CN115778876A - Antioxidant camellia oil composition, shampoo and preparation method thereof - Google Patents
Antioxidant camellia oil composition, shampoo and preparation method thereof Download PDFInfo
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- CN115778876A CN115778876A CN202211598043.5A CN202211598043A CN115778876A CN 115778876 A CN115778876 A CN 115778876A CN 202211598043 A CN202211598043 A CN 202211598043A CN 115778876 A CN115778876 A CN 115778876A
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- antioxidant
- camellia oil
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- camellia
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- 239000010495 camellia oil Substances 0.000 title claims abstract description 120
- 239000000203 mixture Substances 0.000 title claims abstract description 102
- 230000003078 antioxidant effect Effects 0.000 title claims abstract description 87
- 239000003963 antioxidant agent Substances 0.000 title claims abstract description 83
- 239000002453 shampoo Substances 0.000 title claims abstract description 35
- 238000002360 preparation method Methods 0.000 title abstract description 17
- 241001122767 Theaceae Species 0.000 claims abstract description 44
- 240000001548 Camellia japonica Species 0.000 claims abstract description 39
- 235000018597 common camellia Nutrition 0.000 claims abstract description 39
- 239000000284 extract Substances 0.000 claims abstract description 11
- 239000006286 aqueous extract Substances 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims description 66
- 239000004094 surface-active agent Substances 0.000 claims description 45
- 238000010438 heat treatment Methods 0.000 claims description 41
- 238000001816 cooling Methods 0.000 claims description 39
- 239000004475 Arginine Substances 0.000 claims description 31
- 239000000843 powder Substances 0.000 claims description 31
- 238000002156 mixing Methods 0.000 claims description 29
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- 238000001914 filtration Methods 0.000 claims description 24
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims description 22
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- 239000001397 quillaja saponaria molina bark Substances 0.000 claims description 16
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- 235000019198 oils Nutrition 0.000 claims description 15
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- 229940045885 sodium lauroyl sarcosinate Drugs 0.000 claims description 14
- IWIUXJGIDSGWDN-UQKRIMTDSA-M sodium;(2s)-2-(dodecanoylamino)pentanedioate;hydron Chemical group [Na+].CCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CCC(O)=O IWIUXJGIDSGWDN-UQKRIMTDSA-M 0.000 claims description 14
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- PWVUXRBUUYZMKM-UHFFFAOYSA-N 2-(2-hydroxyethoxy)ethyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCOCCO PWVUXRBUUYZMKM-UHFFFAOYSA-N 0.000 claims description 6
- YFHCTDZPVSKZJG-UHFFFAOYSA-N C(CCCCCCCCCCCCCCCCC)(=O)O.C(CCCCCCCCCCCCCCCCC)(=O)O.C(C)O.C(C)O Chemical compound C(CCCCCCCCCCCCCCCCC)(=O)O.C(CCCCCCCCCCCCCCCCC)(=O)O.C(C)O.C(C)O YFHCTDZPVSKZJG-UHFFFAOYSA-N 0.000 claims description 6
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- GLSRFBDXBWZNLH-UHFFFAOYSA-L disodium;2-chloroacetate;2-(4,5-dihydroimidazol-1-yl)ethanol;hydroxide Chemical compound [OH-].[Na+].[Na+].[O-]C(=O)CCl.OCCN1CCN=C1 GLSRFBDXBWZNLH-UHFFFAOYSA-L 0.000 claims description 5
- 229940096501 sodium cocoamphoacetate Drugs 0.000 claims description 5
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 4
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 4
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- PRAKJMSDJKAYCZ-UHFFFAOYSA-N dodecahydrosqualene Natural products CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 abstract description 5
- 229940031439 squalene Drugs 0.000 abstract description 5
- TUHBEKDERLKLEC-UHFFFAOYSA-N squalene Natural products CC(=CCCC(=CCCC(=CCCC=C(/C)CCC=C(/C)CC=C(C)C)C)C)C TUHBEKDERLKLEC-UHFFFAOYSA-N 0.000 abstract description 5
- 229930003427 Vitamin E Natural products 0.000 abstract description 4
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 abstract description 4
- 150000008442 polyphenolic compounds Chemical class 0.000 abstract description 4
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- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 10
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- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 3
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- MIJYXULNPSFWEK-GTOFXWBISA-N 3beta-hydroxyolean-12-en-28-oic acid Chemical compound C1C[C@H](O)C(C)(C)[C@@H]2CC[C@@]3(C)[C@]4(C)CC[C@@]5(C(O)=O)CCC(C)(C)C[C@H]5C4=CC[C@@H]3[C@]21C MIJYXULNPSFWEK-GTOFXWBISA-N 0.000 description 1
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- JKLISIRFYWXLQG-UHFFFAOYSA-N Epioleonolsaeure Natural products C1CC(O)C(C)(C)C2CCC3(C)C4(C)CCC5(C(O)=O)CCC(C)(C)CC5C4CCC3C21C JKLISIRFYWXLQG-UHFFFAOYSA-N 0.000 description 1
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- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 1
- YBRJHZPWOMJYKQ-UHFFFAOYSA-N Oleanolic acid Natural products CC1(C)CC2C3=CCC4C5(C)CCC(O)C(C)(C)C5CCC4(C)C3(C)CCC2(C1)C(=O)O YBRJHZPWOMJYKQ-UHFFFAOYSA-N 0.000 description 1
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- JZLXEKNVCWMYHI-UHFFFAOYSA-N gingerol Natural products CCCCC(O)CC(=O)CCC1=CC=C(O)C(OC)=C1 JZLXEKNVCWMYHI-UHFFFAOYSA-N 0.000 description 1
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Landscapes
- Cosmetics (AREA)
Abstract
The invention provides an antioxidant camellia oil composition, shampoo and a preparation method thereof, and belongs to the technical field of washing and caring products. The antioxidant camellia oil composition provided by the invention comprises a component A and a component B, wherein the component A comprises camellia oil, and the component B comprises a tea seed extracting solution; the camellia oil is winterized; the tea seed extract is an aqueous extract of oil-removed camellia seed residue. According to the invention, the camellia oil and the tea seed extract are matched, and the antioxidant substances such as vitamin E, squalene, sterol, tea polyphenol and the like are abundant, so that the composition has good antioxidant performance, helps to restore the vitality of cells, promotes cell repair and enables damaged hair to restore natural health.
