CN105078850A - Liquid shampoo and preparation method thereof - Google Patents
Liquid shampoo and preparation method thereof Download PDFInfo
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- CN105078850A CN105078850A CN201510607003.6A CN201510607003A CN105078850A CN 105078850 A CN105078850 A CN 105078850A CN 201510607003 A CN201510607003 A CN 201510607003A CN 105078850 A CN105078850 A CN 105078850A
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Abstract
The invention discloses liquid shampoo and a preparation method thereof. The liquid shampoo comprises, by mass, 30-80 parts of black rice, 3-7 parts of lemon, 5-20 parts of pipal tree seeds, 3-10 parts of wild ginseng, 3-15 parts of tea seeds, 15-30 parts of saponin, 2-11 parts of platycodon grandiflorum, 2-10 parts of rhizoma anemarrhenae, 3-10 parts of polygonum multiflorum, 2-13 parts of fresh ginger, 2-18 parts of folium mori, 2-15 parts of angelica sinensis, 2-15 parts of saffron, 2-10 parts of coptis chinensis, 2-13 parts of lucid ganoderma, 2-10 parts of eclipta, 3-8 parts of medlar, 2-12 parts of astragalus membranaceus, 2-10 parts of ligusticum chuanxiong hort and 2-10 parts of aloe. The liquid shampoo is prepared according to the reasonable ratio, the effects of all the raw materials are remained, the synergistic interaction function is played through reasonable matching, and the liquid shampoo has the functions of hair cleaning, hair care, hair nourishing, hair reinforcing, hair loss preventing, hair generation, dandruff removal, itching relieving, radiation protection and dandruff generation prevention and the like.
Description
Technical field
The invention belongs to daily use chemicals product production technical field, be specifically related to a kind of shampoo and preparation method thereof.
Background technology
Cosmetics of everyday use refers to household chemicals, and be the scientific and technological chemicals that people commonly use on ordinary days, it comprises shampoo, bath gel, skin care item, treatment, cosmetics, detergent etc.Along with improving constantly of people's living standard, increasing to the demand of cosmetics of everyday use, also more and more higher to the requirement of quality, and the products such as cosmetics, shampoo, bath gel are the daily necessities that people commonly use, and long-term and contact skin, therefore wash protect product needed meet quality good, safe and reliable, any side effect must not be had, must not the requirements such as health be hindered.
Shampoo mostly in the market is petroleum hydrocarbon chemosynthesis raw material shampoo, this shampoo of life-time service, can cause the problems such as hair hair is dry, withered, fracture, bifurcated, but also can cause various subtle injury to health.So have can clean hair, improve hair quality, gentle non-stimulated, safety and environmental protection, nontoxic green natural shampoo is more and more subject to liking of consumer, also some the plant shampoo water containing plant component and the Chinese medicine shampoo containing Chinese medicine ingredients have been there is in the market, but they are only add certain plants composition or Chinese medicine ingredients in chemical raw material synthesis shampoo, still also containing multiple industrial chemicals, therefore do not tackle the problem at its root, and effect is not obvious, can not satisfy the demands of consumers completely.
Summary of the invention
The invention provides a kind of shampoo, not containing industrial chemicals composition, it is natural does not stimulate, and has well nursing to wash the effect of protecting to hair.
A kind of shampoo, in mass fraction, comprise following raw material: fructus zizaniae caduciflorae 30 ~ 80 parts, 3 ~ 7 parts, Fructus Citri Limoniae, the Fructus Sapindi Mukouossi 5 ~ 20 parts, wild ginseng 3 ~ 10 parts, camellia oleosa seed 3 ~ 15 parts, Fructus Gleditsia 15 ~ 30 parts, Radix Platycodonis 2 ~ 11 parts, the Rhizoma Anemarrhenae 2 ~ 10 parts, Radix Polygoni Multiflori 3 ~ 10 parts, 2 ~ 13 parts, Rhizoma Zingiberis Recens, 2 ~ 18 parts, Folium Mori, Radix Angelicae Sinensis 2 ~ 15 parts, 2 ~ 15 parts, Flos Carthami, Rhizoma Coptidis 2 ~ 10 parts, Ganoderma 2 ~ 13 parts, Herba Ecliptae 2 ~ 10 parts, Fructus Lycii 3 ~ 8 parts, the Radix Astragali 2 ~ 12 parts, Rhizoma Chuanxiong 2 ~ 10 parts, Aloe 2 ~ 10 parts.
