CN104207998B - A kind of Flos Sophorae handwashing liquid and preparation method thereof - Google Patents
A kind of Flos Sophorae handwashing liquid and preparation method thereof Download PDFInfo
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- CN104207998B CN104207998B CN201410478050.0A CN201410478050A CN104207998B CN 104207998 B CN104207998 B CN 104207998B CN 201410478050 A CN201410478050 A CN 201410478050A CN 104207998 B CN104207998 B CN 104207998B
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Abstract
The invention provides a kind of Flos Sophorae handwashing liquid, belong to detergents and cosmetic technical field.Does is every 100 parts of this handwashing liquid made up of following raw materials by weight portion: Flos Sophorae extract 5-15 part, Herba portulacae extract 6-10 part, NaCl? 2-8 part, Cortex cocois radicis oleoyl diethanolamine 1-6 part, Flos Nelumbinis essence 0.5-1 part, glycerol 2-3 part, dehydrated alcohol 0.5-1 part, Kaolin 0.5-1 part, sodium carboxymethyl cellulose 0.1-1 part, dodecyl sodium sulfate 0.1-1 part, vitamin E? 1-2 part, all the other are deionized water.Advantage: can effective antiinflammatory sterilization, simultaneously can delay skin aging, improves skin.Present invention also offers a kind of method of high efficiency extraction Flos Sophorae effective ingredient simultaneously, there is the features such as efficient, quick.
Description
Technical field
The present invention relates to a kind of handwashing liquid, particularly relate to a kind of Flos Sophorae handwashing liquid, belong to detergents and cosmetic technical field.
Background technology
The Flos Sophorae of broad sense refers to the flower and alabastrum of leguminous plant Chinese scholartree (SophorajaponicaL.), but is generally called " Flos Sophorae " by open flower, and also claim " Chinese scholartree stamen ", alabastrum is then called " Flos Sophorae Immaturus ".Flos Sophorae fragrant taste is sweet, is rich in vitamin and multi mineral money, also has effect of heat-clearing and toxic substances removing, removing heat from blood lung moistening, blood pressure lowering, prevention of stroke simultaneously.Flos Sophorae contains rutin (i.e. rutin, Rytub), tannin, sophoradiol (Sophoradiol), glucose and glucuronic acid, has antiinflammatory action, has inhibitory action equally to virus and dermatophytes.
Herba Portulacae (Classification system: PortulacaoleraceaL.) is Portulacaceae annual herb plant.Plump succulence, without hair, high 10 ~ 30cm, is born in the area without shade such as roadside, field and ruins, flower garden.All there is distribution domestic various places.This kind is medicine food dual purpose plant.Herb hyoscine, has clearing away heat-damp and promoting diuresis, removing toxic substances and promoting subsidence of swelling, antiinflammatory, quenches the thirst, diuresis, has the title of " natural antibiotics " simultaneously, has good nourishing effect to human body, can improve the color of skin well, makes skin distribute healthy gloss.
Existing handwashing liquid generally all uses chemical substance to carry out sterilizing, antibacterial, use these handwashing liquid except can cause xerosis cutis coarse except, life-time service also can damage human body skin.A kind of effective draft handwashing liquid preparation method of research, can not only effective antiinflammatory sterilization, simultaneously can delay skin aging, and improve skin, can also reduce the use of chemical substance, protection of the environment, for consumer provides more selection simultaneously.
Summary of the invention
The object of this invention is to provide a kind of is the handwashing liquid of main component by Flos Sophorae extract, and this handwashing liquid can be antibacterial lastingly, gentle moistening hands.
Another object of the present invention is to provide the preparation method of this handwashing liquid.
The present invention is achieved through the following technical solutions:
A kind of Flos Sophorae handwashing liquid, every 100 parts are made up of following raw materials by weight portion: Flos Sophorae extract 5-15 part, Herba portulacae extract 6-10 part, NaCl2-8 part, Cortex cocois radicis oleoyl diethanolamine 1-6 part, Flos Nelumbinis essence 0.5-1 part, glycerol 2-3 part, dehydrated alcohol 0.5-1 part, Kaolin 0.5-1 part, sodium carboxymethyl cellulose 0.1-1 part, dodecyl sodium sulfate 0.1-1 part, vitamin e1-2 parts, all the other are deionized water.
