CN104013565B - A kind of hair protecting shampoo - Google Patents
A kind of hair protecting shampoo Download PDFInfo
- Publication number
- CN104013565B CN104013565B CN201410299143.7A CN201410299143A CN104013565B CN 104013565 B CN104013565 B CN 104013565B CN 201410299143 A CN201410299143 A CN 201410299143A CN 104013565 B CN104013565 B CN 104013565B
- Authority
- CN
- China
- Prior art keywords
- caulis spatholobi
- weight
- semen glycines
- concentrated solution
- obtains
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 210000004209 hair Anatomy 0.000 title claims abstract description 74
- 239000002453 shampoo Substances 0.000 title claims abstract description 42
- 210000000582 semen Anatomy 0.000 claims abstract description 83
- 150000002333 glycines Chemical class 0.000 claims abstract description 67
- 241000628997 Flos Species 0.000 claims abstract description 31
- 229930182490 saponin Natural products 0.000 claims abstract description 30
- 150000007949 saponins Chemical class 0.000 claims abstract description 30
- 239000001397 quillaja saponaria molina bark Substances 0.000 claims abstract description 29
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 27
- 239000002994 raw material Substances 0.000 claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 11
- 230000037308 hair color Effects 0.000 claims abstract description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 54
- 239000007788 liquid Substances 0.000 claims description 37
- 238000003756 stirring Methods 0.000 claims description 36
- 244000269722 Thea sinensis Species 0.000 claims description 31
- 235000013616 tea Nutrition 0.000 claims description 31
- 239000000706 filtrate Substances 0.000 claims description 22
- 239000000284 extract Substances 0.000 claims description 19
- 239000011552 falling film Substances 0.000 claims description 16
- 238000000605 extraction Methods 0.000 claims description 15
- RFVNOJDQRGSOEL-UHFFFAOYSA-N 2-hydroxyethyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCO RFVNOJDQRGSOEL-UHFFFAOYSA-N 0.000 claims description 13
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 12
- 239000006286 aqueous extract Substances 0.000 claims description 12
- 239000003921 oil Substances 0.000 claims description 11
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 10
- 238000003825 pressing Methods 0.000 claims description 10
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 9
- 238000001914 filtration Methods 0.000 claims description 9
- 239000003292 glue Substances 0.000 claims description 8
- 240000008067 Cucumis sativus Species 0.000 claims description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical class [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 7
- 241001116389 Aloe Species 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 241000283153 Cetacea Species 0.000 claims description 6
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 claims description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- 235000011399 aloe vera Nutrition 0.000 claims description 6
- 235000019270 ammonium chloride Nutrition 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 6
- 235000009569 green tea Nutrition 0.000 claims description 6
- MYWUZJCMWCOHBA-VIFPVBQESA-N methamphetamine Chemical compound CN[C@@H](C)CC1=CC=CC=C1 MYWUZJCMWCOHBA-VIFPVBQESA-N 0.000 claims description 6
- 239000002893 slag Substances 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- 230000001954 sterilising effect Effects 0.000 claims description 6
- 241000345998 Calamus manan Species 0.000 claims description 5
- VBIIFPGSPJYLRR-UHFFFAOYSA-M Stearyltrimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCCCC[N+](C)(C)C VBIIFPGSPJYLRR-UHFFFAOYSA-M 0.000 claims description 5
- 239000012528 membrane Substances 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 230000007935 neutral effect Effects 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 5
- 235000012950 rattan cane Nutrition 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 4
- 229940075507 glyceryl monostearate Drugs 0.000 claims description 4
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 claims description 4
- 239000000741 silica gel Substances 0.000 claims description 4
- 229910002027 silica gel Inorganic materials 0.000 claims description 4
- 235000009854 Cucurbita moschata Nutrition 0.000 claims description 3
- 241000287828 Gallus gallus Species 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 3
- 239000012141 concentrate Substances 0.000 claims description 3
- 238000004821 distillation Methods 0.000 claims description 3
- 235000000832 Ayote Nutrition 0.000 claims description 2
- 241000288570 Chionochloa conspicua Species 0.000 claims description 2
- 235000009804 Cucurbita pepo subsp pepo Nutrition 0.000 claims description 2
- 230000010355 oscillation Effects 0.000 claims description 2
- 235000015136 pumpkin Nutrition 0.000 claims description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 3
- 240000001980 Cucurbita pepo Species 0.000 claims 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- 239000010703 silicon Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 24
- 238000005406 washing Methods 0.000 abstract description 9
- 230000003110 anti-inflammatory effect Effects 0.000 abstract description 6
