CN105168037A - Compound natural hair dye and preparation method therefor - Google Patents
Compound natural hair dye and preparation method therefor Download PDFInfo
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- CN105168037A CN105168037A CN201510500135.9A CN201510500135A CN105168037A CN 105168037 A CN105168037 A CN 105168037A CN 201510500135 A CN201510500135 A CN 201510500135A CN 105168037 A CN105168037 A CN 105168037A
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Abstract
The invention discloses a compound natural hair dye. The compound natural hair dye is composed of the following ingredients, by weight, 100-200 parts of walnut green seedcase extract product, 10-40 parts of balsamine extract product, 10-20 parts of galangal extract product, 10-20 parts of mint extract product, 15-30 parts of tea tree oil, 10-20 parts of thickening agent and 300-800 parts of water. The pure natural plant hair dye has good hair dyeing effects, has functions of nourishing and protecting hair, is safe and nontoxic and has no side effects on human health. The invention also discloses a preparation method for the compound natural hair dye. The method is concise in technology, the cost is low, and batch production can be achieved.
Description
Technical field
The invention belongs to hair dye technical field, be specifically related to a kind of composite natural hair dye and preparation method thereof.
Background technology
Along with the fast development of economy, the rhythm of life of modern is fast, operating pressure large, thus causes poliosis rejuvenation, comes from the pursuit to quality of the life and cultural life, and hair dyeing more and more becomes ingredient important in life.At present, hair dyeing product on market is substantially many containing plyability chemicals, these hair dye majorities all contain peroxide, 2, tens kinds of chemical substances such as 4-diamino anisole, phenylenediamine, Ammonium persulfate., Nitrobenzol, these harmful substances may bring out the cell mutation of human body, thus cause allergy, carcinogenic, damage human body hepatic and renal function etc.
The former plant of Semen Juglandis is Juglandaceae (Juglandaceae) Juglans (JuglansL.) plant Semen Juglandis (JuglansregiaL.), China existing Semen Juglandis cultivated area more than 200 ten thousand hm
2, annual production, more than 500,000 t, occupies first of the world, and simultaneously produced Exocarpium Juglandis Immaturus garbage is more than 350,000 t.At present, having in patent documentation to record adopts Exocarpium Juglandis Immaturus to be that raw material dyes to hair, if application number is in the patent of invention of 201310229503.1, it discloses a kind of preparation method of plant source hair dye, be specially a kind of hair dye preparation method based on walnut green husk pigment, Exocarpium Juglandis Immaturus, dries in shady spot; After pulverizing, 70-90 eye mesh screen sieves; Add Pericarpium Citri Reticulatae Viride powder and acetone in a reservoir in the ratio of solid-liquid mass ratio 1:25-35, the concentration of acetone is 70-90%, and solution is oscillation treatment 10-14h at constant temperature 40-50 DEG C; Above-mentioned solution centrifugal process 2-4 time, filter is assorted collects supernatant; Above-mentioned solution concentrating under reduced pressure at 50-65 DEG C of temperature is obtained ointment; Hair dye is become by the proportions of ointment 5-7%, water 85-87%, silicone oil 0.5-1.5%, oil-soluble VE0.5-1.5%, VB0.5-1.5%, olive oil 3-5%, white vaseline 0.5-1.5%.Adopt Exocarpium Juglandis Immaturus as main hair dye in this hair dye, be aided with chemical composition such as silicone oil, VE, VB and white vaseline etc. simultaneously and be mixed with hair dye, the hair dye that the method is made, dyeing is not enriched, effect is single, and containing chemical composition especially silicone oil, studies discovery at present, silicone oil can fill up the space between hair scale sheet, so hair is very smooth after washing head, but due to the impermeability of silicon and inertia, can block pores, easily make people's scalp itch, even alopecia, alopecia etc.At hair washing, hair dyeing or hair care art, studying its substitute products or developing without silicone oil product.
Therefore, the composite natural hair dye developed based on the pure plant of discarded Exocarpium Juglandis Immaturus has very large environment protection significance and economic worth.
