CN103948541A

CN103948541A - Preparation method of blackcurrant hair blackening liquid shampoo

Info

Publication number: CN103948541A
Application number: CN201410219047.7A
Authority: CN
Inventors: 王跃进; 王军锋
Original assignee: Individual
Current assignee: Guangzhou Ousudan Biological Technology Co ltd
Priority date: 2014-05-23
Filing date: 2014-05-23
Publication date: 2014-07-30
Anticipated expiration: 2034-05-23
Also published as: CN103948541B

Abstract

The invention relates to a preparation method of blackcurrant hair blackening liquid shampoo. The preparation method is characterized by comprising the following steps: pulping green walnut skin and walnut fresh leaves, mixing pulp with juice of whole fresh garden nalsam, then mixing with extracting concentrated solutions of fructus psoraleae, prepared fleece flower root, herba ecliptae, semen cuscutae, black mulberry, blackcurrant, black fungus, polyrhachis vicina roger, clove and the like, finally uniformly mixing with cystine, menthol, sodium dodecyl sulfate, stearic acid, magnesium stearate, ammonium chloride, benzoic acid and perfume, and canning, thus obtaining the blackcurrant hair blackening liquid shampoo.

Description

A kind of preparation method of black currant hair color shampoo

Technical field

What the present invention relates to is a kind of preparation method of black currant hair color shampoo.

Background technology

On market, there are the much Related product such as shampoo, hair cream or concept products about black hair, hair color, through retrieval about the shampoo of black hair or spray, liniment class technology, there are tens kinds, but be mostly to mix with the simple processing of traditional Chinese medicine and chemical composition, because technique is simple, middle the effective elements of the medicine is not brought into play, and bioavailability is very low, substantially be to have its black hair concept, but there is no black hair effect or black hair DeGrain.And some product to be exactly one purely wash stain, and be abuse chemically blackening stain, it has increased the various risks to harm greatly.Through research, extraction of natural melanin from the plant of screening, pass through biotechnology, effective ingredient in effective tradition plant amedica is separated, then carried out purification, the two is coordinated mutually, utilize and absorb by targeting, inside and outside dual combination, can effectively reach by hair washing and make its melanin regeneration, the object of medicine for curing poliosis.

Summary of the invention

The object of the invention is to propose a kind of preparation method of black currant hair color shampoo.

The object of the present invention is achieved like this, and preparation method is as follows:

A, get Exocarpium Juglandis Immaturus 40-60% and the fresh leaf 40-60% of Semen Juglandis, pull an oar, filter with beater, obtain juice, collect for subsequent use;

B, get fresh Herba Stellariae Alsines herb and comprise the fresh Flos Impatientis on herb, pull an oar with beater, filter, obtain juice, collect for subsequent use;

C, get Semen Juglandis 20-40%, Semen Sesami Nigrum 20-60%, fresh Cacumen Platycladi 20-40%, mix oil expression, collect for subsequent usely, waste is managed elsewhere;

D, get Fructus Psoraleae 20-30%, Radix Polygoni Multiflori Preparata 10-20%, Herba Ecliptae 20-30%, Semen Cuscutae 10-25%, black Fructus Mori 10-20%, after pulverizing, use 90% ethanol, 100 DEG C of temperature are extracted 1h, filter; Second extraction 80% ethanol, extracts 1h to 90 DEG C of temperature of filtering residue, filters, and extracts for three times and uses 70% ethanol, and 80 DEG C of temperature of filtering residue are extracted to 1h, filters; Merge three times extracting solution, 60 DEG C of concentrated 4h of temperature, collect ethanol, obtain concentrated solution, for subsequent use;

E, get black currant dry product 50-70%, Auricularia 30-50%, with d step method, extract to obtain and extract concentrated solution, for subsequent use;

F, get black thorn ant 60-80%, Flos Caryophylli 20-40%, with d step method, extract and obtain concentrated solution, for subsequent use;