- 239000000126 substance Substances 0.000 abstract description 6
- 230000003115 biocidal effect Effects 0.000 abstract description 4
- 241001122767 Theaceae Species 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 82
- 235000017709 saponins Nutrition 0.000 description 26
- 239000000047 product Substances 0.000 description 10
- 210000003491 skin Anatomy 0.000 description 9
- 239000002537 cosmetic Substances 0.000 description 6
- 210000004761 scalp Anatomy 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 208000001840 Dandruff Diseases 0.000 description 5
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 4
- 230000009471 action Effects 0.000 description 4
- 230000001476 alcoholic effect Effects 0.000 description 4
- 230000006870 function Effects 0.000 description 4
- 230000000844 anti-bacterial effect Effects 0.000 description 3
- 230000003656 anti-hair-loss Effects 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 230000017531 blood circulation Effects 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 230000035764 nutrition Effects 0.000 description 3
- 238000004659 sterilization and disinfection Methods 0.000 description 3
- 239000011573 trace mineral Substances 0.000 description 3
- 235000013619 trace mineral Nutrition 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- 201000004384 Alopecia Diseases 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 240000004244 Cucurbita moschata Species 0.000 description 2
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 2
- DATAGRPVKZEWHA-YFKPBYRVSA-N N(5)-ethyl-L-glutamine Chemical compound CCNC(=O)CC[C@H]([NH3+])C([O-])=O DATAGRPVKZEWHA-YFKPBYRVSA-N 0.000 description 2
- 208000003251 Pruritus Diseases 0.000 description 2
- 231100000360 alopecia Toxicity 0.000 description 2
- 235000001014 amino acid Nutrition 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 230000001139 anti-pruritic effect Effects 0.000 description 2
- 239000003908 antipruritic agent Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- RYYVLZVUVIJVGH-UHFFFAOYSA-N caffeine Chemical compound CN1C(=O)N(C)C(=O)C2=C1N=CN2C RYYVLZVUVIJVGH-UHFFFAOYSA-N 0.000 description 2
- 210000004027 cell Anatomy 0.000 description 2
- 238000005660 chlorination reaction Methods 0.000 description 2
- 230000003750 conditioning effect Effects 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 239000000499 gel Substances 0.000 description 2
- 210000003780 hair follicle Anatomy 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000006210 lotion Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 210000004379 membrane Anatomy 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000003020 moisturizing effect Effects 0.000 description 2
- 230000000144 pharmacologic effect Effects 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 231100000614 poison Toxicity 0.000 description 2
- 150000008442 polyphenolic compounds Chemical class 0.000 description 2
- 235000013824 polyphenols Nutrition 0.000 description 2
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 2
- 235000017557 sodium bicarbonate Nutrition 0.000 description 2
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- 239000010677 tea tree oil Substances 0.000 description 2
- 229940111630 tea tree oil Drugs 0.000 description 2
- 239000003440 toxic substance Substances 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- 206010049865 Achromotrichia acquired Diseases 0.000 description 1
- 241000256846 Apis cerana Species 0.000 description 1
- 241000256844 Apis mellifera Species 0.000 description 1
- 244000105624 Arachis hypogaea Species 0.000 description 1
- 235000010777 Arachis hypogaea Nutrition 0.000 description 1
- 241001098038 Callerya cinerea Species 0.000 description 1
- 241000526900 Camellia oleifera Species 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 244000146462 Centella asiatica Species 0.000 description 1
- 235000004032 Centella asiatica Nutrition 0.000 description 1
- 235000009849 Cucumis sativus Nutrition 0.000 description 1
- 241001289529 Fallopia multiflora Species 0.000 description 1
- UIOFUWFRIANQPC-JKIFEVAISA-N Floxacillin Chemical compound N([C@@H]1C(N2[C@H](C(C)(C)S[C@@H]21)C(O)=O)=O)C(=O)C1=C(C)ON=C1C1=C(F)C=CC=C1Cl UIOFUWFRIANQPC-JKIFEVAISA-N 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 244000018716 Impatiens biflora Species 0.000 description 1
- 235000015912 Impatiens biflora Nutrition 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- LPHGQDQBBGAPDZ-UHFFFAOYSA-N Isocaffeine Natural products CN1C(=O)N(C)C(=O)C2=C1N(C)C=N2 LPHGQDQBBGAPDZ-UHFFFAOYSA-N 0.000 description 1
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 1
- 235000006679 Mentha X verticillata Nutrition 0.000 description 1
- 235000002899 Mentha suaveolens Nutrition 0.000 description 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 1
- 206010030113 Oedema Diseases 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- 241000233805 Phoenix Species 0.000 description 1
- 235000014676 Phragmites communis Nutrition 0.000 description 1
- 208000004880 Polyuria Diseases 0.000 description 1
- 240000001341 Reynoutria japonica Species 0.000 description 1
- 235000018167 Reynoutria japonica Nutrition 0.000 description 1
- LUSZGTFNYDARNI-UHFFFAOYSA-N Sesamol Natural products OC1=CC=C2OCOC2=C1 LUSZGTFNYDARNI-UHFFFAOYSA-N 0.000 description 1
