CN102274473A - Compound natural plant hair loss preventing liquid and preparation method and application thereof in shampoo liquid - Google Patents
Compound natural plant hair loss preventing liquid and preparation method and application thereof in shampoo liquid Download PDFInfo
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- CN102274473A CN102274473A CN2011101981699A CN201110198169A CN102274473A CN 102274473 A CN102274473 A CN 102274473A CN 2011101981699 A CN2011101981699 A CN 2011101981699A CN 201110198169 A CN201110198169 A CN 201110198169A CN 102274473 A CN102274473 A CN 102274473A
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Abstract
The invention discloses compound natural plant hair loss preventing liquid and a preparation method and application thereof in shampoo liquid. The compound natural plant hair loss preventing liquid comprises the following raw materials: yerbadetajo herb, tamariskoid spikemoss herb, parslane herb, raw sessile stemona root, Japanese honeysuckle stem, raw tuber of multiflower knotweed, raw astragalus, densefruit pittany root-bark, frostbitten mulberry leaf, angelica dahurica, chebule flesh, thick dried rehmannia, mume fruit, dried ginger, cochinchnese asparagus root, root of red-rooted salvia, aleppo gall and pomegranate rind. The preparation method comprises the following steps of: mixing the raw materials, and decocting in water to obtain decoction; removing impurities from the decoction, concentrating to form paste, and cooling to obtain a pasty substance; dissolving the pasty substance by using ethanol fully, standing, removing insoluble substances, and concentrating the obtained solution until the content of the ethanol is lower than or equal to 3 percent to obtain the compound natural plant hair loss preventing liquid. The compound natural plant hair loss preventing liquid is reasonable in combination of the raw materials, has the effects of promoting blood stasis, removing blood stasis, warming meridian, removing obstruction in channels, inhibiting bacteria and diminishing inflammation, can promote blood circulation of hair and has the effects of hair loss prevention, hair growth and hair nourishing.
Description
Technical field
The invention belongs to the field of Chinese medicines and daily cosmetics technical field, be specifically related to a kind of compound natural loss preventing plant liquid and preparation method thereof and application in shampoo.
Background technology
Excessive in the modern society people life stress of working at ordinary times, the life-time service computer, anxiety, factor such as do not have enough sleep, people's alopecia phenomenon day by day increases, and is more and more serious, and the alopecia crowd presents the trend of rejuvenation.The pharmaceutical preparation of many treatment alopecias is arranged in the market, Western medicine price comparison costliness, and the course of treatment is longer, has increased patient's financial burden, and the medication meeting brings certain side effect to physical function for a long time.
Summary of the invention
Primary and foremost purpose of the present invention is to overcome above-mentioned the deficiencies in the prior art, and a kind of compound natural loss preventing plant liquid that anti-avulsion is educated outbreak usefulness that has is provided.Compound natural loss preventing plant liquid of the present invention goes for the scalp of various characteristics, does not have irritated reaction after cleaning hair with it, has no side effect, and makes medicine infiltrate skin rapidly, reaches the purpose of anti-alopecia.
Another object of the present invention is to provide the preparation method of described compound natural loss preventing plant liquid; This preparation method is simple, and is with low cost.
A further object of the present invention is to provide the application of described compound natural loss preventing plant liquid in shampoo.