G, get the c step remaining waste that extracts oil, by the method for d step, extract concentrated solution, for subsequent use;

The juice 40-60% that h, the juice 40-60% that gets the acquisition of a step, b step obtain, for subsequent use after mixing;

The extraction concentrated solution 15-30% that i, the extraction concentrated solution 30-50% that gets the acquisition of d step, e step obtain, the extraction concentrated solution 15-30% that f step obtains, the extraction concentrated solution 10-20% that g step obtains, mix, for subsequent use;

The miscella 4-10% that j, the mixed liquor 10-20% that gets the acquisition of h step, c step obtain, mixed liquor 60-70%, cystine 9-15%, the Mentholum 2-4% that i step obtains, mix, for subsequent use;

K, get mixed liquor 44.8%, sodium lauryl sulfate 52%, stearic acid 0.7%, magnesium stearate 1.8%, ammonium chloride 0.25%, benzoic acid 0.15%, spice 0.3% that j step obtains, mix homogeneously, canned and get final product.

Good effect of the present invention is:

Semen Juglandis: warm in nature, taste is fragrant and micro-puckery.Supplementing the brain, Fructus Alpiniae Oxyphyllae, the kidney invigorating, strong waist, skin Caring, lung benefiting Dingchuan, clear and coherent blood vessels, crow palpus hair color, for suffering from a deficiency of the kidney, chills and pain of the waist and kness, heart kidney two loses, the diseases such as constipation.Semen Juglandis abroad, be it is called " strong man's food ", " intelligent promoting fruit ".Enjoy at home " long live ", " Solanum muricatum ", " supporting people's treasured " laudatory title.Often eat Semen Juglandis and can strengthen note second power, the brain-strengthening effect that it is distinguished and abundant nutritive value, by increasing people is praised highly.Modern medicine study is thought, the phospholipid in Semen Juglandis has good health-care effect to cranial nerve, and the unsaturated fatty acid in walnut oil is prevented and treated arteriosclerosis effect.In Semen Juglandis, contain rich in protein, fat, 22 kinds of mineral, multivitamin.Fat and protein are the best nutrient substance of brain, and its protein is high quality protein.Protein 20g in every 100g, unsaturated fatty acid 63g, carbohydrate 10.7g, calcium 108mg, P 32 9mg, ferrum 3.2mg, carotene 30ug, vitamin E 43.21mg, dietary cellulose 9.6g, potassium 385mg, selenium 4.62ug, zinc 2.17mg, manganese 3.44mg, chromium 3.2mg, aminoacid 2.5%, linoleic acid 71%, linolenic acid 12%, also has abundant vitamin A, vitamin B1, vitamin B2, vitamin C, vitamin B6 etc.Have data to show, in human aging process, zinc, manganese content day by day reduce, and often eat Semen Juglandis and are conducive to supplement zinc, manganese, defying age.

Semen Sesami Nigrum: property is flat, enrich and benefit essence and blood, for early whitening of beard and hair, dizziness and blurred vision, moisturizes laxation, for blood deficiency and depleted fluid.Mend in five, physical strength profiting, longue meat, fills out brains, improve visual and auditory acuity, black beard and hair, sharp intestine and small intestine, by rheumatism gas.Containing abundant VE, there is the function of dispelling free radical in biomembrane, destroy its function thereby prevention biomembrane is oxidized, VE can protect islet cells, contributes to alleviate neurological symptom, and can reduce blood glucose.

Cacumen Platycladi: cold in nature, cooling blood for hemostasis, has growing and blacking hair function, for haematemesis, epistaxis, spit blood, have blood in stool, metrostaxis, heat in blood alopecia, early whitening of beard and hair.

