preparation method thereof - Google Patents
Desensitized itching-relieving, dandruff-removing and hair-loss-preventing tea seed shampoo and preparation method thereof Download PDFInfo
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Abstract
A desensitized itching-relieving, dandruff-removing and hair-loss-preventing tea seed shampoo is prepared by uniformly mixing 30-50 parts of tea seed extract, 10-30 parts of traditional Chinese medicine extract, 10-15 parts of ethoxylated alkyl sodium sulfate, 1-2 parts of coconut oil fatty acid diethanolamide, 3-5 parts of cocamidopropyl betaine, 3-6 parts of alkyl glycoside, 0.5-1 part of camellia oil, 100.5-1 parts of polyquaternium, 12-18 parts of deionized water, 1-2 parts of salt, 0.1-0.5 part of essence and 0.1-0.3 part of preservative in parts by mass; the tea seed shampoo has effects of completely desensitizing tea seed extractive solution, removing dandruff and relieving itching after matching with natural Chinese herbal medicine, making hair black and bright due to interaction of tea seed juice and tea oil, and promoting hair growth and preventing alopecia.
Description
Technical Field
The invention relates to a shampoo, in particular to a desensitization-treated tea seed shampoo for relieving itching, removing dandruff and preventing alopecia.
Background
In cosmetics, a shampoo product is used as the most common one, which always occupies a huge share of the cosmetic market, the shampoo product also forms various series according to the requirements of consumer groups, in recent years, products adopting natural active agents and plant source raw materials are more and more on the market, consumers also prefer to purchase the products, the currently known natural active ingredients comprise tea seed powder, Chinese honeylocust fruit and soapberry, and the tea seed powder is used as a natural active agent but has allergen, so that skin itch and eruption of the allergic person are caused, the tea seed powder product cannot use the tea seed powder raw material in a large amount, the problem of the allergen of the tea seed powder is solved, and the tea seed powder product can be better introduced into the market.
Disclosure of Invention
The invention aims to solve the problem of allergy of the existing tea seed extracting solution and provide the tea seed shampoo with the effects of relieving itching, removing dandruff and preventing alopecia after desensitization.
The invention also aims to provide a preparation method of the desensitized itching-relieving, dandruff-removing and hair loss-preventing tea seed shampoo.
The technical scheme of the invention is as follows: a desensitized itching-relieving, dandruff-removing and hair-loss-preventing tea seed shampoo is prepared from, by mass, 30-50 parts of a tea seed extracting solution, 10-30 parts of a traditional Chinese medicine extracting solution, 10-15 parts of ethoxylated alkyl sodium sulfate, 1-2 parts of coconut oil fatty acid diethanolamide, 3-5 parts of cocamidopropyl betaine, 3-6 parts of alkyl glycoside, 0.5-1 part of camellia oil, 100.5-1 parts of polyquaternium, 12-18 parts of deionized water, 1-2 parts of salt, 0.1-0.5 part of essence and 0.1-0.3 part of a preservative.
Preferably, the camellia oil is special-grade virgin camellia oil rich in vitamin E, squalene, camelliaside and other active substances.
The alkyl glycoside is preferably APG 0810.
The antiseptic is preferably rhizoma Ligustici Chuanxiong extract.
The traditional Chinese medicine extracting solution is prepared by heating 2-4 parts of radix sophorae flavescentis powder, 2-4 parts of fructus cnidii, 2-3 parts of fructus kochiae, 1-2 parts of flos caryophyllata and 90 parts of deionized water to 80 ℃, continuously stirring for 2 hours, and filtering through 200-mesh filter cloth.
