CN108096117A

CN108096117A - A kind of composition and its preparation method and application

Info

Publication number: CN108096117A
Application number: CN201810094482.XA
Authority: CN
Inventors: 周金平
Original assignee: Jie Bao Chemical (xiangxi) Co Ltd
Current assignee: Jie Bao Chemical (xiangxi) Co Ltd
Priority date: 2018-01-31
Filing date: 2018-01-31
Publication date: 2018-06-01
Anticipated expiration: 2038-01-31
Also published as: CN108096117B

Abstract

The present invention provides a kind of composition and its preparation method and application, the composition includes following component in parts by weight：200 300 parts of 15 30 parts of Rosemary Oil, 15 parts of Artemisinin and tea bran extract；Inventive formulation is reasonable, each component is synergistic, during scalp care element is prepared, is collocated with each other with a variety of scalp conditioners, further collaboration promotes nursing effect to scalp, not only have effects that clean hair, it is safe and non-stimulating, moreover it is possible to effective pre-Anti-hair loss, promote hair regeneration, black hair brighten the hair, it is crude to improve trichoxerosis, has broad application prospects and market value.

Description

A kind of composition and its preparation method and application

Technical field

Protector for collar domain is washed the invention belongs to daily, is related to a kind of composition and preparation method and application, and in particular to is a kind of Composition containing Artemisinin, Rosemary Oil and tea bran extract and its preparation method and application.

Background technology

Recently, due to environmental pollution, modern life pressure is big, causes a variety of heads using unsafe hair care product Leather point question is inscribed.PM2.5 in air carries various bacteriums, and cuticula hyperplasia is caused to bring bacterium infection scalp irritation simultaneously, The problems such as head is itched, dandruff increase so as to alopecia；Life stress causes people's endocrine imbalance, hair oil, and the alopecia hair, white hair etc. that breaks is asked Topic is following；Hair scale piece is easily damaged using the high shield product of washing of chemical composition, hair moisture-keeping functions are influenced, so as to increasingly Withered crude, natural on-off cycles of hair growth is slow, and hair loss increases.It washes in shield product and chemical synthesis substance is often used to increase cleaning as raw material Function is fuel-displaced to alleviate scalp and hair, dandruff problem, but its irritation is big, and security is low, and easily causes allergy.In recent years Come, the functionality of traditional Chinese medicine ingredients washes shield product and gradually people is subject to favor, and because its is safe, significant effect more and more should For shampoo field.

CN106038388A discloses a kind of traditional Chinese medicine shampoo and preparation method thereof, includes the component A of following parts by weight：Ginger 5-88 parts, 3-85 parts of soapberry, 3-85 parts of tea seed, 3-85 parts of Chinese honey locust, 3-65 parts of prepared fleece flower root, 3-65 parts of wild chrysanthemum, mulberries 3-24 parts, 3-24 parts of cacumen biotae, 3-24 parts of mulberry leaf, 3-23 parts of eclipta, 3-23 parts of Rhizoma Chuanxiong, 3-23 parts of Radix Salviae Miltiorrhizae, 3-23 parts of teasel root, 3-23 parts of sweet wormwood, 3-23 parts of pine needle, Poria cocos, 3-23 parts, 3-21 parts of sealwort, 3-21 parts of Radix Angelicae Sinensis, 3-21 parts of frutus cnidii, Chinese cassia tree 3-18 Part, 3-18 parts of leek seed, 3-15 parts of ginseng, 3-15 parts of Chinese anise, 3-15 parts of cloves, 0.5-3 parts of peppermint oil, camellia oil 2-8 Part；The shampoo that the invention is prepared not toxic chemicals such as silicate-containing oil reach conditioning scalp hair follicle health and dispel with hair care Consider the effect of phalacrosis prevention and hair generation black hair to be worth doing, but the shampoo is numerous and diverse into being grouped into, long preparation period, and gained shampoo Chinese medicine taste is dense Weight differs greatly with daily hair washing product fragrance.

CN105326689A discloses a kind of preparation method of Chinese medicine anti-dandruff shampoo breast, and step is：Chinese medicine mixes in proportion Afterwards, adding in reaction kettle, add 800 parts of water, temperature is heated to 70 DEG C, pressure is 2.6 times of standard atmospheric pressures in reaction kettle, Lasting stirring when heat preservation 2.5 is small, collects liquid and is concentrated into 150 parts；Add in glycerine, zinc pyrithione, hydantoins, lauryl Sodium sulfovinate, alkyl poly glucoside, vitamin E, potassium chloride, bamboo charcoal powder, nano-silica powder, wild rice stem juice, green onion juice, aloe Juice, orange juice are uniformly mixed；Citric acid is added in, it is 6.6 to adjust the mixed material pH closed in container；Then rosemary is sequentially added Extract, grape seed extract, Herba Lysimachiae foenumgraeci extract, black nightshade extract, Artemisinin, ginkgo biloba p.e, Zijin flower carry Take object, temperature 45 C, stir under atmospheric pressure environment more than 10min to get.The Chinese traditional medicine composition composition that the invention contains, except having Outside dirt-removing functions, the function of also antibacterial, antipruritic, anti-dandruff, black hair and Anti-hair loss, but the anti-dandruff shampoo breast focuses on anti-dandruff work( Effect, black hair brighten the hair repair scalp barrier function unobvious, it is necessary to which the cycle used is longer, and pH is not suitable for for a long time directly in alkalescence Scalp is contacted to use.