Fructus Psoraleae: acrid in the mouth hardship, warm in nature, there is the effect of warming and recuperating the kidney-YANG, can emerging positive controlling nocturnal emission with astringent drugs, reducing urination and antidiarrheal, helping inspiration to relieve asthma, the impotence and seminal emission for the treatment of insufficiency of kidney-YANG, soreness of the waist and knees; frequent micturition, the having loose bowels of spleen-kidney vacuity cold, and to tinea, beriberi, alopecia areata, all have good effect.New scientific achievement shows, Fructus Psoraleae tool light sensitization, and it can promote dermal melanin new life, can curing vitiligo, treatment poliosis is had certain effect.

Radix Polygoni Multiflori Preparata: bitter in the mouth, sweet, warm in nature, there are invigorating the liver and kidney, benefiting essence-blood, black beard and hair, the function of bone and muscle strengthening, for blood deficiency and yellow complexion, vertigo and tinnitus, early whitening of beard and hair, soreness of the waist and knees, numb limbs and tense tendons, bleeding not during menses, chronic malaria body void, hyperlipemia.

Herba Ecliptae: sweet in the mouth, acid, cold in nature, there is nourishing the liver and kidney, cooling blood for hemostasis effect, for vertigo and tinnitus, spits blood, epistaxis, hematuria, dysentery, metrostaxis, traumatic hemorrhage, early whitening of beard and hair.

Semen Cuscutae: property is flat, controlling nocturnal emission with astringent drugs reducing urination, the kidney invigorating and essence nourishing, nourishing the liver to improve visual acuity, strengthening the spleen antidiarrheal, frequent micturition, maximum feature is both YANG invigorating, also nourishing YIN, and property is not dry, and blood sugar lowering, heart is had to enhancing contractility, blood pressure is had to decline effect.Can treat vitiligo, proving thus to increase the melanin in body.

Black Fructus Mori: the liver and the kidney tonifying, nourishing blood to promote the production of body fluid, for diseases such as dizzy, tinnitus, blood deficiency, early whitening of hair, constipation; Control and quench one's thirst, sharp the five internal organs, joint, logical vim and vigour, clothes are not hungry for a long time, and spirit sedation, makes us clever, and poliosis becomes black hair, not old.

Black currant: contain abundant VC, VA, phosphorus, magnesium, ferrum, potassium, calcium, zinc, selenium, anthocyanidin, aldehydes matter, be easy to especially absorb.The health-care effect of the black currant of having known at present comprises prevention gout, anemia, edema, arthritis, rheumatism, oral disease, cough etc., and nutritive value is very high.Experiment conclusion proves: black currant has the effect that reduces Experimental Hyperlipemia lipid of mice.Black currant formal name used at school black currant, has another name called Ribes nigrum L., black bean fruit, and purple prunus mume (sieb.) sieb.et zucc., Saxifragales currant belongs to.Black currant is not only a kind of delicious flavour, nutritious fruit, and is to have multiple health preserving effect, as firm gingiva, the liver protecting, slow down aging, blood-enriching qi-invigorating, improve visual function and the anti-ageing effect of waiting for a long time.Mostly be alopecia the early stage that facts have proved poliosis, controls alopecia, supplements black currant concentrated solution after one month, and no longer alopecia, and the trend blackening that has grey hairs, prove that black currant has good hair care effect.

Auricularia: person " meat or fish in element " " meat in element " is the tonic that people know, and is the righting antasthenic of motherland's medical tradition, and modern medicine thinks, Auricularia is natural strong anticoagulant.The juice of Auricularia, mixes with containing hematoblastic blood plasma, and platelet loses cohesion, and this is due to the material that contains a kind of purine nucleosides in Auricularia, has anti-platelet aggregation effect.

Black thorn ant: contain 70 multiple nutrients materials, trace element and the multivitamins such as 18 seed amino acids, zinc, the endocrine regulation of scalable human body, activates internal organs, and liver, kidney disease are had to significant curative effect.