Described Flos Sophorae extract, is obtained by following preparation method:
(1) get dry Flos Sophorae, pulverize, cross 30 mesh sieves, obtain Flos Sophorae powder;
(2) by Flos Sophorae powder and compound enzyme in mass ratio 65:3 mix, the ethanol that concentration is 75% is added again by solid-to-liquid ratio 1:5-10, soak 2-4h, soaking temperature 45-50 DEG C, soaks after terminating, temperature is increased to 70-80 DEG C, carry out reflux, extract, extraction time 1-2h, extracts after terminating, is cooled to 25 DEG C; Described compound enzyme by cellulase, hemicellulase, pectase in mass ratio 3:2:1 form;
(3) cooling terminates rear employing vacuum filtration, gets filtrate; By filtrate centrifugal 2-3 minute under 5000r/min, get supernatant; In supernatant, add the active carbon through special handling by solid-to-liquid ratio 1:3, prolonged agitation 1-2h, then vacuum filtration, get filtrate, by filtrate lyophilization, pulverized 60 mesh sieves, and namely obtained Flos Sophorae extract; The preparation method of the described active carbon through special handling is: in active carbon, add mass fraction by solid-to-liquid ratio 1:3-5 is 50-60%NaCl solution, then under 80-90 DEG C of condition, 2-4h is boiled, boil rear filtration, add by solid-to-liquid ratio 1:5-10 the alcoholic solution that concentration is 60-80% in filtering residue, soak 1-2h, immersion terminates rear filtration, dries putting into baking oven 50-60 DEG C after filtering residue;
Described Herba portulacae extract, obtained by following preparation method: Herba Portulacae is pulverized, cross 30 mesh sieves, obtain Herba Portulacae powder, the ethanol being 40-55% by Herba Portulacae powder and concentration mixes by solid-to-liquid ratio 1:4-7, adopt supersound extraction 15-20min, ultrasonic power is 160-180w, and ultrasonic temperature is 60-70 DEG C, filters after ultrasonic end, by filtrate drying and crushing, obtain Herba portulacae extract;
Flos Sophorae handwashing liquid preparation method of the present invention is as follows:
(1) by Cortex cocois radicis oleoyl diethanolamine, Flos Nelumbinis essence, Kaolin, sodium carboxymethyl cellulose, dodecyl sodium sulfate, deionized water mixing, be heated to 65-75 DEG C, then add vitamin E and glycerol, stir, cooling, obtains mixed liquor;
Etc. (2) when mixeding liquid temperature is down to 25 DEG C, then add Flos Sophorae extract, Herba portulacae extract, dehydrated alcohol, NaCl, stir, temperature is risen to 50 DEG C, stir 1-2h, and then cool the temperature to 25 DEG C, with citric acid by PH to being adjusted to 6.8-7.6.
The effect of Flos Sophorae extract in the present invention: the Flos Sophorae extract main component obtained by the preparation method of Flos Sophorae extract in the present invention is rutin (i.e. rutin, Rytub), sophoradiol (Sophoradiol), vitamin A etc. have the composition of physiologically active, have the effect of antiinflammatory and skin care;
The effect of Herba portulacae extract in the present invention: the Herba portulacae extract main component obtained by the preparation method of Herba portulacae extract in the present invention is the composition that alkaloid, flavonoid, saponin, vitamin A etc. have physiologically active, have antibacterial, go free radical and antioxidation, can delay skin aging, improve skin;
The present invention compared with prior art, has the following advantages and effect:
Containing multiple bioactive ingredients in this handwashing liquid, comprise Flos Sophorae extract, Herba portulacae extract, vitamin E, compatibility science, can sterilize by effective antiinflammatory, delay skin aging, improve skin, product main component of the present invention is natural product simultaneously, has side effect little, safety, the advantages such as environmental protection, have positive facilitation to health.The extracting method of Flos Sophorae extract provided by the invention in addition, repeatedly study through inventor, best results, the advantage such as there is conveniently, efficient, while abundant effective component extracting, avoid some adiaphorous impurity components and add in handwashing liquid the final quality affecting handwashing liquid to.
Specific embodiment
The present invention is set forth further below by way of specific embodiment.
Embodiment 1
A kind of Flos Sophorae handwashing liquid, every 100 parts are made up of following raw materials by weight portion: Flos Sophorae extract 5 parts, Herba portulacae extract 6 parts, NaCl2 part, Cortex cocois radicis oleoyl diethanolamine 1 part, 0.5 part, Flos Nelumbinis essence, glycerol 2 parts, dehydrated alcohol 0.5 part, Kaolin 0.5 part, sodium carboxymethyl cellulose 0.1 part, dodecyl sodium sulfate 0.1 part, vitamin e1 part, all the other are deionized water.