The tea seed extracting solution process comprises the following specific steps:
(1) squeezing: squeezing camellia seeds to obtain camellia seed residues;
(2) leaching: leaching camellia seed residue obtained in the step (1) by using an n-hexane solvent to obtain deoiled camellia seed residue;
(3) crushing: crushing the camellia seed dregs without oil prepared in the step (2), and sieving the crushed camellia seed dregs through a 30-100-mesh sieve to obtain camellia seed powder;
(4) hot extraction: weighing the tea seed powder prepared in the step (3), mixing with deionized water, heating, stirring, cooling, and filtering through a filter cloth of 150 meshes and 200 meshes to obtain a filtrate 1;
(5) enzymolysis: adjusting the pH value of the filtrate 1 obtained in the step (4) to 2.5-4, adding acid protease, heating in a water bath to 50-60 ℃, adding a decolorizing agent, heating to 80-100 ℃, continuously stirring, cooling and filtering to obtain a filtrate 2;
(6) refining: and (3) adding filter aid diatomite into the filtrate 2 obtained in the step (5), adjusting the pH value of the tea seed extracting solution to 5-6, and filtering to obtain clear camellia seed extracting solution.
In the step (4), the mixing ratio of the camellia seed powder to the deionized water is 1 (3-10), the camellia seed powder is heated to 60-100 ℃, the stirring speed is 20-60 r/min, and the stirring time is 40-60 min.
Preferably, the weight ratio of the acidic protease in the step (5) to the filtrate 1 is (0.1-4): 1000, parts by weight; the acid protease in the step (5) is prepared by breeding excellent aspergillus usamii through deep fermentation.
The weight ratio of the decoloring agent to the filtrate 1 in the step (5) is (1-2): 100, respectively; the decolorizing agent is active carbon and activated clay, and has an adsorption specific surface area of 1000m2/g-1500m2The/g or the adsorption capacity reaches 80-100%, and the weight ratio of the activated carbon is as follows: activated clay = 1: (3-10).
And (4) adding the diatomite in the step (6) in an amount which is 1-6% of the weight of the filtrate 2, and filtering by using a leaf filter to obtain a clear camellia seed extracting solution.
The preparation method of the desensitized itching-relieving, dandruff-removing and alopecia-preventing tea seed shampoo sequentially comprises the following steps:
(1) adding Chinese herbal medicine extract, ethoxylated alkyl sodium sulfate, coconut oil fatty acid diethanolamide into the tea seed extract, and heating for dissolving;
(2) dissolving polyquaternium-10 in 1/2-3/4 of deionized water which is totally required, heating, fully stirring, adding into the liquid dissolved in the step (1), and fully stirring for dissolving;
(3) dissolving cocamidopropyl betaine in the rest deionized water, adding into the solution dissolved in step (2) together with alkyl glycoside, stirring, cooling, adding camellia oil, essence, antiseptic, and salt, and emulsifying with an emulsifying machine at 3000 rpm under high speed to obtain shampoo.
The invention has the beneficial effects that:
the shampoo disclosed by the invention can remove dandruff, relieve itching, repair hair and prevent alopecia.
The main raw materials used in the present invention are described as follows:
camellia seeds: the camellia oleifera is a fruit of a camellia oleifera tree, is a main woody oil tree in China, is known as an "oriental tree", belongs to camellia of Theaceae, belongs to a evergreen small tree, and is a woody plant oil resource special in China. The height of the tree is 3-6 m, the diameter at breast height can reach 24-30 cm, and the bark is smooth and grey brown; the camellia oleifera tree grows with single leaf and flower is in amphoteric white, and fruits can be ripe within 10 months of the next year after blooming for 10 months, so that the camellia oleifera tree has rare flower and fruit homologous phenomenon; the fruit is capsule, mostly elliptical and has fine hair; the seeds are mostly yellow brown, glossy and triangular. The tea-oil tree grows in a deep mountain, absorbs natural nutrients, is evergreen and has long life, and the tree age can reach more than 200 years.
Radix sophorae flavescentis powder: is prepared from radix Sophorae Flavescentis by processing and pulverizing, and can be used for treating eczema and skin pruritus.
Fructus cnidii: is dried mature fruit of cnidium monnieri (L.) DC of Umbelliferae, and can be used for treating infantile tinea, malignant boil, skin eczema, allergic dermatitis, and head sore.