The present invention is by combining plurality of Chinese plant component through rational proportion, and each component has respective effect, and its effect is as follows:
Fructus zizaniae caduciflorae: containing nutrients such as protein, carbohydrate, vitamin B group, vitamin E, starch, protein, can be the nutrition that hair provides abundant, wherein vitamin B group can help the pigment cell of hair to generate melanin, help hair blackening, anti-loss, and make pitch-black beautiful, the smooth pliable of hair.Containing alkaloid in its washing water of rice, and alkaloid is natural detergent, and therefore the washing water of rice of fructus zizaniae caduciflorae can well remove grease.
Fructus Citri Limoniae: containing abundant organic acid, there is very strong antioxidation and antitumaous effect, effectively can promote the metabolism of scalp, slow down aging, suppression pigmentation, in addition, also containing the abundant multiple nutritional components such as vitamin B1, B2, C in Fructus Citri Limoniae, can be the nutrition that hair provides abundant, with lemonade hair washing, can removing scurf and relieving itching, promote the growth promoter of hair.
The Fructus Sapindi Mukouossi: have another name called " Fructus Sapindi Mukouossi ", it has abundant Saponin, tyrosine etc., foaming abundancy is fine and smooth, dirt-removing power is strong, can effectively remove scalp oils and fats, be the best natural surfactant of cleaning capacity, also there is antibacterial, convergence pore, dispelling pathogenic wind for improving eyesight, anti-dandruff, antipruritic, anticreep, moisten scalp, make the effects such as the submissive light of hair.
Wild ginseng: it contains the abundant draft nutrient substance such as ginsenoside, phytoprotein, inorganic elements, multivitamin, alkaloid, growth and the reparation of damaged blood vessels neurocyte can be promoted, recover subcutaneous capillary cell viability, skin is reappeared ultimate attainment fine and smooth, abundant nutrition can also be provided for scalp and hair simultaneously, aminoacid wherein can effectively suppress pigment to run off, and prevention hair bleaches.The effects such as it also has heat clearing and damp drying, sterilizing and itch-relieving, Bergamot Mint Extract, dredging and convergence pore, remove skin endotoxin and impurity, antibacterial, antiinflammatory, antitumor, antiallergic.
Camellia oleosa seed: be rich in tea saponin, tea polyphenols, vitamin B and E.Vitamin B and E, very effective for folliculitis, seborrheic dermatitis, also can prevent scalp itch, tinea etc.Tea polyphenols can radioprotective, give protection against cancer, be a kind of natural antiseptic.Tea saponin has antibacterial and antioxidation.Life-time service have only bits, antipruritic, deoil, effect of the damaged hair that sterilizes, repairs, also having obvious black hair, hair regrowth, is one of cleaning agent of the Nature the best.
Fructus Gleditsia: be rich in saponin, effects such as there is good decontamination, the hair follicle except oils and fats, unobstructed blocking, anti-dandruff, antipruritic, smooth, black hair, hair care, anticreep, promotion hair restoration, promote scalp blood circulation, clearing away heat and eliminating dampness, invigorate blood circulation.Impaired hair quality and scalp problems can be helped improve, maintenance hair.
Radix Platycodonis: be rich in saponin, has good decontamination, except the hair follicle of oils and fats, antipruritic, antiinflammatory, blood circulation promoting, unobstructed blocking and heat clearing away, antipyretic effect.
The Rhizoma Anemarrhenae: main containing saponin, rhizome, containing total saponins about 6%, has good decontamination, except oils and fats ability, has nourishing YIN to lower pathogenic fire relieving restlessness in addition, heat clearing away removes the effects such as cold.
Radix Polygoni Multiflori: after hair is blood, hemapodium is then sent out, and Radix Polygoni Multiflori can promote human body hemopoietic function, and again containing abundant vitamin, aminoacid, emodin and lecithin etc., can moisten scalp hair follicles, promote melanic generation.Shampoo coordinates Radix Polygoni Multiflori to strengthen hair quality, makes hair more powerful, closeer, more black, can promote the new regeneration sent out.
Rhizoma Zingiberis Recens: have induce sweat, disperse, warming the lung to resolve fluid-retention, recuperating depleted YANG are promoted blood circulation, effects such as cold relieving of invigorating blood circulation, and can increase blood circulation in addition, hair follicle stimulating is opened, and impel hair regeneration, close hair strengthening.Scalp is unhealthy, is because epidermis gets clogged mostly, after cleaning up, mixes blood circulation, metabolism that Rhizoma Zingiberis Recens can accelerate scalp, thus promote the growth of hair follicle.
