CN107693419A - Nourish moisturizing camellia oleifera fruit shower cream and preparation method thereof - Google Patents
Nourish moisturizing camellia oleifera fruit shower cream and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
One kind nourishes moisturizing camellia oleifera fruit shower cream, in terms of mass fraction, is made up of following component:50 60 parts of deionized water, 10 15 parts of sodium lauroyl glutamate, 5 10 parts of Cocoamidopropyl betaine, 5 10 parts of sodium alkyl sulfate, 25 parts of APG, 28 42 parts of camellia oleifera fruit emulsion, 24 parts of glycerine, 0.8 1.2 parts of EGDS, 0.05 0.1 parts of disodium ethylene diamine tetraacetate, 1.5 3 parts of trehalose, 735 parts of polyquaternium, 12 parts of salt, 0.1 0.5 parts of essence, 0.05 0.1 parts of Kathon CG.The nourishing moisturizing camellia oleifera fruit shower cream uses raw material based on fresh tea fruit pulp, and rich in materials such as camellia oil, Tea Saponin, tea polysaccharide, tea albumen, flavones, being re-dubbed shower cream has extraordinary moist reparation skin effect.
Description
Technical field
It is particularly a kind of to nourish moisturizing camellia oleifera fruit shower cream the present invention relates to a kind of shower cream.
Background technology
Squeezed the juice using fresh tea fruit and extract tea oil and tea fruit juice in tea fruit, retain Tea Saponin, tea polysaccharide, tea egg in tea fruit
In vain, the material such as flavones, this stability is high, the high emulsion of nutritional ingredient, in the exploitation applied to all kinds of cosmetics, have non-
Often good skin nursing effect.
The content of the invention
An object of the present invention be to provide it is a kind of nourish moisturizing camellia oleifera fruit shower cream, by tea fruit latex composite compounding into nourishing
The camellia oleifera fruit shower cream of moisturizing, rich in materials such as camellia oil, tea polysaccharide, starch, Tea Saponins, have to skin and very strong go deep into skin
Moisturizing effect, cleaning effect effect, are a kind of good cosmetics.
The second object of the present invention is the preparation method for providing above-mentioned camellia oleifera fruit shower cream.
The technical scheme is that:One kind nourishes moisturizing camellia oleifera fruit shower cream, in terms of weight fraction, by following component system
Into:Deionized water 50-60 parts, sodium lauroyl glutamate 10-15 parts, Cocoamidopropyl betaine 5-10 parts, sodium alkyl sulfate
5-10 parts, APG 2-5 parts, camellia oleifera fruit emulsion 28-42 parts, glycerine 2-4 parts, EGDS 0.8-1.2 parts, second
Edetate disodium 0.05-0.1 parts, trehalose 1.5-3 parts, the 3-5 of polyquaternium -7 parts, salt 1-2 parts, essence 0.1-
0.5 part, Kathon CG 0.05-0.1 parts.
Wherein described sodium alkyl sulfate preferably sodium dodecyl sulfate.
The preferred APG0810 of wherein described APG.
Preferably, described camellia oleifera fruit emulsion preparation method is as follows:
(1)Selection:Selection just harvesting, fresh full camellia oleifera fruit;
(2)De- shell:By step(1)Gained camellia oleifera fruit machinery peels off, and removes shell, obtains fresh tea seed;
(3)Clean:By step(2)Gained tea seed removes solid impurity;
(4)Washing:By step(3)Gained tea seed is washed, and after removing spot, obtains clean tea seed;
(5)Crush:By step(4)Gained tea seed puts into pulverizer, obtains tea seed particle, moisture 40-60%;
(6)Split-phase:By step(5)Gained tea seed particle puts into juice extractor, and extruding obtains solid fiber powder and serum;
(7)Purification:By step(6)Gained serum is transported in retort, and pH is adjusted to 3.5-4, adds acid protease, water-bath
It is heated to 50-60 DEG C, after 20-30min, adds activated carbon of sorbent or atlapulgite, 20 DEG C -40 DEG C of temperature, mixing time 20-
30 minutes, mixing speed was 20-60 revs/min, adds the 1-6% super-cells of serum weight, passes through leaf-type filter mistake
Filter, obtain clarification camellia oleifera fruit emulsion.