- 244000000231 Sesamum indicum Species 0.000 description 1
- 235000003434 Sesamum indicum Nutrition 0.000 description 1
- 239000004902 Softening Agent Substances 0.000 description 1
- 206010043866 Tinea capitis Diseases 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 230000036592 analgesia Effects 0.000 description 1
- 230000003260 anti-sepsis Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 235000019568 aromas Nutrition 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004204 blood vessel Anatomy 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 230000003925 brain function Effects 0.000 description 1
- VJEONQKOZGKCAK-UHFFFAOYSA-N caffeine Natural products CN1C(=O)N(C)C(=O)C2=C1C=CN2C VJEONQKOZGKCAK-UHFFFAOYSA-N 0.000 description 1
- 229960001948 caffeine Drugs 0.000 description 1
- NKWPZUCBCARRDP-UHFFFAOYSA-L calcium bicarbonate Chemical compound [Ca+2].OC([O-])=O.OC([O-])=O NKWPZUCBCARRDP-UHFFFAOYSA-L 0.000 description 1
- 229910000020 calcium bicarbonate Inorganic materials 0.000 description 1
- 235000021466 carotenoid Nutrition 0.000 description 1
- 150000001747 carotenoids Chemical class 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000035619 diuresis Effects 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 239000002158 endotoxin Substances 0.000 description 1
- 239000010408 film Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 125000005456 glyceride group Chemical group 0.000 description 1
- YQEMORVAKMFKLG-UHFFFAOYSA-N glycerine monostearate Natural products CCCCCCCCCCCCCCCCCC(=O)OC(CO)CO YQEMORVAKMFKLG-UHFFFAOYSA-N 0.000 description 1
- SVUQHVRAGMNPLW-UHFFFAOYSA-N glycerol monostearate Natural products CCCCCCCCCCCCCCCCC(=O)OCC(O)CO SVUQHVRAGMNPLW-UHFFFAOYSA-N 0.000 description 1
- 229940094952 green tea extract Drugs 0.000 description 1
- 235000020688 green tea extract Nutrition 0.000 description 1
- 230000003648 hair appearance Effects 0.000 description 1
- 230000003779 hair growth Effects 0.000 description 1
- 230000003699 hair surface Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 230000001976 improved effect Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 230000000366 juvenile effect Effects 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 1
- 235000020778 linoleic acid Nutrition 0.000 description 1
- 229920006008 lipopolysaccharide Polymers 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 239000002075 main ingredient Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- -1 matter Substances 0.000 description 1
- 230000002175 menstrual effect Effects 0.000 description 1
- 230000005906 menstruation Effects 0.000 description 1
- 239000001699 mentha arvensis leaf oil Substances 0.000 description 1
- 239000010657 mentha arvensis oil Substances 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 229910000403 monosodium phosphate Inorganic materials 0.000 description 1
- 235000019799 monosodium phosphate Nutrition 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 230000000474 nursing effect Effects 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 230000003571 opsonizing effect Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 150000003904 phospholipids Chemical class 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000002040 relaxant effect Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 230000009759 skin aging Effects 0.000 description 1
- 210000004927 skin cell Anatomy 0.000 description 1
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 210000002435 tendon Anatomy 0.000 description 1
- 229940026510 theanine Drugs 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 210000001519 tissue Anatomy 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
A kind of hair protecting shampoo containing tea saponin disclosed by the invention, relate to the hair shampoo article technical field in daily-use chemical industry, it is to be prepared from by the raw material of following weight portion: Caulis Spatholobi extracting solution 14, Oleum Arachidis hypogaeae semen 0.5 1.5, conditioner 35, Herba Centellae extracting solution 14, freshener 35, water quality essence 13, hair color light agent 15 25, Sucus Cucurbitae moschatae 46, Semen Glycines juice 35, Flos Impatientis juice 13, surplus are pure water, adds up to 100 parts；There is antiinflammatory, biocidal efficacies, integrate hair-washing hair-care and the effect feature such as preferably, be suitable for the crowd at each age of men and women, old and young and use.
Description
Technical field
The present invention relates to the hair shampoo article technical field in daily-use chemical industry, particularly a kind of hair-washing hair-care
Liquid.
Background technology
Hair shampoo article numerous and complicated the most on the market, product has dividing of low-medium-high level, high-grade hair washing
Although articles for use effect is preferable, but it is expensive, and general population can not consume；Though middle level products price
Can be so that general population accepts, but its effect allows people become suspicious；Especially some low grade products use chemistry
The composition of synthesis, improper use can make the undue defat of scalp, causes root of hair pruritus, inflammation, makes hair quality
Impaired.