Folium Mori: the effect with clearing heat and removing internal wetness, well can improve the damp and hot symptom of scalp, promote growing up healthy and sound of hair follicle, reach salubrious object.
Radix Angelicae Sinensis: be that one is enriched blood the good Chinese medicine of effect of invigorating blood circulation, have promoting blood circulation and stopping pain, moisturize the effect such as laxation, dredging the meridian, can be hair growth with Radix Angelicae Sinensis hair washing and reduces the heavy burdens, and makes hair soft light, is easy to combing, and can promotes natural on-off cycles of hair growth.
Flos Carthami: have promoting blood circulation to restore menstrual flow, can more easily grow by be obstructed passage, fine hair of blood circulation promoting, cleaning.
Rhizoma Coptidis: people's alopecia, is because have asthenic fire in body, and attacks.Adapted Rhizoma Coptidis, can help reducing internal heat, reach clearing heat and removing internal wetness, makes scalp pure and fresh no longer greasy.
Herba Ecliptae: enriching yin and nourishing kidney, has black hair, hair growth promoting effect.
Fructus Lycii: nourishing the liver and kidney, beneficial intensive culture blood, anticreep alopecia-stopping.
The Radix Astragali: invigorating vital QI, makes hair dense.
Rhizoma Chuanxiong: blood-activating and qi-promoting, improves scalp blood circulation.
Aloe: have the effects such as moisturizing antiinflammatory, can make hair keep moistening smooth, pre-Anti-hair loss.
Shampoo of the present invention can deep layer cleaning hair and scalp, improves hair greasy, effectively can remove dandruff, anti-antidandruff regeneration; The expansible scalp blood capillary of its Chinese medicine ingredients, promotes scalp blood circulation, activates hair follicle cell, strong hair internal structure, consolidates root of hair, promotes that hair healthy is grown up, improper alopecia can be prevented, the nutrient required for hair can be supplemented in addition, nourish layer by layer, deeply send out core and scalp, repair disrupted tissue, give hair healthy vigor, recover hair elastic force and gloss, make hair pitch-black glossy.
As preferably, in mass fraction, comprise following raw material: fructus zizaniae caduciflorae 40 ~ 80 parts, 4 ~ 7 parts, Fructus Citri Limoniae, the Fructus Sapindi Mukouossi 7 ~ 20 parts, wild ginseng 4 ~ 10 parts, camellia oleosa seed 5 ~ 15 parts, Fructus Gleditsia 20 ~ 30 parts, Radix Platycodonis 4 ~ 11 parts, the Rhizoma Anemarrhenae 4 ~ 10 parts, Radix Polygoni Multiflori 4 ~ 10 parts, 4 ~ 13 parts, Rhizoma Zingiberis Recens, 5 ~ 18 parts, Folium Mori, Radix Angelicae Sinensis 4 ~ 15 parts, 4 ~ 15 parts, Flos Carthami, Rhizoma Coptidis 3 ~ 10 parts, Ganoderma 5 ~ 13 parts, Herba Ecliptae 4 ~ 10 parts, Fructus Lycii 4 ~ 8 parts, the Radix Astragali 5 ~ 12 parts, Rhizoma Chuanxiong 5 ~ 10 parts, Aloe 3 ~ 10 parts.
Present invention also offers the preparation method of above-mentioned shampoo, comprise the following steps:
(1) described raw material is distinguished dry, pulverizing, excessively 20 ~ 50 mesh sieves, obtain material powder;
(2), after fructus zizaniae caduciflorae powder is soaked, repeatedly wash by rubbing with the hands, finally filter out fructus zizaniae caduciflorae powder and obtain washing water of rice;
(3) Mulberry Leaf, saffron powder, Golden Thread, Fructus Lycii powder, Radix Astragali powder, Rhizoma Chuanxiong powder, Fructus Citri Limoniae powder, Rhizoma Zingiberis Recens powder and Alose mix homogeneously are obtained mixed-powder, mixed-powder is added in dehydrated alcohol and soak 1 ~ 1.5h, filter after supersound extraction and obtain just extract, finally first extract is concentrated into till dehydrated alcohol all removes, obtains the first extracting solution;
(4) Fructus Sapindi Mukouossi powder, wild ginseng powder, camellia oleosa seed powder, Fructus Gleditsia powder, Platycodon Root and Common Anemarrhena Rhizome mix homogeneously are obtained mixed-powder, mixed-powder is added in described washing water of rice and soak 1 ~ 2h, decoct after immersion, filter after decoction, finally filtration gained filtrate is concentrated into 1/3 ~ 1/2 of filtrate volume, obtains the second extracting solution;
(5) described washing water of rice and dehydrated alcohol are mixed homogeneously and obtained mixed liquor in 1 ~ 2:1 ~ 3 by volume, by the mixed-powder obtained after Radix Polygoni Multiflori powder, Chinese Angelica Root, Herba Ecliptae powder, REISH mix homogeneously, mixed-powder is added in described mixed liquor and soak 1 ~ 3h, after immersion at 40 ~ 60 DEG C supersound extraction 18 ~ 24h, filter and retain filtrate, finally filtrate is concentrated into till dehydrated alcohol all removes, obtains the 3rd extracting solution;
(6) the first extracting solution, the second extracting solution and the 3rd extracting solution mix homogeneously can be obtained described shampoo.