Preferably, step(7)The dosage of middle adsorbent and the weight ratio of serum are 2-4:100.
Step(7)Described in acid protease and the weight ratio of serum be(0.1-4):1000.
Preferably, step(7)Described acid protease is that the excellent Aspergillus usamii of seed selection is made through depth fermentation.
Preferably, step(5)The crusher sifting aperture 2-10 millimeters, pulverized particles are less than 1 millimeter, moisture 40-
60%;Squeeze the juice well.
Preferably, step(6)The juice extractor squeezes 0.1 millimeter ~ 1 millimeter of gap, carries out separation of solid and liquid well.
The preparation method of the present invention for nourishing moisturizing camellia oleifera fruit shower cream in turn includes the following steps:
(1)It is prewired:Camellia oleifera fruit emulsion is heated to 50-80 DEG C, is proportionally added into sodium lauroyl glutamate, cocamidopropyl propyl amide sweet tea
Dish alkali, sodium alkyl sulfate, APG, EGDS, disodium ethylene diamine tetraacetate, heating stirring, mixing time
For 20-30 minutes, mixing speed is 20-60 revs/min, obtains fusions;
(2)Emulsification:In step(1)In, glycerol adding, trehalose, polyquaternium -7, ionized water, stirring, mixing time are in proportion
20-30 minutes, mixing speed are 50-80 revs/min, obtain primary emulsifying thing;
(3)Shaping:In step(2)The primary emulsifying thing of gained squeezes into homogenizer, perfuming essence, Kathon CG, salt, homogeneous 10-30 minutes,
Obtain and nourish moisturizing camellia oleifera fruit shower cream.
The beneficial effects of the present invention are:
(1)This method processing step is simple, effectively desensitization, the characteristics of warm camellia oleifera fruit and other plant juice all components, shape
Into the technology of stabilising system;
(2)It is a kind of natural, stable liquid of emulsification fusion that gained, which nourishes moisturizing camellia oleifera fruit shower cream, more rich in camellia oil, tea
The materials such as sugar, starch, Tea Saponin, have to skin it is very strong go deep into skin moisturizing effect, cleaning effect effect, be it is a kind of well
Cosmetic material.
Primary raw material used in the present invention is described as follows:
Camellia oleifera fruit:It is the fruit of tea oil tree, tea oil tree is the main woody oleiferous plants tree in China, is described as " east tree ", belongs to camellia
Section's Camellia evergreen dungarunga, it is the distinctive woody vegetable oil resource in China, 3-6 meters of the height of tree, the diameter of a cross-section of a tree trunk 1.3 meters above the ground is up to 24-30 lis
Rice, smooth bark is taupe;Tea oil tree list leaf alternate, flower are both sexes white, and October, Post flowering was until fruit between October next year
Can be ripe, therefore, tea oil tree has rare flowers and fruits homophyletic phenomenon.Fruit is capsule, is mostly ellipse, has fine, soft fur, seed
Mostly yellowish-brown, glossy, triangular shape, tea oil tree are grown in remote mountains, inhale natural nutrient to the greatest extent, evergreen longevity, the age of tree up to 200 years with
On.
Sodium lauroyl glutamate:Gentle anion surfactant, no anaphylaxis, it is applicable to various sensitiveness fleshes
Skin and baby products etc., blackhead or hoary hair, resistance to hard water are not led to, there is high biological degradability.
Cocoamidopropyl betaine:A kind of zwitterionic surfactant, it is respectively provided with acid and alkalescence condition excellent
Good stability, cation and anion characteristic is presented respectively under the conditions of acid-base property, often with anions and canons and non-ionic surface
Activating agent is used in combination, and its compatibility is good, and excitant is small, and soluble in water, foam is more, strong detergency, have excellent thickening property,
Flexibility, bactericidal properties, antistatic behaviour, hard water resistance property, softness, conditioning and the low-temperature stability of washing class product can be significantly improved.