CN105287173A discloses a kind of natural shampoo, and component is：Component A：25-35 parts of lye, camellia oil 5- 15 parts, 8-12 parts of olive seed oil；B component：10-20 parts of lavender, 10-20 parts of rosemary, 10-20 parts of peppermint, 10-20 parts of sweet basil, Fresh wormwood 10-20 parts, 10-20 parts of honeysuckle stem, 10-20 parts of wild chrysanthemum, 10-20 parts of mulberry leaf, 10-20 parts of arbor-vitae, Ilex Latifolia Thunb 10-20 Part；Component C：20-30 parts of colored brown rice powder, 8-12 parts of black sesame powder；D components：10-20 parts of gleditsia sinensis, 10-20 parts of soapberry, what 10-20 parts of the tuber of multiflower knotweed, 10-20 parts of Radix Angelicae Sinensis, 10-20 parts of ganoderma lucidum, 10-20 parts of Radix Paeoniae Alba.The invention natural liquid shampoo is without using anyization Learn additive, natural nutrition, can effectively anti-alopecia-stopping, oil-control, inhibit white hair growth, anti-dandruff and itching-relieving effectively cleans hair nutrition Root of hair, improvement hair is thin, improves hair quality, and has wind-dispelling, dispelling cold, the work(living through promoting blood circulation, alleviating dizziness headache, refresh the mind Effect, but the shampoo complicated component, rich in a variety of greases, bactericidal effect is faint, and scalp problems effect is micro- caused by directed toward bacteria It is weak.

Therefore it provides one kind can oil-control pre-Anti-hair loss, hair tonic, black hair brighten the hair, it is withered and yellow to improve drying, and can sterilize and disappear Inflammation, saves preparation time cost, and quick Chinese medicine composition, it is daily wash protector for collar domain have great importance with it is wide Market prospects.

The content of the invention

In view of the deficiencies of the prior art and actual demand, the present invention provide a kind of composition and preparation method thereof and should With for the composition using Artemisinin, Rosemary Oil and tea bran extract as raw material, formula is reasonable, and each component collaboration increases Effect, during scalp care element is prepared, is collocated with each other with a variety of scalp conditioners, and further collaboration promotes the shield to scalp Effect is managed, not only has effects that clean hair, it is safe and non-stimulating, moreover it is possible to which that effective pre-Anti-hair loss promotes hair regeneration, and black hair is bright Hair, it is crude to improve trichoxerosis, has broad application prospects and market value.

For this purpose, the present invention uses following technical scheme：

In a first aspect, the present invention provides a kind of composition, the composition includes following component：Rosemary Oil, sweet wormwood Extract and tea bran extract.

The nature and flavor and effect of each ingredient of the present invention are as follows：

Sweet wormwood is cold in nature, bitter, pungent, Return liver, gallbladder channel, has effects that heat-clearing, relieving summer-heat, except steaming, preventing malaria.Modern medicine shows Sweet wormwood has lethal effect, anti parasitic, antitumor, refrigeration function to various bacteria, virus；Adjust body's immunity；It can Reducing heart rate inhibits myocardial contractive power, reduces coronary flow, reduces blood pressure, and have certain antiarrhythmic effect；It can still protect Liver, protection radiation, shortens the amobarbital length of one's sleep, main containing a variety of sesquiterpene lactones, flavonoids, Coumarins, volatile oil Deng containing ingredients such as qinghaosu, artemisinol, Arteannuic acid, methyl arteannuate, Quercetin, fenchone, escoparones.

Rosemary Oil is a kind of colourless to faint yellow volatile liquid, has very strong contraction, tightens loose flesh Skin can also mitigate the congested, situation of swelling；Dandruff can be improved, stimulate hair growth.Rosemary is very beneficial to respiratory system The respiratory diseases such as place, flu, bronchitis, can promote memory, make one clearheaded, have clear presentation, while rosemary The effect of sharp liver and gall, helpful toxin expelling, purification；Can also diuresis, analgesic, the puzzlements such as rheumatalgia of releiving, gout, headache.

Tea bran is dregs of the seed of Theaceae oil tea after squeezing and removing fat oil, and flavour of a drug are pungent, bitter, containing saponin, tannin, life Alkaloids, can treat traumatic injury, be a kind of function admirable containing 15% or so Tea Saponin in tea bran, and widely used Natural nonionic surface active agent is made of hydrophilic sugar and hydrophobic coordination matrix.Some researches show that it has Foaming characteristic is better than first-class perfumed soap, and is influenced from the hardness of water, has emulsification, disperses, moistening reduces the works such as the surface tension of water With, while the also pharmacological properties of antibacterial anti-inflammatory etc..Contained tea polyphenols are a kind of with anti-aging, anti-spoke in tea seed cake It penetrates, the antioxidant of energy bactericidal antiphlogistic, and stability is good, can play a role for a long time, and low molecular amino acid can stimulate hair The growth of hair, vitamin, minerals, theophylline etc. is all beneficial to hair.

The plant composition of the present invention is using tea seed and rosemary leave as main composition, Artemisinin, rosemary Essential oil and tea bran extract mutually cooperate with, and one side sweet wormwood and tea bran can play cleaning scalp, kill bacterium, anti-dandruff and itching-relieving Effect, another aspect Rosemary Oil moisten scalp, and holding head skin water and oil balance coordinates sweet wormwood and tea bran, in absorption grease, go While except dandruff, pre-Anti-hair loss promotes hair regeneration, and black hair brighten the hair, improvement trichoxerosis is crude, improves hair quality effect.

Preferably, the composition includes following component in parts by weight：15-30 parts of Rosemary Oil, Artemisinin 1-5 parts and 200-300 parts of tea bran extract.

Preferably, the parts by weight of the Rosemary Oil are 15-30 parts, for example, can be 15 parts, 16 parts, 17 parts, 18 Part, preferably 19 parts, 20 parts, 22 parts, 24 parts, 26 parts, 28 parts or 30 parts, 18-26 parts.

Preferably, the parts by weight of the Artemisinin are 1-5 parts, such as can be 1 part, 2 parts, 3 parts, 4 parts or 5 Part, it is preferably 1-3 parts.

Preferably, the parts by weight of the tea bran extract are 200-300 parts, for example, can be 200 parts, 230 parts, 250 Part, preferably 260 parts, 270 parts, 280 parts, 290 parts or 300 parts, 250-280 parts.

In the present invention, inventor has found that three components of the composition are combined according to above-mentioned parts by weight, can be with The synergistic effect of three components is further improved, each component gives full play to function, and oil-control Anti-hair loss, scalp effect of releiving are further It is promoted.

As preferred technical solution, the composition includes following component in parts by weight：20 parts of Rosemary Oil, green grass or young crops 260 parts of 2 parts of parthenium extract and tea bran extract.

Second aspect, the present invention provide a kind of hair products, and the hair products include the composition described in first aspect.

Preferably, the additive amount of the composition accounts for the mass percent of the hair products as 1-8%, such as can be 1%th, 2%, 3%, 4%, 5%, 6%, 7% or 8%, it is preferably 2-5%, composition additive amount is in the mass percent scope Interior hair care effect is notable, and have no toxic side effect generation.

Preferably, the hair products include any one in shampoo, hair conditioner, hair film, hair jelly or scalp care element Kind or at least two combination, such as can be the composition of the composition of shampoo and hair conditioner, hair conditioner and hair jelly, hair film With the composition of hair jelly, the composition of shampoo and scalp care element is preferably scalp care element.

Preferably, the hair products further include zinc pyrithione, piroctone olamine salt, dimethyl silicone polymer, In PPG-3 nutmegs alcohol ether, hydrolysis of keratin or olive oil PEG-7 esters any one or at least two combination, it is described Combination for example can be zinc pyrithione and piroctone olamine salt, zinc pyrithione, piroctone olamine salt and poly dimethyl Siloxanes, piroctone olamine salt, dimethyl silicone polymer and PPG-3 nutmeg alcohol ethers, PPG-3 nutmegs alcohol ether, hydrolysis Keratin and olive oil PEG-7 esters or zinc pyrithione, piroctone olamine salt, dimethyl silicone polymer, PPG-3 nutmegs Alcohol ether, hydrolysis of keratin and olive oil PEG-7 esters.

Preferably, the zinc pyrithione accounts for the mass percent of the hair products as 0.5-5%, such as can be 0.5%th, 0.8%, 1%, 1.2%, 1.4%, 1.6%, 1.8%, 2%, 2.5%, 3%, 3.5%, 4%, 4.5% or 5%, it is excellent Elect 1-3% as.

Preferably, the piroctone olamine salt accounts for the mass percent of the hair products as 0.1-3%, such as can It is preferably 0.3-1% to be 0.1%, 0.3%, 0.5%, 0.7%, 1%, 1.5%, 2%, 2.5% or 3%.

Preferably, the dimethyl silicone polymer accounts for the mass percents of the hair products as 0.8-5%, such as can be with It is 0.8%, 1%, 1.2%, 1.5%, 1.7%, 2%, 2.5%, 3%, 3.5%, 4%, 4.5% or 5%, is preferably 1-3%.

Preferably, the PPG-3 nutmegs alcohol ether accounts for the mass percent of the hair products as 0.1-3%, such as can It is preferably 0.3-1% to be 0.1%, 0.3%, 0.5%, 0.7%, 1%, 1.5%, 2%, 2.5% or 3%.

Preferably, the hydrolysis of keratin accounts for the mass percent of the hair products as 0.1-3%, such as can be 0.1%th, 0.3%, 0.5%, 0.7%, 1%, 1.5%, 2%, 2.5% or 3%, it is preferably 0.3-1%.

Preferably, the olive oil PEG-7 esters account for the mass percent of the hair products as 0.1-3%, such as can It is preferably 0.3-1% to be 0.1%, 0.3%, 0.5%, 0.7%, 1%, 1.5%, 2%, 2.5% or 3%.

Preferably, the hair products further include appointing in surfactant, suspending agent, softener, preservative and essence It anticipates a kind of or at least two combinations, such as can be the group of the combination of surfactant and suspending agent, suspending agent and softener It closes, the combination of the combination of softener and essence or surfactant, suspending agent, softener, preservative and essence.

Preferably, the surfactant is appointing in Plantacare 818, Cocoamidopropyl betaine or coconut oleoyl amine It anticipates a kind of or at least two combinations, such as can be the combination of Plantacare 818 and Cocoamidopropyl betaine, cocounut oil acyl Combination or Plantacare 818, the combination of Cocoamidopropyl betaine and coconut oleoyl amine of amine propyl betaine and coconut oleoyl amine.

Preferably, the suspending agent is acrylic acid (ester) analog copolymer.

Preferably, the softener is polyquaternium -7.

Preferably, the preservative is sodium benzoate.

Preferably, the surfactant accounts for the mass percent of the hair products as 15-30%, such as can be 15%th, 16%, 18%, 20%, 24%, 26%, 28% or 30%, it is preferably 18-26%.

Preferably, the suspending agent accounts for the mass percents of the hair products as 1-5%, for example, can be 1%, 2%, 3%th, 4% or 5%, it is preferably 1-3%.

Preferably, the softener accounts for the mass percents of the hair products as 0.1-2%, such as can be 0.1%, 0.3%th, 0.5%, 0.7%, 1%, 1.3%, 1.5%, 1.7% or 2%, it is preferably 0.5-1%.

Preferably, the preservative accounts for the mass percents of the hair products as 0.1-1%, such as can be 0.1%, 0.2%th, 0.4%, 0.6%, 0.8% or 1%, it is preferably 0.1-0.8%.

Preferably, the essence accounts for the mass percents of the hair products as 0.1-3%, such as can be 0.1%, 0.3%th, 0.5%, 0.7%, 0.9%, 1%, 1.3%, 1.5%, 2%, 2.3%, 2.5% or 3%, it is preferably 0.5-2%.

Preferably, the hair products include：

Surplus is deionized water.

Preferably, the hair products include：

Surplus is deionized water.

As optimal technical scheme, scalp element is prepared into, the scalp element includes following component：Combination described in first aspect Object 3%, zinc pyrithione 2%, piroctone olamine salt 0.8%, dimethyl silicone polymer 2%, PPG-3 nutmeg alcohol ethers 0.8%, hydrolysis of keratin 0.8%, olive oil PEG-7 esters 0.8%, surfactant 20%, suspending agent 2%, softener 0.8%, journey is alleviated in preservative 0.5%, essence 1% and deionized water 57.7%, realization best results, oil-control effect, alopecia Degree and scalp level of comfort are in crowd's test evaluation, more than 90% user feedback significant effect.

The third aspect, the present invention provides a kind of method for preparing the hair products as described in second aspect, including following step Suddenly：

(1) by zinc pyrithione, piroctone olamine salt, dimethyl silicone polymer, PPG-3 nutmegs alcohol ether, hydrolysis angle At least one of albumen and olive oil PEG-7 esters sequentially add water phase pot, and insulated and stirred is to being uniformly dispersed；

(2) temperature of water phase pot is reduced, the composition described in essence and first aspect is added in into water phase pot, stirring heat preservation is extremely It is uniformly dispersed；

(3) the water phase pot for again obtaining surfactant, suspending agent, softener and preservative addition step (2), stirring is extremely It is uniformly dispersed, obtains the hair products.

Preferably, the temperature of step (1) described heat preservation is 75-90 DEG C, for example, can be 75 DEG C, 78 DEG C, 80 DEG C, 83 DEG C, 85 DEG C, 87 DEG C or 90 DEG C, be preferably 80-85 DEG C.

Preferably, the time of step (1) described stirring be 5-20min, such as can be 5min, 8min, 11min, 13min, 15min, 19min or 20min are preferably 8-15min.

Preferably, step (2) temperature for reducing water phase pot is 35-50 DEG C, for example, can be 35 DEG C, 37 DEG C, 38 DEG C, 39 DEG C, 40 DEG C, 43 DEG C, 45 DEG C, 47 DEG C or 50 DEG C, be preferably 38-45 DEG C.

Preferably, the time of step (2) described stirring be 3-10min, such as can be 3min, 4min, 5min, 6min, 7min, 8min, 9min or 10min are preferably 4-8min.

Preferably, the time of step (3) described stirring be 3-10min, such as can be 3min, 4min, 5min, 6min, 7min, 8min, 9min or 10min are preferably 4-8min.

Preferably, the preparation method of step (2) described composition is as follows：

Sweet wormwood and tea bran are smashed it through 80-120 mesh sieves by (1 ') respectively, are placed in high pressure homogenizer, are 1 by solid-liquid ratio: (10-15) adds in high pressure homogenization method 20-30min, pressure 10-30MPa after pure water；

(2 ') purified using large aperture resin, after activated carbon decolorizing, obtain extract；

(3 ') are mixed step (the 2 ') extract with Rosemary Oil by formula ratio, obtain the composition.

Preferably, the mesh number of step (the 1 ') sieving is 80-120 mesh, such as can be 80 mesh, 82 mesh, 84 mesh, 88 Mesh, 90 mesh, 94 mesh, 96 mesh, 98 mesh, 100 mesh or 120 mesh.

Preferably, step (the 1 ') solid-liquid ratio is 1:(10-15), such as can be 1:10、1:11、1:12、1:13、1: 14 or 1:15.

Preferably, step (the 1 ') extraction time be 20-30min, such as can be 20min, 22min, 25min, 26min, 28min or 30min.

Preferably, step (the 1 ') pressure be 10-30Mpa, such as can be 10Mpa, 15Mpa, 20Mpa, 25Mpa or 30Mpa。

Compared with prior art, the present invention has the advantages that：

(1) three kinds of medicinal material synergy of the present invention, are prepared under special formulation ratio provided by the invention Composition realizes that effect maximizes, and composition composition species is terse, prevents the adverse reaction between a variety of medicinal materials, non-stimulated, It has no toxic side effect, while grease, removal dandruff is adsorbed, pre-Anti-hair loss promotes hair regeneration, and black hair brighten the hair improves hair Drying is crude, improves hair quality effect, and oil-control effect, alopecia alleviate degree and scalp level of comfort in crowd's test evaluation, More than 90% user feedback significant effect；

(2) hair products of the invention are in zinc pyrithione, piroctone olamine salt, dimethyl silicone polymer, PPG-3 meat Cardamom alcohol ether, hydrolysis of keratin, olive oil PEG-7 esters and surfactant, suspending agent, softener, essence, preservative Under coordinated, can notable oil-control, scalp of releiving, pre-Anti-hair loss, promote natural on-off cycles of hair growth；

(3) preparation method of composition stabilization simple for process of the invention, it is quality controllable, be conducive to utilization and extention and application In industrial production.

Specific embodiment

The technological means and its effect taken for the present invention is further explained, the present invention is made with reference to embodiments into Illustrate to one step.It is understood that the specific embodiments described herein are used only for explaining the present invention rather than to this hair Bright restriction.

In the examples where no specific technique or condition is specified, according to the described technology of document in the art or condition, Or it is carried out according to product description.Reagents or instruments used without specified manufacturer, be can be by regular channel commercially available from The conventional products of acquisition.

Embodiment 1

Composition is mainly prepared by mass percentage by the following raw material：

20 parts of Rosemary Oil

2 parts of Artemisinin

260 parts of tea bran extract；

Specific preparation method is as follows：

Sweet wormwood and tea bran are smashed it through 100 mesh sieves by (1 ') respectively, are placed in high pressure homogenizer, are 1 by solid-liquid ratio:12 add Enter high pressure homogenization method 25min, pressure 25MPa after pure water；

Embodiment 2

18 parts of Rosemary Oil

1 part of Artemisinin

250 parts of tea bran extract；

Specific preparation method is as follows：

Sweet wormwood and tea bran are smashed it through 90 mesh sieves by (1 ') respectively, are placed in high pressure homogenizer, are 1 by solid-liquid ratio:11 add Enter high pressure homogenization method 22min, pressure 20MPa after pure water；

Embodiment 3

26 parts of Rosemary Oil

3 parts of Artemisinin

280 parts of tea bran extract；

Specific preparation method is as follows：

Sweet wormwood and tea bran are smashed it through 110 mesh sieves by (1 ') respectively, are placed in high pressure homogenizer, are 1 by solid-liquid ratio:14 add Enter high pressure homogenization method 20min, pressure 16MPa after pure water；

Embodiment 4

15 parts of Rosemary Oil

5 parts of Artemisinin

200 parts of tea bran extract；

Specific preparation method is as follows：

Sweet wormwood and tea bran are smashed it through 80 mesh sieves by (1 ') respectively, are placed in high pressure homogenizer, are 1 by solid-liquid ratio:10 add Enter high pressure homogenization method 20min, pressure 10MPa after pure water；

Embodiment 5

30 parts of Rosemary Oil

1 part of Artemisinin

300 parts of tea bran extract；

Specific preparation method is as follows：

Sweet wormwood and tea bran are smashed it through 120 mesh sieves by (1 ') respectively, are placed in high pressure homogenizer, are 1 by solid-liquid ratio:15 add Enter high pressure homogenization method 30min, pressure 30MPa after pure water；

Comparative example 1

Compared with Example 1, except composition does not include Rosemary Oil, the parts by weight of Artemisinin in the composition Number is 5 parts, and the parts by weight of tea bran extract in the composition are 277 parts, and other components are with preparation method with embodiment 1.

Comparative example 2

Compared with Example 1, except composition does not include Artemisinin, the parts by weight of Rosemary Oil in the composition Number is 22 parts, and other components are with preparation method with embodiment 1.

Comparative example 3

Compared with Example 1, composition does not include tea bran extract, and the parts by weight of Artemisinin in the composition are 5 parts, the parts by weight of Rosemary Oil in the composition are 277 parts, and other components are with preparation method with embodiment 1.

Comparative example 4

Compared with Example 1, the parts by weight except Rosemary Oil in the composition are 10 parts, and other components are with preparing Method is the same as embodiment 1.

Comparative example 5

Compared with Example 1, the parts by weight except Rosemary Oil in the composition are 35 parts, and other components are with preparing Method is the same as embodiment 1.

Comparative example 6

Compared with Example 1, the parts by weight except Artemisinin in the composition are 8 parts, and other components are with preparing Method is the same as embodiment 1.

Comparative example 7

Compared with Example 1, the parts by weight except tea bran extract in the composition are 320 parts, other components and system Preparation Method is the same as embodiment 1.

Comparative example 8

Compared with Example 1, the parts by weight except tea bran extract in the composition are 180 parts, other components and system Preparation Method is the same as embodiment 1.

Patch test

Example and the composition of comparative example carry out safety evaluatio test.Choose will of 30 ages at 22-40 Sui Hope person, will equipped with the spot of 0.02mL samples try adhesive tape be affixed on volunteer's scalp, 24 it is small when after remove spot examination device, after opening patch It is checked in half an hour according to CTFA guides (1981).Standard of perfection is shown in Table 1, the results are shown in Table 2.

1 standard of perfection of table

Grade	Symbol	Standard of perfection
			0	-	Negative reaction：It is non-stimulated, without erythema
1	±	Suspicious reaction：Slight erythema
			2	+	Weakly positive is reacted：Erythema
3	++	Strong positive reaction：Erythema, papule, blister
			4	+++	Pole positive reaction：Serious edema, bulla

2 patch experimental result of table

The results show that the composition property of embodiment 1-5 and comparative example 4 and 8 is mild, irritation is weak, and allergy does not occur There are 5 suspicious reactions in reaction, comparative example 3, and 7 suspicious reactions occurs in the composition of comparative example 6, and the appearance of comparative example 74 is suspicious Reaction, it may be possible to excessive Rosemary Oil, Artemisinin and tea bran extract has certain sensitization, according to《Makeup Product hygienic practice》(version in 2015) provides, can determine that the hair products of embodiment and comparative example not to this batch subject's skin Skin causes adverse reaction.But it was found from data statistics meaning, what the hair products of embodiment caused that skin irritation reacts can Energy property is lower, property milder, and the hair products of comparative example may have certain irritation.

Embodiment 6

Scalp element is added with the composition of embodiment 1, and specific formula is shown in Table 3.

Table 3

Preparation method is as follows：

(1) by zinc pyrithione, piroctone olamine salt, dimethyl silicone polymer, PPG-3 nutmegs alcohol ether, hydrolysis angle Albumen and olive oil PEG-7 esters sequentially add water phase pot, and 80 DEG C of insulated and stirred 10min are to being uniformly dispersed；

(2) temperature of water phase pot is reduced to 40 DEG C, and essence and the composition are added in into water phase pot, insulated and stirred 5min To being uniformly dispersed；

(3) the water phase pot for again obtaining surfactant, suspending agent, softener and preservative addition step (2), stirring is extremely It is uniformly dispersed, obtains the scalp element.

Embodiment 7

Shampoo is added with the composition of embodiment 2, and specific formula is shown in Table 4.

Table 4

Preparation method is as follows：

(1) by zinc pyrithione, piroctone olamine salt, dimethyl silicone polymer, PPG-3 nutmegs alcohol ether, hydrolysis angle Albumen and olive oil PEG-7 esters sequentially add water phase pot, and 85 DEG C of insulated and stirred 8min are to being uniformly dispersed；

(2) temperature of water phase pot is reduced to 45 DEG C, and essence and the composition are added in into water phase pot, insulated and stirred 8min To being uniformly dispersed；

(3) the water phase pot for again obtaining surfactant, suspending agent, softener and preservative addition step (2), stirring is extremely It is uniformly dispersed, obtains the shampoo.