Description
Technical Field
The invention relates to the technical field of washing and caring products, and particularly relates to an antioxidant camellia oil composition, shampoo and a preparation method thereof.
Background
Hair plays an important role in the overall image of a human body and is also an important index of the health condition of the human body. With the continuous improvement of living standard, people pay more and more attention to the self image and health, and pay more and more attention to the hair care correspondingly. However, modern people play more and more quickly, work pressure increases day by day, people have full energy, and environmental pollution is serious, so that the hair of people is more and more problematic.
The hair care product is an essential daily article for daily life of people, along with the improvement of living standard, the health consciousness and the image consciousness of people are gradually enhanced, the hair care frequency is gradually increased, especially in summer, a plurality of people can wash and care hair every day, however, the existing hair care product is mainly used for meeting the effects of removing dirt, removing dandruff, smoothing and the like of people, and the capacity in the aspect of oxidation resistance is not enough.
Disclosure of Invention
In view of the above, the invention aims to provide an antioxidant camellia oil composition, a shampoo and a preparation method thereof.
In order to achieve the purpose, the invention provides the following technical scheme:
an antioxidant camellia oil composition comprises a component A and a component B, wherein the component A comprises camellia oil, and the component B comprises a tea seed extracting solution; the camellia oil is winterized; the tea seed extract is an aqueous extract of oil-removed camellia seed residue.
Preferably, the weight ratio of the component A to the component B is (3-8): (15 to 25).
The invention also provides a preparation method of the antioxidant camellia oil composition, which comprises the following steps:
preparing a component A: placing camellia oil in a container, heating to 50-60 ℃, stirring for 25-35 min, stopping heating, cooling to room temperature while stirring, transferring to an ice water bath, cooling to 0 ℃, standing, preserving heat for 22-26 h, and filtering to obtain a component A;
preparing a component B: crushing the camellia seed dregs without oil, sieving to obtain camellia seed dregs powder, and mixing the camellia seed powder and water according to the weight ratio of (0.8-1.2): and (2) mixing and uniformly mixing the components in the proportion of (2) to (4), heating and stirring the mixture, cooling the mixture to room temperature, and filtering the mixture to obtain a component B.
The invention also provides an antioxidant camellia oil shampoo of the antioxidant camellia oil composition, which comprises the following components:
18 to 33 portions of antioxidant camellia oil composition, 0.5 to 2 portions of tea saponin, 3 to 8 portions of lauryl surfactant, 0.5 to 2 portions of guar gum hydroxypropyl trimethyl ammonium chloride, 2 to 5 portions of coconut oil based surfactant, 2 to 6 portions of plant extract, 0.8 to 3 portions of softener, 0.1 to 0.5 portion of conjugated linoleic acid-arginine composition, 0.1 to 0.3 portion of essence and 30 to 70 portions of deionized water.
Preferably, the lauryl surfactant is sodium lauroyl glutamate, ammonium laureth sulfate and sodium lauroyl sarcosinate, and the weight ratio of the sodium lauroyl glutamate to the ammonium laureth sulfate to the sodium lauroyl sarcosinate is (1.8-2.2): (0.8-1.3): (0.8-1.3).
Preferably, the plant extract is an aqueous extract of ginger, glossy privet fruit, polygonum multiflorum and eclipta alba; the weight ratio of the ginger to the glossy privet fruit to the polygonum multiflorum to the eclipta alba in the plant extract is (4-6): (1-3): (1-3): (2-4).
Preferably, the cocoyl surfactant is cocamidopropyl betaine and sodium cocoamphoacetate, and the weight ratio of the cocamidopropyl betaine to the sodium cocoamphoacetate is (2-3) to (0.8-1.1); the softener is one or more of diethanol distearate, diethylene glycol monostearate and polydimethylsiloxane.
Preferably, the weight ratio of the conjugated linoleic acid to the arginine in the conjugated linoleic acid-arginine composition is (1.5-1.7): (0.9-1.1).