Lauryl sodium sulfate:Anion surfactant, it is soluble in water, compounded with anion, amphion, nonionic
5 property are good, have good emulsification, foaming, infiltration, decontamination and dispersive property.
APG:Synthesized by renewable resource natural fat alcohol and glucose, be that a kind of performance is more comprehensively new
Nonionic surfactant, have the characteristic of conventional nonionic and anion surfactant concurrently, with high surface, well
Ecological security and intermiscibility, it is internationally recognized preferred " green " functional surfactant.
Fresh tea fruit juice:It is untouched to retain fresh tea fruit nutritional ingredient using fresh tea fruit cold pressing, rich in unsaturation
Oil, protein, starch, Tea Saponin, flavones, polyphenol, VE etc., there is moisturizing, moist, antibacterial, anti-inflammatory and other effects.
Disodium ethylene diamine tetraacetate:A kind of important complexing agent, complex compound easily is formed with reference to calcium ions and magnesium ions in water, prevents calcium
Magnesium ion and surfactant fluid, so that it is guaranteed that the cleaning of surfactant, foaming effect.
Glycerine:A kind of polyalcohol NMF, hair washing process surfactant is avoided to remain, while it is steady to improve shampoo low temperature
It is qualitative.
EGDS:Pearling agent and tax ester agent, there is provided product is pleasing.
Deionized water:Eliminate in the pure water after ionic species impurity, produced using the method for RO counter-infiltrations, using ion
The anion and cation that exchanger resin is gone in water removal, make solvent and carrier.
Trehalose:Pure natural carbohydrate, very safety and stability, all contain in many organisms, trehalose has superpower guarantor
Cell viability and large biological molecule activity are held, one layer of special diaphragm can be formed in cell surface layer, skin can not only be kept former
Some nutrition and moisture, moreover it is possible to nourishes rough skin cell.
Polyquaternium 7:Cationic polymer, there are antistatic, lubrication, submissive, sterilizing function, skin conditioning agent can be used as,
The stimulation of surfactant and other compositions is reduced, ventilated membrane can be formed in skin surface, makes skin smooth, comfortable.
Salt:Main component is NaCl, and the viscosity of liquid is matched somebody with somebody in increase.
Essence:The smell of finished product is adjusted, is allowed to pleasant comfortable.
Kathon CG:The aqueous solution is light amber transparency liquid, and smell is gentle, is mainly used in cosmetics anti-corrosion, toxicity is low, antibacterial
Sphere of action is wide, effect is strong and cosmetic material compatibility is good.
Embodiment
Sodium alkyl sulfate is lauryl sodium sulfate in embodiment, APG APG0810.
Camellia oleifera fruit emulsion preparation technology is:
(1)Selection:Selection just harvesting, fresh full camellia oleifera fruit machinery peel off, and remove shell, cleaning obtains fresh tea seed;
(2)Crush:By step(1)Gained tea seed puts into pulverizer(4 millimeters of crusher sifting aperture), obtain plant material particle
(Particle is less than 1 millimeter), moisture 51%;
(3)Split-phase:By step(2)Gained tea seed feed particles put into juice extractor(Squeeze 0.4 millimeter of gap), extrude and consolidated
Body fiber powder and serum;
(4)Purification:By step(3)Gained serum is transported in retort, and PH is adjusted to 4, and it is (excellent for seed selection to add acid protease
Good Aspergillus usamii is made through depth fermentation), the weight ratio with serum is 3:1000;Heating water bath is to 50-60 DEG C, 20-30min
Afterwards, the weight ratio of addition activated carbon of sorbent, dosage and serum is 3:100,25 DEG C of temperature, mixing time is 40 minutes, stirring
Speed is 40 revs/min, adds 4% super-cell of serum weight, is filtered by leaf-type filter, obtains clarification oil tea
Fruit emulsion.