Embodiment 8

Hair conditioner is added with the composition of embodiment 3, and specific formula is shown in Table 5.

Table 5

Preparation method is as follows：

(3) the water phase pot for again obtaining surfactant, suspending agent, softener and preservative addition step (2), stirring is extremely It is uniformly dispersed, obtains the hair conditioner.

Embodiment 9

Composition of the hair care spraying added with embodiment 4, specific formula are shown in Table 6.

Table 6

Preparation method is as follows：

(3) the water phase pot for again obtaining surfactant, suspending agent, softener and preservative addition step (2), stirring is extremely It is uniformly dispersed, obtains the hair care spraying.

Embodiment 10

Compared with Example 6, the composition of embodiment 1 is only included, not comprising other components, other preparation methods and reality It is identical to apply example 6.

Comparative example 7

Compared with Example 6, the composition of comparative example 1 is added in scalp element, other preparation methods are same as Example 6.

Comparative example 8

Compared with Example 6, the composition of comparative example 2 is added in scalp element, other preparation methods are same as Example 6.

Comparative example 9

Compared with Example 6, the composition of comparative example 3 is added in scalp element, other preparation methods are same as Example 6.

Comparative example 10

Compared with Example 6, the composition of comparative example 4 is added in scalp element, other preparation methods are same as Example 6.

Comparative example 11

Compared with Example 6, the composition of comparative example 5 is added in scalp element, other preparation methods are same as Example 6.

Comparative example 12

Compared with Example 6, the composition of comparative example 6 is added in scalp element, other preparation methods are same as Example 6.

Comparative example 13

Compared with Example 6, the composition of comparative example 7 is added in scalp element, other preparation methods are same as Example 6.

Comparative example 14

Compared with Example 6, the composition of comparative example 8 is added in scalp element, other preparation methods are same as Example 6.

Comparative example 15

Compared with Example 6, the additive amount of composition is 0.5%, other preparation methods are same as Example 6.

Comparative example 16

Compared with Example 6, the additive amount of composition is 10%, other preparation methods are same as Example 6.

Comparative example 17

Compared with Example 6, composition is not added in hair products, other preparation methods are same as Example 6.

Crowd's test evaluation

The hair products of Example and comparative example carry out use feeling evaluation test, choose 50 volunteers and carry out half a head pair Than test, the cycle is 28 days, and effect return visit was carried out every 2 weeks.It is commented respectively in terms of scalp moisturizing degree, scalp degree two Point, questionnaire is filled according to use feeling, standards of grading for 1 point-without effect, 2 points-effective, very weak, 3 points-have It is effect, with obvious effects, 4 points-effective, effect it is preferable, 5 points-effective, effect it is very good.Scoring " >=3 points " is judged as imitating Fruit is apparent, counts the total number of persons of scoring " >=3 points ", and counts and cause the number that dandruff head is itched, and investigation result is shown in Table 7.

7 use feeling evaluation test of table

The result shows that the hair products of embodiment are superior to the hair care production of comparative example in terms of oil-control anticreep, scalp of releiving There is dandruff using several volunteers after the product 4 weeks of comparative example in product, and head is itched, the scalp malaise symptoms that scalp is felt nervous.

Hair care effect can be influenced as can be seen that lacking any component by comparing comparative example 7-9 and embodiment 6, Three kinds of components synergistic effect is indispensable, and only these three components exist simultaneously lower competence exertion its synergistic effect, hair care effect Most significantly；Compare comparative example 10-14 and embodiment 6 as can be seen that any one component in composition is not in the model of the application In enclosing, effect can all decline；Compare comparative example 15-16 with embodiment 6 as can be seen that composition is added with the mass fraction Hair care effect into hair products is best, declines more than the scope hair care effect；Comparing comparative example 17 and embodiment 6 can be with Find out, it is worst not add the hair products effect of the composition, almost without hair care effect.

In conclusion three kinds of medicinal material synergy of the present invention, prepare under special formulation ratio provided by the invention Obtained composition realizes that effect maximizes, and the composition composition species is terse, prevents the adverse reaction between a variety of medicinal materials, nothing It stimulates, have no toxic side effect, while grease, removal dandruff is adsorbed, pre-Anti-hair loss promotes hair regeneration, and black hair brighten the hair improves Trichoxerosis is crude, improves hair quality effect, and oil-control effect, alopecia alleviate degree and scalp level of comfort in crowd's test evaluation In, more than 90% user feedback significant effect.

Applicant states that the present invention illustrates the method detailed of the present invention, but not office of the invention by above-described embodiment It is limited to above-mentioned method detailed, that is, does not mean that the present invention has to rely on above-mentioned method detailed and could implement.Technical field Technical staff it will be clearly understood that any improvement in the present invention, equivalence replacement and auxiliary element to each raw material of product of the present invention Addition, selection of concrete mode etc., all fall within protection scope of the present invention and the open scope.

