Summary of the invention
The object of this invention is to provide a kind of is the handwashing liquid of main component by Flos Sophorae extract, and this handwashing liquid can be antibacterial lastingly, gentle moistening hands.
Another object of the present invention is to provide the preparation method of this handwashing liquid.
The present invention is achieved through the following technical solutions:
A kind of Flos Sophorae handwashing liquid, every 100 parts are made up of following raw materials by weight portion: Flos Sophorae extract 5-15 part, Herba portulacae extract 6-10 part, NaCl 2-8 part, Cortex cocois radicis oleoyl diethanolamine 1-6 part, Flos Nelumbinis essence 0.5-1 part, glycerol 2-3 part, dehydrated alcohol 0.5-1 part, Kaolin 0.5-1 part, sodium carboxymethyl cellulose 0.1-1 part, dodecyl sodium sulfate 0.1-1 part, vitamin E 1-2 part, all the other are deionized water.
Described Flos Sophorae extract, is obtained by following preparation method:
(1) get dry Flos Sophorae, pulverize, cross 30 mesh sieves, obtain Flos Sophorae powder;
(2) Flos Sophorae powder and compound enzyme are mixed in mass ratio at 65: 3, the ethanol that solubility is 75% is added again by solid-to-liquid ratio 1: 5-10, soak 2-4h, soaking temperature 45-50 DEG C, soaks after terminating, temperature is increased to 70-80 DEG C, carry out reflux, extract, extraction time 1-2h, extracts after terminating, is cooled to 25 DEG C; Described compound enzyme to be made up of in mass ratio cellulase, hemicellulase, pectase at 3: 2: 1;
(3) cooling terminates rear employing vacuum filtration, gets filtrate; By filtrate centrifugal 2-3 minute under 5000r/min, get supernatant; In supernatant, add the active carbon through special handling by solid-to-liquid ratio 1: 3, prolonged agitation 1-2h, then vacuum filtration, get filtrate, by filtrate lyophilization, pulverized 60 mesh sieves, and namely obtained Flos Sophorae extract; The preparation method of the described active carbon through special handling is: in active carbon, add mass fraction by solid-to-liquid ratio 1: 3-5 is 50-60%NaCl solution, then under 80-90 DEG C of condition, 2-4h is boiled, boil rear filtration, add by solid-to-liquid ratio 1: 5-10 the alcoholic solution that solubility is 60-80% in filtering residue, soak 1-2h, immersion terminates rear filtration, dries putting into baking oven 50-60 DEG C after filtering residue;
Described Herba portulacae extract, obtained by following preparation method: Herba Portulacae is pulverized, crossing 30 mesh sieves, obtain Herba Portulacae powder, is that the ethanol of 40-55% mixes by solid-to-liquid ratio 1: 4-7 by Herba Portulacae powder and solubility, adopt supersound extraction 15-20min, ultrasonic power is 160-180w, and ultrasonic temperature is 60-70 DEG C, filters after ultrasonic end, by filtrate drying and crushing, obtain Herba portulacae extract;
Flos Sophorae handwashing liquid preparation method of the present invention is as follows:
(1) by Cortex cocois radicis oleoyl diethanolamine, Flos Nelumbinis essence, Kaolin, sodium carboxymethyl cellulose, dodecyl sodium sulfate, deionized water mixing, be heated to 65-75 DEG C, then add vitamin E and glycerol, stir, cooling, obtains mixed liquor;
Etc. (2) when mixeding liquid temperature is down to 25 DEG C, then add Flos Sophorae extract, Herba portulacae extract, dehydrated alcohol, citric acid and NaCl, stir, temperature is risen to 50 DEG C, stir 1-2h, and then cool the temperature to 25 DEG C, with citric acid by PH to being adjusted to 6.8-7.6.
The effect of Flos Sophorae extract in the present invention: the Flos Sophorae extract main component obtained by the preparation method of Flos Sophorae extract in the present invention is rutin (i.e. rutin, Rytub), sophoradiol (Sophoradiol), vitamin A etc. have the composition of physiologically active, have the effect of antiinflammatory and skin care;
The effect of Herba portulacae extract in the present invention: the Herba portulacae extract main component obtained by the preparation method of Herba portulacae extract in the present invention is the composition that alkaloid, flavonoid, saponin, vitamin A etc. have physiologically active, have antibacterial, go free radical and antioxidation, can delay skin aging, improve skin;
The present invention compared with prior art, has the following advantages and effect:
Containing multiple bioactive ingredients in this handwashing liquid, comprise Flos Sophorae extract, Herba portulacae extract, vitamin E, compatibility science, can sterilize by effective antiinflammatory, delay skin aging, improve skin, product main component of the present invention is natural product simultaneously, has side effect little, safety, the advantages such as environmental protection, have positive facilitation to health.The extracting method of Flos Sophorae extract provided by the invention in addition, repeatedly study through inventor, best results, the advantage such as there is conveniently, efficient, while abundant effective component extracting, avoid some adiaphorous impurity components and add in handwashing liquid the final quality affecting handwashing liquid to.