Mode dry in the present invention can have multiple, be not destroyed to make the constituent of raw material inside, as preferably, adopt the mode of dry in the sun to carry out drying described in described step (1) during raw material drying, or by raw material 50 ~ 80 DEG C dry to moisture lower than 5 ~ 10%.
In order to fully extract the effective ingredient in raw material, the present invention repeatedly repeats to extract to raw material, as preferably, in described step (2), fructus zizaniae caduciflorae powder being added quality is fructus zizaniae caduciflorae powder quality 30 ~ 40 times, and water temperature is soak 0.5 ~ 1h in the deionized water of 40 ~ 60 DEG C, after repeatedly washing by rubbing with the hands, filter out fructus zizaniae caduciflorae powder and obtain first-time filtrate, and then in the fructus zizaniae caduciflorae powder filtered out, add the deionized water that quality is fructus zizaniae caduciflorae powder quality 20 ~ 30 times, after repeatedly washing by rubbing with the hands, filtration obtains secondary filtrate, repeat aforesaid operations, add the deionized water that quality is fructus zizaniae caduciflorae powder quality 10 ~ 20 times, after repeatedly washing by rubbing with the hands, filtration obtains three filtrates, finally by first-time filtrate, described washing water of rice is obtained after secondary filtrate and three filtrate mix homogeneously.
As preferably, in described step (3), mixed-powder being added quality is soak 1h in the dehydrated alcohol of mixed-powder quality 1:30 ~ 40 times, supersound extraction 48 ~ 60h at normal temperatures, filtration obtains first-time filtrate, the dehydrated alcohol that quality is mixed-powder quality 1:20 ~ 30 times is added again in mixed-powder, supersound extraction 24 ~ 48 hours at normal temperatures, filtration obtains secondary filtrate, repeat aforesaid operations, add the dehydrated alcohol that quality is mixed-powder quality 10 ~ 20 times, supersound extraction 12 ~ 24 hours at normal temperatures, filtration obtains three filtrates, finally by first-time filtrate, secondary filtrate and three filtrate mix homogeneously obtain just extract and are finally concentrated into by first extract till dehydrated alcohol all removes.
As preferably, mixed-powder adds quality in described step (4) is soak 1h in the washing water of rice of mixed-powder quality 1:30 ~ 40 times, after immersion, first decoct 0.3 ~ 0.5h with little fire, 2 ~ 4h is decocted again with big fire, after decoction completes, filtration obtains first-time filtrate, the washing water of rice that quality is mixed-powder quality 1:20 ~ 30 times is added again in mixed-powder, repeat the process of described decoction, filtration obtains secondary filtrate, the washing water of rice that quality is mixed-powder quality 1:10 ~ 20 times is added again in mixed-powder, repeat described decoction process, filtration obtains three filtrates, finally by first-time filtrate, after secondary filtrate and three filtrate mix homogeneously after vacuum concentration to mixing cumulative volume 1/2.
As preferably, in described step (5), the volume ratio of washing water of rice and dehydrated alcohol is 1:1.
As preferably, in described step (5), the mass ratio of mixed liquor and mixed-powder is 1:10 ~ 30, and described concentrated method is concentrating under reduced pressure.