Embodiment 1
The nourishing moisturizing camellia oleifera fruit shower cream of embodiment 1, is made up of following processing step:
(1)It is prewired:Fresh oil tea emulsion is heated to 60 DEG C, is proportionally added into sodium lauroyl glutamate, cocamidopropyl propyl amide sweet tea
Dish alkali, sodium alkyl sulfate, APG, EGDS, disodium ethylene diamine tetraacetate, heating stirring, mixing time
For 25 minutes, mixing speed was 40 revs/min, obtains fusions;
(2)Emulsification:In step(1)In, glycerol adding, trehalose, polyquaternium, ionized water, are stirred, mixing time 25 in proportion
Minute, mixing speed is 60 revs/min, obtains primary emulsifying thing;
(3)Shaping:In step(2)The primary emulsifying thing of gained squeezes into homogenizer, perfuming essence, Kathon CG, salt, homogeneous 20 minutes, obtains
Nourish moisturizing camellia oleifera fruit shower cream.
Embodiment 2-6
Embodiment 2-6 nourishing moisturizing camellia oleifera fruit shower cream, its preparation process condition is substantially with embodiment 1, simply reaction raw materials
And the condition such as proportion scale, temperature, time is slightly different, specifically as listed in table 1.
The embodiment 1-6 of table 1 nourishing moisturizing camellia oleifera fruit shower cream preparation process condition
。
The formula of comparative example 1 is consistent with embodiment 6, and difference is that the preparation method of camellia oleifera fruit emulsion is different, comparative example 1
Using neutral proteinase-subtilopeptidase A.
Comparative example 2
The formula of comparative example 2 is consistent with embodiment 6, and difference is that the preparation method of camellia oleifera fruit emulsion is different, and comparative example 2 uses
Alkali protease-serine protease.
Comparative example 3
Camellia oleifera fruit emulsion dosage is 70 parts in the formula of comparative example 3, other consistent with embodiment 6.
By the nourishing moisturizing camellia oleifera fruit shower cream obtained by embodiment 1-6, comparative example 1-3 test its cold-resistant heat-resistant stability,
Anaphylaxis, moisten moisturizing, cleaning.
Its functional attributes test result of the embodiment of table 2, comparative example camellia oleifera fruit shower cream
。
Its functional attributes and physical and chemical index of nourishing moisturizing camellia oleifera fruit shower cream obtained by embodiment 1-6, comparative example 1-3 are surveyed
The used method of testing of examination has:
(1)Cold-resistant heat-resistant stability
Carried out according to 6.2.1 in GB/T 29680 and 6.2.2.
(2)Degree of allergic reaction is tested
Step 1:The gauze of four thickness is cut into a diameter of 1cm circle with scissors, totally 8, with 1 gram of embodiment 1-6 of steel bale-out,
Comparative example 1-3 nourishing moisturizing camellia oleifera fruit shower cream, is coated on circular gauze, blank is done with deionized water;
Step 2:The gripping of gauze tweezers is placed at the anteflexion arm of subject, fixed with adhesive tape, starts timing;
Step 3:Torn after 48h adhesive tape, and observe the reaction of skin at gauze covering immediately.Observe result.
(3)Cleanliness testing, specific method are as follows:
Nourishing moisturizing camellia oleifera fruit shower cream obtained by embodiment 1-6, comparative example 1-3 is uniformly applied to standard cleaning disk, tested
Clean effect.
(4)The method of testing for moistening maintenance performance of keeping humidity is tested for arm, and specific method is as follows:
Nourishing moisturizing camellia oleifera fruit shower cream obtained by embodiment 1-6, comparative example 1-3 is uniformly applied to coarse, dry skin, felt
By moist moistening effect and situation is repaired, and is recorded(- expression almost do not have ,+represents, ++ represent very well, +++ expression is very
It is good), moisture preserving time is recorded, untill no moisture feeling, contrasts coarse, dry skin.