The invention also provides a preparation method of the antioxidant camellia oil shampoo, which comprises the following steps:
weighing the raw materials according to the formula;
adding deionized water, lauryl surfactant and coconut oil-based surfactant into a reaction vessel, and heating while stirring uniformly;
sequentially adding tea saponin, guar gum hydroxypropyl trimethyl ammonium chloride, component B of the antioxidant camellia oil composition and the plant extract, and stirring uniformly;
sequentially adding the softener and the component A of the antioxidant camellia oil composition while stirring, and gradually cooling to 38-42 ℃ after uniformly stirring;
adding essence and conjugated linoleic acid-arginine composition, stirring, and cooling to room temperature to obtain antioxidant camellia oil shampoo.
Preferably, the heating while stirring uniformly is performed by heating to 55 to 65 ℃.
The beneficial technical effects are as follows: the invention provides an antioxidant camellia oil composition, shampoo and a preparation method thereof, and the antioxidant camellia oil composition provided by the invention comprises a component A and a component B, wherein the component A comprises camellia oil, and the component B comprises a tea seed extracting solution; the camellia oil is winterized; the tea seed extract is an aqueous extract of oil-removed camellia seed residue. According to the invention, the camellia oil and the tea seed extract are matched, and the antioxidant substances such as vitamin E, squalene, sterol, tea polyphenol and the like are enriched, so that the composition has good antioxidant performance, helps to restore the vitality of cells, promotes cell repair and enables damaged hair to restore the natural health.
Detailed Description
The invention provides an antioxidant camellia oil composition, which comprises a component A and a component B, wherein the component A comprises camellia oil, and the component B comprises a tea seed extracting solution; the camellia oil is winterized; the tea seed extract is an aqueous extract of oil-removed camellia seed residue.
In the invention, the camellia oil mainly comprises fatty glyceride, wherein the fatty acid mainly comprises oleic acid, linoleic acid and a certain amount of saturated fatty acid, wherein the content of the oleic acid reaches 74-89%, and the fatty acid is similar to the fatty acid composition of olive oil and is called as 'east olive oil'; meanwhile, the camellia oil also contains rich antioxidant substances such as vitamin E, squalene, sterol, tea polyphenol and the like, and oleic acid in the camellia oil is easily absorbed by hair and skin and supplies nutrition required by metabolism; the natural squalene can restore the cell activity of a human body, promote cell repair and help damaged scalp to restore natural health; the vitamin E can prevent and treat withered and broken hair, so that the hair is glossy and smooth; the synergistic effect of tea polyphenols and squalene can also kill bacteria and remove dandruff.
In the invention, the tea seed extracting solution contains rich tea seed polysaccharide and tea saponin, wherein the tea seed polysaccharide has the functions of removing free radicals and enhancing the immunity of the organism; the tea saponin has antibacterial, antiinflammatory, and anti-stress physiological activities. Meanwhile, the camellia oil-removed seed residues are subjected to water re-extraction, so that the camellia oil-removed seed residues are recycled, and can be matched with antioxidant components in camellia oil, and the antioxidant effect is better realized.
In the present invention, the weight ratio of the a component and the B component is preferably (3 to 8): (15 to 25), more preferably (5 to 6): (18 to 19). According to the invention, the matching of antioxidant components in the A, B is better realized and the antioxidant effect is enhanced by controlling the proportion of the A, B.
The invention also provides a preparation method of the antioxidant camellia oil composition, which comprises the following steps:
preparing a component A: placing camellia oil in a container, heating to 50-60 ℃, stirring for 25-35 min, stopping heating, cooling to room temperature while stirring, transferring to an ice water bath, cooling to 0 ℃, standing, preserving heat for 22-26 h, and filtering to obtain a component A;
preparing a component B: crushing the camellia seed dregs without oil, sieving to obtain camellia seed dregs powder, and mixing the camellia seed powder and water according to the weight ratio of (0.8-1.2): and (2) mixing and uniformly mixing the components in the proportion of (2) to (4), heating and stirring the mixture, cooling the mixture to room temperature, and filtering the mixture to obtain a component B.
The preparation method of the antioxidant camellia oil composition preferably comprises the following steps: placing camellia oil in a container, heating to 50-60 ℃, stirring for 25-35 min, stopping heating, cooling to room temperature while stirring, transferring to an ice water bath, cooling to 0 ℃, standing, preserving heat for 22-26 h, and filtering to obtain the component A.
In the invention, the camellia oil is the commercially available camellia oil, the container can be selected according to the amount of the camellia oil conventionally, the stirring is slow stirring, and the filtering is filtering with 300-mesh diatomite. The winterization treatment is carried out on the camellia oil, so that the stability of the camellia oil at high temperature and low temperature can be improved.
The preparation method of the antioxidant camellia oil composition preferably comprises the following steps: crushing the camellia seed dregs without oil, sieving to obtain camellia seed dregs powder, and mixing the camellia seed powder and water according to the weight ratio of (0.8-1.2): and (2) mixing uniformly according to the proportion of (2) to (4), heating and stirring, cooling to room temperature, and filtering to obtain the component B.
In the present invention, the sieving is preferably performed by using a sieve of 80 to 120 meshes; the heating and stirring are preferably carried out to 55-65 ℃, and the mixture is fully stirred for 25-35 min; the filtration is preferably performed with a 120-180 mesh screen, and more preferably with a 150 mesh screen.