Compared with prior art, beneficial effect of the present invention is mainly reflected in:
(1) the present invention is through rational proportion, material composition combination is prepared shampoo of the present invention, shampoo of the present invention not only remains effect of respective material composition, and pass through reasonable preparation, serve the effect of Synergistic, integrate clean, hair care, hair care, hair strengthening, anticreep, hair growth promoting, anti-dandruff, antipruritic, radioprotective, prevention dandruff the effect such as to grow.
(2) all the components of the present invention is natural plant composition, and without any chemical addition agent, safety and Health, not polluted source, be conducive to environmental conservation.
(3) scope of application of the present invention is comparatively wide, and especially applicable fat secretion is too much, head pruritus, dandruff, scalp pomade puzzlement crowd; Dry withered and yellow, the alopecia of hair hair, disconnected loss of hairs send out crowd serious; Dye is scalded and is badly damaged and malnutrition hair quality crowd.
Detailed description of the invention
Embodiment 1
The present embodiment Raw is composed as follows:
Fructus zizaniae caduciflorae 80 parts, 3 parts, Fructus Citri Limoniae, the Fructus Sapindi Mukouossi 14 parts, wild ginseng 4 parts, camellia oleosa seed 5 parts, Fructus Gleditsia 20 parts, Radix Platycodonis 4 parts, the Rhizoma Anemarrhenae 4 parts, Radix Polygoni Multiflori 5 parts, 3 parts, Rhizoma Zingiberis Recens, 4 parts, Folium Mori, Radix Angelicae Sinensis 4 parts, 3 parts, Flos Carthami, Rhizoma Coptidis 5 parts, Ganoderma 4 parts, Herba Ecliptae 4 parts, Fructus Lycii 4 parts, the Radix Astragali 3 parts, Rhizoma Chuanxiong 3 parts, Aloe 3 parts.
The preparation method of the shampoo of the present embodiment is as follows:
(1) respectively by after above-mentioned raw materials difference routinely screening, selecting crude drugs with winnower remove impurity, dry or 50 ~ 80 DEG C dry to moisture lower than 5 ~ 10%, take out afterwards and be placed in cooling in drying baker, then pulverize with pulverizer, cross 20 ~ 50 object sieves, obtain material powder, store in dark dry place, for subsequent use.
(2) fructus zizaniae caduciflorae powder being added quality is fructus zizaniae caduciflorae powder quality 30 times, and water temperature is soak 0.5 ~ 1h in the deionized water of 40 ~ 60 DEG C, after repeatedly washing by rubbing with the hands, filter out fructus zizaniae caduciflorae powder and obtain first-time filtrate, and then in fructus zizaniae caduciflorae powder, add the deionized water that quality is fructus zizaniae caduciflorae powder quality 20 times, after repeatedly washing by rubbing with the hands, filtration obtains secondary filtrate, the deionized water that quality is fructus zizaniae caduciflorae powder quality 10 times is added again in fructus zizaniae caduciflorae powder, after repeatedly washing by rubbing with the hands, filtration obtains three filtrates, finally by first-time filtrate, washing water of rice is obtained after secondary filtrate and three filtrate mix homogeneously, place 24 hours, store for future use,
(3) by Mulberry Leaf, saffron powder, Golden Thread, Fructus Lycii powder, Radix Astragali powder, Rhizoma Chuanxiong powder, Fructus Citri Limoniae powder, Rhizoma Zingiberis Recens powder and Alose mix homogeneously obtain mixed-powder, mixed-powder being added quality is soak 1h in the dehydrated alcohol of mixed-powder quality 1:30 ~ 40 times, supersound extraction 48 ~ 60h at normal temperatures, filtration obtains first-time filtrate, the dehydrated alcohol that quality is mixed-powder quality 1:20 ~ 30 times is added again in mixed-powder, supersound extraction 24 ~ 48 hours at normal temperatures, filtration obtains secondary filtrate, repeat aforesaid operations, add the dehydrated alcohol that quality is mixed-powder quality 10 ~ 20 times, supersound extraction 12 ~ 24 hours at normal temperatures, filtration obtains three filtrates, finally by first-time filtrate, secondary filtrate and three filtrate mix homogeneously obtain just extract, finally first extract is concentrated into till dehydrated alcohol all removes, obtain the first extracting solution,