Purpose of the present invention is achieved through the following technical solutions: a kind of compound natural loss preventing plant liquid is prepared from by following crude drug according to the mass fraction:
50～100 parts of Herba Ecliptaes, 10～50 parts of Herba Selaginellaes, 10～50 parts of Herba portulacaes, 10～50 parts of Radix Stemonae, 10～50 parts of Caulis Loniceraes, 1～35 part of Radix Polygoni Multiflori, 1～30 part of Radix Astragali, 1～30 part of Cortex Dictamni, 1～35 part of Folium Mori, 1～20 part of the Radix Angelicae Dahuricae, 1～20 part of Fructus Chebulae meat, 1～20 part of Radix Rehmanniae, 1～20 part of Fructus Mume, 1～20 part of Rhizoma Zingiberis, 1～20 part of Radix Asparagi, 1～20 part of Radix Salviae Miltiorrhizae, 1～20 part of Galla Turcica (Galla Helepensis), 1～20 part of Pericarpium Granati;
Described compound natural loss preventing plant liquid preferably is prepared from by following crude drug according to the mass fraction:
50～65 parts of Herba Ecliptaes, 30～35 parts of Herba Selaginellaes, 20～35 parts of Herba portulacaes, 25～35 parts of Radix Stemonae, 15～25 parts of Caulis Loniceraes, 20～35 parts of Radix Polygoni Multifloris, 10～30 parts of Radix Astragali, 10～25 parts of Cortex Dictamni, 15～35 parts of Folium Mori, 8～12 parts of the Radixs Angelicae Dahuricae, 5～8 parts of Fructus Chebulae meat, 3～5 parts of Radix Rehmanniae, 3～5 parts of Fructus Mume, 3～5 parts of Rhizoma Zingiberiss, 2～5 parts of Radix Asparagi, 2～5 parts of Radix Salviae Miltiorrhizae, 1～5 part of Galla Turcica (Galla Helepensis), 1～5 part of Pericarpium Granati;
Described compound natural loss preventing plant liquid more preferably is prepared from by following crude drug according to the mass fraction:
55 parts of Herba Ecliptaes, 30 parts of Herba Selaginellaes, 30 parts of Herba portulacaes, 25 parts of Radix Stemonae, 25 parts of Caulis Loniceraes, 20 parts of Radix Polygoni Multifloris, 20 parts of Radix Astragali, 20 parts of Cortex Dictamni, 20 parts of Folium Mori, 10 parts of the Radixs Angelicae Dahuricae, 5 parts of Fructus Chebulae meat, 5 parts of Radix Rehmanniae, 5 parts of Fructus Mume, 5 parts of Rhizoma Zingiberiss, 5 parts of Radix Asparagi, 5 parts of Radix Salviae Miltiorrhizae, 5 parts of Galla Turcica (Galla Helepensis)s, 5 parts of Pericarpium Granatis;
The preparation method of above-mentioned compound natural loss preventing plant liquid comprises the steps:
(1) with 50～100 mass parts Herba Ecliptae, 10～50 mass parts Herba Selaginellaes, 10～50 mass parts Herba portulacaes, 10～50 mass parts Radix Stemonae, 10～50 mass parts Caulis Loniceraes, 1～35 mass parts Radix Polygoni Multiflori, 1～30 mass parts Radix Astragali, 1～30 mass parts Cortex Dictamni, 1～35 mass parts Folium Mori, 1～20 mass parts Radix Angelicae Dahuricae, 1～20 mass parts Fructus Chebulae meat, 1～20 mass parts Radix Rehmanniae, 1～20 mass parts Fructus Mume, 1～20 mass parts Rhizoma Zingiberis, 1～20 mass parts Radix Asparagi, 1～20 mass parts Radix Salviae Miltiorrhizae, 1～20 mass parts Galla Turcica (Galla Helepensis) and 1～20 mass parts Pericarpium Granati mix, decocting obtains decocting liquid;
(2) decocting liquid is removed impurity after, be concentrated into paste, the cooling, obtain pasty masses;
(3) with ethanol the pasty masses that step (2) obtains is fully dissolved, leave standstill, remove insoluble substance, again solution concentration to the ethanol content that obtains is not higher than percent by volume 3%, obtain compound natural loss preventing plant liquid;
Described compound natural loss preventing plant liquid is dark-brown clarification magma, and deposit-free, no suspended substance have the distinctive hay-scented of Chinese medicine, have no irritating odor, and proportion is about 1.10, and every milliliter of magma contains about 1 gram of crude drug in whole;
Decocting described in the step (1) is preferably undertaken by the high pressure extract jar;
The number of times of the decocting described in the step (1) is preferably 3 times, and the time of decoction preferably was respectively 60 minutes, 60 minutes and 90 minutes;
Impurity described in the step (2) can be by filtering or the centrifugation removal;
Cooling described in the step (2) is preferably and naturally cools to room temperature;
The proportion of the pasty masses described in the step (2) is preferably 1.1;
Consumption of ethanol described in the step (3) is preferably 3 times that are equivalent to described pasty masses volume;
The time of leaving standstill described in the step (3) is preferably 12 hours;
The mode of removing insoluble substance described in the step (3) is preferably filtered or is centrifugal; More preferably filter by the plate and frame filter;
Spissated mode described in the step (3) is preferably concentrating under reduced pressure;
Described compound natural loss preventing plant liquid is educated the application of sending out in the preparation in anti-avulsion;
Described anti-avulsion is educated a preparation and is preferably shampoo;
A kind of compound natural loss preventing plant shampoo contains above-mentioned compound natural loss preventing plant liquid;