The invention also provides an antioxidant camellia oil shampoo of the antioxidant camellia oil composition, which comprises the following components:
18 to 33 portions of antioxidant camellia oil composition, 0.5 to 2 portions of tea saponin, 3 to 8 portions of lauryl surfactant, 0.5 to 2 portions of guar gum hydroxypropyl trimethyl ammonium chloride, 2 to 5 portions of coconut oil based surfactant, 2 to 6 portions of plant extract, 0.8 to 3 portions of softener, 0.1 to 0.5 portion of conjugated linoleic acid-arginine composition, 0.1 to 0.3 portion of essence and 30 to 70 portions of deionized water.
In the present invention, the lauryl surfactant is preferably sodium lauroyl glutamate, ammonium laureth sulfate, or sodium lauroyl sarcosinate, and the weight ratio of the sodium lauroyl glutamate, the ammonium laureth sulfate, or the sodium lauroyl sarcosinate is preferably (1.8 to 2.2): (0.8-1.3): (0.8 to 1.3), more preferably 2. In the present invention, the cocoyl surfactant is preferably cocoamidopropyl betaine and sodium cocoamphoacetate, and the weight ratio of cocoamidopropyl betaine and sodium cocoamphoacetate is preferably (2-3) to (0.8-1.1), more preferably 2.5; the softener is one or more of diethanol distearate, diethylene glycol monostearate and polydimethylsiloxane. According to the invention, the specific lauryl surfactant and the coconut oil-based surfactant are selected, the proportion of each component is respectively limited, and the two surfactants effectively fuse the component A and the component B of the antioxidant camellia oil through the synergistic effect, so that the stability of the shampoo at high temperature and low temperature is effectively improved.
In the invention, the plant extract is preferably an aqueous extract of ginger, glossy privet fruit, polygonum multiflorum and eclipta alba; the weight ratio of the ginger, the glossy privet fruit, the tuber fleeceflower root and the eclipta alba in the plant extracting solution is preferably (4-6): (1-3): (1-3): (2 to 4), more preferably 5:2:2:3. the ginger contains gingerol and other components, and can stimulate scalp hyperemia, promote scalp blood circulation and promote hair growth when being externally applied to scalp; the glossy privet fruit has the effects of tonifying kidney, nourishing yin, nourishing liver and improving eyesight, can be used for early graying hair, contains abundant oleanolic acid in the glossy privet fruit extract, can improve the microcirculation around hair follicles, regulate the periodic growth of the hair follicles, promote the growth of the hairs, can also promote the synthesis of prostaglandin, obviously expand blood vessels, and has very strong effect on the growth of the hairs; the polygonum multiflorum has the effects of tonifying liver and kidney, promoting hair growth, preventing alopecia, preventing premature graying of hair and enabling hair to be black and glossy; the Ecliptae herba has effects of blackening and nourishing hair, nourishing liver and kidney, cooling blood and stopping bleeding. The invention combines the ginger, the glossy privet fruit, the tuber fleeceflower root and the eclipta alba for use, can effectively improve the state of the scalp and realize the effect of maintaining the hair.
In the present invention, the method for preparing the plant extract is preferably: weighing ginger, glossy privet fruit, polygonum multiflorum and eclipta alba according to a certain proportion, uniformly mixing, crushing, sieving by a 50-mesh sieve to obtain plant powder, uniformly mixing distilled water 8-12 times of the weight of the plant powder with the plant powder, carrying out ultrasonic treatment for 25-35 min, heating to a reflux state, extracting for 2-4 h, filtering to obtain filtrate, extracting the filtrate by using petroleum ether (boiling range: 30-60 ℃), and volatilizing the petroleum ether to obtain the plant extract.
In the present invention, the weight ratio of the conjugated linoleic acid to the arginine in the conjugated linoleic acid-arginine composition is preferably (1.5 to 1.7): (0.9 to 1.1), more preferably 1.6. The conjugated linoleic acid-arginine composition has good antioxidant activity, and can effectively improve the antioxidant effect of shampoo products by reasonably controlling the weight ratio of the conjugated linoleic acid to the arginine and matching with the antioxidant camellia oil composition.
In the invention, the essence can be specifically selected according to actual conditions and requirements.
The invention also provides a preparation method of the antioxidant camellia oil shampoo, which comprises the following steps:
weighing the raw materials according to a formula;
adding deionized water, lauryl surfactant and coconut oil-based surfactant into a reaction vessel, and heating while stirring uniformly;
sequentially adding tea saponin, guar gum hydroxypropyl trimethyl ammonium chloride, component B of the antioxidant camellia oil composition and the plant extract, and stirring uniformly;
sequentially adding the softener and the component A of the antioxidant camellia oil composition while stirring, and gradually cooling to 38-42 ℃ after uniformly stirring;
adding essence and conjugated linoleic acid-arginine composition, stirring, and cooling to room temperature to obtain antioxidant camellia oil shampoo.
In the invention, the heating while stirring is carried out to 55-65 ℃. The raw materials in the shampoo, especially the water-soluble component and the oil-soluble component, can be uniformly mixed by fully and uniformly stirring and then adding other components or carrying out the next operation.
In order to better understand the present invention, the following examples are further provided to illustrate the present invention, but the present invention is not limited to the following examples. Materials, reagents and the like used in the examples and test examples of the present invention can be obtained commercially unless otherwise specified; the methods used in the examples and test examples of the present invention are conventional methods unless otherwise specified.