(4) by Fructus Sapindi Mukouossi powder, wild ginseng powder, camellia oleosa seed powder, Fructus Gleditsia powder, Platycodon Root and Common Anemarrhena Rhizome mix homogeneously obtain mixed-powder, it is soak 1h in the washing water of rice of mixed-powder quality 1:30 ~ 40 times that mixed-powder adds quality, after immersion, first decoct 0.3 ~ 0.5h with little fire, 2 ~ 4h is decocted again with big fire, after decoction completes, filtration obtains first-time filtrate, the washing water of rice that quality is mixed-powder quality 1:20 ~ 30 times is added again in mixed-powder, repeat the process of described decoction, filtration obtains secondary filtrate, the washing water of rice that quality is mixed-powder quality 1:10 ~ 20 times is added again in mixed-powder, repeat described decoction process, filtration obtains three filtrates, finally by first-time filtrate, after secondary filtrate and three filtrate mix homogeneously after vacuum concentration to mixing cumulative volume 1/2, obtain the second extracting solution,
(5) by described washing water of rice and dehydrated alcohol by volume 1:1 mix homogeneously and obtain mixed liquor, by the mixed-powder obtained after Radix Polygoni Multiflori powder, Chinese Angelica Root, Herba Ecliptae powder, REISH mix homogeneously, mixed-powder is added in described mixed liquor and soak 1 ~ 3h, wherein the mass ratio of mixed liquor and mixed-powder is 1:10 ~ 30, after immersion at 40 ~ 60 DEG C supersound extraction 18 ~ 24h, filter and retain filtrate, finally by filtrate till being evaporated to dehydrated alcohol and all removing, obtain the 3rd extracting solution;
(6) the first extracting solution, the second extracting solution and the 3rd extracting solution mix homogeneously can be obtained shampoo of the present invention.
Embodiment 2
The present embodiment Raw is composed as follows:
Fructus zizaniae caduciflorae 60 parts, 5 parts, Fructus Citri Limoniae, the Fructus Sapindi Mukouossi 3 parts, wild ginseng 4 parts, camellia oleosa seed 5 parts, Fructus Gleditsia 18 parts, Radix Platycodonis 6 parts, the Rhizoma Anemarrhenae 6 parts, Radix Polygoni Multiflori 8 parts, 9 parts, Rhizoma Zingiberis Recens, 6 parts, Folium Mori, Radix Angelicae Sinensis 8 parts, Flos Carthami spend 8 parts, Rhizoma Coptidis 7 parts, Ganoderma 6 parts, Herba Ecliptae 5 parts, Fructus Lycii 8 parts, the Radix Astragali 5 parts, Rhizoma Chuanxiong 7 parts, Aloe 5 parts.
The preparation method of the shampoo of the present embodiment is identical with embodiment 1.
Embodiment 3
The present embodiment Raw is composed as follows:
Fructus zizaniae caduciflorae 50 parts, 8 parts, Fructus Citri Limoniae, the Fructus Sapindi Mukouossi 10 parts, wild ginseng 8 parts, camellia oleosa seed 10 parts, Fructus Gleditsia 12 parts, Radix Platycodonis 8 parts, the Rhizoma Anemarrhenae 8 parts, Radix Polygoni Multiflori 6 parts, 4 parts, Rhizoma Zingiberis Recens, 7 parts, Folium Mori, Radix Angelicae Sinensis 5 parts, Flos Carthami spend 5 parts, Rhizoma Coptidis 8 parts, Ganoderma 7 parts, Herba Ecliptae 4 parts, Fructus Lycii 4 parts, the Radix Astragali 6 parts, Rhizoma Chuanxiong 4 parts, Aloe 6 parts.
The preparation method of the shampoo of the present embodiment is identical with embodiment 1.
Embodiment 1 ~ 3 prepares shampoo through relevant physical and chemical inspection, and result all shows: noxious substance arsenic, lead, hydrargyrum all do not detect; Excrement colibacillus group, Pseudomonas aeruginosa and staphylococcus aureus all do not detect; Total plate count < 10CFU/ml; Yeast and mold sum < 10CFU/ml.Keep 24h in (40 ± 1) DEG C, return to after room temperature all without lamination; Keep 24h in (-8 ± 2) DEG C, return to after room temperature all without lamination; Foam (40 DEG C) >=80mm, each index all meets the requirement of shampoo (GB/T29679-2013) and " cosmetics health specification " version specification in 2007.
Shampoo of the present invention is through relevant toxicology test, and rinse through acute ocular irritation test (30s), result is nonirritant; Through acute skin irritation test, result display nonirritant; Through skin Phototoxicity experiment, result is shown as and has no skin phototoxicity; Through Skin allergy test, result is indicated as and has no skin allergic reaction.