Described compound natural loss preventing plant shampoo also comprises laureth ammonium sulfate, ammonium lauryl sulfate, dodecanamide propyl betanin, dimethiconol, glycol distearate, hexadecyltrimethylammonium chloride, guar hydroxypropyltrimonium chloride, castor oil-base maleic acid esters, CI 77266 (aluminum color ingot), oxidic polyethylene, Methylisothiazolinone, methylchloroisothiazandnone, sodium chloride and citric acid;
Described compound natural loss preventing plant shampoo is preferably and comprises following component by mass percentage:
The preparation method of described compound natural loss preventing plant shampoo comprises following steps:
(1) with water, laureth ammonium sulfate, ammonium lauryl sulfate, dodecanamide propyl betanin, dimethiconol, glycol distearate, dodecane hexadecyltrimethylammonium chloride and guar hydroxypropyltrimonium chloride mixing, obtains the A phase;
(2) with castor oil-base maleic acid esters, CI 77266, oxidic polyethylene, Methylisothiazolinone and methylchloroisothiazandnone mixing, obtain the B phase;
(3), add compound natural loss preventing plant liquid, mixing with A heat phase to 85 ℃; Be cooled to 45 ℃, add the B phase, again mixing; Then add sodium chloride and citric acid, obtain compound natural loss preventing plant shampoo;
Wherein, used material is as follows by mass percentage: compound natural loss preventing plant liquid 15～25%, laureth ammonium sulfate 5～10%, ammonium lauryl sulfate 3～6%, dodecanamide propyl betanin 0.5～3%, dimethiconol 0.5～3%, glycol distearate 0.5～3%, hexadecyltrimethylammonium chloride 0.1～0.5%, guar hydroxypropyltrimonium chloride 0.1～0.5%, castor oil-base maleic acid esters 0.5～3%, CI 77266 (aluminum color ingot) 0.05～1%, oxidic polyethylene 0.1～0.5%, Methylisothiazolinone 0.1～0.5%, methylchloroisothiazandnone 0.1～0.5%, sodium chloride 0.1～1%, citric acid 0.01～0.5%.
Beneficial effect of the present invention:
(1) material matching of compound natural loss preventing plant liquid of the present invention is reasonable, and the compound natural loss preventing plant liquid that obtains has the effect of blood circulation promoting and blood stasis dispelling, promoting the flow of QI in the collateral by warming the meridian, inhibiting bacteria and diminishing inflammation, can promote the hair blood circulation, has the effect of anti-avulsion, generating and nourishing hair.
(2) preparation method of this compound natural loss preventing plant liquid is simple, with low cost.
(3) compound natural loss preventing plant shampoo of the present invention is dark-brown clarification magma, and no foreign body has the distinctive hay-scented of Chinese medicine, have no irritating odor, it not only has the effect of compound natural loss preventing plant liquid, and uses the back hair sliding along sheen, and certain anti-dandruff effect is arranged.
The specific embodiment
The present invention is further illustrated below in conjunction with specific embodiment.But technical scope of the present invention is not subjected to the qualification of these embodiment.
Embodiment 1
The crude drug quality of present embodiment is:
The adjuvant of the compound natural loss preventing plant shampoo of present embodiment is composed as follows:
The A phase: laureth ammonium sulfate 8kg, ammonium lauryl sulfate 3kg, dodecanamide propyl betanin 3kg, dimethiconol 0.5kg, glycol distearate 3kg, hexadecyltrimethylammonium chloride 0.1kg, guar hydroxypropyltrimonium chloride 0.3kg, water 62.29kg (A+B+C+ compound natural loss preventing plant liquid=100kg);
B phase: castor oil-base maleic acid esters 3kg, CI 77266 (aluminum color ingot) 0.3kg, oxidic polyethylene 0.1kg, Methylisothiazolinone 0.2kg, methylchloroisothiazandnone 0.2kg;
C: sodium chloride 1kg, citric acid 0.01kg.
Preparation process is as follows:
(1) preparation compound natural loss preventing plant liquid: crude drug is mixed, insert in the high pressure extract jar, add water, decoct 3 times, the time was respectively 60 minutes, 60 minutes and 90 minutes.Fried liquid is merged, filter, leave standstill clarification; Clarifying fried liquid is placed concentration tank, and evaporation and concentration is to the thick paste shape, and proportion was placed 12 hours about 1: 1, and thick paste is fully cooled off; Slowly add ethanol (95%v/v) inwards, make the interior ethanol content of extractum reach percent by volume (according to Chinese Pharmacopoeia, if no special instructions, alcoholic acid content ratio is percent by volume) 75% o'clock, stirred 30 minutes, make its abundant mixing, placed 24 hours, and made it abundant precipitation.Reuse plate and frame filter filters, and with decompression filtrate recycling ethanol, makes that ethanol content is not higher than 3% in the filtrate, obtains compound natural loss preventing plant liquid.This compound natural loss preventing plant liquid is dark-brown clarification magma, and deposit-free, no suspended substance have the distinctive hay-scented of Chinese medicine, have no irritating odor, and proportion is about 1.10, and every milliliter of ointment contains about 1 gram of crude drug in whole.