Flos Caryophylli: acrid in the mouth, hot in nature, its fragrance is dry, can control gastrofrigid vomiting, Deficiency and coldness of spleen and stomach, warming the kidney to activate YANG, impotence due to deficiency of the kidney, external application for curing carbuncle, newborn lump and detumescence effect, containing volatile oil, main component eugenol, acetyleugenol etc.Multiple pathogenic bacteria and fungus are had to inhibitory action.In we, mainly play osmotic absorption effect.

Cystine: i.e. CYSTINE, it is a kind of sulfur-containing amino acid, has a small amount of existence in protein, is contained in the keratin of hair, paw etc. more.Also can adopt synthetic method to obtain.Industrially from hair, extract, yield can reach 7.5-8%.What in actual production, have only reaches 5%.CYSTINE is the one of the aminoacid of needed by human, and it,, pharmaceutically with as nutrition enhancer, also for food industry, all has important value.It is mainly to extract from hair at present except available chemical synthesis makes.Human body is not had to ill effect.Purposes: for biochemistry and nutrient research, pharmaceutically have the oxidation of the body cell of promotion and reduction function, increase leukocyte and stop the effects such as pathogen growth.Be mainly used in various baldness.Also for the acute infectious disease such as dysentery, typhoid fever, influenza, asthma, neuralgia, eczema and various poisoning illness etc., and there is the effect of Protein requirement configuration.Cystine is amino acid drug, can promote cellular oxidation restoring function, makes liver function vigorous, and can neutralize a toxin, promote leucocyte hyperplasia, prevention pathogen to grow.

Mentholum: play refreshment, refrigerant effect in we.

Exocarpium Juglandis Immaturus and fresh leaf of Semen Juglandis: Exocarpium Juglandis Immaturus is also Exocarpium Juglandis Immaturum, useful this material among the people is squeezed the juice and is done dyestuff, can dye black especially to skin, is difficult for returning, and has just started jaundice, is then overstrike, finally becomes black; Among the people gathering when Semen Juglandis, peel off fresh Cortex walnut, causes skin to dye black, washes for a long time and does not fall, and after half a year, just can disappear; It is also very effective to hair dyeing, pure natural; In this formula, play the effect of dying that helps, after hair color element new life, it plays and makes the brighter effect with preventing and treating tinea capitis of Fa Genghei.Containing volatile oil, fatty acid, Semen Juglandis polysaccharide, juglone, juglansin, cupreol, nucin, Quercetin etc., wherein juglone is poisonous, but does not stay toxic and side effects, to people without injury.Exocarpium Juglandis Immaturus belongs to parts of generic medicinal plants, has heat-clearing and toxic substances removing, diuresis, remuval of damp and hot, detumescence, killing parasites for relieving itching effect; Sterilization aspect has one's own knack, especially the intestines and stomach inflammation, and the antibacterial of the intestines and stomach infects fine effect; Also can be used for chronic tracheitis, diarrhoea, dysentery, leucorrhea, conjunctival congestion, gynecological inflammation, conjunctivitis, external curing psoriasis, stubborn dermatitis, tinea capitis.Also have soothing the channels and quicking the network vessels, vessel softening and antitumaous effect.Useful branch of Semen Juglandis boiled egg among the people is treated cancer patient.

Herba Stellariae Alsines: useful this raw material among the people is squeezed the juice, paints the fingernails, and can paint a night afterwards, be difficult for fading, and the easy blackening of its juice gray-off poliosis, pure natural, nontoxic, existing hair dyeing application with the combination of Cortex walnut juice, more strengthens dying black effect in this formula.

Sodium lauryl sulfate: be used as detergent and emulsifying agent in this agent.

Stearic acid: be used as emollient in this agent.

Magnesium stearate: claim again magnesium octadecanate, sterling is white lightweight powdery, tasteless, is slightly soluble in water, is dissolved in hot ethanol.Meet strong acid and can resolve into stearic acid and corresponding magnesium salt.In this agent, be used as emollient and filler.