From table 2, the present invention nourishes moisturizing camellia oleifera fruit shower cream and uses raw material based on fresh tea fruit pulp, rich in camellia
The materials such as oil, Tea Saponin, tea polysaccharide, tea albumen, flavones, decontamination is compounded, maintenance composition, Low-foam and easily cleaning can deep enough skin
Water lock is cleaned, is moistened, and without anaphylaxis.
In addition, by the nourishing moisturizing camellia oleifera fruit shower cream obtained by embodiment 1-6, by examining microbiological indicator, health to refer to
Mark《Cosmetics safety technical specification》(Version in 2015), obtain the testing result shown in table 3 below.
Moisturizing camellia oleifera fruit shower cream microorganism, sanitary index are nourished obtained by the embodiment 1-6 of table 3
。
The present invention nourishes moisturizing camellia oleifera fruit shower cream toxicology test:Skin irritation test(Multiple skin irritation examination
Test).
Test objective:Caused skin irritation is anti-after observing rabbit intact skin long-time multiple-contact tested material
Should, provide security foundation for the nourishing moisturizing camellia oleifera fruit shower cream of the embodiment of the present invention.
Test basis:《Cosmetics safety technical specification》Version in 2015;Test method:From white New Zealand rabbits 8, with
Machine is divided into 2 groups, every group 4;A groups:Experimental group, B groups:Deionized water control group.24h is by family's rabbit back backbone both sides before experiment
Hair is cut, and skin surface is not damaged in cropping, and unhairing scope is 3cm × 3cm, and application area is 2.5cm × 2.5cm, tested
Nourishing moisturizing camellia oleifera fruit shower cream of the thing group to various embodiments of the present invention, takes tested material 0.5ml to be coated directly on back backbone
Side, opposite side apply 0.5ml control group deionized waters, smear 1 time daily, continuously smear 14d;Since second day, apply every time
Cropping when smearing, residual tested material is removed with deionized water;Result is observed after one hour, according to《Cosmetics safety technical specification》
(Version in 2015)Skin irritation test table scoring, check plot and trial zone are equally handled.
Evaluation of result:Every rabbit average integral daily is calculated according to the following formula, is pierced by specification list deciding rabbit skin
Swash intensity, and observe other toxic actions in addition to excitant.
。
Result of the test:Tested material was carried out in the multiple skin irritation test observation period, gave various embodiments of the present invention
Nourishing moisturizing camellia oleifera fruit shower cream after, rabbit has no erythema, oedema;Have no systemic toxicity profiles performance and death condition, animal body
Increase again, on breathing, circulating, central nervous system, four limbs activity etc. is without influence.
Conclusion (of pressure testing):The nourishing moisturizing camellia oleifera fruit shower cream of various embodiments of the present invention to white New Zealand rabbits intact skin without
Excitant.
Claims (10)
1. one kind nourishes moisturizing camellia oleifera fruit shower cream, in terms of weight fraction, it is made up of following component:Deionized water 50-60 parts, the moon
Osmanthus acyl sodium glutamate 10-15 parts, Cocoamidopropyl betaine 5-10 parts, sodium alkyl sulfate 5-10 parts, APG 2-5 parts,
Camellia oleifera fruit emulsion 28-42 parts, glycerine 2-4 parts, EGDS 0.8-1.2 parts, disodium ethylene diamine tetraacetate 0.05-
0.1 part, trehalose 1.5-3 parts, the 3-5 of polyquaternium -7 parts, salt 1-2 parts, essence 0.1-0.5 parts, Kathon CG 0.05-0.1 parts.
2. nourishing moisturizing camellia oleifera fruit shower cream according to claim 1, it is characterised in that:Wherein described sodium alkyl sulfate
For lauryl sodium sulfate.