Specific embodiment
The present invention is set forth further below by way of specific embodiment.
Embodiment 1
A kind of Flos Sophorae handwashing liquid, every 100 parts are made up of following raw materials by weight portion: Flos Sophorae extract 5 parts, Herba portulacae extract 6 parts, NaCl 2 parts, Cortex cocois radicis oleoyl diethanolamine 1 part, 0.5 part, Flos Nelumbinis essence, glycerol 2 parts, dehydrated alcohol 0.5 part, Kaolin 0.5 part, sodium carboxymethyl cellulose 0.1 part, dodecyl sodium sulfate 0.1 part, vitamin E 1 part, all the other are deionized water.
Described Flos Sophorae extract, is obtained by following preparation method:
(1) get dry Flos Sophorae, pulverize, cross 30 mesh sieves, obtain Flos Sophorae powder;
(2) Flos Sophorae powder and compound enzyme are mixed in mass ratio at 65: 3, then add by solid-to-liquid ratio 1: 5 ethanol that solubility is 75%, soak 2h, soaking temperature 45 DEG C, after immersion terminates, temperature is increased to 70 DEG C, carries out reflux, extract, extraction time 1h, extracts after terminating, is cooled to 25 DEG C; Described compound enzyme to be made up of in mass ratio cellulase, hemicellulase, pectase at 3: 2: 1;
(3) cooling terminates rear employing vacuum filtration, gets filtrate; By filtrate under 5000r/min centrifugal 2 minutes, get supernatant; In supernatant, add the active carbon through special handling by solid-to-liquid ratio 1: 3, prolonged agitation 1h, then vacuum filtration, get filtrate, by filtrate lyophilization, pulverized 60 mesh sieves, and namely obtained Flos Sophorae extract; The preparation method of the described active carbon through special handling is: in active carbon, add mass fraction by solid-to-liquid ratio 1: 3 is 50%NaCl solution, then under 80 DEG C of conditions, 2h is boiled, boil rear filtration, add by solid-to-liquid ratio 1: 5 alcoholic solution that solubility is 60% in filtering residue, soak 1h, immersion terminates rear filtration, dries putting into 50 DEG C, baking oven after filtering residue;
Described Herba portulacae extract, obtained by following preparation method: Herba Portulacae is pulverized, crossing 30 mesh sieves, obtain Herba Portulacae powder, is that the ethanol of 40% mixes by solid-to-liquid ratio 1: 4 by Herba Portulacae powder and solubility, adopt supersound extraction 15min, ultrasonic power is 160W, and ultrasonic temperature is 60 DEG C, filters after ultrasonic end, by filtrate drying and crushing, obtain Herba portulacae extract;
Flos Sophorae handwashing liquid preparation method of the present invention is as follows:
(1) by Cortex cocois radicis oleoyl diethanolamine, Flos Nelumbinis essence, Kaolin, sodium carboxymethyl cellulose, dodecyl sodium sulfate, deionized water mixing, be heated to 65 DEG C, then add vitamin E and glycerol, stir, cooling, obtains mixed liquor;
Etc. (2) when mixeding liquid temperature is down to 25 DEG C, then add Flos Sophorae extract, Herba portulacae extract, dehydrated alcohol, citric acid and NaCl, stir, temperature is risen to 50 DEG C, stir 1h, and then cool the temperature to 25 DEG C, with citric acid by PH to being adjusted to 6.8.Embodiment 2
A kind of Flos Sophorae handwashing liquid, every 100 parts are made up of following raw materials by weight portion: Flos Sophorae extract 10 parts, Herba portulacae extract 8 parts, NaCl 6 parts, Cortex cocois radicis oleoyl diethanolamine 4 parts, 0.7 part, Flos Nelumbinis essence, glycerol 2.5 parts, dehydrated alcohol 0.8 part, Kaolin 0.8 part, sodium carboxymethyl cellulose 0.5 part, dodecyl sodium sulfate 0.5 part, vitamin E 1.5 parts, all the other are deionized water.