The preparation method comprises the following steps of (1) preparing broom cypress fruit: is dry mature fruit of Kochia scoparia belonging to Chenopodiaceae, and has effects of clearing heat, promoting diuresis, dispelling pathogenic wind and relieving itching.
Flos caryophyllata: flos caryophylli is a common traditional Chinese medicine, is one of the traditional imported south medicines in China, and is listed in the treatise on the property of the medicine, and the modern research shows that the flos caryophylli contains volatile oil which mainly contains components such as syringoleic acid, acetyl syringoleic acid, caryophyllene, methyl n-pentanone, methyl n-heptanone, vanillin and the like, has the effects of inhibiting bacteria and expelling worms, and is used as an aromatic, spasmolytic and wind-dispelling agent.
Sodium ethoxylated alkyl sulfate-a colorless, white or pale yellow viscous liquid, alkaline anionic surfactant with a typical soap odor. Is easy to dissolve in water, has excellent decontamination, emulsification and foaming performances and hard water resistance, and has mild washing property without damaging the skin. Widely applied to washing cosmetics such as shampoo, bath lotion, tableware detergent, compound soap and the like; it can be used as wetting agent and cleaning agent in textile industry.
The coconut oil fatty acid diethanolamide belongs to a nonionic surfactant, has no cloud point, is a yellowish to amber viscous liquid, is easy to dissolve in water, has good functions of foaming, foam stabilization, penetration decontamination, hard water resistance and the like, has a particularly obvious thickening effect when being compatible with an anionic surfactant when the anionic surfactant is acidic, and can be compatible with various surfactants.
Cocamidopropyl betaine is an amphoteric ion surfactant, has excellent stability under acidic and alkaline conditions, respectively presents positive and negative ion properties, is often used together with an anionic surfactant, a cationic surfactant and a nonionic surfactant, has good compatibility, small irritation, is easy to dissolve in water, is stable to acid and alkali, has more foams and strong detergency, has excellent thickening property, flexibility, bactericidal property, antistatic property and hard water resistance, and can remarkably improve the softness, conditioning property and low-temperature stability of washing products.
Alkyl glycoside: synthesized by renewable resources, namely natural fatty alcohol and glucose, is a novel nonionic surfactant with comprehensive performance, has the characteristics of common nonionic and anionic surfactants, has high surface activity, good ecological safety and intermiscibility, and is a preferred 'green' functional surfactant internationally recognized.
Camellia oil: the camellia seed kernel is obtained by cleaning, air drying (at a temperature lower than 100 ℃), shelling, selecting seeds, sterilizing, and squeezing at 20-50 ℃, and has abundant active substances, usually containing 200mg/Kg of vitamin E, 30mg/Kg of sterol, and 100mg/Kg of squalene.
Polyquaternium-10: the cationic cellulose polymer with excellent water solubility and adsorption capacity is compatible with anionic, cationic, nonionic and zwitterionic surfactants, has low irritation, and the unique cationic performance can repair damaged hair protein matrix, keep hair moist, and endow hair with excellent combing performance and bright and smooth feeling.
Deionized water: means pure water from which impurities in the form of ions have been removed, and the definition of "deionization" specified by the international organization for standardization ISO/TC 147 is: the deionized water is prepared by adopting a Reverse Osmosis (RO) method, and anion and cation in the water are removed by using ion exchange resin.
Salt: the main component is NaCl, which can increase the viscosity of the prepared liquid.
Essence: regulating the smell of the finished product to make the finished product pleasant and comfortable.
And (3) ligusticum wallichii extract: the rhizoma Ligustici Chuanxiong extract has inhibitory effect on various gram-negative intestinal bacteria, such as Escherichia coli, Bacillus dysenteriae, Bacillus proteus, Pseudomonas aeruginosa, Salmonella typhi, Salmonella paratyphi and Vibrio cholerae, and has certain inhibitory effect on pathogenic dermatophyte and viruses.
Detailed Description
The alkyl glycoside used in the examples was APG 0810.