Select 100 triers, use the shampoo that on market, the good shampoo of a certain sales volume and the embodiment of the present invention 1 ~ 3 prepare, use every three days once, use 10 times respectively, finally to each kind shampoo carry out evaluation marking, table 1 for evaluation score average after result.
Table 1 trier is to the in-service evaluation used after the present embodiment 1 ~ 3 and existing market product
| Detection of content | Embodiment 1 | Embodiment 2 | Embodiment 3 | Existing market product |
| Cleaning effect (20 points) | 20 | 20 | 20 | 19.9 |
| Scalp comfort level (20 points) | 19.7 | 19.7 | 19.8 | 16.6 |
| Hair quality degree of improvement (20 points) | 18.9 | 19.3 | 19.2 | 15.2 |
| Fragrance delicate fragrance degree (20 points) | 19.3 | 19.4 | 19.2 | 16.1 |
| Total score (80 points) | 77.9 | 78.6 | 77.8 | 67.8 |
Claims (9)
1. a shampoo, it is characterized in that, in mass fraction, comprise following raw material: fructus zizaniae caduciflorae 30 ~ 80 parts, 3 ~ 7 parts, Fructus Citri Limoniae, the Fructus Sapindi Mukouossi 5 ~ 20 parts, wild ginseng 3 ~ 10 parts, camellia oleosa seed 3 ~ 15 parts, Fructus Gleditsia 15 ~ 30 parts, Radix Platycodonis 2 ~ 11 parts, the Rhizoma Anemarrhenae 2 ~ 10 parts, Radix Polygoni Multiflori 3 ~ 10 parts, 2 ~ 13 parts, Rhizoma Zingiberis Recens, 2 ~ 18 parts, Folium Mori, Radix Angelicae Sinensis 2 ~ 15 parts, 2 ~ 15 parts, Flos Carthami, Rhizoma Coptidis 2 ~ 10 parts, Ganoderma 2 ~ 13 parts, Herba Ecliptae 2 ~ 10 parts, Fructus Lycii 3 ~ 8 parts, the Radix Astragali 2 ~ 12 parts, Rhizoma Chuanxiong 2 ~ 10 parts, Aloe 2 ~ 10 parts.
2. shampoo as claimed in claim 1, it is characterized in that, in mass fraction, comprise following raw material: fructus zizaniae caduciflorae 40 ~ 80 parts, 4 ~ 7 parts, Fructus Citri Limoniae, the Fructus Sapindi Mukouossi 7 ~ 20 parts, wild ginseng 4 ~ 10 parts, camellia oleosa seed 5 ~ 15 parts, Fructus Gleditsia 20 ~ 30 parts, Radix Platycodonis 4 ~ 11 parts, the Rhizoma Anemarrhenae 4 ~ 10 parts, Radix Polygoni Multiflori 4 ~ 10 parts, 4 ~ 13 parts, Rhizoma Zingiberis Recens, 5 ~ 18 parts, Folium Mori, Radix Angelicae Sinensis 4 ~ 15 parts, 4 ~ 15 parts, Flos Carthami, Rhizoma Coptidis 3 ~ 10 parts, Ganoderma 5 ~ 13 parts, Herba Ecliptae 4 ~ 10 parts, Fructus Lycii 4 ~ 8 parts, the Radix Astragali 5 ~ 12 parts, Rhizoma Chuanxiong 5 ~ 10 parts, Aloe 3 ~ 10 parts.
3. the preparation method of the shampoo as described in as arbitrary in claim 1 ~ 2, is characterized in that, comprise the following steps:
(1) described raw material is distinguished dry, pulverizing, excessively 20 ~ 50 mesh sieves, obtain material powder;
(2), after fructus zizaniae caduciflorae powder is soaked, repeatedly wash by rubbing with the hands, finally filter out fructus zizaniae caduciflorae powder and obtain washing water of rice;
(3) Mulberry Leaf, saffron powder, Golden Thread, Fructus Lycii powder, Radix Astragali powder, Rhizoma Chuanxiong powder, Fructus Citri Limoniae powder, Rhizoma Zingiberis Recens powder and Alose mix homogeneously are obtained mixed-powder, mixed-powder is added in dehydrated alcohol and soak 1 ~ 1.5h, filter after supersound extraction and obtain just extract, finally first extract is concentrated into till dehydrated alcohol all removes, obtains the first extracting solution;
(4) Fructus Sapindi Mukouossi powder, wild ginseng powder, camellia oleosa seed powder, Fructus Gleditsia powder, Platycodon Root and Common Anemarrhena Rhizome mix homogeneously are obtained mixed-powder, mixed-powder is added in described washing water of rice and soak 1 ~ 2h, decoct after immersion, filter after decoction, finally filtration gained filtrate is concentrated into 1/3 ~ 1/2 of filtrate volume, obtains the second extracting solution;
(5) described washing water of rice and dehydrated alcohol are mixed homogeneously and obtained mixed liquor in 1 ~ 2:1 ~ 3 by volume, by the mixed-powder obtained after Radix Polygoni Multiflori powder, Chinese Angelica Root, Herba Ecliptae powder, REISH mix homogeneously, mixed-powder is added in described mixed liquor and soak 1 ~ 3h, after immersion at 40 ~ 60 DEG C supersound extraction 18 ~ 24h, filter and retain filtrate, finally filtrate is concentrated into till dehydrated alcohol all removes, obtains the 3rd extracting solution;
(6) the first extracting solution, the second extracting solution and the 3rd extracting solution mix homogeneously can be obtained described shampoo.