Described Flos Sophorae extract, is obtained by following preparation method:
(1) get dry Flos Sophorae, pulverize, cross 30 mesh sieves, obtain Flos Sophorae powder;
(2) by Flos Sophorae powder and compound enzyme in mass ratio 65:3 mix, then add by solid-to-liquid ratio 1:5 the ethanol that concentration is 75%, soak 2h, soaking temperature 45 DEG C, after immersion terminates, temperature is increased to 70 DEG C, carries out reflux, extract, extraction time 1h, extracts after terminating, is cooled to 25 DEG C; Described compound enzyme by cellulase, hemicellulase, pectase in mass ratio 3:2:1 form;
(3) cooling terminates rear employing vacuum filtration, gets filtrate; By filtrate under 5000r/min centrifugal 2 minutes, get supernatant; In supernatant, add the active carbon through special handling by solid-to-liquid ratio 1:3, prolonged agitation 1h, then vacuum filtration, get filtrate, by filtrate lyophilization, pulverized 60 mesh sieves, and namely obtained Flos Sophorae extract; The preparation method of the described active carbon through special handling is: in active carbon, add mass fraction by solid-to-liquid ratio 1:3 is 50%NaCl solution, then under 80 DEG C of conditions, 2h is boiled, boil rear filtration, add by solid-to-liquid ratio 1:5 the alcoholic solution that concentration is 60% in filtering residue, soak 1h, immersion terminates rear filtration, dries putting into 50 DEG C, baking oven after filtering residue;
Described Herba portulacae extract, obtained by following preparation method: Herba Portulacae is pulverized, cross 30 mesh sieves, obtain Herba Portulacae powder, the ethanol being 40% by Herba Portulacae powder and concentration mixes by solid-to-liquid ratio 1:4, adopt supersound extraction 15min, ultrasonic power is 160W, and ultrasonic temperature is 60 DEG C, filters after ultrasonic end, by filtrate drying and crushing, obtain Herba portulacae extract;
Flos Sophorae handwashing liquid preparation method of the present invention is as follows:
(1) by Cortex cocois radicis oleoyl diethanolamine, Flos Nelumbinis essence, Kaolin, sodium carboxymethyl cellulose, dodecyl sodium sulfate, deionized water mixing, be heated to 65 DEG C, then add vitamin E and glycerol, stir, cooling, obtains mixed liquor;
Etc. (2) when mixeding liquid temperature is down to 25 DEG C, then add Flos Sophorae extract, Herba portulacae extract, dehydrated alcohol, NaCl, stir, temperature is risen to 50 DEG C, stir 1h, and then cool the temperature to 25 DEG C, with citric acid by PH to being adjusted to 6.8.
Embodiment 2
A kind of Flos Sophorae handwashing liquid, every 100 parts are made up of following raw materials by weight portion: Flos Sophorae extract 10 parts, Herba portulacae extract 8 parts, NaCl6 part, Cortex cocois radicis oleoyl diethanolamine 4 parts, 0.7 part, Flos Nelumbinis essence, glycerol 2.5 parts, dehydrated alcohol 0.8 part, Kaolin 0.8 part, sodium carboxymethyl cellulose 0.5 part, dodecyl sodium sulfate 0.5 part, vitamin e1 .5 part, all the other are deionized water.
Described Flos Sophorae extract, is obtained by following preparation method:
(1) get dry Flos Sophorae, pulverize, cross 30 mesh sieves, obtain Flos Sophorae powder;
(2) by Flos Sophorae powder and compound enzyme in mass ratio 65:3 mix, then add by solid-to-liquid ratio 1:8 the ethanol that concentration is 75%, soak 3h, soaking temperature 48 DEG C, after immersion terminates, temperature is increased to 75 DEG C, carries out reflux, extract, extraction time 1.5h, extracts after terminating, is cooled to 25 DEG C; Described compound enzyme by cellulase, hemicellulase, pectase in mass ratio 3:2:1 form;
(3) cooling terminates rear employing vacuum filtration, gets filtrate; By filtrate under 5000r/min centrifugal 3 minutes, get supernatant; In supernatant, add the active carbon through special handling by solid-to-liquid ratio 1:3, prolonged agitation 1.5h, then vacuum filtration, get filtrate, by filtrate lyophilization, pulverized 60 mesh sieves, and namely obtained Flos Sophorae extract; The preparation method of the described active carbon through special handling is: in active carbon, add mass fraction by solid-to-liquid ratio 1:4 is 55%NaCl solution, then under 85 DEG C of conditions, 3h is boiled, boil rear filtration, add by solid-to-liquid ratio 1:8 the alcoholic solution that concentration is 70% in filtering residue, soak 1.5h, immersion terminates rear filtration, dries putting into 55 DEG C, baking oven after filtering residue;
Described Herba portulacae extract, obtained by following preparation method: Herba Portulacae is pulverized, cross 30 mesh sieves, obtain Herba Portulacae powder, the ethanol being 50% by Herba Portulacae powder and concentration mixes by solid-to-liquid ratio 1:6, adopt supersound extraction 18min, ultrasonic power is 170w, and ultrasonic temperature is 65 DEG C, filters after ultrasonic end, by filtrate drying and crushing, obtain Herba portulacae extract;
Flos Sophorae handwashing liquid preparation method of the present invention is as follows:
(1) by Cortex cocois radicis oleoyl diethanolamine, Flos Nelumbinis essence, Kaolin, sodium carboxymethyl cellulose, dodecyl sodium sulfate, deionized water mixing, be heated to 70 DEG C, then add vitamin E and glycerol, stir, cooling, obtains mixed liquor;
Etc. (2) when mixeding liquid temperature is down to 25 DEG C, then add Flos Sophorae extract, Herba portulacae extract, dehydrated alcohol, NaCl, stir, temperature is risen to 50 DEG C, stir 1.5h, and then cool the temperature to 25 DEG C, with citric acid by PH to being adjusted to 7.2.
Embodiment 3
A kind of Flos Sophorae handwashing liquid, every 100 parts are made up of following raw materials by weight portion: Flos Sophorae extract 15 parts, Herba portulacae extract 10 parts, NaCl8 part, Cortex cocois radicis oleoyl diethanolamine 6 parts, 1 part, Flos Nelumbinis essence, glycerol 3 parts, dehydrated alcohol 1 part, Kaolin 1 part, sodium carboxymethyl cellulose 1 part, dodecyl sodium sulfate 1 part, vitamin E2 part, all the other are deionized water.
Described Flos Sophorae extract, is obtained by following preparation method:
(1) get dry Flos Sophorae, pulverize, cross 30 mesh sieves, obtain Flos Sophorae powder;
(2) by Flos Sophorae powder and compound enzyme in mass ratio 65:3 mix, then add by solid-to-liquid ratio 1:10 the ethanol that concentration is 75%, soak 4h, soaking temperature 50 DEG C, after immersion terminates, temperature is increased to 80 DEG C, carries out reflux, extract, extraction time 2h, extracts after terminating, is cooled to 25 DEG C; Described compound enzyme by cellulase, hemicellulase, pectase in mass ratio 3:2:1 form;
(3) cooling terminates rear employing vacuum filtration, gets filtrate; By filtrate under 5000r/min centrifugal 3 minutes, get supernatant; In supernatant, add the active carbon through special handling by solid-to-liquid ratio 1:3, prolonged agitation 2h, then vacuum filtration, get filtrate, by filtrate lyophilization, pulverized 60 mesh sieves, and namely obtained Flos Sophorae extract; The preparation method of the described active carbon through special handling is: in active carbon, add mass fraction by solid-to-liquid ratio 1:5 is 60%NaCl solution, then under 90 DEG C of conditions, 4h is boiled, boil rear filtration, add by solid-to-liquid ratio 1:10 the alcoholic solution that concentration is 80% in filtering residue, soak 2h, immersion terminates rear filtration, dries putting into 60 DEG C, baking oven after filtering residue;
Described Herba portulacae extract, obtained by following preparation method: Herba Portulacae is pulverized, cross 30 mesh sieves, obtain Herba Portulacae powder, the ethanol being 55% by Herba Portulacae powder and concentration mixes by solid-to-liquid ratio 1:7, adopt supersound extraction 20min, ultrasonic power is 180w, and ultrasonic temperature is 70 DEG C, filters after ultrasonic end, by filtrate drying and crushing, obtain Herba portulacae extract;
Flos Sophorae handwashing liquid preparation method of the present invention is as follows:
(1) by Cortex cocois radicis oleoyl diethanolamine, Flos Nelumbinis essence, Kaolin, sodium carboxymethyl cellulose, dodecyl sodium sulfate, deionized water mixing, be heated to 75 DEG C, then add vitamin E and glycerol, stir, cooling, obtains mixed liquor;
Etc. (2) when mixeding liquid temperature is down to 25 DEG C, then add Flos Sophorae extract, Herba portulacae extract, dehydrated alcohol, NaCl, stir, temperature is risen to 50 DEG C, stir 2h, and then cool the temperature to 25 DEG C, with citric acid by PH to being adjusted to 7.6.
Claims (3)
1. a Flos Sophorae handwashing liquid, is characterized in that every 100 parts are made up of following raw materials by weight portion: Flos Sophorae extract 5-15 part, Herba portulacae extract 6-10 part, NaCl2-8 part, Cortex cocois radicis oleoyl diethanolamine 1-6 part, Flos Nelumbinis essence 0.5-1 part, glycerol 2-3 part, dehydrated alcohol 0.5-1 part, Kaolin 0.5-1 part, sodium carboxymethyl cellulose 0.1-1 part, dodecyl sodium sulfate 0.1-1 part, vitamin e1-2 parts, all the other are deionized water;
Described Flos Sophorae extract, is obtained by following preparation method:
(1) get dry Flos Sophorae, pulverize, cross 30 mesh sieves, obtain Flos Sophorae powder;
(2) by Flos Sophorae powder and compound enzyme in mass ratio 65:3 mix, the ethanol that concentration is 75% is added again by solid-to-liquid ratio 1:5-10, soak 2-4h, soaking temperature 45-50 DEG C, soaks after terminating, temperature is increased to 70-80 DEG C, carry out reflux, extract, extraction time 1-2h, extracts after terminating, is cooled to 25 DEG C; Described compound enzyme by cellulase, hemicellulase, pectase in mass ratio 3:2:1 form;
(3) cooling terminates rear employing vacuum filtration, gets filtrate; By filtrate centrifugal 2-3 minute under 5000r/min, get supernatant; In supernatant, add the active carbon through special handling by solid-to-liquid ratio 1:3, prolonged agitation 1-2h, then vacuum filtration, get filtrate, by filtrate lyophilization, pulverized 60 mesh sieves, and namely obtained Flos Sophorae extract; The preparation method of the described active carbon through special handling is: in active carbon, add mass fraction by solid-to-liquid ratio 1:3-5 is 50-60%NaCl solution, then under 80-90 DEG C of condition, 2-4h is boiled, boil rear filtration, add by solid-to-liquid ratio 1:5-10 the alcoholic solution that concentration is 60-80% in filtering residue, soak 1-2h, immersion terminates rear filtration, dries putting into baking oven 50-60 DEG C after filtering residue;
Described Herba portulacae extract, obtained by following preparation method: Herba Portulacae is pulverized, cross 30 mesh sieves, obtain Herba Portulacae powder, the ethanol being 40-55% by Herba Portulacae powder and concentration mixes by solid-to-liquid ratio 1:4-7, adopt supersound extraction 15-20min, ultrasonic power is 160-180w, and ultrasonic temperature is 60-70 DEG C, filters after ultrasonic end, by filtrate drying and crushing, obtain Herba portulacae extract.