Example 1
The antioxidant camellia oil composition comprises: the camellia oil and tea seed extracting solution comprises camellia oil and a tea seed extracting solution, wherein the weight ratio of the camellia oil to the tea seed extracting solution is 8:25.
preparing a component A: placing camellia oil in a container, heating to 50 deg.C, stirring for 35min, stopping heating, cooling to room temperature while stirring, transferring to ice water bath, cooling to 0 deg.C, standing, keeping the temperature for 22 hr, and filtering with 300 mesh diatomaceous earth;
preparing a component B: crushing the camellia seed dregs without oil, sieving the crushed camellia seed dregs by a 80-mesh sieve to obtain camellia seed dregs powder, and mixing the camellia seed powder with water according to the weight ratio of 0.8:2, heating and stirring, cooling to room temperature, and filtering with a 150-mesh screen to obtain a component B;
the anti-oxidation camellia oil shampoo comprises the following components: 33 parts of antioxidant camellia oil composition, 2 parts of tea saponin, 8 parts of lauryl surfactant, 2 parts of guar gum hydroxypropyl trimethyl ammonium chloride, 5 parts of coconut oil based surfactant, 6 parts of plant extract, 3 parts of softener, 0.5 part of conjugated linoleic acid-arginine composition, 0.3 part of essence and 70 parts of deionized water;
wherein, the component A in the antioxidant camellia oil composition is 8 parts, and the component B is 25 parts; the lauryl surfactant is sodium lauroyl glutamate, ammonium laureth sulfate and sodium lauroyl sarcosinate, wherein the weight ratio of the sodium lauroyl glutamate to the ammonium laureth sulfate to the sodium lauroyl sarcosinate is 1.8:0.8:0.8; the cocoyl surfactant is cocoamidopropyl betaine and sodium cocoyl amphoacetate, wherein the weight ratio of the cocoamidopropyl betaine to the sodium cocoyl amphoacetate is 2:0.8; the softener is diethanol distearate; the weight ratio of conjugated linoleic acid to arginine in the conjugated linoleic acid-arginine composition is 1.5:0.9.
the preparation of the plant extract comprises the following steps: according to the weight ratio of ginger, glossy privet fruit, tuber fleeceflower root and eclipta alba of 5:2:2:3, uniformly mixing, crushing, sieving by a 50-mesh sieve to obtain plant powder, uniformly mixing distilled water 12 times the weight of the plant powder and the plant powder, performing ultrasonic treatment for 35min, heating to a reflux state, extracting for 4h, filtering to obtain filtrate, extracting the filtrate by using petroleum ether (the boiling range is 30-60 ℃), and volatilizing the petroleum ether to obtain the plant extracting solution.
The preparation method of the antioxidant camellia oil shampoo comprises the following steps:
weighing the raw materials according to the formula; adding deionized water, lauryl surfactant and coconut oil surfactant into a reaction vessel, heating to 55 ℃, and stirring uniformly; sequentially adding tea saponin, guar gum hydroxypropyl trimethyl ammonium chloride, component B of the antioxidant camellia oil composition and the plant extract, and stirring uniformly; sequentially adding the softener and the component A of the antioxidant camellia oil composition while stirring, and gradually cooling to 38 ℃ after uniformly stirring; adding essence and conjugated linoleic acid-arginine composition, stirring, and cooling to room temperature to obtain antioxidant camellia oil shampoo.
Example 2
The antioxidant camellia oil composition comprises: the camellia oil-tea seed extracting solution comprises camellia oil and a tea seed extracting solution, wherein the weight ratio of the camellia oil to the tea seed extracting solution is 3.
Preparing a component A: placing camellia oil in a container, heating to 60 deg.C, stirring for 25min, stopping heating, cooling to room temperature under stirring, transferring to ice water bath, cooling to 0 deg.C, standing, keeping the temperature for 26 hr, and filtering with 300 mesh diatomaceous earth;
preparing a component B: crushing the camellia seed dregs without oil, sieving the crushed camellia seed dregs by a 120-mesh sieve to obtain camellia seed dregs powder, and mixing the camellia seed powder with water according to the weight ratio of 1.2:4, heating and stirring, cooling to room temperature, and filtering with a 120-mesh screen to obtain a component B;
the anti-oxidation camellia oil shampoo comprises the following components: 18 parts of antioxidant camellia oil composition, 0.5 part of tea saponin, 3 parts of lauryl surfactant, 0.5 part of guar hydroxypropyl trimethyl ammonium chloride, 2 parts of coconut oil based surfactant, 2 parts of plant extract, 0.8 part of softener, 0.1 part of conjugated linoleic acid-arginine composition, 0.1 part of essence and 30 parts of deionized water;
wherein, the component A in the antioxidant camellia oil composition is 3 parts, and the component B is 15 parts; the lauryl surfactant is sodium lauroyl glutamate, ammonium laureth sulfate and sodium lauroyl sarcosinate, wherein the weight ratio of the sodium lauroyl glutamate to the ammonium laureth sulfate to the sodium lauroyl sarcosinate is 2.2:1.3:1.3; the cocoyl surfactant is cocoamidopropyl betaine and sodium cocoyl amphoacetate, wherein the weight ratio of the cocoamidopropyl betaine to the sodium cocoyl amphoacetate is 3:1.1; the softener is diethylene glycol monostearate; the weight ratio of conjugated linoleic acid to arginine in the conjugated linoleic acid-arginine composition is 1.7:1.1.
preparing a plant extracting solution: according to the weight ratio of ginger, glossy privet fruit, tuber fleeceflower root and eclipta alba of 4:1:1:2, uniformly mixing and crushing the mixture, sieving the crushed mixture by a 50-mesh sieve to obtain plant powder, uniformly mixing distilled water which is 8 times of the weight of the plant powder and the plant powder, performing ultrasonic treatment for 25min, heating the mixture to a reflux state for extraction for 2h, filtering the mixture to obtain filtrate, extracting the filtrate by using petroleum ether (the boiling range is between 30 and 60 ℃) and volatilizing the petroleum ether to obtain the plant extracting solution.