Tea saponin, as the natural surfactant material that natural product is that daily use chemicals industry is rare, utilizes tea
The surface-active action of Saponin, can be used to do shampoo, shampoo etc., has hair-washing hair-care dual
Effect, not only makes that hair is glossy, feel good, the specified elongation elasticity rate of hair and coefficient of friction etc.
Index, also superior to like product, has the pharmacology such as hair care skin-care effect, anti-inflammatory anti-itch and antidandruff efficacy
Effect, and, allergy effect non-stimulated to skin, use safety.Thus, in the last few years, occur
Some use tea saponins as the hair washing products of Main Ingredients and Appearance.Such as Chinese patent, (number of patent application is
201210297044.6) disclosed " a kind of shampoo Han tea saponin ", comprise tea saponin, tea tree oil,
Auxiliary agent and water, the purity of wherein said tea saponin is 90%～99.98%.The present invention containing tea saponin
Shampoo uses high-purity tea saponin and natural tea tree oil, greatly reduces albumen in common tea Saponin
The impact on the anti-dandruff effect that sterilizes of the impurity such as matter, resin, organic acid, pigment, strengthens shampoo simultaneously
Sterilize anti-dandruff effect, has reached All Pure Nature hair washing, nursing effect.
Summary of the invention
It is an object of the invention to provide one and there is antiinflammatory, biocidal efficacies, integrate hair-washing hair-care,
And the preferable hair shampoo article of effect.
For achieving the above object, the technical measures that the present invention is taked are a kind of hair protecting shampoos of invention,
It is to be prepared from by the raw material of following weight portion:
Its preparation process is as follows:
(1), pretreatment of raw material:
1., prepared by Sucus Cucurbitae moschatae: is cleaned by Fructus Cucurbitae moschatae, after removing Semen Cucurbitae, is cut into 0.1-0.25cm thick
Pumpkin slice, then, add 1-2 times of weight, the warm water of 50-65 DEG C, constant temperature soaks 7-12h, pressure
Filter, obtains Fructus Cucurbitae moschatae Aqueous extracts；By Fructus Cucurbitae moschatae Aqueous extracts vacuum be 0.55-0.7MPa, temperature be
Being concentrated into solid content in the falling film condenser of 40-50 DEG C is 0.085-0.175mg/ml, obtains Fructus Cucurbitae moschatae
Concentrated solution；Thereafter, at normal temperatures, in Fructus Cucurbitae moschatae concentrated solution, addition accounts for Fructus Cucurbitae moschatae concentrated solution weight
The glyceryl monostearate of 2.5-4.5% and the Mel accounting for Fructus Cucurbitae moschatae concentrated solution volume 2.0-5.0%, stirring
0.1-0.3h, transfers to stand in freezer 10-18h, filters, obtain Fructus Cucurbitae moschatae filtrate；Fructus Cucurbitae moschatae is filtered
Liquid, through the centrifuge of 3000-5000r/min, obtains Fructus Cucurbitae moschatae centrifugal liquid, then in Fructus Cucurbitae moschatae centrifugal liquid
Add the tea saponin accounting for Fructus Cucurbitae moschatae centrifugal liquid weight 0.6-1.2%, stir evenly, stand 3-5h, then, by upper
Layer Fructus Cucurbitae moschatae solution, through the centrifuge of 10000-15000r/min, obtains Sucus Cucurbitae moschatae, standby；
2., prepared by Semen Glycines juice: is cleaned by Semen Glycines, puts into 1.5-2.5 times of weight, the temperature of 40-50 DEG C
In water, it is dipped to fully expand；Adequately expanded Semen Glycines is processed through extruder, obtains Semen Glycines filter liquor
With Semen Glycines slag；Add equivalent weight in Semen Glycines slag, volumetric concentration is the ethanol of 45-55%, often
Soak 1.5-3.0h under temperature, filter, obtain Semen Glycines alcohol extract；By Semen Glycines alcohol extract and Semen Glycines filter liquor
Mixing, obtains Semen Glycines mixed liquor；At normal temperatures, in Semen Glycines mixed liquor, addition accounts for Semen Glycines mixed liquor weight
Amount 1.5-3% ethylene glycol monostearate, stir evenly, then by its vacuum be 0.55-0.7 MPa,
Temperature is to be concentrated into without alcohol in the falling film condenser of 40-50 DEG C, obtains Semen Glycines concentrated solution；Concentrate to Semen Glycines
Liquid adds the tea saponin accounting for Semen Glycines concentrated solution weight 0.2-0.5%, stirs evenly, add and account for Semen Glycines concentration
Liquid weight 10-15%, the neutral silica gel (model is ZC-001) of 100-200 mesh, along clockwise direction
Stirring 2-4h, is then transferred in freezer stand 4-8h, filters, obtain Semen Glycines filtrate；Again by Semen Glycines
Filtrate, through the centrifuge of 10000-15000r/min, obtains Semen Glycines juice, standby；