Described Flos Sophorae extract, is obtained by following preparation method:
(1) get dry Flos Sophorae, pulverize, cross 30 mesh sieves, obtain Flos Sophorae powder;
(2) Flos Sophorae powder and compound enzyme are mixed in mass ratio at 65: 3, then add by solid-to-liquid ratio 1: 8 ethanol that solubility is 75%, soak 3h, soaking temperature 48 DEG C, after immersion terminates, temperature is increased to 75 DEG C, carries out reflux, extract, extraction time 1.5h, extracts after terminating, is cooled to 25 DEG C; Described compound enzyme to be made up of in mass ratio cellulase, hemicellulase, pectase at 3: 2: 1;
(3) cooling terminates rear employing vacuum filtration, gets filtrate; By filtrate under 5000r/min centrifugal 3 minutes, get supernatant; In supernatant, add the active carbon through special handling by solid-to-liquid ratio 1: 3, prolonged agitation 1.5h, then vacuum filtration, get filtrate, by filtrate lyophilization, pulverized 60 mesh sieves, and namely obtained Flos Sophorae extract; The preparation method of the described active carbon through special handling is: in active carbon, add mass fraction by solid-to-liquid ratio 1: 4 is 55%NaCl solution, then under 85 DEG C of conditions, 3h is boiled, boil rear filtration, add by solid-to-liquid ratio 1: 8 alcoholic solution that solubility is 70% in filtering residue, soak 1.5h, immersion terminates rear filtration, dries putting into 55 DEG C, baking oven after filtering residue;
Described Herba portulacae extract, obtained by following preparation method: Herba Portulacae is pulverized, crossing 30 mesh sieves, obtain Herba Portulacae powder, is that the ethanol of 50% mixes by solid-to-liquid ratio 1: 6 by Herba Portulacae powder and solubility, adopt supersound extraction 18min, ultrasonic power is 170w, and ultrasonic temperature is 65 DEG C, filters after ultrasonic end, by filtrate drying and crushing, obtain Herba portulacae extract;
Flos Sophorae handwashing liquid preparation method of the present invention is as follows:
(1) by Cortex cocois radicis oleoyl diethanolamine, Flos Nelumbinis essence, Kaolin, sodium carboxymethyl cellulose, dodecyl sodium sulfate, deionized water mixing, be heated to 70 DEG C, then add vitamin E and glycerol, stir, cooling, obtains mixed liquor;
Etc. (2) when mixeding liquid temperature is down to 25 DEG C, then add Flos Sophorae extract, Herba portulacae extract, dehydrated alcohol, citric acid and NaCl, stir, temperature is risen to 50 DEG C, stir 1.5h, and then cool the temperature to 25 DEG C, with citric acid by PH to being adjusted to 7.2.Embodiment 3
A kind of Flos Sophorae handwashing liquid, every 100 parts are made up of following raw materials by weight portion: Flos Sophorae extract 15 parts, Herba portulacae extract 10 parts, NaCl 8 parts, Cortex cocois radicis oleoyl diethanolamine 6 parts, 1 part, Flos Nelumbinis essence, glycerol 3 parts, dehydrated alcohol 1 part, Kaolin 1 part, sodium carboxymethyl cellulose 1 part, dodecyl sodium sulfate 1 part, vitamin E 2 parts, all the other are deionized water.
Described Flos Sophorae extract, is obtained by following preparation method:
(1) get dry Flos Sophorae, pulverize, cross 30 mesh sieves, obtain Flos Sophorae powder;
(2) Flos Sophorae powder and compound enzyme are mixed in mass ratio at 65: 3, then add by solid-to-liquid ratio 1: 10 ethanol that solubility is 75%, soak 4h, soaking temperature 50 DEG C, after immersion terminates, temperature is increased to 80 DEG C, carries out reflux, extract, extraction time 2h, extracts after terminating, is cooled to 25 DEG C; Described compound enzyme to be made up of in mass ratio cellulase, hemicellulase, pectase at 3: 2: 1;
(3) cooling terminates rear employing vacuum filtration, gets filtrate; By filtrate under 5000r/min centrifugal 3 minutes, get supernatant; In supernatant, add the active carbon through special handling by solid-to-liquid ratio 1: 3, prolonged agitation 2h, then vacuum filtration, get filtrate, by filtrate lyophilization, pulverized 60 mesh sieves, and namely obtained Flos Sophorae extract; The preparation method of the described active carbon through special handling is: in active carbon, add mass fraction by solid-to-liquid ratio 1: 5 is 60%NaCl solution, then under 90 DEG C of conditions, 4h is boiled, boil rear filtration, add by solid-to-liquid ratio 1: 10 alcoholic solution that solubility is 80% in filtering residue, soak 2h, immersion terminates rear filtration, dries putting into 60 DEG C, baking oven after filtering residue;
Described Herba portulacae extract, obtained by following preparation method: Herba Portulacae is pulverized, crossing 30 mesh sieves, obtain Herba Portulacae powder, is that the ethanol of 55% mixes by solid-to-liquid ratio 1: 7 by Herba Portulacae powder and solubility, adopt supersound extraction 20min, ultrasonic power is 180w, and ultrasonic temperature is 70 DEG C, filters after ultrasonic end, by filtrate drying and crushing, obtain Herba portulacae extract;
Flos Sophorae handwashing liquid preparation method of the present invention is as follows:
(1) by Cortex cocois radicis oleoyl diethanolamine, Flos Nelumbinis essence, Kaolin, sodium carboxymethyl cellulose, dodecyl sodium sulfate, deionized water mixing, be heated to 75 DEG C, then add vitamin E and glycerol, stir, cooling, obtains mixed liquor;
Etc. (2) when mixeding liquid temperature is down to 25 DEG C, then add Flos Sophorae extract, Herba portulacae extract, dehydrated alcohol, citric acid and NaCl, stir, temperature is risen to 50 DEG C, stir 2h, and then cool the temperature to 25 DEG C, with citric acid by PH to being adjusted to 7.6.