4. the preparation method of shampoo as claimed in claim 3, it is characterized in that, adopt the mode of dry in the sun to carry out drying described in described step (1) during raw material drying, or raw material is dried at 50 ~ 80 DEG C to moisture content of raw material lower than 5 ~ 10%.
5. the preparation method of shampoo as claimed in claim 3, it is characterized in that, in described step (2), fructus zizaniae caduciflorae powder being added quality is fructus zizaniae caduciflorae powder quality 30 ~ 40 times, and water temperature is soak 0.5 ~ 1h in the deionized water of 40 ~ 60 DEG C, after repeatedly washing by rubbing with the hands, filter out fructus zizaniae caduciflorae powder and obtain first-time filtrate, and then in the fructus zizaniae caduciflorae powder filtered out, add the deionized water that quality is fructus zizaniae caduciflorae powder quality 20 ~ 30 times, after repeatedly washing by rubbing with the hands, filtration obtains secondary filtrate, repeat aforesaid operations, add the deionized water that quality is fructus zizaniae caduciflorae powder quality 10 ~ 20 times, after repeatedly washing by rubbing with the hands, filtration obtains three filtrates, finally by first-time filtrate, described washing water of rice is obtained after secondary filtrate and three filtrate mix homogeneously.
6. the preparation method of shampoo as claimed in claim 3, it is characterized in that, in described step (3), mixed-powder being added quality is soak 1h in the dehydrated alcohol of mixed-powder quality 1:30 ~ 40 times, supersound extraction 48 ~ 60h at normal temperatures, filtration obtains first-time filtrate, the dehydrated alcohol that quality is mixed-powder quality 1:20 ~ 30 times is added again in mixed-powder, supersound extraction 24 ~ 48 hours at normal temperatures, filtration obtains secondary filtrate, repeat aforesaid operations, add the dehydrated alcohol that quality is mixed-powder quality 10 ~ 20 times, supersound extraction 12 ~ 24 hours at normal temperatures, filtration obtains three filtrates, finally by first-time filtrate, secondary filtrate and three filtrate mix homogeneously obtain just extract, finally first extract is concentrated into till dehydrated alcohol all removes.
7. the preparation method of shampoo as claimed in claim 3, it is characterized in that, mixed-powder adds quality in described step (4) is soak 1h in the washing water of rice of mixed-powder quality 1:30 ~ 40 times, after immersion, first decoct 0.3 ~ 0.5h with little fire, 2 ~ 4h is decocted again with big fire, after decoction completes, filtration obtains first-time filtrate, the washing water of rice that quality is mixed-powder quality 1:20 ~ 30 times is added again in mixed-powder, repeat the process of described decoction, filtration obtains secondary filtrate, the washing water of rice that quality is mixed-powder quality 1:10 ~ 20 times is added again in mixed-powder, repeat described decoction process, filtration obtains three filtrates, finally by first-time filtrate, after secondary filtrate and three filtrate mix homogeneously after vacuum concentration to mixing cumulative volume 1/2.
8. the preparation method of shampoo as claimed in claim 3, is characterized in that, in described step (5), the volume ratio of washing water of rice and dehydrated alcohol is 1:1.
9. the preparation method of shampoo as claimed in claim 3, is characterized in that, in described step (5), the mass ratio of mixed liquor and mixed-powder is 1:10 ~ 30, and described concentrated method is concentrating under reduced pressure.
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