Ammonium chloride: be commonly called as Sal Ammoniacus, white crystal, easily deliquescence, water-soluble and glycerol, is slightly soluble in ethanol, in medical treatment, as expectorant, is used as washing assisant in this agent.

Benzoic acid: be used as antiseptic in this agent.

With after this agent hair washing, can not only make hair fluffy, shinny, pitch-black, high resilience, is easy to wash and dress molding, and can also enhance metabolism, melanin regeneration, comprehensively regulating, has a healthy hair color.

Hair washing test:

Select 20 to occur poliosis and more poliosis volunteer, between 30-50 year, men and women half and half, is divided into two groups, first group of 5 male 5 female, and everyone issues 2 bottles of this shampoos, every bottle of 400ml.Within 10 days, check once, first group of reflection, hair washing white hair overstrike on the rear same day, just becomes black for second day.Second group of reflection is unchanged.While reexamining after 20 days, first group of reflection, the poliosis of root is constantly longer, about 2mm left and right, blackening again after washing.Second group of reflection, poliosis still.After 30 days, when inspection, first group of situation is the same, and second group of situation is also the same.

After two first quarter moons, when unified inspection, first group of situation changes to some extent, except, when the poliosis at every turn growing can be washed rear blackening, its root of hair appearance hair color in various degree, account for greatly 30%, this has proved that this shampoo not only has illicit sexual relations black and white outbreak with (Cortex walnut juice and the effect of fingernail grass juice factor), also truly has and makes melanin regeneration effect, if adhere to using, can expand gradually hair color rate.And second group of situation is without any variation.

Sum up: by the multi-level extraction of raw material and compatibility, make its positive role of finally making a concerted effort to have brought into play black hair, and easily absorb, improved bioavailability, the Radix Glycyrrhizae finally adding, not only coordinates the property of medicine, also have removing toxic substances and toxin expelling effect, use safer.

Detailed description of the invention

Embodiment mono-

A, get Exocarpium Juglandis Immaturus 60% and the fresh leaf 40% of Semen Juglandis, pull an oar, filter with beater, obtain juice, collect for subsequent use;

C, get Semen Juglandis 20%, Semen Sesami Nigrum 60%, fresh Cacumen Platycladi 20% and mix oil expression, collect for subsequent usely, waste is managed elsewhere;

D, get Fructus Psoraleae 20%, Radix Polygoni Multiflori Preparata 20%, Herba Ecliptae 20%, Semen Cuscutae 20%, black Fructus Mori 20%, after pulverizing, use 90% ethanol, 100 DEG C of temperature are extracted 1h, filter; Second extraction 80% ethanol, extracts 1h to 90 DEG C of temperature of filtering residue, filters; Extract for three times and use 70% ethanol, 80 DEG C of temperature of filtering residue are extracted to 1h, filter; Merge three times extracting solution, 60 DEG C of concentrated 4h of temperature, collect ethanol, obtain concentrated solution, for subsequent use;

E, get black currant dry product 70%, Auricularia 30%, with d step method, extract and obtain concentrated solution, for subsequent use;

F, get black thorn ant 60%, Flos Caryophylli 40%, with d step method, extract and obtain concentrated solution, for subsequent use;

G, get the c step remaining waste that extracts oil, by the method for d step, extract and obtain concentrated solution, for subsequent use;

The juice 50% that h, the juice 50% of getting the acquisition of a step, b step obtain, for subsequent use after mixing;

The extraction concentrated solution 20% of the extraction concentrated solution 30% that i, the extraction concentrated solution 30% of getting the acquisition of d step, e step obtain, the extraction concentrated solution 20% that f step obtains, the acquisition of g step, mixes, for subsequent use;

The miscella 4% that j, the mixed liquor 20% of getting the acquisition of h step, c step obtain, mixed liquor 60%, cystine 14%, the Mentholum 2% that i step obtains, mix, for subsequent use;