The preparation method of the antioxidant camellia oil shampoo comprises the following steps:
weighing the raw materials according to a formula; adding deionized water, lauryl surfactant and coconut oil-based surfactant into a reaction vessel, and heating to 65 ℃ while uniformly stirring; sequentially adding tea saponin, guar gum hydroxypropyl trimethyl ammonium chloride, component B of the antioxidant camellia oil composition and the plant extract, and stirring uniformly; sequentially adding the softener and the component A of the antioxidant camellia oil composition while stirring, and gradually cooling to 42 ℃ after uniformly stirring; adding essence and conjugated linoleic acid-arginine composition, stirring, and cooling to room temperature to obtain antioxidant camellia oil shampoo.
Example 3
The antioxidant camellia oil composition comprises: the camellia oil and tea seed extracting solution comprises camellia oil and tea seed extracting solution, wherein the weight ratio of the camellia oil to the tea seed extracting solution is 6:19.
preparing a component A: placing camellia oil in a container, heating to 55 deg.C, stirring for 30min, stopping heating, cooling to room temperature while stirring, transferring to ice water bath, cooling to 0 deg.C, standing, keeping the temperature for 24 hr, and filtering with 300 mesh diatomaceous earth;
preparing a component B: crushing the camellia seed dregs without oil, sieving the crushed camellia seed dregs by a 100-mesh sieve to obtain camellia seed dregs powder, and mixing the camellia seed powder and water according to the weight ratio of 1:3, heating and stirring, cooling to room temperature, and filtering with a 180-mesh screen to obtain a component B;
the anti-oxidation camellia oil shampoo comprises the following components: 25 parts of an antioxidant camellia oil composition, 1 part of tea saponin, 5 parts of a lauryl surfactant, 1 part of guar gum hydroxypropyl trimethyl ammonium chloride, 4 parts of a coconut oil-based surfactant, 4 parts of a plant extracting solution, 1.5 parts of a softener, 0.3 part of a conjugated linoleic acid-arginine composition, 0.2 part of essence and 50 parts of deionized water;
wherein, the component A in the antioxidant camellia oil composition is 6 parts, and the component B is 19 parts; the lauryl surfactant is sodium lauroyl glutamate, ammonium laureth sulfate and sodium lauroyl sarcosinate, wherein the weight ratio of the sodium lauroyl glutamate to the ammonium laureth sulfate to the sodium lauroyl sarcosinate is 2:1:1; the cocoyl surfactant is cocoamidopropyl betaine and sodium cocoyl amphoacetate, wherein the weight ratio of the cocoamidopropyl betaine to the sodium cocoyl amphoacetate is 2.5:1; the softener is diethanol distearate and diethylene glycol monostearate, and the weight ratio of the diethanol distearate to the diethylene glycol monostearate is 1:1; the weight ratio of conjugated linoleic acid to arginine in the conjugated linoleic acid-arginine composition is 1.6:1.
preparing a plant extracting solution: according to the weight ratio of ginger, glossy privet fruit, tuber fleeceflower root and eclipta alba of 6:3:3:4, uniformly mixing and crushing the mixture, sieving the crushed mixture by a 50-mesh sieve to obtain plant powder, uniformly mixing distilled water which is 10 times of the weight of the plant powder and the plant powder, carrying out ultrasonic treatment for 30min, heating the mixture to a reflux state, extracting the mixture for 3h, filtering the mixture to obtain filtrate, extracting the filtrate by using petroleum ether (the boiling range is between 30 and 60 ℃), and volatilizing the petroleum ether to obtain the plant extracting solution.
The preparation method of the antioxidant camellia oil shampoo comprises the following steps:
weighing the raw materials according to a formula; adding deionized water, lauryl surfactant and coconut oil-based surfactant into a reaction vessel, heating to 60 ℃, and uniformly stirring; sequentially adding tea saponin, guar gum hydroxypropyl trimethyl ammonium chloride, component B of the antioxidant camellia oil composition and the plant extract, and stirring uniformly; sequentially adding the softener and the component A of the antioxidant camellia oil composition while stirring, and gradually cooling to 40 ℃ after uniformly stirring; adding essence and conjugated linoleic acid-arginine composition, stirring, and cooling to room temperature to obtain antioxidant camellia oil shampoo.