The tea seed extracting solution used in the embodiment is prepared by the following process steps:
(1) squeezing: squeezing camellia seeds to obtain camellia seed residues;
(2) leaching: leaching camellia seed residue obtained in the step (1) by using an n-hexane solvent to obtain deoiled camellia seed residue;
(3) crushing: crushing the camellia seed dregs without oil prepared in the step (2), and sieving the crushed camellia seed dregs through a 50-mesh sieve to obtain camellia seed powder;
(4) hot extraction: weighing the camellia seed powder prepared in the step (3), mixing the camellia seed powder with deionized water according to the mixing ratio of 1:4, heating, stirring, cooling, and filtering through a filter cloth of 200 meshes to obtain a filtrate 1;
(5) enzymolysis: adjusting the pH value of the filtrate 1 obtained in the step (4) to 3, adding acid protease (prepared by deep fermentation of the acid protease which is used for breeding excellent aspergillus usamii and has a weight ratio of 0.5: 1000 to the filtrate 1), heating in water bath to 55 ℃, adding decolorant activated carbon and activated clay, wherein the average adsorption specific surface areas are 1200m respectively2(iv)/g and 1300m2The weight ratio of activated carbon is as follows: activated clay = 1:4, the weight ratio of the decoloring agent to the filtrate 1 is 2: 100, respectively; heating to 80 ℃, continuously stirring, cooling and filtering to obtain filtrate 2;
(6) refining: and (3) adding 3% by weight of filter aid diatomite into the filtrate 2 obtained in the step (5), adjusting the pH value of the tea seed extracting solution to 5.5, and filtering to obtain clear camellia seed extracting solution.
Performing spot test on the tea seed extract, wherein the result of the spot test is no anaphylactic reaction; the test method is as follows:
the method comprises the following steps: cutting four layers of gauze into 8 circles with the diameter of 1cm by using a pair of scissors, respectively sucking 25uL of tea seed extracting solution by using a liquid-transferring gun, dripping the tea seed extracting solution on the circular gauze, and performing blank comparison by using deionized water;
step two: clamping gauze with forceps, placing on the anteflexion arm of the subject (allergic to tea seed extractive solution), fixing with adhesive tape, and timing;
step three: after 48h the tape was removed and the gauze covered skin was immediately observed for reaction.
The traditional Chinese medicine extracting solution is prepared by heating 3 parts of radix sophorae flavescentis powder, 3 parts of fructus cnidii, 2.5 parts of fructus kochiae, 1.5 parts of flos caryophyllata and 90 parts of deionized water to 80 ℃, continuously stirring for 2 hours, and filtering through 200-mesh filter cloth.
Example 1
Taking 300 g of the tea seed extracting solution, adding 300 g of Chinese herbal medicine extracting solution, 120 g of ethoxylated alkyl sodium sulfate and 15 g of coconut oil fatty acid diethanolamide, heating to dissolve, dissolving 3 g of polyquaternium-10 in 110 g of deionized water, properly heating, adding into the dissolved liquid after fully stirring, fully stirring to dissolve, dissolving 40 g of cocamidopropyl betaine in 40.9 g of deionized water, adding into 50 g of alkyl glycoside together, uniformly stirring, cooling, adding 5 g of camellia oil, 1 g of essence, 1 g of ligusticum wallichii extract and 15 g of table salt, and stirring and emulsifying at a high speed by using an emulsifying machine at 3000 rpm to obtain shampoo.
Examples 2 to 7
The shampoo of examples 1-5 and comparative examples 1-2 was prepared under the same conditions as in example 1 except that the reaction materials and the blending ratio were slightly different, as shown in Table 1.
TABLE 1 preparation of shampoo for examples 1-5 and comparative examples 1-2
Comparative example 3
Comparative example 3 the cnidium monnieri was removed from example 1, and the amount of cloves was 4.5 parts, which was otherwise the same as in example 1.
Comparative example 4
Comparative example 4 the same procedure as in example 1 was repeated except that the clove was removed from the composition of example 1 and the amount of cnidium fruit was 4.5 parts.
