CN107595707A - Camellia seed stoste and preparation method thereof - Google Patents
Camellia seed stoste and preparation method thereof Download PDFInfo
- Publication number
- CN107595707A CN107595707A CN201710973005.6A CN201710973005A CN107595707A CN 107595707 A CN107595707 A CN 107595707A CN 201710973005 A CN201710973005 A CN 201710973005A CN 107595707 A CN107595707 A CN 107595707A
- Authority
- CN
- China
- Prior art keywords
- camellia seed
- stoste
- preparation
- slag
- obtains
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
A kind of preparation method of camellia seed stoste, in turn includes the following steps：（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；（2）Leach：By step（1）Camellia seed slag is obtained by extraction, obtains the camellia seed slag that deoils；（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, sieving, obtains camellia seed powder；（4）Heat extraction：By step（3）Obtained camellia seed powder and deionized water proportionally mix, and after heating stirring, add adsorbent, continuous heating stirring, filter to get filtrate；（5）It is refined：By step（4）The filtrate addition filter aid of acquisition, is filtered by filter, obtains clarification camellia seed stoste.The technique realizes the extraction skill of Tea Saponin in ancient method camellia seed, while causes the reservation of the benefit materials such as Tea Polyphenols contained therein, tea polysaccharide, and desensitizes completely so that camellia seed stoste can be able to extensive use in Cosmetic Market, improve its security.
Description
Technical field
The present invention relates to a kind of camellia seed stoste and preparation method thereof, particularly a kind of camellia seed stoste through desensitization process
And preparation method thereof.
Background technology
The Aqueous extracts of teaseed cake dregs are a kind of abstersive cleaning suppliess of traditional tool in south China, wherein containing
Tea Saponin be a kind of natural nonionic surfactant, there is the effect such as anti-inflammation and sterilization, can also be by tea seed cake with water extraction
The materials such as water soluble tea cake protein, tea polysaccharide in the dregs of rice extract, long-term use have it is anti-dandruff, antipruritic, deoil, sterilize, black hair
The effect of, but its Aqueous extracts is applied can allergic phenomena in cosmetics, causes user's skin erythema, itch, its safety
Property certain risk be present, therefore find one kind and can effectively desensitize, the method that and can is effectively retained effectively nutritional ingredient therein is
Solves the unique channel of tea seed stoste application in cosmetics.
The content of the invention
The purpose of the present invention is to overcome existing tea seed stoste allergic problem, finds a kind of extracting method that can effectively desensitize.
The technical scheme is that the preparation method of camellia seed stoste, in turn includes the following steps：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, sieving, obtains camellia seed powder；
（4）Heat extraction：By step（3）Obtained camellia seed powder and deionized water proportionally mix, after heating stirring, addition absorption
Agent, continuous heating stirring, filters to get filtrate；
（5）It is refined：By step（4）The filtrate addition filter aid of acquisition, is filtered by filter, obtains clarification camellia seed stoste.
Wherein step（2）Described in solvent be n-hexane.
Wherein step（3）Described in camellia seed powder particles degree be the mesh of 30 mesh -100.
Wherein step（4）Described in camellia seed powder and deionized water mixed proportion be 1:（3-10）, heating-up temperature 60
DEG C -100 DEG C, mixing time is 40-60 minutes, and mixing speed is 20-60 revs/min.
Wherein step（4）Described in adsorbent addition be to be with the weight ratio of tea seed powder（1-2）：10, heating-up temperature
For 60 DEG C -100 DEG C, mixing time is 20-30 minutes, and mixing speed is 20-60 revs/min.
Wherein described decolorising agent is activated carbon and atlapulgite compounding（Adsorption specific surface area 1000m2/g-1500m2/ g or
Adsorption capacity reaches 80%-100%）, activated carbon：Atlapulgite=1：（3-10）.Wherein step（4）Described in filtering using heavy
Centrifuge is dropped, under specific adsorption specific surface area or adsorption capacity, is combined, can effectively removed by activated carbon and atlapulgite
Sensitizer and pigment, and retentive activity thing very well.
Wherein step（5）Described in filtering use leaf-type filter.
Wherein step（5）Using filter aid diatomite, addition is the 1-6% of liquid weight.
Present invention additionally comprises the camellia seed stoste that the above method obtains.
Beneficial effects of the present invention are as follows：
The technique realizes the skill of Tea Saponin in ancient method extraction camellia seed, while causes Tea Polyphenols contained therein, tea polysaccharide
Deng the extraction of benefit materials, and desensitize completely so that camellia seed extraction liquid energy is able to extensive use in Cosmetic Market, improves it
Security.
Primary raw material used in the present invention is described as follows：
Camellia seed：It is the fruit of tea oil tree；Tea oil tree is the main woody oleiferous plants tree in China, is described as " east tree ", belongs to camellia
Section's Camellia evergreen dungarunga, it is the distinctive woody vegetable oil resource in China；3-6 meters of the height of tree, the diameter of a cross-section of a tree trunk 1.3 meters above the ground is up to 24-30 lis
Rice, smooth bark is taupe.Tea oil tree list leaf alternate, flower are both sexes white, and October, Post flowering was until fruit between October next year
Can be ripe, therefore, tea oil tree has rare flowers and fruits homophyletic phenomenon.Fruit is capsule, is mostly ellipse, has fine, soft fur.Seed
Mostly yellowish-brown, glossy, triangular shape；Tea oil tree is grown in remote mountains, inhales natural nutrient to the greatest extent, evergreen longevity, the age of tree was up to 200 years
More than.
Deionized water：Refer to eliminate the pure water in after ionic species impurity, International Organization for standardization ISO/TC 147 is advised
Fixed " deionization " is defined as：" deionized water is complete or incompletely removes ionic species；" using the method system of RO counter-infiltrations
Take, the anion and cation gone using ion exchange resin in water removal.
Embodiment
In order to illustrate more clearly of the present invention, following examples are enumerated, but its scope to invention is without any restrictions.
Wherein in embodiment the average adsorption specific surface area of activated carbon of sorbent and atlapulgite be respectively 1200m2/g and
1300m2/g。
Embodiment 1
The tea seed stoste of embodiment 1, is made up of following processing step：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, is sieved through 60 eye mesh screens, obtains camellia seed powder；
（4）Heat extraction：By step（3）Obtained 1000 grams of camellia seed powder mixes for 6000 grams with deionized water, is heated to 60 DEG C, stirring
After 50min, 159 grams of adsorbent is added, is heated to 80 DEG C, after stirring 25min, sedimentation centrifuge filters to get filtrate 5310 grams；
（5）It is refined：By step（4）The filtrate of acquisition adds 60 grams of diatomite, is filtered by leaf-type filter, obtains clarification camellia
5270 grams of seed stoste.
Embodiment 2-6
Embodiment 2-6 tea seed extract solution process of preparing, its preparation process condition is substantially with embodiment 1, and simply reaction is former
The condition such as material and proportion scale, temperature, time is slightly different, specifically as listed in table 1.
The embodiment 1-6 of table 1 tea seed extract solution preparation process condition
。
Color and luster and active quantities detection are carried out according to the gained tea seed stoste of table 1, the results are shown in Table 2.
The tea seed stoste testing result of table 2
。
Color and luster influences cosmetic appearance, and yellowish-brown is natural tea seed color.Active matter content influences clean effect.
Embodiment 1-6 and comparative example 1-5 tea seed extract solution is subjected to patch test, patch test results such as table 3 arranges.
The tea seed extract solution patch test results of table 3
。
Note：- without allergic reaction；± doubtful allergy；+ slight allergy；++ allergy；+++ severe allergy
Used method of testing is as follows in table 3:
Step 1：The gauze of four thickness is cut into a diameter of 1cm circle with scissors, totally 8, draws 25uL mountains respectively with liquid-transfering gun
Tea seed stoste, is dropped on circular gauze, and blank is done with deionized water；
Step 2：The gripping of gauze tweezers is placed on subject（To tea seed stoste allergy sufferers）At anteflexion arm, consolidated with adhesive tape
Set, start timing；
Step 3：Torn after 48h adhesive tape, and observe the reaction of skin at gauze covering immediately, observation result such as table 3 above institute
Show.
As can be seen from Table 3, the desensitization effect of embodiment is good, and is best suitable for cosmetics on tea seed stoste color and luster and activity and answers
With.
Camellia seed stoste toxicology test of the present invention：Skin irritation test（Multiple skin irritation test）.
Test objective：Observe rabbit intact skin long-time multiple-contact tested material（The camellia seed of embodiments of the invention
Stoste）Caused skin irritation reaction afterwards, security foundation is provided for the camellia seed stoste of embodiments of the invention.
Test basis：《Cosmetics health specification》Version in 2007；Test method：From white New Zealand rabbits 8, random point
For 2 groups, every group 4；A groups:Experimental group, B groups:Deionized water control group；24h is by family's rabbit back backbone both sides hair before experiment
Cut, do not damage skin surface in cropping, unhairing scope is 3cm × 3cm, and application area is 2.5cm × 2.5cm, tested material group
To the camellia seed stoste of various embodiments of the present invention, tested material 0.5ml is taken to be coated directly on the side of back backbone, opposite side applies
0.5ml control group deionized waters, smear 1 time daily, continuously smear 14d；Since second day, cropping when smearing every time, spend
Ionized water removes residual tested material；Result is observed after one hour, according to《Cosmetics health specification》The skin thorn of version in 2007
Swash property experiment table scoring, check plot and trial zone are equally handled.
Evaluation of result：Every rabbit average integral daily is calculated according to the following formula, is pierced by specification list deciding rabbit skin
Swash intensity, and observe other toxic actions in addition to excitant.
。
Result of the test：Tested material was carried out in the multiple skin irritation test observation period, gave various embodiments of the present invention
Through desensitize PROCESS FOR TREATMENT tea seed stoste after, rabbit has no erythema, oedema；Systemic toxicity profiles performance and death condition are had no, is moved
Thing increased weight, on breathing, circulating, central nervous system, four limbs activity etc. is without influence.
Conclusion (of pressure testing)：The camellia seed stoste of various embodiments of the present invention is nonirritant to white New Zealand rabbits intact skin.
Claims (9)
1. a kind of preparation method of camellia seed stoste, in turn includes the following steps：
（1）Squeezing：Tea seed is squeezed and obtains camellia seed slag；
（2）Leach：By step（1）Camellia seed slag is obtained by extraction, obtains the camellia seed slag that deoils；
（3）Crush：By step（2）The obtained camellia seed ground-slag that deoils is broken, sieving, obtains camellia seed powder；
（4）Heat extraction：By step（3）Obtained camellia seed powder and deionized water proportionally mix, after heating stirring, addition absorption
Agent, continuous heating stirring, filters to get filtrate；
（5）It is refined：By step（4）The filtrate addition filter aid of acquisition, is filtered by filter, obtains clarification camellia seed stoste；
Wherein step（4）Described adsorbent is activated carbon and atlapulgite, adsorption specific surface area 1000-1500m2/ g or suction
Attached ability reaches 80-100%, activated carbon：Atlapulgite=1：（3-10）.
2. the preparation method of camellia seed stoste according to claim 1, it is characterised in that step（2）Described in solvent be
N-hexane.
3. the preparation method of camellia seed stoste according to claim 1, it is characterised in that step（3）Described in camellia seed
Powder particles degree is 30-100 mesh.
4. according to the preparation method of the camellia seed stoste described in claim 1, it is characterised in that step（4）Described in camellia
Seed powder and deionized water mixed proportion are 1:（3-10）, heating-up temperature is 60-100 DEG C, and mixing time is 40-60 minutes, stirring
Speed is 20-60 revs/min.
5. according to the preparation method of the camellia seed stoste described in claim 1, it is characterised in that step（4）Described in absorption
Agent addition is to be with the weight ratio of tea seed powder（1-2）：10, heating-up temperature is 60-100 DEG C, and mixing time is 20-30 minutes,
Mixing speed is 20-60 revs/min.
6. according to the preparation method of the camellia seed stoste described in claim 1, it is characterised in that step（4）Described in filtering
Using sedimentation centrifuge.
7. according to the preparation method of the camellia seed stoste described in claim 1, it is characterised in that step（5）Described in filtering
Using leaf-type filter.
A kind of 8. preparation method of camellia seed stoste according to claim 1, it is characterised in that：The step（5）Using
Filter aid diatomite, addition are the 1-6% of filtrate weight.
9. the camellia seed stoste obtained using any camellia seed stoste preparation methods of claim 1-8.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710973005.6A CN107595707A (en) | 2017-10-18 | 2017-10-18 | Camellia seed stoste and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710973005.6A CN107595707A (en) | 2017-10-18 | 2017-10-18 | Camellia seed stoste and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107595707A true CN107595707A (en) | 2018-01-19 |
Family
ID=61077402
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710973005.6A Pending CN107595707A (en) | 2017-10-18 | 2017-10-18 | Camellia seed stoste and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107595707A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110637836A (en) * | 2019-09-29 | 2020-01-03 | 湖南粮食集团有限责任公司 | Extraction method of nanoscale bacteriostatic camellia seed extract |
| CN110787122A (en) * | 2019-12-10 | 2020-02-14 | 武汉轻工大学 | Camellia seed oil skin cream and preparation method thereof |
| CN117778095A (en) * | 2023-08-07 | 2024-03-29 | 湖南金昌生物技术有限公司 | Preparation method of camellia seed extract |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103833819A (en) * | 2014-02-12 | 2014-06-04 | 安徽省华银茶油有限公司 | New technology for extraction of tea saponin from tea seed meal |
| CN105461778A (en) * | 2015-10-29 | 2016-04-06 | 广东星汇生物科技有限公司 | Method for extracting tea saponin from sasangua cake |
| CN106635453A (en) * | 2016-12-30 | 2017-05-10 | 湖南林之神生物科技有限公司 | Fruit and vegetable cleaning fluid containing oiltea seed extract and preparation method of fruit and vegetable cleaning fluid |
-
2017
- 2017-10-18 CN CN201710973005.6A patent/CN107595707A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103833819A (en) * | 2014-02-12 | 2014-06-04 | 安徽省华银茶油有限公司 | New technology for extraction of tea saponin from tea seed meal |
| CN105461778A (en) * | 2015-10-29 | 2016-04-06 | 广东星汇生物科技有限公司 | Method for extracting tea saponin from sasangua cake |
| CN106635453A (en) * | 2016-12-30 | 2017-05-10 | 湖南林之神生物科技有限公司 | Fruit and vegetable cleaning fluid containing oiltea seed extract and preparation method of fruit and vegetable cleaning fluid |
Non-Patent Citations (1)
| Title |
|---|
| 秦卫东: "《食品添加剂学》", 28 February 2014 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110637836A (en) * | 2019-09-29 | 2020-01-03 | 湖南粮食集团有限责任公司 | Extraction method of nanoscale bacteriostatic camellia seed extract |
| CN110637836B (en) * | 2019-09-29 | 2021-05-14 | 湖南粮食集团有限责任公司 | Extraction method of nanoscale bacteriostatic camellia seed extract |
| CN110787122A (en) * | 2019-12-10 | 2020-02-14 | 武汉轻工大学 | Camellia seed oil skin cream and preparation method thereof |
| CN117778095A (en) * | 2023-08-07 | 2024-03-29 | 湖南金昌生物技术有限公司 | Preparation method of camellia seed extract |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105997735B (en) | A kind of natural hair-washing hair-care articles and its preparation method and application | |
| CN109157454B (en) | Camellia japonica combined extract, preparation method thereof and application thereof in cosmetics | |
| CN107595707A (en) | Camellia seed stoste and preparation method thereof | |
| CN109247627A (en) | A kind of preparation method of Chinese medicine antibacterial underwear fabric | |
| KR20130113729A (en) | The functional beauti-pacl and its manufacturing method | |
| CN107693419A (en) | Nourish moisturizing camellia oleifera fruit shower cream and preparation method thereof | |
| CN107568548B (en) | Sophora flower bud solid beverage and preparation method thereof | |
| KR101809182B1 (en) | Composition for wound dressing with natural extract | |
| CN107496270A (en) | A kind of moist moisturizing anti-inflammatory anti-acne tea seed mildy wash and preparation method thereof | |
| CN107496275A (en) | Camellia seed washes clean stoste and preparation method thereof | |
| JP2001519657A (en) | A bifurcation method for processing whole aloe leaves | |
| CN107550796B (en) | Desensitized itching-relieving, dandruff-removing and hair-loss-preventing tea seed shampoo and preparation method thereof | |
| CN108066228B (en) | Moisturizing antibacterial shower gel and preparation method thereof | |
| CN107496272A (en) | Black hair tea seed shampoo and preparation method thereof | |
| CN110693797A (en) | Essence for bright eyes | |
| CN107496308A (en) | Facial mask stoste and preparation method thereof is nourished in the reparation of camellia anti-acne | |
| CN107510639A (en) | Camellia oleifera fruit facial mask stoste and preparation method thereof | |
| CN107496306A (en) | Anti-inflammatory anti-acne tea seed foam mildy wash through desensitization process and preparation method thereof | |
| CN107550797B (en) | Desensitized anti-inflammation moistening and repairing tea seed shower gel and preparation method thereof | |
| CN107625688A (en) | Camellia seed extract solution and preparation method thereof | |
| CN107625689B (en) | Camellia oleifera fruit washing-free hair cleaning agent, preparation method and use method | |
| CN107648107A (en) | Camellia replenishing water and preserving moisture toner and preparation method thereof | |
| CN107213098A (en) | A kind of longan seed Deacne pack and preparation method thereof | |
| WO2022018618A1 (en) | An anti-burn herbal gel emulsion and a method for preparation thereof | |
| CN107496273A (en) | Camellia oleifera fruit mildy wash and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180119 |