(2) preparation compound natural loss preventing plant shampoo: with A heat phase to 85 ℃, add 15kg compound natural loss preventing plant liquid, stirring and evenly mixing is cooled to 45 ℃ then, adds the B phase, the restir mixing; Then add C and regulate viscosity and pH, obtain compound natural loss preventing plant shampoo.The compound natural loss preventing plant shampoo that obtains is dark-brown clarification magma, and no foreign body has the distinctive hay-scented of Chinese medicine, has no irritating odor.
Embodiment 2
The crude drug quality of present embodiment is:
The adjuvant of the compound natural loss preventing plant shampoo of present embodiment is composed as follows:
The A phase: laureth ammonium sulfate 5kg, ammonium lauryl sulfate 6kg, dodecanamide propyl betanin 1.5kg, dimethiconol 1.5kg, glycol distearate 1.5kg, hexadecyltrimethylammonium chloride 0.3kg, guar hydroxypropyltrimonium chloride 0.1kg, water 65.05kg (A+B+C+ compound natural loss preventing plant liquid=100kg);
B phase: castor oil-base maleic acid esters 1.5kg, CI 77266 (aluminum color ingot) 0.05kg, oxidic polyethylene 0.5kg, Methylisothiazolinone 0.5kg, methylchloroisothiazandnone 0.5kg;
C: sodium chloride 0.5kg, citric acid 0.5kg.
(1) preparation compound natural loss preventing plant liquid: the above-mentioned raw materials medicine is mixed, insert in the high pressure extract jar, add water, decoct 3 times, the time was respectively 60 minutes, 60 minutes and 90 minutes.Fried liquid is merged, filter, leave standstill clarification; Clarifying fried liquid is placed concentration tank, and evaporation and concentration is to the thick paste shape, and proportion was placed 12 hours about 1: 1, and thick paste is fully cooled off; Slowly add ethanol (95%v/v) inwards, make the interior ethanol content of extractum reach at 75% o'clock, stirred 30 minutes, make its abundant mixing, placed 24 hours, make it abundant precipitation.Reuse plate and frame filter filters, and with decompression filtrate recycling ethanol, makes that ethanol content is not higher than 3% in the filtrate, obtains compound natural loss preventing plant liquid.This compound natural loss preventing plant liquid is dark-brown clarification magma, and deposit-free, no suspended substance have the distinctive hay-scented of Chinese medicine, have no irritating odor, and proportion is about 1.10, and every milliliter of ointment contains about 1 gram of crude drug in whole.
(2) preparation compound natural loss preventing plant shampoo: with A heat phase to 85 ℃, add 15kg compound natural loss preventing plant liquid, stirring and evenly mixing is cooled to 45 ℃ then, adds the B phase, the restir mixing; Then add C and regulate viscosity and pH, obtain compound natural loss preventing plant shampoo.The compound natural loss preventing plant shampoo that obtains is dark-brown clarification magma, and no foreign body has the distinctive hay-scented of Chinese medicine, has no irritating odor.
Embodiment 3
The crude drug quality of present embodiment is:
The adjuvant of the compound natural loss preventing plant shampoo of present embodiment is composed as follows:
The A phase: laureth ammonium sulfate 10kg, ammonium lauryl sulfate 4.5kg, dodecanamide propyl betanin 0.5kg, dimethiconol 3kg, glycol distearate 0.5kg, hexadecyltrimethylammonium chloride 0.5kg, guar hydroxypropyltrimonium chloride 0.5kg, water 63.3kg (A+B+C+ compound natural loss preventing plant liquid=100kg);
B phase: castor oil-base maleic acid esters 0.5kg, CI 77266 (aluminum color ingot) 1kg, oxidic polyethylene 0.3kg, Methylisothiazolinone 0.1kg, methylchloroisothiazandnone 0.1kg;
C: sodium chloride 0.1kg, citric acid 0.1kg.
(1) preparation compound natural loss preventing plant liquid: will go up crude drug and mix, and insert in the high pressure extract jar, and add water, and decoct 3 times, the time was respectively 60 minutes, 60 minutes and 90 minutes.Fried liquid is merged, filter, leave standstill clarification; Clarifying fried liquid is placed concentration tank, and evaporation and concentration is to the thick paste shape, and proportion was placed 12 hours about 1: 1, and thick paste is fully cooled off; Slowly add ethanol (95%v/v) inwards, make the interior ethanol content of extractum reach at 75% o'clock, stirred 30 minutes, make its abundant mixing, placed 24 hours, make it abundant precipitation.Reuse plate and frame filter filters, and with decompression filtrate recycling ethanol, makes that ethanol content is not higher than 3% in the filtrate, obtains compound natural loss preventing plant liquid.This compound natural loss preventing plant liquid is dark-brown clarification magma, and deposit-free, no suspended substance have the distinctive hay-scented of Chinese medicine, have no irritating odor, and proportion is 1.10, and every milliliter of ointment contains about 1 gram of crude drug in whole.
(2) preparation compound natural loss preventing plant shampoo: with A heat phase to 85 ℃, add 15kg compound natural loss preventing plant liquid, stirring and evenly mixing is cooled to 45 ℃ then, adds the B phase, the restir mixing; Then add C and regulate viscosity and pH, obtain compound natural loss preventing plant shampoo.The compound natural loss preventing plant shampoo that obtains is dark-brown clarification magma, and no foreign body has the distinctive hay-scented of Chinese medicine, has no irritating odor.
Embodiment 4
The crude drug quality of present embodiment is:
The adjuvant of the compound natural loss preventing plant shampoo of present embodiment is composed as follows:
The A phase: laureth ammonium sulfate 10kg, ammonium lauryl sulfate 4.5kg, dodecanamide propyl betanin 0.5kg, dimethiconol 3kg, glycol distearate 0.5kg, hexadecyltrimethylammonium chloride 0.5kg, guar hydroxypropyltrimonium chloride 0.5kg, water 53.3kg (A+B+C+ compound natural loss preventing plant liquid=100kg);
B phase: castor oil-base maleic acid esters 0.5kg, CI 77266 (aluminum color ingot) 1kg, oxidic polyethylene 0.3kg, Methylisothiazolinone 0.1kg, methylchloroisothiazandnone 0.1kg;
C: sodium chloride 0.1kg, citric acid 0.1kg.
(1) preparation compound natural loss preventing plant liquid: the above-mentioned raw materials medicine is mixed, insert in the high pressure extract jar, add water, decoct 3 times, the time was respectively 60 minutes, 60 minutes and 90 minutes.Fried liquid is merged, filter, leave standstill clarification; Clarifying fried liquid is placed concentration tank, and evaporation and concentration is to the thick paste shape, and proportion was placed 12 hours about 1: 1, and thick paste is fully cooled off; Slowly add ethanol (95%v/v) inwards, make the interior ethanol content of extractum reach at 75% o'clock, stirred 30 minutes, make its abundant mixing, placed 24 hours, make it abundant precipitation.Reuse plate and frame filter filters, and with decompression filtrate recycling ethanol, makes that ethanol content is not higher than 3% in the filtrate, obtains compound natural loss preventing plant liquid.This compound natural loss preventing plant liquid is dark-brown clarification magma, and deposit-free, no suspended substance have the distinctive hay-scented of Chinese medicine, have no irritating odor, and proportion is 1.10, and every milliliter of ointment contains about 1 gram of crude drug in whole.
(2) preparation compound natural loss preventing plant shampoo: with A heat phase to 85 ℃, add 25kg compound natural loss preventing plant liquid, stirring and evenly mixing is cooled to 45 ℃ then, adds the B phase, the restir mixing; Then add C and regulate viscosity and pH, obtain compound natural loss preventing plant shampoo.The compound natural loss preventing plant shampoo that obtains is dark-brown clarification magma, and no foreign body has the distinctive hay-scented of Chinese medicine, has no irritating odor.
Embodiment 5
The crude drug quality of present embodiment is:
The adjuvant of compound natural loss preventing plant shampoo of the present invention is composed as follows:
The A phase: laureth ammonium sulfate 8kg, ammonium lauryl sulfate 3kg, dodecanamide propyl betanin 3kg, dimethiconol 0.5kg, glycol distearate 3kg, hexadecyltrimethylammonium chloride 0.1kg, guar hydroxypropyltrimonium chloride 0.3kg, water 57.29kg (A+B+C+ compound natural loss preventing plant liquid=100kg);
B phase: castor oil-base maleic acid esters 3kg, CI 77266 (aluminum color ingot) 0.3kg, oxidic polyethylene 0.1kg, Methylisothiazolinone 0.2kg, methylchloroisothiazandnone 0.2kg;
C: sodium chloride 1kg, citric acid 0.01kg.
(1) preparation compound natural loss preventing plant liquid: the above-mentioned raw materials medicine is mixed, insert in the high pressure extract jar, add water, decoct 3 times, the time was respectively 60 minutes, 60 minutes and 90 minutes.Fried liquid is merged, filter, leave standstill clarification; Clarifying fried liquid is placed concentration tank, and evaporation and concentration is to the thick paste shape, and proportion was placed 12 hours about 1: 1, and thick paste is fully cooled off; Slowly add ethanol (95%v/v) inwards, make the interior ethanol content of extractum reach at 75% o'clock, stirred 30 minutes, make its abundant mixing, placed 24 hours, make it abundant precipitation.Reuse plate and frame filter filters, and with decompression filtrate recycling ethanol, makes that ethanol content is not higher than 3% in the filtrate, obtains compound natural loss preventing plant liquid.This compound natural loss preventing plant liquid is dark-brown clarification magma, and deposit-free, no suspended substance have the distinctive hay-scented of Chinese medicine, have no irritating odor, and proportion is about 1.10, and every milliliter of ointment contains about 1 gram of crude drug in whole.
(2) preparation compound natural loss preventing plant shampoo: with A heat phase to 85 ℃, add 20kg compound natural loss preventing plant liquid, stirring and evenly mixing is cooled to 45 ℃ then, adds the B phase, the restir mixing; Then add C and regulate viscosity and pH, obtain compound natural loss preventing plant shampoo.The compound natural loss preventing plant shampoo that obtains is dark-brown clarification magma, and no foreign body has the distinctive hay-scented of Chinese medicine, has no irritating odor.
Effect embodiment
Above embodiment is prepared compound natural loss preventing plant liquid carry out activity test, with observing effect.
The experiment number of every kind of compound natural loss preventing plant liquid is 20 people, male 10 examples, and women 10 examples all have pathologic baldness shape, the age: 18～45 years old.
Using method: (clean hair, every day 1 time, using 1 month continuously is 1 course of treatment, and 6 courses of treatment are as observation of curative effect to use compound natural loss preventing plant liquid.
Experimental result:
Criterion of therapeutical effect is divided into: (1) produce effects: do not have obvious alopecia, have a large amount of new hairs to generate; (2) effective: alopecia is controlled, has a small amount of new hair to generate; (3) invalid: no change before and after the treatment.
The curative effect of compound natural loss preventing plant liquid is as shown in table 1.
Table 1
| Produce effects | Effectively | Invalid | Total effective rate | |
| Embodiment 1 | 13 | 5 | 2 | 90％ |
| Embodiment 2 | 14 | 5 | 1 | 95％ |
| Embodiment 3 | 16 | 3 | 1 | 95％ |
| Embodiment 4 | 12 | 4 | 4 | 80％ |
| Embodiment 5 | 12 | 4 | 4 | 80％ |
The foregoing description is a preferred implementation of the present invention; but embodiments of the present invention are not restricted to the described embodiments; other any do not deviate from change, the modification done under spirit of the present invention and the principle, substitutes, combination, simplify; all should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (10)
1. compound natural loss preventing plant liquid is characterized in that this compound natural loss preventing plant liquid is prepared from by following crude drug according to the mass fraction:
1～20 part of 50～100 parts of Herba Ecliptaes, 10～50 parts of Herba Selaginellaes, 10～50 parts of Herba portulacaes, 10～50 parts of Radix Stemonae, 10～50 parts of Caulis Loniceraes, 1～35 part of Radix Polygoni Multiflori, 1～30 part of Radix Astragali, 1～30 part of Cortex Dictamni, 1～35 part of Folium Mori, 1～20 part of the Radix Angelicae Dahuricae, 1～20 part of Fructus Chebulae meat, 1～20 part of Radix Rehmanniae, 1～20 part of Fructus Mume, 1～20 part of Rhizoma Zingiberis, 1～20 part of Radix Asparagi, 1～20 part of Radix Salviae Miltiorrhizae, 1～20 part of Galla Turcica (Galla Helepensis) and Pericarpium Granati.
2. compound natural loss preventing plant liquid according to claim 1 is characterized in that this compound natural loss preventing plant liquid is prepared from by following crude drug according to the mass fraction:
1～5 part of 50～65 parts of Herba Ecliptaes, 30～35 parts of Herba Selaginellaes, 20～35 parts of Herba portulacaes, 25～35 parts of Radix Stemonae, 15～25 parts of Caulis Loniceraes, 20～35 parts of Radix Polygoni Multifloris, 10～30 parts of Radix Astragali, 10～25 parts of Cortex Dictamni, 15～35 parts of Folium Mori, 8～12 parts of the Radixs Angelicae Dahuricae, 5～8 parts of Fructus Chebulae meat, 3～5 parts of Radix Rehmanniae, 3～5 parts of Fructus Mume, 3～5 parts of Rhizoma Zingiberiss, 2～5 parts of Radix Asparagi, 2～5 parts of Radix Salviae Miltiorrhizae, 1～5 part of Galla Turcica (Galla Helepensis) and Pericarpium Granati.