2. a kind of Flos Sophorae extract handwashing liquid according to claim 1, is characterized in that every 100 parts are made up of following raw materials by weight portion: Flos Sophorae extract 10 parts, Herba portulacae extract 8 parts, NaCl6 part, Cortex cocois radicis oleoyl diethanolamine 4 parts, 0.7 part, Flos Nelumbinis essence, glycerol 2.5 parts, dehydrated alcohol 0.8 part, Kaolin 0.8 part, sodium carboxymethyl cellulose 0.5 part, dodecyl sodium sulfate 0.5 part, vitamin e1 .5 part, all the other are deionized water;
Described Flos Sophorae extract, is obtained by following preparation method:
(1) get dry Flos Sophorae, pulverize, cross 30 mesh sieves, obtain Flos Sophorae powder;
(2) by Flos Sophorae powder and compound enzyme in mass ratio 65:3 mix, then add by solid-to-liquid ratio 1:8 the ethanol that concentration is 75%, soak 3h, soaking temperature 48 DEG C, after immersion terminates, temperature is increased to 75 DEG C, carries out reflux, extract, extraction time 1.5h, extracts after terminating, is cooled to 25 DEG C; Described compound enzyme by cellulase, hemicellulase, pectase in mass ratio 3:2:1 form;
(3) cooling terminates rear employing vacuum filtration, gets filtrate; By filtrate under 5000r/min centrifugal 3 minutes, get supernatant; In supernatant, add the active carbon through special handling by solid-to-liquid ratio 1:3, prolonged agitation 1.5h, then vacuum filtration, get filtrate, by filtrate lyophilization, pulverized 60 mesh sieves, and namely obtained Flos Sophorae extract; The preparation method of the described active carbon through special handling is: in active carbon, add mass fraction by solid-to-liquid ratio 1:4 is 55%NaCl solution, then under 85 DEG C of conditions, 3h is boiled, boil rear filtration, add by solid-to-liquid ratio 1:8 the alcoholic solution that concentration is 70% in filtering residue, soak 1.5h, immersion terminates rear filtration, dries putting into 55 DEG C, baking oven after filtering residue;
Described Herba portulacae extract, obtained by following preparation method: Herba Portulacae is pulverized, cross 30 mesh sieves, obtain Herba Portulacae powder, the ethanol being 50% by Herba Portulacae powder and concentration mixes by solid-to-liquid ratio 1:6, adopt supersound extraction 18min, ultrasonic power is 170w, and ultrasonic temperature is 65 DEG C, filters after ultrasonic end, by filtrate drying and crushing, obtain Herba portulacae extract.
3. a kind of Flos Sophorae handwashing liquid according to claim 1 or 2, is characterized in that its preparation method is as follows:
(1) by Cortex cocois radicis oleoyl diethanolamine, Flos Nelumbinis essence, Kaolin, sodium carboxymethyl cellulose, dodecyl sodium sulfate, deionized water mixing, be heated to 65-75 DEG C, then add vitamin E and glycerol, stir, cooling, obtains mixed liquor;
Etc. (2) when mixeding liquid temperature is down to 25 DEG C, then add Flos Sophorae extract, Herba portulacae extract, dehydrated alcohol, NaCl, stir, temperature is risen to 50 DEG C, stir 1-2h, and then cool the temperature to 25 DEG C, with citric acid by PH to being adjusted to 6.8-7.6.
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| CN105362195A (en) * | 2015-12-15 | 2016-03-02 | 北京健旭康技术有限公司 | Beijing tourism cosmetics and preparation technology |
| CN107669547B (en) * | 2017-10-24 | 2021-02-26 | 山东朱氏药业集团有限公司 | Bacteriostatic hand sanitizer containing purslane and preparation method thereof |
| CN108567143A (en) * | 2018-03-28 | 2018-09-25 | 广西玉阳绿州生物科技有限公司 | Lowiaceae plant extraction liquid, production method and its application in treatment of cancer |
| CN116076713A (en) * | 2022-11-14 | 2023-05-09 | 仙乐健康科技股份有限公司 | Edible plant ferment composition for synergistically improving skin moisture and inflammation |
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| CN1298293A (en) * | 1998-04-24 | 2001-06-06 | 宝洁公司 | Cleansing articles for skin and/or hair which also deposits skin care actives |
| CN1673336A (en) * | 2005-04-20 | 2005-09-28 | 王浩贵 | Eucalyptus robusta leaves cleaning products |
| CN102525857A (en) * | 2012-01-18 | 2012-07-04 | 李军 | Hand wash for disinfection and sterilization |
| CN103109880A (en) * | 2013-03-01 | 2013-05-22 | 胡昱 | Environment-friendly disinfectant |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1298293A (en) * | 1998-04-24 | 2001-06-06 | 宝洁公司 | Cleansing articles for skin and/or hair which also deposits skin care actives |
| CN1673336A (en) * | 2005-04-20 | 2005-09-28 | 王浩贵 | Eucalyptus robusta leaves cleaning products |
| CN102525857A (en) * | 2012-01-18 | 2012-07-04 | 李军 | Hand wash for disinfection and sterilization |
| CN103109880A (en) * | 2013-03-01 | 2013-05-22 | 胡昱 | Environment-friendly disinfectant |
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Effective date of registration: 20170725 Address after: 361101 Fujian Province, Xiamen city Xiangan District Ma Xiang Lin had No. 161 Patentee after: Xiamen Haida daily necessities Co., Ltd. Address before: 325000, Zhejiang province Ruian city town of Victoria Village glory Village Patentee before: Wu Yueze |
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