3. nourishing moisturizing camellia oleifera fruit shower cream according to claim 1, it is characterised in that:Wherein described APG is
APG0810。
4. nourishing moisturizing camellia oleifera fruit shower cream according to claim 1, it is characterised in that:It is prepared by described camellia oleifera fruit emulsion
Technique is:
(1)Selection:Selection just harvesting, fresh full camellia oleifera fruit;
(2)De- shell:By step(1)Gained camellia oleifera fruit machinery peels off, and removes shell, obtains fresh tea seed;
(3)Clean:By step(2)Gained tea seed removes solid impurity;
(4)Washing:By step(3)Gained tea seed is washed, and after removing spot, obtains clean tea seed;
(5)Crush:By step(4)Gained tea seed puts into pulverizer, obtains tea seed particle, moisture 40-60%;
(6)Split-phase:By step(5)Gained tea seed particle puts into juice extractor, and extruding obtains solid fiber powder and serum;
(7)Purification:By step(6)Gained serum is transported in retort, and pH value is adjusted to 3.5-4, adds acid protease, water
Bath is heated to 50-60 DEG C, after 20-30min, adds activated carbon of sorbent or atlapulgite, 20 DEG C -40 DEG C of temperature, mixing time is
20-30 minutes, mixing speed are 20-60 revs/min, add the 1-6% super-cells of serum weight, pass through filter blade
Machine filters, and obtains clarification camellia oleifera fruit emulsion.
5. nourishing moisturizing camellia oleifera fruit shower cream according to claim 4, it is characterised in that:Step(7)The use of middle adsorbent
Amount and the weight ratio of serum are 2-4:100.
6. nourishing moisturizing camellia oleifera fruit shower cream according to claim 4, it is characterised in that:Step(5)The crusher sifting
Aperture 2-10 millimeters, pulverized particles are less than 1 millimeter.
7. nourishing moisturizing camellia oleifera fruit shower cream according to claim 4, it is characterised in that:Step(6)The juice extractor squeezes
0.1 millimeter ~ 1 millimeter of gap.
8. nourishing moisturizing camellia oleifera fruit shower cream according to claim 4, it is characterised in that:Step(7)Described in acidity
The weight of protease and serum ratio is(0.1-4):1000.
9. nourishing moisturizing camellia oleifera fruit shower cream according to claim 4, it is characterised in that:Step(7)Described acid egg
White enzyme is that the excellent Aspergillus usamii of seed selection is made through depth fermentation.
10. the preparation method of moisturizing camellia oleifera fruit shower cream is nourished according to claim 1, it is characterised in that:Include successively such as
Lower step:
(1)It is prewired:Camellia oleifera fruit emulsion is heated to 50-80 DEG C, is proportionally added into sodium lauroyl glutamate, cocamidopropyl propyl amide sweet tea
Dish alkali, sodium alkyl sulfate, APG, EGDS, disodium ethylene diamine tetraacetate, heating stirring, mixing time
For 20-30 minutes, mixing speed is 20-60 revs/min, obtains fusions;
(2)Emulsification:In step(1)In, glycerol adding, trehalose, polyquaternium -7, ionized water, stirring, mixing time are in proportion
20-30 minutes, mixing speed are 50-80 revs/min, obtain primary emulsifying thing;
(3)Shaping:In step(2)The primary emulsifying thing of gained squeezes into homogenizer, perfuming essence, Kathon CG, salt, homogeneous 10-30 minutes,
Obtain and nourish moisturizing camellia oleifera fruit shower cream.
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CN109172407A (en) * | 2018-10-25 | 2019-01-11 | 汕头市大千高新科技研究中心有限公司 | A kind of purposes of macromolecule cation polymer and its skin care item of preparation |
CN109350553A (en) * | 2018-12-04 | 2019-02-19 | 浙江大学自贡创新中心 | A kind of mineral salt amino acid shower cream |
CN112022786A (en) * | 2020-10-16 | 2020-12-04 | 湖南金昌生物技术有限公司 | Camellia bath powder capable of moistening and cleaning skin and preparation method of camellia bath powder |
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