Comparative example 5
Comparative example 5 the same procedure as in example 1 was repeated except that Kochia scoparia was removed from example 1 and 4 parts of Syzygium aromaticum was used.
Comparative example 6
The comparative example 6 is different from example 1 only in the preparation method of the tea seed extract.
The tea seed extract used in comparative example 6 was prepared by the following process steps:
(1) squeezing: squeezing camellia seeds to obtain camellia seed residues;
(2) leaching: leaching camellia seed residue obtained in the step (1) by using an n-hexane solvent to obtain deoiled camellia seed residue;
(3) crushing: crushing the camellia seed dregs without oil prepared in the step (2), and sieving the crushed camellia seed dregs through a 50-mesh sieve to obtain camellia seed powder;
(4) hot extraction: weighing the camellia seed powder prepared in the step (3), mixing the camellia seed powder with deionized water according to the mixing ratio of 1:4, heating, stirring, cooling, and filtering through a filter cloth of 200 meshes to obtain a filtrate;
(5) refining: and (4) adding 3% by weight of filter aid diatomite into the filtrate obtained in the step (4), filtering, and adjusting the pH value of the tea seed extracting solution to 5.5 to obtain clear camellia seed extracting solution.
The shampoos obtained in examples 1 to 5 and comparative examples 1 to 6 were tested for combing property, antipruritic and antidandruff effect, lather, rinsing property, repairing property, and anti-hair loss effect.
TABLE 2 results of functional index test of hair shampoo obtained in examples 1 to 5 and comparative examples 1 to 6
The functional index and physicochemical index of the shampoo obtained in examples 1 to 5 and comparative examples 1 to 6 were measured by the following methods:
(1) the method for testing the foaming, rinsing, itching relieving and scurf removing effects, carding and repairing performances comprises the following steps of collecting questionnaires after trial investigation, and obtaining results after statistical analysis:
6 testers, 2 oily hair patients, 2 neutral hair patients and 2 dry hair patients are respectively selected from the desensitized itching relieving, scurf removing and hair loss preventing tea seed shampoos obtained in examples 1-5 and comparative examples 1-6 and the tea seed shampoos sold in the market, and after 3 times of continuous trial, the testers fill a trial feedback table shown in a table 3.
TABLE 3 feedback chart for trial use of tea seed shampoo
After the trial is finished, collecting a trial questionnaire, counting and calculating the average score as the following table 4:
TABLE 4 table of average values of the test results of the tea seed shampoo for examples 1 to 5 and comparative examples 1 to 6
From table 4, it can be seen that the embodiment of the invention has the best effect, the ratio of the Chinese herbal medicine extract is closely related to the effect of relieving itching and removing dandruff, and some of the commercially available tea seed shampoo has no desensitization treatment, so that the scalp itching and dandruff generation of some testers occur, but no severe allergy phenomenon exists, and the repairing effect is not good.
The desensitized antipruritic, anti-dandruff and anti-hair loss tea seed shampoo of examples 1-5 and comparative examples 1-6 has the following anti-hair loss effect test method:
8 persons having alopecia were selected from the desensitized antipruritic, anti-dandruff and anti-alopecia tea seed shampoos of examples 1 to 5 and comparative examples 1 to 6, and the commercial tea seed shampoo (as a control), and the hair loss was counted in the second day after each trial for 10 consecutive trials, and the number of hairs dropped was counted in the second day after each trial, and the statistics are shown in Table 5.
TABLE 5 results of the tea seed shampoo anticreep Effect test of examples 1 to 5 and comparative examples 1 to 6
From table 5, it can be seen that the addition amount of the tea seed extract and the addition amount of the camellia oil play a decisive role in the anti-hair loss effect, and the anti-hair loss effect of the commercially available tea seed shampoo is quite poor, mainly because the addition amount of the tea seed extract is reduced due to the failure to solve the allergy cause, so that the effect is not good.
