CN108451818A - A kind of elm bark extracting solution and its preparation method and application - Google Patents
A kind of elm bark extracting solution and its preparation method and application Download PDFInfo
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- CN108451818A CN108451818A CN201810358983.4A CN201810358983A CN108451818A CN 108451818 A CN108451818 A CN 108451818A CN 201810358983 A CN201810358983 A CN 201810358983A CN 108451818 A CN108451818 A CN 108451818A
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- Prior art keywords
- elm bark
- extracting solution
- preparation
- bark extracting
- skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Dermatology (AREA)
- Microbiology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of elm bark extracting solution and its preparation method and application, elm bark drying and crushing is crossed into 100~150 mesh sieve in the present invention, is packed into the gauze bag to sterilize；According to solid-liquid ratio 1:10~15 are added digestion agent, extracting through microwave heating, and filtering takes filtrate；By vacuum distillation, elm bark extracting solution is obtained.And applied in shower cream, there is significant antibacterial and whitening function, property is mild, non-stimulated skin effect；Elm bark extracting solution is applied in preparing shower cream, each ingredient in combined formulation so that shower cream not only has good detergency, moreover it is possible to generate good bacteriostasis, reduce the itch of skin, and skin whitening, neck skin is more pale beautiful.
Description
Technical field
The present invention relates to cosmetic fields, and in particular to a kind of elm bark extracting solution and its preparation method and application.
Background technology
As the improvement of people's living standards, more and more people seeking beauties pursue the effective skin-protection product of health, plant
Active constituent is because it is mild, and effect is good, and is favored by each cosmetics developer, and active components of plants includes essential oil, polyphenol, life
Alkaloids, lignans, saponin(e, polysaccharide etc. are widely present in the leaf of plant, wood, skin, pulp.Traditional active components of plants
Extraction process includes organic solvent extraction, hot water extraction method, system solvent extraction method etc., these do not need special instrument,
Using more universal, but have the shortcomings that time-consuming, recovery rate is low.Microwave extraction technology using substance, send out by the molecule in microwave field
The frequency that changes moves, and diffusion rate increases, and good effect, extraction process tool can be obtained using this method extraction active components of plants
There is the characteristics of high efficiency, and easy to operate, recovery rate is high, and plant fine powder is not agglomerated, is not gelatinized during extraction, is overcome
The deficiency that hot-water process easily agglomerates, is easily gelatinized, therefore using more and more extensive in the production of people, microwave combination organic solvent is total
With extraction so that more active constituents are extracted and are applied.
People often can effectively be gone out the grease on skin and scurf with the shower cream product overwhelming majority at present, make us feeling
Must be clearly comfortable, and part shower cream addition albumen, a small amount of active components of plants, dirt is removed to a certain extent, but
It is that the excessive additive of addition has also taken away normal sebum while removing dirt, dry skin can be made tight, or even hair
Itch, to cause different degrees of skin injury.
Invention content
Based on this, the purpose of the present invention is to provide a kind of elm bark extracting solutions, and are applied in shower cream, have
Antibacterial, whitening skin effect.
To achieve the above object, the present invention provides the following technical solution：
A kind of preparation method of elm bark extracting solution, includes the following steps：
(1) elm bark drying and crushing is crossed into 100~150 mesh sieve, be fitted into the gauze bag to sterilize；
(2) according to solid-liquid ratio 1:10~15 are added digestion agent, extracting through microwave heating, and filtering takes filtrate；
(3) filtrate decompression is distilled, you can.
And the digestion agent in the step (2) by acetone and water according to 1:3 ratio obtains；Microwave Extraction power is 300
~350W, Extracting temperature are 40~50 DEG C, and extraction time is 1~3h.
In addition, the answering in preparing the cosmetics with antibacterial and skin whitening by obtained elm bark extracting solution
With, and the additive amount in cosmetics is 20~60%.
The present invention provides a kind of shower cream, includes the component of following mass percent：Elm bark extracting solution 20~60%, the moon
It is laureth sodium sulfovinate 4~12%, Cocoamidopropyl betaine 1.2~3.6%, polyquaternium -70.1~1.2%, sweet
Oil 0.1~1%, isopropyl palmitate 1~3%, citric acid 0.01~0.03%, EDETATE SODIUM 0.01~0.02%, benzene oxygen second
Alcohol 0.01~0.03%, deionized water surplus.
Compared with prior art, the device have the advantages that it is as follows：The extraction side of the elm bark extracting solution of the present invention
Method is simple to operation, and takes few, recovery rate height；Extracting obtained elm bark extracting solution, there is significant antibacterial and whitening to make
With, property is mild, non-stimulated skin effect；Elm bark extracting solution is applied in preparing shower cream, in combined formulation it is each at
Point so that shower cream not only has good detergency, moreover it is possible to generate good bacteriostasis, reduce the itch of skin, and beautiful
White muscle skin, neck skin are more pale beautiful.
Specific implementation mode
With reference to embodiment, the invention will be further described.
Embodiment 1
A kind of shower cream is made of the ingredient of following mass percent：Elm bark extracting solution 20%, laureth sulfuric acid
Ester sodium 4%, Cocoamidopropyl betaine 1.2%, polyquaternium -70.1%, glycerine 0.1%, isopropyl palmitate 1%, lemon
Lemon acid 0.01%, EDETATE SODIUM 0.01%, Phenoxyethanol 0.01%, deionized water 73.57%.
It should be noted that：The preparation method of elm bark extracting solution is as follows：
(1) elm bark drying and crushing is sieved with 100 mesh sieve, is fitted into the gauze bag to sterilize；
(2) according to solid-liquid ratio 1:10 additional proportions are 1:3 acetone and aqueous mixtures is in power as digestion agent
300W, under conditions of 40 DEG C of temperature, extracting through microwave heating 1h, filtering takes filtrate；
(3) filtrate decompression is distilled, you can.
Embodiment 2
A kind of shower cream is made of the ingredient of following mass percent：Elm bark extracting solution 60%, laureth sulfuric acid
Ester sodium 12%, Cocoamidopropyl betaine 3.6%, polyquaternium -71.2%, glycerine 1%, isopropyl palmitate 3%, lemon
Acid 0.03%, EDETATE SODIUM 0.02%, Phenoxyethanol 0.03%, deionized water 19.12%.
It should be noted that：The preparation method of elm bark extracting solution is as follows：
(1) elm bark drying and crushing is crossed into 150 mesh sieve, be fitted into the gauze bag to sterilize；
(2) according to solid-liquid ratio 1:15 additional proportions are 1:3 acetone and aqueous mixtures is in power as digestion agent
350W, under conditions of temperature 50 C, extracting through microwave heating 3h, filtering takes filtrate；
(3) filtrate decompression is distilled, you can.
Embodiment 3
A kind of shower cream is made of the ingredient of following mass percent：Elm bark extracting solution 40%, laureth sulfuric acid
Ester sodium 8%, Cocoamidopropyl betaine 2.4%, polyquaternium -70.6%, glycerine 0.5%, isopropyl palmitate 2%, lemon
Lemon acid 0.02%, EDETATE SODIUM 0.015%, Phenoxyethanol 0.02%, deionized water 46.445%.
It should be noted that：The preparation method of elm bark extracting solution is as follows：
(1) elm bark drying and crushing is crossed into 125 mesh sieve, be fitted into the gauze bag to sterilize；
(2) according to solid-liquid ratio 1:12 additional proportions are 1:3 acetone and aqueous mixtures is in power as digestion agent
325W, under conditions of temperature 45 C, extracting through microwave heating 2h, filtering takes filtrate；
(3) filtrate decompression is distilled, you can.
Comparative example 1
A kind of shower cream is made of the ingredient of following mass percent：Elm bark extracting solution 40%, laureth sulfuric acid
Ester sodium 8%, Cocoamidopropyl betaine 2.4%, polyquaternium -70.6%, glycerine 0.5%, isopropyl palmitate 2%, lemon
Lemon acid 0.02%, EDETATE SODIUM 0.015%, Phenoxyethanol 0.02%, deionized water 46.445%.
It should be noted that：The preparation method of elm bark extracting solution is as follows：
(1) elm bark drying and crushing is crossed into 60 mesh sieve, be fitted into the gauze bag to sterilize；
(2) according to solid-liquid ratio 1:7 additional proportions are 1:5 acetone and aqueous mixtures is 500W in power as digestion agent,
Under conditions of temperature 60 C, extracting through microwave heating 5h, filtering takes filtrate；
(3) filtrate decompression is distilled, you can.
Comparative example 2
A kind of shower cream is made of the ingredient of following mass percent：Laureth sodium sulfovinate 8%, coconut oleoyl amine
Propyl betaine 2.4%, polyquaternium -70.6%, glycerine 0.5%, isopropyl palmitate 2%, citric acid 0.02%, EDTA bis-
Sodium 0.015%, Phenoxyethanol 0.02%, deionized water 86.445%.
Efficacy validation：
60 volunteers are selected, are randomly divided into 6 groups, every group of 10 people try out Examples 1 to 3, comparative example 1~2, city respectively
It sells and declares to have antibacterial, white-skinned face function shower cream.
Observation index：(1) pruitus degree, seizure frequency, duration；(2) change of secondary skin lesion；(3) whole body
Skin state.
Evaluation criteria：(1) effective：Itch all disappears, and secondary skin lesion disappears, and skin condition improvement is notable；(2) effectively：
Itch mitigates, and secondary skin lesion improves；(3) invalid：Skin is not any change or even skin lesion aggravates.
Result on trial shows that there is the elm bark extracting solution of the present invention good bacteriostatic skin-care effect, long-time service can make flesh
Skin is more healthy.
Finally it should be noted that：The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention,
Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used
With technical scheme described in the above embodiments is modified or equivalent replacement of some of the technical features.
All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in the present invention's
Within protection domain.
Claims (6)
1. a kind of preparation method of elm bark extracting solution, which is characterized in that include the following steps：
(1) elm bark drying and crushing is crossed into 100~150 mesh sieve, be fitted into the gauze bag to sterilize；
(2) according to solid-liquid ratio 1:10~15 are added digestion agent, extracting through microwave heating, and filtering takes filtrate；
(3) filtrate decompression is distilled, you can.
2. the preparation method of elm bark extracting solution according to claim 1, which is characterized in that the leaching in the step (2)
Agent is proposed by acetone and water according to 1:3 ratio obtains.
3. the preparation method of elm bark extracting solution according to claim 1, which is characterized in that micro- in the step (2)
It is 300~350W that wave, which extracts power, and Extracting temperature is 40~50 DEG C, and extraction time is 1~3h.
4. the elm bark extracting solution as obtained by claim 1 is in preparing the cosmetics with antibacterial and skin whitening
Using.
5. application according to claim 4, which is characterized in that the quality percentage of elm bark extracting solution in the cosmetics
It is 20~60% than dosage.
6. a kind of shower cream, which is characterized in that include the component of following mass percent：Elm bark extracting solution 20~60%, the moon
It is laureth sodium sulfovinate 4~12%, Cocoamidopropyl betaine 1.2~3.6%, polyquaternium -70.1~1.2%, sweet
Oil 0.1~1%, isopropyl palmitate 1~3%, citric acid 0.01~0.03%, EDETATE SODIUM 0.01~0.02%, benzene oxygen second
Alcohol 0.01~0.03%, deionized water surplus.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810358983.4A CN108451818A (en) | 2018-04-19 | 2018-04-19 | A kind of elm bark extracting solution and its preparation method and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810358983.4A CN108451818A (en) | 2018-04-19 | 2018-04-19 | A kind of elm bark extracting solution and its preparation method and application |
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| Publication Number | Publication Date |
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| CN108451818A true CN108451818A (en) | 2018-08-28 |
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| CN201810358983.4A Withdrawn CN108451818A (en) | 2018-04-19 | 2018-04-19 | A kind of elm bark extracting solution and its preparation method and application |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111544351A (en) * | 2020-05-15 | 2020-08-18 | 姜庚明 | A facial mask composition containing water extract of wood shavings, and its preparation method |
| WO2021227700A1 (en) * | 2020-05-15 | 2021-11-18 | 广州市科能化妆品科研有限公司 | Anti-dry and anti-sensitivity composition and preparation method therefor |
| CN117598954A (en) * | 2023-12-14 | 2024-02-27 | 中国中医科学院中医药健康产业研究所 | Elm wood shavings glue and preparation method and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106466264A (en) * | 2015-08-19 | 2017-03-01 | 哈尔滨灵草舒生物科技有限公司 | A kind of Pollen Typhae hemostasis bath gel and preparation method thereof |
-
2018
- 2018-04-19 CN CN201810358983.4A patent/CN108451818A/en not_active Withdrawn
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106466264A (en) * | 2015-08-19 | 2017-03-01 | 哈尔滨灵草舒生物科技有限公司 | A kind of Pollen Typhae hemostasis bath gel and preparation method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 左夏林，等: ""自由基清除剂在美容化妆品中的应用研究"", 《第十二届东南亚地区医学美容学术大会论文汇编》 * |
| 杨明非: ""榆树皮粗多糖组成及体外抗氧化作用"", 《东北林业大学学报》 * |
| 王东，等: ""榆树根皮的化学成分"", 《沈阳药科大学学报》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111544351A (en) * | 2020-05-15 | 2020-08-18 | 姜庚明 | A facial mask composition containing water extract of wood shavings, and its preparation method |
| WO2021227700A1 (en) * | 2020-05-15 | 2021-11-18 | 广州市科能化妆品科研有限公司 | Anti-dry and anti-sensitivity composition and preparation method therefor |
| CN117598954A (en) * | 2023-12-14 | 2024-02-27 | 中国中医科学院中医药健康产业研究所 | Elm wood shavings glue and preparation method and application thereof |
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Application publication date: 20180828 |
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