Summary of the invention
First object of the present invention is to provide a kind of composite natural hair dye, and this pure natural plant hair dye hair dyeing effect is good, and have concurrently simultaneously and moisten and hair care effect, safety non-toxic, can not produce any side effect to health.
The present invention also aims to the preparation method that above-mentioned composite natural hair dye is provided, this preparation method concise in technology, with low cost, can produce in batches.
First object of the present invention is realized by following technological means: a kind of composite natural hair dye, is made up of the component of following mass distribution ratio: walnut peel extract 100 ~ 200, Extracts from Flowers of Impatiens balsamina L 10 ~ 40, Rhizoma Alpiniae Officinarum extract 10 ~ 20, Folium Menthae extract 10 ~ 20, tea tree oil 15 ~ 30, thickening agent 10 ~ 20, water 300 ~ 800.
Further: the proportion by weight of each component is as follows: walnut peel extract 130 ~ 180, Extracts from Flowers of Impatiens balsamina L 20 ~ 30, Rhizoma Alpiniae Officinarum extract 12 ~ 18, Folium Menthae extract 12 ~ 18, tea tree oil 20 ~ 25, thickening agent 12 ~ 18, water 500 ~ 600.
In above-mentioned composite natural hair dye:
Described walnut peel extract prepares preferably by the method comprised the following steps: choose Exocarpium Juglandis Immaturus, dry, the rear soak with ethanol of pulverizing, then microwave ultrasound is adopted to extract the Exocarpium Juglandis Immaturus after immersion, by extracting liquid filtering after extraction, obtain filtrate, filtrate reduced in volume gained ointment is walnut peel extract.
Described ethanol is preferably the industrial alcohol that volumn concentration is 85 ~ 95%, and the consumption of ethanol is preferably 5 ~ 20 times of Exocarpium Juglandis Immaturus gross mass.
When microwave ultrasound is extracted, microwave power is preferably 600 ~ 800W, and microwave frequency is preferably 2000 ~ 2500MHz; Ultrasonic power is preferably 1000 ~ 1300W, and ultrasonic frequency is preferably 20 ~ 30KHz, and the microwave ultrasound time is preferably 30 ~ 35min.
Filtrate is walnut peel extract at 45 ~ 55 DEG C of concentrating under reduced pressure gained ointment.
The present invention adopts the collaborative extraction of microwave ultrasound, the hair dye ingredient in Exocarpium Juglandis Immaturus can be extracted fast and effectively.
Extracts from Flowers of Impatiens balsamina L of the present invention, Rhizoma Alpiniae Officinarum extract and Folium Menthae extract prepare preferably by the method comprised the following steps: choose Flos Impatientis, Rhizoma Alpiniae Officinarum and Herba Menthae, be placed in ethanol respectively to extract, extract obtainedly namely obtain Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract and Folium Menthae extract through concentrating under reduced pressure.
Namely by each raw material Flos Impatientis, Rhizoma Alpiniae Officinarum and Herba Menthae, adopt ethanol to extract separately, obtain respective extract, be convenient to the composite hair dye of subsequent formulation.
The consumption of ethanol is 5 ~ 20 times of Flos Impatientis, Rhizoma Alpiniae Officinarum or Herba Menthae gross mass, and ethanol is preferably the industrial alcohol that volumn concentration is 80% ~ 95%, and extraction time is 1 ~ 3 time, extracts 10 ~ 30min at every turn.
Thickening agent of the present invention is preferably sesbania gum, guar gum or xanthan gum.These thickening agents are derived from plant source, and safety is natural.
In above-mentioned composite natural hair dye, effect of each component is as follows:
Walnut peel extract in the present invention is preferably the ethanol extraction of Exocarpium Juglandis Immaturus, this alcohol extract contains abundant Exocarpium Juglandis Immaturus melanin, also have simultaneously and carry the better light stability of product, pigment heat stability, antioxidation and resistance to reduction higher than water extraction or alkali, and antibacterial and antioxidant activity preferably.Simultaneously in Exocarpium Juglandis Immaturus ethanol extraction the effective content of staining components also far above the acetone extract of Exocarpium Juglandis Immaturus.