In addition, the desensitized antipruritic, anti-dandruff and anti-alopecia tea seed shampoo obtained in examples 1 to 5 was tested for microbiological indicators and health indicators "technical safety standards for cosmetics" (2015 edition) to obtain the following test results shown in table 6:
TABLE 6 EXAMPLES 1-5 microbial hygiene indicators for desensitized antipruritic, anti-dandruff and anti-hair loss tea seed shampoos
The desensitized itching-relieving, dandruff-removing and hair-loss-preventing tea seed shampoo toxicology test: skin irritation test (multiple skin irritation tests).
The purpose of the test is as follows: the skin irritation reaction generated after the rabbit intact skin is contacted with a test object (the tea seed shampoo of the embodiment of the invention) for a plurality of times for a long time is observed, and the safety basis is provided for the desensitized itching-relieving, scurf-removing and hair loss-preventing tea seed shampoo of the embodiment of the invention.
The inspection basis is as follows: technical standards for cosmetic safety 2015 edition; the test method comprises the following steps: selecting 8 white New Zealand rabbits, and randomly dividing the white New Zealand rabbits into 2 groups, wherein each group comprises 4 rabbits; group A is experimental group, group B is deionized water control group; shearing off hairs on two sides of a spinal column of the back of a rabbit 24 hours before a test, wherein the skin surface is not damaged in shearing, the hair removing range is 3cm multiplied by 3cm, the smearing area is 2.5cm multiplied by 2.5cm, 0.5ml of a tested object is directly smeared on one side of the spinal column of the back, 0.5ml of deionized water of a control group is smeared on the other side of the spinal column of the back, and the tested object is smeared for 1 time every day and is smeared for 14 days continuously; from the next day on, the hair was cut at each application and the residual test substance was removed with deionized water. The results were observed after one hour and scored according to the skin irritation test table of the technical specifications for cosmetic safety (2015 edition), with the control and test areas treated the same.
And (4) evaluating the results: the average integral of each rabbit per day is calculated according to the following formula, the skin irritation intensity of the rabbits is judged according to a standard table, and other toxic effects except irritation are observed.
And (3) test results: after the test object is given the tea seed shampoo of the embodiment of the invention in a plurality of observation periods of skin irritation tests, no erythema and edema are observed in the rabbits. The general poisoning and death conditions are not seen, the weight of the animals is increased, and the animals have no influence on respiration, circulation, central nervous system, limb activities and the like.
And (4) test conclusion: the desensitized itching-relieving, dandruff-removing and hair-loss-preventing tea seed shampoo of each embodiment of the invention has no irritation to the intact skin of white New Zealand rabbits.
Claims (3)
1. A desensitized itching-relieving, dandruff-removing and hair-loss-preventing tea seed shampoo is prepared from, by mass, 30-50 parts of a tea seed extracting solution, 10-30 parts of a traditional Chinese medicine extracting solution, 10-15 parts of ethoxylated alkyl sodium sulfate, 1-2 parts of coconut oil fatty acid diethanolamide, 3-5 parts of cocamidopropyl betaine, 3-6 parts of alkyl glycoside, 0.5-1 part of camellia oil, 100.5-1 parts of polyquaternium, 12-18 parts of deionized water, 1-2 parts of salt, 0.1-0.5 part of essence and 0.1-0.3 part of a preservative; the traditional Chinese medicine extracting solution is prepared by heating 3 parts of radix sophorae flavescentis powder, 3 parts of fructus cnidii, 2.5 parts of fructus kochiae, 1.5 parts of flos caryophylli and 90 parts of deionized water to 80 ℃, continuously stirring for 2 hours, and filtering through 200-mesh filter cloth;
the tea seed extracting solution process comprises the following specific steps:
(1) squeezing: squeezing camellia seeds to obtain camellia seed residues;
(2) leaching: leaching camellia seed residue obtained in the step (1) by using an n-hexane solvent to obtain deoiled camellia seed residue;
(3) crushing: crushing the camellia seed dregs without oil prepared in the step (2), and sieving the crushed camellia seed dregs through a 50-mesh sieve to obtain camellia seed powder;
(4) hot extraction: weighing the camellia seed powder prepared in the step (3), mixing the camellia seed powder with deionized water according to the mixing ratio of 1:4, heating, stirring, cooling, and filtering through a filter cloth of 200 meshes to obtain a filtrate 1;
(5) enzymolysis: adjusting the pH value of the filtrate 1 obtained in the step (4) to 3, adding acid protease, wherein the acid protease is prepared by deep fermentation of the bred excellent aspergillus usamii, and the weight ratio of the acid protease to the filtrate 1 is 0.5: 1000, heating to 55 ℃ in water bath, adding decolorizing agents of active carbon and activated clay, wherein the average adsorption specific surface areas are 1200m respectively2(iv)/g and 1300m2The weight ratio of activated carbon is as follows: activity deviceCarclazyte = 1:4, the weight ratio of the decoloring agent to the filtrate 1 is 2: 100, respectively; heating to 80 ℃, continuously stirring, cooling and filtering to obtain filtrate 2;
(6) refining: adding 3% by weight of filter aid diatomite into the filtrate 2 obtained in the step (5), adjusting the pH value of the tea seed extracting solution to 5.5, and filtering to obtain a camellia seed extracting solution;
the alkyl glycoside is APG 0810; the antiseptic is rhizoma Ligustici Chuanxiong extract.
2. The desensitized antipruritic, anti-dandruff and anti-alopecia tea seed shampoo according to claim 1, wherein: the camellia oil is special-grade virgin camellia oil.
3. The method for preparing the desensitized itching-relieving, dandruff-removing and alopecia-preventing tea seed shampoo according to claim 1, wherein the desensitized itching-relieving, dandruff-removing and alopecia-preventing tea seed shampoo comprises the following steps: the method sequentially comprises the following steps:
(1) adding Chinese herbal medicine extract, ethoxylated alkyl sodium sulfate, coconut oil fatty acid diethanolamide into the tea seed extract, and heating for dissolving;
(2) dissolving polyquaternium-10 in deionized water, wherein the amount of the deionized water is 1/2-3/4 of the total required deionized water, heating, fully stirring, adding into the liquid dissolved in the step (1), and fully stirring for dissolving;
(3) dissolving cocamidopropyl betaine in the rest deionized water, adding into the solution dissolved in step (2) together with alkyl glycoside, stirring, cooling, adding camellia oil, essence, antiseptic, and salt, and emulsifying with an emulsifying machine at 3000 rpm under high speed to obtain shampoo.
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| CN104490644A (en) * | 2014-11-22 | 2015-04-08 | 青岛海芬海洋生物科技有限公司 | Plant composition for hair care |
| CN104975061A (en) * | 2015-08-11 | 2015-10-14 | 重庆都好生物科技有限公司 | Preparation method of camellia seeds |
| CN105213292A (en) * | 2015-09-25 | 2016-01-06 | 黄中庆 | Herbal essences tea bran hair cream |
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| CN104490644A (en) * | 2014-11-22 | 2015-04-08 | 青岛海芬海洋生物科技有限公司 | Plant composition for hair care |
| CN104975061A (en) * | 2015-08-11 | 2015-10-14 | 重庆都好生物科技有限公司 | Preparation method of camellia seeds |
| CN105213292A (en) * | 2015-09-25 | 2016-01-06 | 黄中庆 | Herbal essences tea bran hair cream |
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Effective date of registration: 20200515 Address after: 421311 Hengnan County, Hunan City, Hengyang Province, gathered in the Industrial Park Applicant after: HUNAN GREAT SANXIANG CAMELLIA OIL RESOURCES Co.,Ltd. Address before: 410205 16 layer of 588 core city science park, Yuelu West Avenue, Changsha high development zone, Hunan Province Applicant before: HUNAN DASAN XIANG TEA OIL E-COMMERCE Co.,Ltd. |
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