Embodiment bis-

A, get Exocarpium Juglandis Immaturus 50% and the fresh leaf 50% of Semen Juglandis, pull an oar, filter with beater, obtain juice, collect for subsequent use;

C, get Semen Juglandis 30%, Semen Sesami Nigrum 40%, fresh Cacumen Platycladi 30%, mix oil expression, collect for subsequent usely, waste is managed elsewhere;

D, get Fructus Psoraleae 30%, Radix Polygoni Multiflori Preparata 15%, Herba Ecliptae 30%, Semen Cuscutae 10%, black Fructus Mori 15%, after pulverizing, use 90% ethanol, 100 DEG C of temperature are extracted 1h, filter; Second extraction 80% ethanol, extracts 1h to 90 DEG C of temperature of filtering residue, filters; Extract for three times and use 70% ethanol, 80 DEG C of temperature of filtering residue are extracted to 1h, filter; Merge three times extracting solution, 60 DEG C of concentrated 4h of temperature, collect ethanol, obtain concentrated solution, for subsequent use;

E, get black currant dry product 50%, Auricularia 50%, with d step method, extract and obtain concentrated solution, for subsequent use;

F, get black thorn ant 80%, Flos Caryophylli 20%, with d step method, extract and obtain concentrated solution, for subsequent use;

The juice 60% that h, the juice 40% of getting the acquisition of a step, b step obtain, for subsequent use after mixing;

The extraction concentrated solution 10% of the extraction concentrated solution 15% that i, the extraction concentrated solution 45% of getting the acquisition of d step, e step obtain, the extraction concentrated solution 30% that f step obtains, the acquisition of g step, mixes, for subsequent use;

The miscella 8% that j, the mixed liquor 10% of getting the acquisition of h step, c step obtain, mixed liquor 70%, cystine 9%, the Mentholum 3% that i step obtains, mix, for subsequent use;

Embodiment tri-

A, get Exocarpium Juglandis Immaturus 40% and the fresh leaf 60% of Semen Juglandis, pull an oar, filter with beater, obtain juice, collect for subsequent use;

C, get Semen Juglandis 40%, Semen Sesami Nigrum 20%, fresh Cacumen Platycladi 40%, mix oil expression, collect for subsequent usely, waste is managed elsewhere;

D, get Fructus Psoraleae 30%, Radix Polygoni Multiflori Preparata 10%, Herba Ecliptae 25%, Semen Cuscutae 25%, black Fructus Mori 10%, after pulverizing, use 90% ethanol, 100 DEG C of temperature are extracted 1h, filter; Second extraction 80%7 alcohol, extract 1h to 90 DEG C of temperature of filtering residue, filter; Extract for three times and use 70% ethanol, 80 DEG C of temperature of filtering residue are extracted to 1h, filter; Merge three times extracting solution, 60 DEG C of concentrated 4h of temperature, collect ethanol, obtain concentrated solution, for subsequent use;

E, get black currant dry product 60%, Auricularia 40%, with d step method, extract and obtain concentrated solution, for subsequent use;

F, get black thorn ant 70%, Flos Caryophylli 30%, with d step method, extract and obtain concentrated solution, for subsequent use;

The juice 40% that h, the juice 60% of getting the acquisition of a step, b step obtain, for subsequent use after mixing;

The extraction concentrated solution 15% of the extraction concentrated solution 20% that i, the extraction concentrated solution 50% of getting the acquisition of d step, e step obtain, the extraction concentrated solution 15% that f step obtains, the acquisition of g step, mixes, for subsequent use;

The miscella 10% that j, the mixed liquor 15% of getting the acquisition of h step, c step obtain, mixed liquor 61%, cystine 10%, the Mentholum 4% that i step obtains, mix, for subsequent use;

Claims

1. a preparation method for black currant hair color shampoo, its preparation process is: