CN107496306A - Anti-inflammatory anti-acne tea seed foam mildy wash through desensitization process and preparation method thereof - Google Patents
Anti-inflammatory anti-acne tea seed foam mildy wash through desensitization process and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
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- A—HUMAN NECESSITIES
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61Q19/10—Washing or bathing preparations
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
A kind of anti-inflammatory anti-acne tea seed foam mildy wash through desensitization process, is uniformly mixed according to mass fraction by following component:65 80 parts of tea seed extract solution, 6 10 parts of ethoxylated alkyl sulfate, 38 parts of Cocoamidopropyl betaine, 4 10 parts of glycerine, 14 parts of water-soluble jojoba oil, 13 parts of Aloe Vera Gel, 0.1 0.5 parts of essence, 0.005 0.03 parts of preservative.The tea seed foam mildy wash realizes the complete desensitization of tea seed extract solution, arrange in pairs or groups water-soluble jojoba oil and Aloe Vera Gel, the face cleaning skin care having had the function that, anti-inflammatory anti-acne.
Description
Technical field
The present invention relates to a kind of foam mildy wash, particularly a kind of anti-inflammatory anti-acne tea seed foam through desensitization process is washed one's face
Milk.
Background technology
Family's washing product occupies very big share for a long time in Cosmetic Market, and in the last few years, in the market uses natural activity
The product of agent and plant source raw material is more and more, and consumer also increasingly likes buying such product, and what is be currently known is natural
Active component has tea seed powder, Chinese honey locust (fruit), soapberry, and as a kind of natural agents, tea seed powder but has anaphylactogen so that allergy sufferers
Pruitus, play erythema so that tea seed powder class product can not largely use tea seed powder raw material, so solving the anaphylactogen of tea seed powder
Problem, just tea seed powder class product can be enabled preferably to import market.
The content of the invention
An object of the present invention is to overcome existing tea seed extract solution allergic problem, there is provided a kind of anti-inflammatory through desensitization process
Anti-acne tea seed foam mildy wash.
The second object of the present invention is to provide the preparation method of above-mentioned mildy wash.
The technical scheme is that：
A kind of anti-inflammatory anti-acne tea seed foam mildy wash through desensitization process, is made up according to mass fraction of following component:Tea seed carries
Take liquid 65-80 parts, ethoxylated alkyl sulfate 6-10 parts, Cocoamidopropyl betaine 3-8 parts, glycerine 4-10 parts, water-soluble
Property jojoba oil 1-4 parts, Aloe Vera Gel 1-3 parts, essence 0.1-0.5 parts, preservative 0.005-0.03 parts.
Described raw material tea seed extract solution technique is specific as follows：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by n-hexane extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through 30-100 eye mesh screens, obtains camellia seed powder；
（4）Heat extraction：By step（3）Obtained camellia seed powder and deionized water mixing, mixed proportion 1:（3-10）, it is heated to 60
DEG C -100 DEG C, mixing speed is 20-60 revs/min, after stirring 40-60 minutes, adds adsorbent, and adsorbent addition is and tea
The weight ratio of seed powder is（1-2）：10, heating-up temperature is 60 DEG C -100 DEG C, and mixing time is 20-30 minutes, mixing speed 20-
60 revs/min, sedimentation centrifuge filters to get filtrate；Adsorbent is activated carbon and atlapulgite, adsorption specific surface area 1000m2/
g-1500m2/ g or adsorption capacity reach 80%-100%, are calculated with part by weight, activated carbon：Atlapulgite=1：（3-10）；
（5）It is refined：By step（4）The 1-6% diatomite of the filtrate addition filtrate weight of acquisition, is filtered by leaf-type filter, obtained
Camellia seed extract solution must be clarified.
Described preservative is Rhizoma Chuanxiong extract.
The preparation method of anti-inflammatory anti-acne tea seed foam mildy wash of the invention through desensitization process is as follows：
Ethoxylated alkyl sulfate heating stirring will be added in tea seed extract solution, Cocoamidopropyl betaine is added after dissolving
Stir, add glycerine, water-soluble jojoba oil, essence, Aloe Vera Gel and preservative after cooling, stir, obtain foam
Mildy wash.