3. compound natural loss preventing plant liquid according to claim 2 is characterized in that this compound natural loss preventing plant liquid is prepared from by following crude drug according to the mass fraction:
5 parts of 55 parts of Herba Ecliptaes, 30 parts of Herba Selaginellaes, 30 parts of Herba portulacaes, 25 parts of Radix Stemonae, 25 parts of Caulis Loniceraes, 20 parts of Radix Polygoni Multifloris, 20 parts of Radix Astragali, 20 parts of Cortex Dictamni, 20 parts of Folium Mori, 10 parts of the Radixs Angelicae Dahuricae, 5 parts of Fructus Chebulae meat, 5 parts of Radix Rehmanniae, 5 parts of Fructus Mume, 5 parts of Rhizoma Zingiberiss, 5 parts of Radix Asparagi, 5 parts of Radix Salviae Miltiorrhizae, 5 parts of Galla Turcica (Galla Helepensis)s and Pericarpium Granatis.
4. the preparation method of the described compound natural loss preventing plant of claim 1 liquid is characterized in that comprising the steps:
(1) with 50～100 mass parts Herba Ecliptae, 10～50 mass parts Herba Selaginellaes, 10～50 mass parts Herba portulacaes, 10～50 mass parts Radix Stemonae, 10～50 mass parts Caulis Loniceraes, 1～35 mass parts Radix Polygoni Multiflori, 1～30 mass parts Radix Astragali, 1～30 mass parts Cortex Dictamni, 1～35 mass parts Folium Mori, 1～20 mass parts Radix Angelicae Dahuricae, 1～20 mass parts Fructus Chebulae meat, 1～20 mass parts Radix Rehmanniae, 1～20 mass parts Fructus Mume, 1～20 mass parts Rhizoma Zingiberis, 1～20 mass parts Radix Asparagi, 1～20 mass parts Radix Salviae Miltiorrhizae, 1～20 mass parts Galla Turcica (Galla Helepensis) and 1～20 mass parts Pericarpium Granati mix, decocting obtains decocting liquid;
(2) decocting liquid is removed impurity after, be concentrated into paste, the cooling, obtain pasty masses;
(3) with ethanol the pasty masses that step (2) obtains is fully dissolved, leave standstill, remove insoluble substance, again solution concentration to the ethanol content that obtains is not higher than percent by volume 3%, obtain compound natural loss preventing plant liquid.
5. the preparation method of compound natural loss preventing plant liquid according to claim 4 is characterized in that:
Decocting described in the step (1) is for to be undertaken by the high pressure extract jar;
The number of times of the decocting described in the step (1) is 3 times, and the time of decoction was respectively 60 minutes, 60 minutes and 90 minutes;
Impurity described in the step (2) is for removing by filtration or centrifugation;
Being cooled to described in the step (2) naturally cools to room temperature;
The proportion of the pasty masses described in the step (2) is 1.1;
Consumption of ethanol described in the step (3) is to be equivalent to 3 times of described pasty masses volume;
The time of leaving standstill described in the step (3) is 12 hours;
The mode of removing insoluble substance described in the step (3) is filtration or centrifugal;
Spissated mode described in the step (3) is a concentrating under reduced pressure.
6. the application of each described compound natural loss preventing plant liquid of claim 1～3 is characterized in that: described compound natural loss preventing plant liquid is used to prepare anti-avulsion and educates a preparation.
7. a compound natural loss preventing plant shampoo contains each described compound natural loss preventing plant liquid of claim 1～3.
8. compound natural loss preventing plant shampoo according to claim 7 is characterized in that: described compound natural loss preventing plant shampoo also comprises laureth ammonium sulfate, ammonium lauryl sulfate, dodecanamide propyl betanin, dimethiconol, glycol distearate, hexadecyltrimethylammonium chloride, guar hydroxypropyltrimonium chloride, castor oil-base maleic acid esters, aluminum color ingot CI 77266, oxidic polyethylene, Methylisothiazolinone, methylchloroisothiazandnone, sodium chloride and citric acid.
9. compound natural loss preventing plant shampoo according to claim 8 is characterized in that comprising following component by mass percentage:
10. the preparation method of the described compound natural loss preventing plant of claim 9 shampoo is characterized in that comprising following steps:
(1) with water, laureth ammonium sulfate, ammonium lauryl sulfate, dodecanamide propyl betanin, dimethiconol, glycol distearate, dodecane hexadecyltrimethylammonium chloride and guar hydroxypropyltrimonium chloride mixing, obtains the A phase;
(2) with castor oil-base maleic acid esters, aluminum color ingot CI 77266, oxidic polyethylene, Methylisothiazolinone and methylchloroisothiazandnone mixing, obtain the B phase;
(3), add compound natural loss preventing plant liquid, mixing with A heat phase to 85 ℃; Be cooled to 45 ℃, add the B phase, again mixing; Then add sodium chloride and citric acid, obtain compound natural loss preventing plant shampoo;
Wherein, used material is as follows by mass percentage: compound natural loss preventing plant liquid 15～25%, laureth ammonium sulfate 5～10%, ammonium lauryl sulfate 3～6%, dodecanamide propyl betanin 0.5～3%, dimethiconol 0.5～3%, glycol distearate 0.5～3%, hexadecyltrimethylammonium chloride 0.1～0.5%, guar hydroxypropyltrimonium chloride 0.1～0.5%, castor oil-base maleic acid esters 0.5～3%, aluminum color ingot CI 772660.05～1%, oxidic polyethylene 0.1～0.5%, Methylisothiazolinone 0.1～0.5%, methylchloroisothiazandnone 0.1～0.5%, sodium chloride 0.1～1%, citric acid 0.01～0.5%.
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| CN102919419A (en) * | 2012-11-26 | 2013-02-13 | 李虹霖 | Puer tea composition with healthcare functions |
| CN103054776A (en) * | 2013-01-08 | 2013-04-24 | 李鹏 | Functional traditional Chinese medicinal stock shampoo and its preparation method |
| CN103505386A (en) * | 2012-06-26 | 2014-01-15 | 刘子平 | Fresh eclipta composition |
| CN103893050A (en) * | 2012-12-28 | 2014-07-02 | 漳州市格莱雅化妆品有限公司 | Anti-hair loss shampoo |
| CN104546663A (en) * | 2014-12-26 | 2015-04-29 | 广州市植美化妆品有限公司 | Liquid shampoo containing paenibacillus for preventing hair loss and thickening hair |
| CN104622785A (en) * | 2015-02-13 | 2015-05-20 | 南通蛇类治疗研究所 | Snakeskin, snake gall and natural plant functional shampoo |
| CN105997836A (en) * | 2016-05-13 | 2016-10-12 | 江燕馨 | Ferment liquid shampoo and preparation method thereof |
| CN107468618A (en) * | 2017-09-14 | 2017-12-15 | 贵州云上苗家康养有限公司 | A kind of Miao ethnic group's external application shampoo |
| CN108096174A (en) * | 2018-03-09 | 2018-06-01 | 广州市娇兰化妆品有限公司 | A kind of compound plant extract with hair care anti-off effect and preparation method and application |
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| CN103505386A (en) * | 2012-06-26 | 2014-01-15 | 刘子平 | Fresh eclipta composition |
| CN103505386B (en) * | 2012-06-26 | 2015-08-19 | 刘子平 | Fresh eclipta composition |
| CN102919419A (en) * | 2012-11-26 | 2013-02-13 | 李虹霖 | Puer tea composition with healthcare functions |
| CN103893050A (en) * | 2012-12-28 | 2014-07-02 | 漳州市格莱雅化妆品有限公司 | Anti-hair loss shampoo |
| CN103054776A (en) * | 2013-01-08 | 2013-04-24 | 李鹏 | Functional traditional Chinese medicinal stock shampoo and its preparation method |
| CN104546663A (en) * | 2014-12-26 | 2015-04-29 | 广州市植美化妆品有限公司 | Liquid shampoo containing paenibacillus for preventing hair loss and thickening hair |
| CN104546663B (en) * | 2014-12-26 | 2017-08-25 | 广州市植美化妆品有限公司 | A kind of phalacrosis prevention and hair generation shampoo containing series bacillus |
| CN104622785A (en) * | 2015-02-13 | 2015-05-20 | 南通蛇类治疗研究所 | Snakeskin, snake gall and natural plant functional shampoo |
| CN105997836A (en) * | 2016-05-13 | 2016-10-12 | 江燕馨 | Ferment liquid shampoo and preparation method thereof |
| CN105997836B (en) * | 2016-05-13 | 2018-10-16 | 江燕馨 | A kind of ferment shampoo and its preparation method |
| CN107468618A (en) * | 2017-09-14 | 2017-12-15 | 贵州云上苗家康养有限公司 | A kind of Miao ethnic group's external application shampoo |
| CN108096174A (en) * | 2018-03-09 | 2018-06-01 | 广州市娇兰化妆品有限公司 | A kind of compound plant extract with hair care anti-off effect and preparation method and application |
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