Containing neutral red brown pigment in Flos Impatientis (having another name called Flos Impatientis) extract, be called lawsone, also be rich in multiple nutritional components in Extracts from Flowers of Impatiens balsamina L simultaneously, in Extracts from Flowers of Impatiens balsamina L, the plants herb elite of pure natural can thoroughly tighten up hair surface scale, be beneficial to hair to absorb completely, reach nourishing hair, eliminate that hair dries up, the effect of jag, make hair gloss high resilience, soft nature.
Present invention applicant finds through a large amount of creationary test, both walnut peel extract and Extracts from Flowers of Impatiens balsamina L are used for hair-dyeing jointly, can enrich the kind of dyeing, and can produce collaborative hyperchromic effect, the hair dye made also has the effect of nourishing hair.
The present invention finds through overtesting; Rhizoma Alpiniae Officinarum extract to drop and the hair problem such as to drop has and has certain curative effect for preventing and treating the dandruff; therefore added in hair dye of the present invention; while hair dyeing; can protect scalp, minimizing has the raw material of hair dyeing effect if walnut peel extract and Extracts from Flowers of Impatiens balsamina L are to the stimulation of scalp.
Herba Menthae is Chinese conventional Chinese medicine, and young tender stem point can make vegetable edible, and herb can be used as medicine again, and cure cold heating laryngalgia, and headache, conjunctival congestion with ophthalmalgia, myalgia, skin rubella is scratched where it itches, the diseases such as measles without adequate eruption, also effective to carbuncle, cellulitis, scabies, tinea, dermatitis rhus in addition.Effective ingredient in the alcohol extract of Herba Menthae has antiinflammatory, antibacterial and antioxidant activity, and Folium Menthae extract can permeate when having hair dyed sends out core, play nutritional supplementation effect, make healthy hair smooth as silk, allow hair recover elastic force, be full of gloss and moisture, tough hair makes it not rupture, make hair healthy have vigor, there is during hair dyeing refrigerant fragrance and refrigerant pleasant sense, strengthen hair dyeing effect.
Tea tree oil, botany is called as titrol, because it is mainly from Myrtaceae, the several plants of Melaleuca, its topmost one is called Melaleuca Alternifolia (MelaleucaalternifoliaCheel), there is characteristic perfume and antibacterial, antiinflammatory, anthelmintic, kill effect of demodicid mite, also have and convergence is provided, releive and wake effect of skin up, contain unique elite, head fat secretion can be balanced, moisten and maintenance hair simultaneously, scalp and hair overdrying can not be caused, also can repair withered, jag, the hair of fracture, to the dyeing of walnut peel extract and Extracts from Flowers of Impatiens balsamina L, there is tint retention.
In sum, each raw material that the present invention adopts respectively has unique function, present invention utilizes the characteristic of walnut peel extract and Extracts from Flowers of Impatiens balsamina L dyeing, tea tree oil can balance head fat secretion, moisten and maintenance hair and fixation characteristic, the dandruff that what Rhizoma Alpiniae Officinarum extract had prevent and treat drops and the hair effect of dropping, and effect having sterilizing and itch-relieving concurrently of Folium Menthae extract, promote characteristic and the blood circulation promoting of infiltration, the effect that hair dye is absorbed better by hair can be made, therefore, Rhizoma Alpiniae Officinarum extract and the composite use of Folium Menthae extract, synergistic protective effect can be played to the hair after hair dyeing effect and hair dyeing and scalp, each raw material in hair dye of the present invention is arranged in pairs or groups use mutually, there is good hair dyeing effect.