Example 4
Antioxidant camellia oil composition: the camellia oil-tea camellia seed extract liquid comprises camellia oil and a tea seed extract liquid, wherein the weight ratio of the camellia oil to the tea seed extract liquid is 5:18.
preparing a component A: placing camellia oil in a container, heating to 58 deg.C, stirring for 32min, stopping heating, cooling to room temperature while stirring, transferring to ice water bath, cooling to 0 deg.C, standing, keeping the temperature for 25 hr, and filtering with 300 mesh diatomaceous earth;
preparing a component B: crushing the camellia seed dregs without oil, sieving the crushed camellia seed dregs by a 100-mesh sieve to obtain camellia seed dregs powder, and mixing the camellia seed powder with water according to the weight ratio of 0.9:3.2, uniformly mixing, heating and stirring, cooling to room temperature, and filtering by using a 160-mesh screen to obtain a component B;
the anti-oxidation camellia oil shampoo comprises the following components: 23 parts of an antioxidant camellia oil composition, 0.8 part of tea saponin, 6 parts of a lauryl surfactant, 1.2 parts of guar hydroxypropyl trimethyl ammonium chloride, 3 parts of a coconut oil-based surfactant, 5 parts of a plant extracting solution, 2 parts of a softener, 0.4 part of a conjugated linoleic acid-arginine composition, 0.2 part of essence and 55 parts of deionized water;
wherein, the component A in the antioxidant camellia oil composition is 5 parts, and the component B is 18 parts; the lauryl surfactant is sodium lauroyl glutamate, ammonium laureth sulfate and sodium lauroyl sarcosinate, wherein the weight ratio of the sodium lauroyl glutamate to the ammonium laureth sulfate to the sodium lauroyl sarcosinate is 2:1:1; the cocoyl surfactant is cocoamidopropyl betaine and sodium cocoyl amphoacetate, wherein the weight ratio of the cocoamidopropyl betaine to the sodium cocoyl amphoacetate is 2.5:1; the softener is polydimethylsiloxane; the weight ratio of conjugated linoleic acid to arginine in the conjugated linoleic acid-arginine composition is 1.6:1.
preparing a plant extracting solution: according to the weight ratio of ginger, glossy privet fruit, tuber fleeceflower root and eclipta alba of 4:1:1:3, uniformly mixing and crushing the mixture, sieving the mixture by a 50-mesh sieve to obtain plant powder, uniformly mixing distilled water 9 times the weight of the plant powder and the plant powder, performing ultrasonic treatment for 32min, heating the mixture to a reflux state for extraction for 3h, filtering the mixture to obtain filtrate, extracting the filtrate by using petroleum ether (the boiling range is between 30 and 60 ℃) and volatilizing the petroleum ether to obtain the plant extracting solution.
The preparation method of the antioxidant camellia oil shampoo comprises the following steps:
weighing the raw materials according to a formula; adding deionized water, lauryl surfactant and coconut oil-based surfactant into a reaction vessel, heating to 60 ℃, and uniformly stirring; sequentially adding tea saponin, guar gum hydroxypropyl trimethyl ammonium chloride, component B of the antioxidant camellia oil composition and the plant extract, and stirring uniformly; sequentially adding the softener and the component A of the antioxidant camellia oil composition while stirring, and gradually cooling to 40 ℃ after uniformly stirring; adding essence and conjugated linoleic acid-arginine composition, stirring, and cooling to room temperature to obtain antioxidant camellia oil shampoo.
Comparative example 1
In this comparative example, only the component A of the antioxidant camellia oil composition was added, and the remaining raw materials and operations were the same as in example 1.
Comparative example 2
In this comparative example, only the B component of the antioxidant camellia oil composition was added, and the remaining raw materials and operations were the same as in example 1.
Comparative example 3
In this comparative example, no plant extract was added, and the other raw materials and operations were the same as in example 1.
Comparative example 4
In this comparative example, the conjugated linoleic acid-arginine composition was not added, and the remaining raw materials and operations were the same as in example 1.
Comparative example 5
The component A of the antioxidant camellia oil composition added in the comparative example is not winterized, and the rest of the raw materials and operation are the same as those of example 1.
Test example 1DPPH resistance measurement
The final products of examples 1 to 4 and comparative examples 1 to 5 were measured for their DPPH resistance, and the DPPH removal ability was expressed as a drop in the UV absorption peak after the addition of the product.
A) 4mg of DPPH.is accurately weighed and added with 50mL of absolute ethanol to prepare a DPPH.solution with the concentration of 0.2 mmol/L. And measuring the absorbance of the solution by using a UV-1600 ultraviolet-visible spectrophotometer, and collecting the absorption peak value of the solution at 517 nm.
B) And accurately weighing the final products obtained in the examples 1-4 and the comparative examples 1-5 in conical flasks respectively, and diluting the final products to 500mg/L by using absolute ethyl alcohol to obtain a sample solution to be detected. Respectively taking 5mL of sample solution to be detected, 5mL of DPPH solution, mixing uniformly, and reacting for 30min in a dark place. The absorbance of the mixed solution at a wavelength of 517nm was measured using 95% ethanol as a reference, and the result was recorded as A S . And (3) uniformly mixing 5mL of sample solution to be detected with 5mL of 95% ethanol, and reacting for 30min in a dark place. The absorbance of the mixed solution at a wavelength of 517nm was measured using 95% ethanol as a reference, and the result was recorded as A R . Mixing 5mL of 95% ethanol and 5mL of DPPH solution uniformly, and reacting for 30min in a dark place. The absorbance of the mixed solution at a wavelength of 517nm was measured using 95% ethanol as a reference, and the result was recorded as A R 。
C) The formula for calculating the DPPH clearance of free radicals is as follows:
the results of measurement of DPPH resistance and the ability of the final products of examples 1 to 4 and comparative examples 1 to 5 are shown in Table 1.
Test example 2 thermal stability test
5mL of each of the final products obtained in examples 1 to 4 and comparative examples 1 to 5 was taken and put into a transparent sample bottle, and 20 groups of samples were taken for each sample. The obtained sample is put into an incubator to be preserved for 60 days at the constant temperature of 55 ℃. And then observing whether the oil phase is aggregated, separated out and separated in the sample.
Evaluation criteria:
a level: no oil phase aggregation, oil separation and separation phenomena more than or equal to 95 groups.
B stage: and the 95 groups have no oil phase aggregation, oil precipitation and separation phenomena more than or equal to 85 groups.
C level: no oil phase aggregation, oil separation and separation phenomena less than 85 groups.
The results of the thermal stability test of the finally obtained products of examples 1 to 4 and comparative examples 1 to 5 are shown in Table 1.
TABLE 1DPPH clearance and thermal stability test results
As can be seen from Table 1, the DPPH and clearance of the final products obtained in the embodiments 1 to 4 of the present invention can reach more than 90%, and the highest DPPH and clearance can reach 92.6%. Meanwhile, the heat stability of the final products obtained in the examples 1 to 4 is good and can reach A grade, while the component A of the antioxidant camellia oil in the comparative example 5 is not winterized, and the heat stability of the final products is only B grade.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and decorations can be made without departing from the principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the present invention.
Claims (10)
1. An antioxidant camellia oil composition is characterized by comprising a component A and a component B, wherein the component A comprises camellia oil, and the component B comprises a camellia seed extracting solution; the camellia oil is winterized; the tea seed extract is an aqueous extract of oil-removed camellia seed residue.
2. The antioxidant camellia oil composition as claimed in claim 1, wherein the weight ratio of the component A to the component B is (3-8): (15 to 25).
3. A method for preparing the antioxidant camellia oil composition of claim 1 or 2, comprising the steps of:
preparing a component A: placing camellia oil in a container, heating to 50-60 ℃, stirring for 25-35 min, stopping heating, cooling to room temperature while stirring, transferring to an ice water bath, cooling to 0 ℃, standing, preserving heat for 22-26 h, and filtering to obtain a component A;
preparing a component B: crushing the camellia seed dregs without oil, sieving to obtain camellia seed dregs powder, and mixing the camellia seed powder and water according to the weight ratio of (0.8-1.2): and (2) mixing and uniformly mixing the components in the proportion of (2) to (4), heating and stirring the mixture, cooling the mixture to room temperature, and filtering the mixture to obtain a component B.
4. An antioxidant camellia oil shampoo comprising the antioxidant camellia oil composition of claim 1 or 2, comprising the following components:
18 to 33 portions of antioxidant camellia oil composition, 0.5 to 2 portions of tea saponin, 3 to 8 portions of lauryl surfactant, 0.5 to 2 portions of guar gum hydroxypropyl trimethyl ammonium chloride, 2 to 5 portions of coconut oil based surfactant, 2 to 6 portions of plant extract, 0.8 to 3 portions of softener, 0.1 to 0.5 portion of conjugated linoleic acid-arginine composition, 0.1 to 0.3 portion of essence and 30 to 70 portions of deionized water.
5. The antioxidant camellia oil shampoo as claimed in claim 4, wherein the lauryl surfactant is sodium lauroyl glutamate, ammonium laureth sulfate and sodium lauroyl sarcosinate, and the weight ratio of the sodium lauroyl glutamate, the ammonium laureth sulfate and the sodium lauroyl sarcosinate is (1.8-2.2): (0.8-1.3): (0.8-1.3).
6. The antioxidant camellia oil shampoo as defined in claim 4, wherein the plant extract is an aqueous extract of ginger, glossy privet fruit, polygonum multiflorum and eclipta alba; the weight ratio of ginger, glossy privet fruit, tuber fleeceflower root and eclipta alba in the plant extract is (4-6): (1-3): (1-3): (2-4).
7. The antioxidant camellia oil shampoo as defined in claim 4 wherein the cocoyl surfactant is cocamidopropyl betaine and sodium cocoamphoacetate in a weight ratio of (2-3) to (0.8-1.1); the softener is one or more of diethanol distearate, diethylene glycol monostearate and polydimethylsiloxane.
8. The antioxidant camellia oil shampoo as defined in claim 4, wherein the conjugated linoleic acid-arginine composition has a weight ratio of conjugated linoleic acid to arginine of (1.5-1.7): (0.9-1.1).
9. A method for preparing the anti-oxidation camellia oil shampoo as defined in any one of claims 4 to 8, wherein the method comprises the following steps:
weighing the raw materials according to a formula;
adding deionized water, lauryl surfactant and coconut oil-based surfactant into a reaction vessel, and heating while stirring uniformly;
sequentially adding tea saponin, guar gum hydroxypropyl trimethyl ammonium chloride, component B of the antioxidant camellia oil composition and the plant extract, and stirring uniformly;
sequentially adding the softener and the component A of the antioxidant camellia oil composition while stirring, and gradually cooling to 38-42 ℃ after uniformly stirring;
adding essence and conjugated linoleic acid-arginine composition, stirring, and cooling to room temperature to obtain antioxidant camellia oil shampoo.
10. The method for preparing the antioxidant camellia oil shampoo as defined in claim 9, wherein the heating while stirring is performed to 55-65 ℃.
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