3., prepared by Caulis Spatholobi extracting solution: is cleaned by Caulis Spatholobi rattan, is cut into wide 0.5-1.0cm, length
The Caulis Spatholobi sheet of 2.0-4.0cm, then addition 2-4 times of weight, volumetric concentration are in Caulis Spatholobi sheet
The ethanol of 40-55%, boils extraction 0.6-0.9h, filters, obtain milletol extract；By Caulis Spatholobi
Alcohol extract vacuum be 0.55-0.7MPa, temperature be the falling film condenser of 40-50 DEG C in be concentrated into
Alcoholic degree is 25-32%, obtains Caulis Spatholobi concentrated solution；In Caulis Spatholobi concentrated solution, add that to account for Caulis Spatholobi dense again
The ethylene glycol monostearate of contracting liquid weight 5.5-9.5%, stirs 0.1-0.3h, adds and account for Sanguis Gallus domesticus
The acid activated carbon (model is Norit-GC) of rattan concentrated solution weight 12-16%, and at 40-50 DEG C
After stirring 0.5-0.8h, it is transferred in freezer, stands 15-20h, filter, obtain Caulis Spatholobi filtrate；
By Caulis Spatholobi filtrate pressure be 1.15-2.25Mpa, aperture be 25-35nm filter membrane device in mistake
Filter, collects Caulis Spatholobi pressing filtering liquid；Add in Caulis Spatholobi pressing filtering liquid and account for Caulis Spatholobi pressing filtering liquid weight
The tea saponin of 0.6-1%, stirs 0.1-0.3h, adds the ethyl acetate of equal volume, at room temperature
Lower stirring 0.2-0.5h, stands, is layered, filters, and obtains the alcohol liquid after Caulis Spatholobi extraction；Then will
Alcohol liquid after Caulis Spatholobi extraction vacuum be 0.55-0.7Mpa, temperature be that the falling liquid film of 40-50 DEG C is dense
Contracting device is concentrated into without alcohol, obtains Caulis Spatholobi extraction concentrated solution；Again Caulis Spatholobi is extracted concentrated solution to be transferred to
In freezer, stand 10-15h, filter, obtain Caulis Spatholobi extraction concentrated filtrate；Again Caulis Spatholobi is extracted
Take the concentrated filtrate centrifuge through 10000-15000r/min, obtain Caulis Spatholobi extracting solution, standby
With；
4., prepared by Herba Centellae extracting solution: cleaned by Herba Centellae, puts into 2-3 times of weight, pH value is
In the aqueous alkali of 7-9 (alkali used is sodium bicarbonate or calcium bicarbonate or sodium dihydrogen phosphate), boil
1.5-2.0h is extracted in boiling, filters, obtains Herba Centellae Aqueous extracts；Again by Herba Centellae Aqueous extracts in vacuum
It is the falling film condenser of 65-75 DEG C to be concentrated into solid content be for 0.55-0.7MPa, temperature
0.45-0.7mg/ml, filters, obtains Herba Centellae concentrated solution；In Herba Centellae concentrated solution, addition accounts for long-pending again
Avenge the ethylene glycol monostearate of grass concentrated solution weight 0.15-0.45% and account for Herba Centellae concentrated solution volume
The Mel of 2.0-5.0%, stirs 0.1-0.3h, and stands 10-15h at normal temperatures, then, then add
Enter to account for the 200-300 mesh neutral silica gel (model is GF-245) of Herba Centellae concentrated solution weight 10-15%,
And stir 0.5-0.7h in the counterclockwise direction, then, stand 3-6h at normal temperatures, filter, collect
Upper strata Herba Centellae solution；Again by upper strata Herba Centellae solution through 10000-15000r/min centrifuge from
The heart, obtains Herba Centellae extracting solution, standby；
5., prepared by Flos Impatientis juice: cleaned by Flos Impatientis (note: Flos Impatientis petal), with 3-5 times
Weight, volumetric concentration are that the ethanol of 50-60% puts in distillation container together, steam at 85-100 DEG C
Evaporate 8-12h, collect Flos Impatientis distillate；It is 0.55-0.7 by Flos Impatientis distillate in vacuum again
MPa, temperature are that to be concentrated into alcoholic degree in the falling film condenser of 40-50 DEG C be 30-40%, filter, obtain phoenix
Celestial flower concentrated solution；Add in Flos Impatientis concentrated solution again and account for Flos Impatientis concentrated solution weight 1.2-1.75%
Ethylene glycol monostearate, stirs 0.2-0.4h the most in the counterclockwise direction, stands 2-3h,
Then, through the centrifuge of 10000-15000r/min, obtain Flos Impatientis juice, standby；
(2), get the raw materials ready: take each raw material respectively by above-mentioned weight portion, standby；
(3), mixing: above-mentioned standby each raw material is put in agitator, is 80-100MHz in frequency
Lower oscillation treatment, to mix homogeneously, filters, obtains compound, standby；
(4), sterilizing: by standby compound through pasteurize, obtain the hair protecting shampoo of the present invention.