Second object of the present invention is achieved through the following technical solutions: the preparation method of above-mentioned composite natural hair dye, comprises the following steps:
(1) walnut peel extract is prepared: choose Exocarpium Juglandis Immaturus, dry, the rear soak with ethanol of pulverizing, then adopts microwave ultrasound to extract, by extracting liquid filtering after extraction the Exocarpium Juglandis Immaturus after immersion, obtain filtrate, filtrate reduced in volume gained ointment is walnut peel extract;
(2) prepare Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract and Folium Menthae extract: choose Flos Impatientis, Rhizoma Alpiniae Officinarum and Herba Menthae, be placed in ethanol respectively and extract, extract obtainedly namely obtain Extracts from Flowers of Impatiens balsamina L Rhizoma Alpiniae Officinarum extract and Folium Menthae extract through concentrating under reduced pressure;
(3) by above-mentioned dose relationship, walnut peel extract, Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract, Folium Menthae extract, tea tree oil, thickening agent and water is got respectively, mixing, i.e. obtained composite natural hair dye.
In the preparation method of above-mentioned composite natural hair dye:
Ethanol described in step (1) is preferably the industrial alcohol that volumn concentration is preferably 85 ~ 95%, and the consumption of ethanol is preferably 5 ~ 20 times of Exocarpium Juglandis Immaturus gross mass; When microwave ultrasound is extracted, microwave power is preferably 600 ~ 800W, and microwave frequency is preferably 2000 ~ 2500MHz; Ultrasonic power is preferably 1000 ~ 1300W, and ultrasonic frequency is preferably 20 ~ 30KHz, and the microwave ultrasound time is preferably 30 ~ 35min; Filtrate is preferably walnut peel extract at 45 ~ 55 DEG C of concentrating under reduced pressure gained ointment; In step (2), the consumption of ethanol is preferably 5 ~ 20 times of Flos Impatientis, Rhizoma Alpiniae Officinarum or Herba Menthae gross mass, described ethanol is preferably the industrial alcohol that volumn concentration is preferably 80% ~ 95%, extraction time is preferably 1 ~ 3 time, extracts 10 ~ 30min at every turn.
Tool of the present invention has the following advantages:
(1) hair dye in the present invention is pure botanical hair dye, not containing any chemical industry synthesis material, does not hinder hair, does not hinder scalp, can not produce any side effect to health;
(2) raw material that the present invention adopts is natural plants, safety non-toxic, and is easy to gather;
(3) hair dye in the present invention also has antiinflammatory, itching-relieving action, and not containing antiseptic;
(4) hair dyeing effect in the present invention, can according to different proportioning raw materials just as natural hair color, hair are dyed black, lividity, brown, brown etc.;
(5) preparation method of the hair dyeing in the present invention, its concise in technology, with low cost, can produce in batches.
Detailed description of the invention
Embodiment 1
The composite natural hair dye that the present embodiment provides, is made up of the component of following mass distribution ratio: walnut peel extract 100, Extracts from Flowers of Impatiens balsamina L 40, Rhizoma Alpiniae Officinarum extract 10, Folium Menthae extract 20, tea tree oil 15, thickening agent 10, water 800.
Wherein walnut peel extract is prepared by the method comprised the following steps: choose Exocarpium Juglandis Immaturus, dry, pulverizing is rear soaks with the industrial alcohol that 10 times of volumn concentrations are 95%, then microwave ultrasound is adopted to extract the Exocarpium Juglandis Immaturus after immersion, microwave power is 600W, and microwave frequency is 2450MHz; Ultrasonic power is 1000W, and ultrasonic frequency is 30KHz, and the microwave ultrasound time is 30min, by extracting liquid filtering after extraction, obtains filtrate, and filtrate is walnut peel extract at 45 DEG C of concentrating under reduced pressure gained ointment.
Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract and Folium Menthae extract are its ethanol extraction, concrete leaching process is: choose Flos Impatientis, Rhizoma Alpiniae Officinarum and Herba Menthae, the volumn concentration being placed in 10 times of quality be respectively 95% industrial alcohol extract, extract 2 times, namely each extraction 15min, extract obtainedly obtain Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract and Folium Menthae extract through concentrating under reduced pressure.
Thickening agent is sesbania gum.