Being capable of anti-inflammatory anti-acne the beneficial effects of the present invention are gained mildy wash.
Primary raw material used in the present invention is described as follows：
Camellia seed：It is the fruit of tea oil tree；Tea oil tree is the main woody oleiferous plants tree in China, is described as " east tree ", belongs to camellia
Section's Camellia evergreen dungarunga, it is the distinctive woody vegetable oil resource in China；3-6 meters of the height of tree, the diameter of a cross-section of a tree trunk 1.3 meters above the ground is up to 24-30 lis
Rice, smooth bark is taupe；Tea oil tree list leaf alternate, flower are both sexes white, and October, Post flowering was until fruit between October next year
Can be ripe, therefore, tea oil tree has rare flowers and fruits homophyletic phenomenon；Fruit is capsule, is mostly ellipse, has fine, soft fur；Seed
Mostly yellowish-brown, glossy, triangular shape；Tea oil tree is grown in remote mountains, inhales natural nutrient to the greatest extent, evergreen longevity, the age of tree up to 200 years with
On.
Ethoxylated alkyl sulfate:Colourless, white or pale yellow viscous liquid, smell for typical scent alkalescence it is cloudy from
Sub- surfactant；It is soluble in water, there is excellent decontamination, emulsification, foam performance and hard water resistance performance, gentle washing property
Skin will not be damaged, is widely used in the washing cosmetic articles for use such as shampoo, body lotion, dish washing detergent, compound soap.
Cocoamidopropyl betaine:It is a kind of zwitterionic surfactant, is respectively provided with acid and alkalescence condition
Excellent stability, presentation male and female is ionic respectively, is often used in combination with anions and canons and nonionic surfactant, its compatibility
Functional, excitant is small, soluble in water, and to ph stability, foam is more, strong detergency, has excellent thickening property, softness
Property, bactericidal properties, antistatic behaviour, hard water resistance property, can significantly improve washing class product softness, conditioning and low-temperature stability.
Glycerine：It is colourless sweet clear and bright thick liquid, it is odorless, there is warm sweet taste, there is good moisture-keeping function.
Deionized water：Refer to eliminate the pure water in after ionic species impurity, International Organization for standardization ISO/TC 147 is advised
Fixed " deionization " is defined as：" deionized water is complete or incompletely removes ionic species ", using the method system of RO counter-infiltrations
Take, the anion and cation gone using ion exchange resin in water removal.
Salt：Main component is NaCl, can increase the viscosity of matched somebody with somebody liquid.
Essence：The smell of finished product is adjusted, is allowed to pleasant comfortable.
Aloe Vera Gel：It is a kind of product formed with " freeze-stable method " technology from the middle extraction of natural herbs " aloe "；
Its purity is very high, has no toxic side effect；It is to hurting, abrading, wound festers, and operative scar etc. has obvious booster action, also
It is safe and reliable with good anti-inflammation and sterilization beauty functions.
Rhizoma Chuanxiong extract：Rhizoma Chuanxiong extract is to a variety of Gram-negative enteric bacterium, such as Escherichia coli, shigella dysenteriae, deformation
Bacillus, Pseudomonas aeruginosa, typhoid bacillus, paratyphosum Bacterium and comma bacillus etc. have inhibitory action, in addition in some pathogenic skins
Skin fungi and virus also have certain inhibitory action.
Water-soluble jojoba oil：Jojoba is be grown in South West USA and Mexico northwest one with Arid desert region one
Kind wild plant, the king of Ren Cheng worlds oil plant.The seed of Jojoba is extracted after squeezing, then with organic solvent, refines and obtains
Jojoba oil.Jojoba oil ethoxylation and propoxylation are obtained into water-soluble jojoba oil, are preferably applied for all kinds of cosmetics
In product.It is adapted to all skin quality, particularly dry, coarse, dark and gloomy, oiliness, whelk skin quality.Its permeability and heat-resisting quantity pole
Good, molecules align is very similar with the sebum of people, there is very significant beauty functions to skin.Unimpeded pore is can be used to, is adjusted
The fat secretion of oiliness or Combination skin, improve skin inflammation and sensitivity, eczema, chronic eczema, pimples etc..Its moist and moisturizing
Effect is very good, can increase moisture of skin, pre- anti-wrinkle and aging.
Embodiment
Embodiment 1
Tea seed extract solution used, is made up of following processing step in embodiment：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by n-hexane extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through the eye mesh screen of 30 mesh -100, obtains camellia seed
Powder；
（4）Heat extraction：By step（3）Obtained camellia seed powder and deionized water mixing, mixed proportion 1:4,70 DEG C are heated to, is stirred
Speed is mixed as 50 revs/min, after stirring 50 minutes, adds adsorbent, adsorbent addition is 2 for the weight ratio with tea seed powder：
10, heating-up temperature is 70 DEG C, and mixing time is 25 minutes, and mixing speed is 40 revs/min, and sedimentation centrifuge filters to get filtrate；
Described adsorbent is activated carbon and atlapulgite, and average adsorption specific surface area is respectively 1200m2/ g and 1300m2/ g, with weight
Ratio calculates, activated carbon：Atlapulgite=1：4；
（5）It is refined：By step（4）4% diatomite of the filtrate addition filtrate weight of acquisition, is filtered by leaf-type filter, obtained
Clarify camellia seed extract solution.
Above-mentioned tea seed extract solution is subjected to patch test, patch test results are without allergic reaction.
Method of testing is as follows:
Step 1：The gauze of four thickness is cut into a diameter of 1cm circle with scissors, totally 8, draws 25uL's respectively with liquid-transfering gun
Tea seed extract solution, is dropped on circular gauze, and blank is done with deionized water；
Step 2：The gripping of gauze tweezers is placed on subject（To tea seed extract solution allergy sufferers）At anteflexion arm, adhesive tape is used
Fix, start timing；
Step 3：Torn after 48h adhesive tape, and observe the reaction of skin at gauze covering immediately.
The tea seed extract solution that above-mentioned technique is obtained, 698.9 grams are taken, add 80 grams of heating of ethoxylated alkyl sulfate and stir
Mix, 60 grams of Cocoamidopropyl betaines are added after dissolving and are stirred, add 100g glycerine after cooling, 30g water solubilitys are suddenly
Bar oil suddenly, 1 gram of essence, 30 grams of Aloe Vera Gels, 0.1 gram of preservative Rhizoma Chuanxiong extract, stir, obtain foam mildy wash.
Embodiment 2-5, comparative example 1-2
Embodiment 2-5, comparative example 1-2 foam mildy wash, its preparation process condition simply raw material and are matched somebody with somebody substantially with embodiment 1
The conditions such as material ratio are slightly different, specifically as listed in table 1.
The embodiment 2-5 of table 1, comparative example 1-2 foam mildy wash preparation method
。
Comparative example 3
Comparative example 3 is only in that tea seed extraction liquid and preparation method thereof is different from the difference of embodiment 1.
Tea seed extract solution used in comparative example 3, is made up of following processing step：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by n-hexane extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through 50 eye mesh screens, obtains camellia seed powder；
（4）Heat extraction：By step（3）Obtained camellia seed powder and deionized water mixing, mixed proportion 1:4,70 DEG C are heated to, is stirred
Speed is mixed as 50 revs/min, after stirring 50 minutes, adds adsorbent, adsorbent addition is 2 for the weight ratio with tea seed powder：
10, heating-up temperature is 70 DEG C, and mixing time is 25 minutes, and mixing speed is 40 revs/min, and sedimentation centrifuge filters to get filtrate；
For described adsorbent only with activated carbon, dosage is identical with total dosage of activated carbon in embodiment 1 and atlapulgite；
（5）It is refined：By step（4）4% diatomite of the filtrate addition filtrate weight of acquisition, is filtered by leaf-type filter, obtained
Clarify camellia seed extract solution.
Foam mildy wash obtained by embodiment 1-5, comparative example 1-3 is tested into its oil-control, acne-removing inflammation-diminishing.
Its functional attributes test result of foam mildy wash obtained by the embodiment 1-5 of table 2, comparative example 1-3
。
Used in its functional attributes and the physical and chemical index test of foam mildy wash obtained by embodiment 2-5, comparative example 1-3
Method of testing has：
(1) method of testing of oil-control is tested for facial skin, and specific method is as follows：
By a kind of anti-inflammatory anti-acne tea seed foam mildy wash through desensitization process obtained by embodiment 2-5, comparative example 1-3 with it is commercially available
Anti-acne foam mildy wash, make two pumps with pump head and be uniformly applied to the palm of the hand that has drenched, after rubbing, be applied to the face's skin drenched
Skin, and repeated massage is washed by rubbing with the hands, when foam fully it is abundant can not be further added by when, experience foaming abundancy degree, then rinsed with clear water
Totally, record was rinsed to the clean time, and untill not glutinous soapy feeling, with clean towel water purification beads, skin is used after 2 hours
Physiological function tester detection face T areas oil quantity（Note：Face's oil quantity is detected before being washed one's face using mildy wash, and is remembered
Record）.Statistical result such as table 3：
A kind of anti-inflammatory anti-acne tea seed foam mildy wash trial effect through desensitization process of table 3
。
From table 3, it can be seen that its oil-control effect is related to the addition of tea seed extract and the addition of active matter is related,
The Controlling oil effect of simple addition surfactant is very poor, and collocation tea seed extract oil-control effect is fairly good.
Embodiment 2-5, the comparative example 1-3 anti-inflammatory anti-acne tea seed foam mildy wash anti-inflammatory anti-acne effect through desensitization process are surveyed
Method for testing is as follows：
Embodiment 2-5, comparative example 1-3 the anti-inflammatory anti-acne tea seed foam mildy wash through desensitization process are washed with commercially available tea seed foam
Face milk（Make to ratio）10 triers for having whelk are chosen respectively, are tried out 2 months, count rehabilitation situation quantity, count feelings
Condition such as table 4.
The tea seed foam mildy wash anti-inflammatory repairing effect quantity statistics table of table 4
。
From table 4, it can be seen that treatment and reparation to whelk play the role of it is apparent, arrange in pairs or groups Aloe Vera Gel after effect more
It is good.
In addition, by the anti-inflammatory anti-acne tea seed foam mildy wash through desensitization process obtained by embodiment 2-5, comparative example 1-3, lead to
Cross inspection microbiological indicator, sanitary index《Cosmetics safety technical specification》（Version in 2015）, obtain the detection shown in table 5 below
As a result：
The embodiment 2-5 of table 5, comparative example 1-3 foam mildy wash microorganism sanitary index
。
Anti-inflammatory anti-acne tea seed foam mildy wash toxicology test of the invention through desensitization process：Skin irritation test（It is more
Secondary skin irritation test）
Test objective：Observe rabbit intact skin long-time multiple-contact tested material（The mildy wash of embodiments of the invention）Afterwards
Caused skin irritation reaction, is carried for the anti-inflammatory anti-acne tea seed foam mildy wash through desensitization process of embodiments of the invention
For security foundation.
Test basis：《Cosmetics safety technical specification》Version in 2015；Test method：From white New Zealand rabbits 8, with
Machine is divided into 2 groups, every group 4.A groups:Experimental group, B groups:Deionized water control group；24h is by family's rabbit back backbone both sides before experiment
Hair is cut, and skin surface is not damaged in cropping, and unhairing scope is 3cm × 3cm, and application area is 2.5cm × 2.5cm, tested
Anti-inflammatory anti-acne tea seed foam mildy wash through desensitization process of the thing group to various embodiments of the present invention, takes tested material 0.5ml direct
The side of back backbone is coated in, opposite side applies 0.5ml control group deionized waters, smears 1 time daily, continuously smear 14d；From second
It starts, cropping when smearing every time, and residual tested material is removed with deionized water.Result is observed after one hour, according to《Cosmetics
Technical specification of security》（Version in 2015）Skin irritation test table scoring, check plot and trial zone are equally handled.
Evaluation of result：Every rabbit average integral daily is calculated according to the following formula, is pierced by specification list deciding rabbit skin
Swash intensity, and observe other toxic actions in addition to excitant.
。
Result of the test：Tested material was carried out in the multiple skin irritation test observation period, gave various embodiments of the present invention
After the anti-inflammatory anti-acne tea seed foam mildy wash of desensitization process, rabbit has no erythema, oedema；Have no systemic toxicity profiles performance and dead
Die situation, the weight of animals increase, on breathing, circulating, central nervous system, four limbs activity etc. is without influence.
Conclusion (of pressure testing)：The anti-inflammatory anti-acne tea seed foam mildy wash through desensitization process of various embodiments of the present invention is new to white
Western blue rabbit intact skin is nonirritant.
Claims (6)
1. a kind of anti-inflammatory anti-acne tea seed foam mildy wash through desensitization process, is made up according to mass fraction of following component:Tea seed
Extract solution 65-80 parts, ethoxylated alkyl sulfate 6-10 parts, Cocoamidopropyl betaine 3-8 parts, glycerine 4-10 parts, water
Dissolubility jojoba oil 1-4 parts, Aloe Vera Gel 1-3 parts, essence 0.1-0.5 parts, preservative 0.005-0.03 parts.
2. the anti-inflammatory anti-acne tea seed foam mildy wash according to claim 1 through desensitization process, it is characterised in that：Described
Tea seed extract solution technique is specific as follows：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag by n-hexane extraction, acquisition is deoiled camellia seed slag；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through the eye mesh screen of 30 mesh -100, obtains camellia seed
Powder；
（4）Heat extraction：By step（3）Obtained camellia seed powder and deionized water mixing, mixed proportion 1:（3-10）, it is heated to
60-100 DEG C, mixing speed is 20-60 revs/min, after stirring 40-60 minutes, adds adsorbent, adsorbent addition is and tea
The weight ratio of seed powder is（1-2）：10, heating-up temperature is 60-100 DEG C, and mixing time is 20-30 minutes, mixing speed 20-60
Rev/min, sedimentation centrifuge filters to get filtrate；
（5）It is refined：By step（4）The filtrate of acquisition re-adds filtrate weight 1-6% diatomite, is filtered by leaf-type filter,
Obtain clarification camellia seed extract solution.
3. the anti-inflammatory anti-acne tea seed foam mildy wash according to claim 2 through desensitization process, it is characterised in that：Step
（4）Described in adsorbent be activated carbon and atlapulgite, calculated with part by weight, activated carbon：Atlapulgite=1：（3-10）.
4. the anti-inflammatory anti-acne tea seed foam mildy wash according to claim 2 through desensitization process, it is characterised in that：Step
（4）Described in activated carbon of sorbent and atlapulgite, average adsorption specific surface area is 1200-1500m2/g。
5. the anti-inflammatory anti-acne tea seed foam mildy wash according to claim 1 through desensitization process, it is characterised in that：Described
Preservative is Rhizoma Chuanxiong extract.
6. the preparation method of the anti-inflammatory anti-acne tea seed foam mildy wash through desensitization process, its feature exist according to claim 1
In comprising the following steps：Ethoxylated alkyl sulfate heating stirring will be added in tea seed extract solution, cocounut oil acyl is added after dissolving
Amine CAB stirs, and adds glycerine, water-soluble jojoba oil, essence, Aloe Vera Gel and preservative, stirring after cooling
Uniformly, foam mildy wash is obtained.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109674668A (en) * | 2019-01-21 | 2019-04-26 | 秋臣化妆品有限公司 | A kind of anti-acne draft stoste and preparation method thereof |
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Application publication date: 20171222 |