Described conditioner refers to octadecyl trimethyl ammonium chloride, three whale METH ammonium chloride, poly-season
One or more in ammonium salt-7, when for time two or more, the ratio of each component is etc. weight portion or
Other ratio.
Described freshener is one or more in Oleum menthae, Oleum Camelliae, Aloe glue, when for two kinds with
Time upper, weight portion or other ratio such as the ratio of each component is.
Described water quality essence is the one in oleum Citri sinensis, Fructus Citri Limoniae oil or two kinds, when for two kinds, respectively
The proportioning of component is for waiting weight portion or other ratio.
Described hair color light agent is cucumber extract, Semen Sesami Nigrum extracting solution, Radix Polygoni Multiflori extracting solution, green tea
One or more in extracting solution, when for time two or more, the ratio of each component is etc. weight portion or its
Its ratio.
Its technical scheme one optimized is to be prepared from by the raw material of following weight portion:
Its technical scheme two optimized is to be prepared from by the raw material of following weight portion:
Its technical scheme three optimized is to be prepared from by the raw material of following weight portion:
The hair protecting shampoo of the present invention, its primary raw material include conditioner, freshener, water quality essence,
Hair color light agent, Sucus Cucurbitae moschatae, Semen Glycines juice, Caulis Spatholobi extracting solution, Herba Centellae extracting solution, Oleum Arachidis hypogaeae semen,
Flos Impatientis juice and pure water, also include and be added on Flos Impatientis juice, Herba Centellae extracting solution, Sanguis Gallus domesticus
Ethylene glycol monostearate in rattan extracting solution, Semen Glycines juice, is added on Mel in Herba Centellae extracting solution,
It is added on the tea saponin in Caulis Spatholobi extracting solution, Semen Glycines juice, Sucus Cucurbitae moschatae, the list being added in Sucus Cucurbitae moschatae
Tristerin.
Ethylene glycol monostearate [molecular formula: CH3(CH2)16COOCH2CH2OH)] wash at liquid
Wash product uses and can produce obvious pearl effect, and the viscosity of product can be increased, also have moist
Skin, hair care hair care and antistatic property；It is meanwhile, good with other type of surfactant intermiscibility,
And its stable pearl effect and thickening conditioning functions can be embodied；And non-stimulated to skin, to hair without
Damage.It is mainly used in shampoo, body lotion, skin lotion and high-grade liquid detergent etc..
Tea saponin (Tea Saponin) is the natural nonionic surfactant of a kind of function admirable,
It has foaming, emulsifying, dispersion, a performance such as gentle, and has the aspects such as impervious, antiinflammatory, analgesia
Pharmacological action.Tea saponin wash my hair have send out loose, smooth, anti-dandruff, the advantage such as antipruritic, have clean
Effect of hair care.
Glyceryl monostearate (molecular formula: C42H84O8) live as emulsifying agent and surface in cosmetics
Property agent.
Conditioner includes octadecyl trimethyl ammonium chloride, three whale METH ammonium chloride, polyquaternary ammonium salt-7.
Wherein: octadecyl trimethyl ammonium chloride (molecular formula: C21H46ClN) it is a kind of softening agent, can make
Hair is bulk, soft, be commonly used for the raw material of hair conditioner.Three whale METH ammonium chloride (model:
VARISOFT TC 90) it is a kind of cationic surfactant, it is adaptable to manufacture hair conditioner, conditioning
Shampoo.Polyquaternary ammonium salt-7 (molecular formula: C11H21ClN2O) it is a kind of cation opsonizing agent, is used for
Shampoo, bath gel, shaving emulsion, sizing water, also act as hair ornamenting conditioner, shampoo,
The cosmetics such as hair conditioner, setting agent, skin moistening skin protectant, cold wave, shaving emulsion, bath foam, blue or green
There is sterilization, sterilization and antisepsis.
Freshener includes Oleum menthae, Oleum Camelliae, Aloe glue, wherein: Oleum menthae [Mentha arvensis
oil(Mint oil；Cornmint oil)] pungent to dissipate, cool with heat clearing away, clear light cool scattered, after using
Refrigerant sense can be produced.Rich in oleic acid, linoleic acid in Oleum Camelliae (Camellia oleifera Abel),
There is skin care, black hair effect, can ultraviolet light, and antibacterial, kill germ；Meanwhile, Oleum Camelliae both contained
There is tea saponin, also contain the active substance of the multiple beneficial such as tea polyphenols, shampoo can be made and hair conditioner makes
With, tinea capitis, alopecia, scurf (Dandruff) and antipruritic can be prevented.Aloe glue includes abundant dimension
Raw element, aminoacid, fatty acid, polysaccharose substance；There is natural antiinflammatory, antibiotic effect, also have
There are moisturizing, the function such as sun-proof, hair can be protected not encroached on by ultraviolet.
Water quality essence includes oleum Citri sinensis, Fructus Citri Limoniae oil, wherein: Fructus Citri sinensis (skin) oil has special Fructus Citri junoris gas
Taste and gentle fragrant flavour.Fructus Citri Limoniae oil has strong citris aromas, can refreshment.
Hair color light agent includes commercially available cucumber extract, Semen Sesami Nigrum extracting solution, Radix Polygoni Multiflori extracting solution, green
Tea extract, wherein: Fructus Cucumidis sativi (Cucumis sativus Linn) extracting solution has heat-clearing and toxic substances removing and makees
With, hair surface can be made to form smooth hygroscopic mem-brane, increase the water content of hair.Semen Sesami Nigrum (Sesamum
Indicum L.) extracting solution is contained within antioxidant, vitamin E, sesamol, Semen Sesami melanin
And trace element, it is mainly used in the cosmetics such as shampoo, hair care, skin protection, is a kind of preferably sky
So cosmetics additive.The Radix Polygoni Multiflori (Polygonum multiflorum Thunb.) extracting solution contains
The nutritions such as phospholipid, energy hairy root nourishing, make hair black pigment generate, hair can be made more black, also may be used
To become hair nutrition conditioner, it is used for taking care of hair, hair care or the cosmetics of hair growth promoting, hair can be made to be prone to
Combing, pitch-black light, there is good therapeutical effect for juvenile poliosis disease.Green tea (greentea)
Extracting solution contains the benefit materials such as tea polyphenols, caffeine, lipopolysaccharide, theanine, has moisturizing, resists
Scorching, sterilize, wash, take care of hair, the pharmacological action such as fat-reducing, have preferably hair washing, hair care effect.
Sucus Cucurbitae moschatae uses Fructus Cucurbitae moschatae to prepare, containing multiple to people in Fructus Cucurbitae moschatae (Cucurbita moschata)
The composition that body is useful, such as polysaccharide, aminoacid, activated protein carotenoid and various trace elements etc.,
The pectin especially included has good adsorptivity, the dirt that can bond and eliminate on hair and antibacterial
Toxin and other harmful substances.
Semen Glycines juice uses Semen Glycines to prepare, the Semen Glycines (Glycine max) ammonia containing multiple needed by human
The beneficiating ingredients such as base acid, play important Nutrition, both can improve human body and exempt from human tissue cell
Epidemic disease function, also can improve skin aging, has preferable maintenance action to hair.
Caulis Spatholobi extracting solution uses Caulis Spatholobi to prepare, and Caulis Spatholobi (Millettia dielsiana) has
Relaxing muscles and tendons to promote blood circulation, effect of nourishing blood for regulating menstruation, can unfold scalp meridians and blood vessel, increases scalp blood flow,
Play hair care hair care effect.
Herba Centellae extracting solution uses Herba Centellae to prepare, and Herba Centellae (Centellaasiatica) can heat clearing away
Removing toxic substances, inducing diuresis and reducing edema, also can refresh oneself by benefit brain, the replacement of scalp deep skin cell can be stimulated, play
Hair care hair care effect.
Flos Impatientis juice uses Flos Impatientis to prepare, and Flos Impatientis (Impatiens balsamina) has work
Blood blood stasis dispelling, deep effect of stimulating the menstrual flow, its pollen can be effectively improved the blood circulation of scalp and hair follicle to increase
Strong scalp and hair follicle activity.
Semen arachidis hypogaeae (Arachishypogaea) oil glyceride containing multiple fatty acid, has preferably hair
Lubrication；Possibly together with multiple aging ingredient, there is the effect delaying brain function old and feeble.
Mel (Apis cerana Fabr or Apis mellifera L.) is containing multiple human body not
The trace element that can or lack and vitamin, be natural cosmetic health product.
Pure water does not contains any harmful substance and antibacterial, can supplement moisture content to human body, tool effective and safe
There is the strongest dissolubility, therefore very strong with human body cell affinity, there is the effect enhanced metabolism.
Therefore, the hair protecting shampoo of the present invention, there is antiinflammatory, biocidal efficacies, meanwhile, containing multiple
The active ingredient useful to hair, can take care of hair, and clean result is preferable in hair care.