This composite natural hair dye, its preparation method is as follows:
(1) walnut peel extract is prepared as stated above: choose Exocarpium Juglandis Immaturus, dry, the rear soak with ethanol of pulverizing, then microwave ultrasound is adopted to extract the Exocarpium Juglandis Immaturus after immersion, by extracting liquid filtering after extraction, obtain filtrate, filtrate reduced in volume gained ointment is walnut peel extract;
(2) Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract and Folium Menthae extract is prepared as stated above: choose Flos Impatientis, Rhizoma Alpiniae Officinarum and Herba Menthae, be placed in ethanol respectively to extract, extract obtainedly namely obtain Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract and Folium Menthae extract through concentrating under reduced pressure;
(3) by above-mentioned dose relationship, walnut peel extract, Extracts from Flowers of Impatiens balsamina L, tea tree oil, Rhizoma Alpiniae Officinarum extract, Folium Menthae extract, thickening agent and water is got respectively, mixing, i.e. obtained composite natural hair dye.
The hair dye uniform application made by the present embodiment is on hair, and heating cap 30 minutes on cover, can dye brown by hair.
Embodiment 2
The composite natural hair dye that the present embodiment provides, is made up of the component of following mass distribution ratio: walnut peel extract 150, Extracts from Flowers of Impatiens balsamina L 30, Rhizoma Alpiniae Officinarum extract 15, Folium Menthae extract 15, tea tree oil 25, thickening agent 15, water 550.
Wherein walnut peel extract is prepared by the method comprised the following steps: choose Exocarpium Juglandis Immaturus, dry, pulverizing is rear soaks with the industrial alcohol that 5 times of volumn concentrations are 90%, then microwave ultrasound is adopted to extract the Exocarpium Juglandis Immaturus after immersion, microwave power is 700W, and microwave frequency is 2450MHz; Ultrasonic power is 1100W, and ultrasonic frequency is 25KHz, and the microwave ultrasound time is 32min, by extracting liquid filtering after extraction, obtains filtrate, and filtrate is walnut peel extract at 50 DEG C of concentrating under reduced pressure gained ointment.
Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract or Folium Menthae extract are its ethanol extraction, concrete leaching process is: choose Flos Impatientis, Rhizoma Alpiniae Officinarum or Herba Menthae, the volumn concentration being placed in 5 times of quality be respectively 90% industrial alcohol extract, extract 3 times, namely each extraction 30min, extract obtainedly obtain Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract or Folium Menthae extract through concentrating under reduced pressure.
Thickening agent is guar gum.
This composite natural hair dye, its preparation method is with embodiment 1.
The hair dye uniform application made by the present embodiment is on hair, and on cover, heating cap 25 minutes, can dye brown by hair.
Embodiment 3
The composite natural hair dye that the present embodiment provides, is made up of the component of following mass distribution ratio: walnut peel extract 200, Extracts from Flowers of Impatiens balsamina L 10, Rhizoma Alpiniae Officinarum extract 15, Folium Menthae extract 20, tea tree oil 30, thickening agent 10, water 300.
Wherein walnut peel extract is prepared by the method comprised the following steps: choose Exocarpium Juglandis Immaturus, dry, pulverizing is rear soaks with the industrial alcohol that 20 times of volumn concentrations are 85%, then microwave ultrasound is adopted to extract the Exocarpium Juglandis Immaturus after immersion, microwave power is 800W, and microwave frequency is 2450MHz; Ultrasonic power is 1300W, and ultrasonic frequency is 20KHz, and the microwave ultrasound time is 35min, by extracting liquid filtering after extraction, obtains filtrate, and filtrate is walnut peel extract at 55 DEG C of concentrating under reduced pressure gained ointment.
Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract and Folium Menthae extract are its ethanol extraction, concrete leaching process is: choose Flos Impatientis, Rhizoma Alpiniae Officinarum or Herba Menthae, the volumn concentration being placed in 20 times of quality be respectively 80% industrial alcohol extract, extract 1 time, namely each extraction 20min, extract obtainedly obtain Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract and Folium Menthae extract through concentrating under reduced pressure.
Thickening agent is xanthan gum.
This composite natural hair dye, its preparation method is with embodiment 1.
The hair dye uniform application made by the present embodiment is on hair, and on cover, heating cap 20 minutes, can dye black by hair.
The hair care hair care effect of hair dye of the present invention is verified below by way of specific experiment:
With poliosis crowd for object of study, have 60 people and test use, be divided into the embodiment 1-3 in the corresponding the present invention of 3 test group difference, often organize each 20 people, wherein male 10 people, women 10 people.3 test group are had hair dyed with the hair dye prepared in embodiment of the present invention 1-3 respectively, and experimental result is as follows:
The hair dyeing effect of hair dye in table 1 embodiment 1-3
| Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| Hair color | Brown | Brown | Black |
| Hair dyeing effectiveness | 15 | 16 | 18 |
| Hair moistens | 19 | 18 | 20 |
| Scalp irritation, pruritus | 0 | 0 | 0 |
Result shows, poliosis can be dyed the hair of different colours by hair dye of the present invention effectively, and in addition, hair dye of the present invention also has the effects such as moist hair, effectively can solve the problems such as dry puckery, the inflammation in hair dyeing back, scalp itch.
The present invention will be described more than to enumerate specific embodiment; it is pointed out that above embodiment is only for the invention will be further described, does not represent protection scope of the present invention; the nonessential amendment that other people prompting according to the present invention is made and adjustment, still belong to protection scope of the present invention.
Claims (10)
1. a composite natural hair dye, is characterized in that being made up of the component of following mass distribution ratio: walnut peel extract 100 ~ 200, Extracts from Flowers of Impatiens balsamina L 10 ~ 40, Rhizoma Alpiniae Officinarum extract 10 ~ 20, Folium Menthae extract 10 ~ 20, tea tree oil 15 ~ 30, thickening agent 10 ~ 20, water 300 ~ 800.
2. composite natural hair dye according to claim 1, it is characterized in that: described walnut peel extract is prepared by the method comprised the following steps: choose Exocarpium Juglandis Immaturus, dry, the rear soak with ethanol of pulverizing, then microwave ultrasound is adopted to extract the Exocarpium Juglandis Immaturus after immersion, by extracting liquid filtering after extraction, obtain filtrate, filtrate reduced in volume gained ointment is walnut peel extract.
3. composite natural hair dye according to claim 2, is characterized in that: described ethanol to be volumn concentration be 85 ~ 95% industrial alcohol, the consumption of ethanol is 5 ~ 20 times of Exocarpium Juglandis Immaturus gross mass.
4. composite natural hair dye according to claim 2, is characterized in that: when microwave ultrasound is extracted, microwave power is 600 ~ 800W, and microwave frequency is 2000 ~ 2500MHz; Ultrasonic power is 1000 ~ 1300W, and ultrasonic frequency is 20 ~ 30KHz, and the microwave ultrasound time is 30 ~ 35min.
5. composite natural hair dye according to claim 2, is characterized in that: filtrate is walnut peel extract at 45 ~ 55 DEG C of concentrating under reduced pressure gained ointment.
6. composite natural hair dye according to claim 1, it is characterized in that: described Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract and Folium Menthae extract are prepared by the method comprised the following steps: choose Flos Impatientis, Rhizoma Alpiniae Officinarum and Herba Menthae, be placed in ethanol respectively to extract, extract obtainedly namely obtain Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract and Folium Menthae extract through concentrating under reduced pressure.
7. composite natural hair dye according to claim 6, it is characterized in that: the consumption of ethanol is 5 ~ 20 times of Flos Impatientis, Rhizoma Alpiniae Officinarum or Herba Menthae gross mass, ethanol to be volumn concentration be 80% ~ 95% industrial alcohol, extraction time is 1 ~ 3 time, extracts 10 ~ 30min at every turn.
8. composite natural hair dye according to claim 1, is characterized in that: described thickening agent is sesbania gum, guar gum or xanthan gum.