Claims

1. a kind of composition, which is characterized in that the composition includes following component：Rosemary Oil, Artemisinin and tea Bran extract.

2. composition according to claim 1, which is characterized in that the composition includes following component in parts by weight： 200-300 parts of 15-30 parts of Rosemary Oil, 1-5 parts of Artemisinin and tea bran extract；

Preferably, the composition includes following component in parts by weight：18-26 parts of Rosemary Oil, 1-3 parts of Artemisinin With 250-280 parts of tea bran extract.

3. a kind of hair products, which is characterized in that the hair products include the composition described in claim 1 or 2；

Preferably, the additive amount of the composition accounts for the mass percent of the hair products as 1-8%, is preferably 2-5%.

4. hair products according to claim 3, which is characterized in that the hair products include shampoo, hair conditioner, hair In film, hair jelly or scalp care element any one or at least two combination, be preferably scalp care element.

5. the hair products according to claim 3 or 4, which is characterized in that the hair products further include zinc pyrithione, pyrrole In Roc ketone ethanolamine salt, dimethyl silicone polymer, PPG-3 nutmegs alcohol ether, hydrolysis of keratin or olive oil PEG-7 esters Any one or at least two combination；

Preferably, the zinc pyrithione accounts for the mass percent of the hair products as 0.5-5%, is preferably 1-3%；

Preferably, the piroctone olamine salt accounts for the mass percent of the hair products as 0.1-3%, is preferably 0.3- 1%；

Preferably, the dimethyl silicone polymer accounts for the mass percent of the hair products as 0.8-5%, is preferably 1-3%；

Preferably, the PPG-3 nutmegs alcohol ether accounts for the mass percent of the hair products as 0.1-3%, is preferably 0.3- 1%；

Preferably, the hydrolysis of keratin accounts for the mass percent of the hair products as 0.1-3%, is preferably 0.3-1%；

Preferably, the olive oil PEG-7 esters account for the mass percent of the hair products as 0.1-3%, are preferably 0.3- 1%.

6. according to the hair products any one of claim 3-5, which is characterized in that the hair products further include surface In activating agent, suspending agent, softener, preservative and essence any one or at least two combination；

Preferably, the surfactant is any one in Plantacare 818, Cocoamidopropyl betaine or coconut oleoyl amine Kind or at least two combination；

Preferably, the suspending agent is acrylic acid (ester) analog copolymer；

Preferably, the softener is polyquaternium -7；

Preferably, the preservative is sodium benzoate.

7. according to the hair products described in claim 4-6, which is characterized in that the surfactant accounts for the hair products Mass percent is 15-30%, is preferably 18-26%；

Preferably, the suspending agent accounts for the mass percent of the hair products as 1-5%, is preferably 1-3%；

Preferably, the softener accounts for the mass percent of the hair products as 0.1-2%, is preferably 0.5-1%；

Preferably, the preservative accounts for the mass percent of the hair products as 0.1-1%, is preferably 0.1-0.8%；

Preferably, the essence accounts for the mass percent of the hair products as 0.1-3%, is preferably 0.5-2%.

8. according to the hair products described in claim 4-7, which is characterized in that the hair products include：

Preferably, the hair products include：

9. a kind of prepare such as the method for the hair products any one of claim 3-8, which is characterized in that including following step Suddenly：

(1) by zinc pyrithione, piroctone olamine salt, dimethyl silicone polymer, PPG-3 nutmegs alcohol ether, hydrolysis of keratin Water phase pot is sequentially added at least one of olive oil PEG-7 esters, and insulated and stirred is to being uniformly dispersed；

(2) temperature of water phase pot is reduced, the composition described in essence and claim 1 or 2 is added in into water phase pot, stirring heat preservation is extremely It is uniformly dispersed；

(3) the water phase pot for again obtaining surfactant, suspending agent, softener and preservative addition step (2) is stirred to scattered Uniformly, the hair products are obtained；

Preferably, the temperature of step (1) described heat preservation is 75-90 DEG C, is preferably 80-85 DEG C；

Preferably, the time of step (1) described stirring is 5-20min, is preferably 8-15min；

Preferably, step (2) temperature for reducing water phase pot is 35-50 DEG C, is preferably 38-45 DEG C；

Preferably, the time of step (2) described stirring is 3-10min, is preferably 4-8min；

Preferably, the time of step (3) described stirring is 3-10min, is preferably 4-8min.

10. according to the method described in claim 9, it is characterized in that, the preparation method of step (2) described composition is as follows：

Sweet wormwood and tea bran are smashed it through 80-120 mesh sieves by (1 ') respectively, are placed in high pressure homogenizer, are 1 by solid-liquid ratio:(10- 15) high pressure homogenization method 20-30min, pressure 10-30MPa after addition pure water；