9. the preparation method of the composite natural hair dye according to any one of claim 1-8, is characterized in that comprising the following steps:
(1) walnut peel extract is prepared: choose Exocarpium Juglandis Immaturus, dry, the rear soak with ethanol of pulverizing, then adopts microwave ultrasound to extract, by extracting liquid filtering after extraction the Exocarpium Juglandis Immaturus after immersion, obtain filtrate, filtrate reduced in volume gained ointment is walnut peel extract;
(2) Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract and Folium Menthae extract is prepared: choose Flos Impatientis, Rhizoma Alpiniae Officinarum and Herba Menthae, be placed in ethanol respectively to extract, extract obtainedly namely obtain Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract and Folium Menthae extract through concentrating under reduced pressure;
(3) by above-mentioned dose relationship, walnut peel extract, Extracts from Flowers of Impatiens balsamina L, Rhizoma Alpiniae Officinarum extract, Folium Menthae extract, tea tree oil, thickening agent and water is got respectively, mixing, i.e. obtained composite natural hair dye.
10. the preparation method of composite natural hair dye according to claim 9, is characterized in that: the ethanol described in step (1) to be volumn concentration be 85 ~ 95% industrial alcohol, the consumption of ethanol is 5 ~ 20 times of Exocarpium Juglandis Immaturus gross mass; When microwave ultrasound is extracted, microwave power is 600 ~ 800W, and microwave frequency is 2000 ~ 2500MHz; Ultrasonic power is 1000 ~ 1300W, and ultrasonic frequency is 20 ~ 30KHz, and the microwave ultrasound time is 30 ~ 35min; Filtrate is walnut peel extract at 45 ~ 55 DEG C of concentrating under reduced pressure gained ointment; The consumption of ethanol is 5 ~ 20 times of Flos Impatientis, Rhizoma Alpiniae Officinarum or Herba Menthae gross mass in step (2), described ethanol to be volumn concentration be 80% ~ 95% industrial alcohol, extraction time is 1 ~ 3 time, extracts 10 ~ 30min at every turn.
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| CN105663010A (en) * | 2016-02-29 | 2016-06-15 | 广西南岜仔科技有限公司 | Fructus mume hair dye and preparation method of fructus mume hair dye |
| CN105748394A (en) * | 2016-04-11 | 2016-07-13 | 马鞍山中粮生物化学有限公司 | Hair dye capable of fixing and protecting hair |
| CN109431933A (en) * | 2018-11-28 | 2019-03-08 | 山东师范大学 | A kind of sun-proof color protection hair-cream and its preparation method and application |
| CN110755330A (en) * | 2019-12-03 | 2020-02-07 | 浙江章华保健美发实业有限公司 | Compound pure natural hair dye and production method thereof |
| CN115317428A (en) * | 2022-09-19 | 2022-11-11 | 广州楚颜化妆品有限公司 | Natural plant extract hair-dyeing composition |
| CN115381760A (en) * | 2022-07-18 | 2022-11-25 | 高州市人民医院 | Preparation method of hair dye |
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| CN105663010A (en) * | 2016-02-29 | 2016-06-15 | 广西南岜仔科技有限公司 | Fructus mume hair dye and preparation method of fructus mume hair dye |
| CN105748394A (en) * | 2016-04-11 | 2016-07-13 | 马鞍山中粮生物化学有限公司 | Hair dye capable of fixing and protecting hair |
| CN109431933A (en) * | 2018-11-28 | 2019-03-08 | 山东师范大学 | A kind of sun-proof color protection hair-cream and its preparation method and application |
| CN109431933B (en) * | 2018-11-28 | 2021-11-09 | 山东师范大学 | Sunscreen and color-care hair cream and preparation method and application thereof |
| CN110755330A (en) * | 2019-12-03 | 2020-02-07 | 浙江章华保健美发实业有限公司 | Compound pure natural hair dye and production method thereof |
| CN115381760A (en) * | 2022-07-18 | 2022-11-25 | 高州市人民医院 | Preparation method of hair dye |
| CN115317428A (en) * | 2022-09-19 | 2022-11-11 | 广州楚颜化妆品有限公司 | Natural plant extract hair-dyeing composition |
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