The hair protecting shampoo containing tea saponin of the present invention, once carried out Anti-hair loss and tested:
Subject 50, the age between 20-40 year, be randomly divided into test group (30 people) and
Matched group (20 people), test group personnel, use the hair protecting shampoo containing tea saponin of the present invention；
Matched group personnel, use commercially available shampoo (middle-grade product on the upper side) as reference.Hair washing in every 3 days
Once, 3 combing hairs of every natural gift morning, noon and afternoon, collect the hair come off and record radical, obtaining average
Its integer is taken after value.Test starts from early autumn, and the product that test is used, is as prepared by embodiment three
The hair protecting shampoo containing tea saponin.
After the test of 60 days, statistical data, its result sees below table 1.
Table 1 Anti-hair loss statistical effect
From the data in table 1 above, testing through Anti-hair loss, the hair protecting shampoo of the present invention has
Significantly improve the effect of alopecia.Thus, the hair protecting shampoo of the present invention possesses preferable hair care effect.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.Description below is to enumerate
Mode, but protection scope of the present invention is not limited thereto.
Embodiment one
The hair protecting shampoo containing tea saponin of the present embodiment, its preparation process is as follows:
(1), pretreatment of raw material:
1., prepared by Sucus Cucurbitae moschatae: is cleaned by Fructus Cucurbitae moschatae, after removing Semen Cucurbitae, is cut into the thick south of 0.15cm
Green tea produced in Anhui Province (length uniformity), then, add 2 times of weight, warm water of 60 DEG C, and constant temperature soaks 10h,
Filter pressing, obtains Fructus Cucurbitae moschatae Aqueous extracts；By Fructus Cucurbitae moschatae Aqueous extracts vacuum be 0.6MPa, temperature be 45 DEG C
Being concentrated into solid content in falling film condenser is 0.125mg/ml, obtains Fructus Cucurbitae moschatae concentrated solution；Thereafter,
At normal temperatures, in Fructus Cucurbitae moschatae concentrated solution, addition accounts for the glycerol monostearate of Fructus Cucurbitae moschatae concentrated solution weight 3.5%
Ester and the Mel accounting for Fructus Cucurbitae moschatae concentrated solution volume 4%, stir 0.2h, transfers to stand in freezer 15h,
Filter, obtain Fructus Cucurbitae moschatae filtrate；By Fructus Cucurbitae moschatae filtrate through the centrifuge of 4000r/min, obtain Fructus Cucurbitae moschatae and be centrifuged
Liquid, then adds the tea saponin accounting for Fructus Cucurbitae moschatae centrifugal liquid weight 0.9% in Fructus Cucurbitae moschatae centrifugal liquid, stirs evenly, quiet
Put 4h, then, by upper strata Fructus Cucurbitae moschatae solution through the centrifuge of 12000r/min, obtain Sucus Cucurbitae moschatae,
Standby；
2., prepared by Semen Glycines juice: cleaned by Semen Glycines, puts in 2 times of weight, the warm water of 45 DEG C, leaching
Steep to fully expanding；Adequately expanded Semen Glycines is processed through extruder, obtains Semen Glycines filter liquor and Semen Glycines slag；
Add equivalent weight in Semen Glycines slag, volumetric concentration is the ethanol of 50%, soaks 2h, mistake at normal temperatures
Filter, obtains Semen Glycines alcohol extract；Semen Glycines alcohol extract is mixed with Semen Glycines filter liquor, obtains Semen Glycines mixed liquor；?
Under room temperature, in Semen Glycines mixed liquor, add the ethylene glycol monostearate accounting for Semen Glycines mixed liquor weight 2.2%
Ester, stirs evenly, then by its vacuum be 0.6MPa, temperature be the falling film condenser of 45 DEG C in dense
It is reduced to without alcohol, obtains Semen Glycines concentrated solution；Add in Semen Glycines concentrated solution and account for Semen Glycines concentrated solution weight 0.35%
Tea saponin, stir evenly, add the neutral silica gel (type accounting for Semen Glycines concentrated solution weight 12%, 150 mesh
Number it is ZC-001), stir 3h along clockwise direction, be then transferred in freezer stand 6h, filter,
Obtain Semen Glycines filtrate；Again by Semen Glycines filtrate through the centrifuge of 12000r/min, obtain Semen Glycines juice,
Standby；
3., prepared by Caulis Spatholobi extracting solution: is cleaned by Caulis Spatholobi rattan, is cut into wide 0.8cm, long 3cm
Caulis Spatholobi sheet, then in Caulis Spatholobi sheet add 3 times of weight, volumetric concentrations be the ethanol of 50%,
Boil extraction 0.8h, filter, obtain milletol extract；It is 0.6 by milletol extract in vacuum
MPa, temperature are that to be concentrated into alcoholic degree in the falling film condenser of 45 DEG C be that 30% (that is: the volume of ethanol is dense
Degree is 30%), obtain Caulis Spatholobi concentrated solution；Add in Caulis Spatholobi concentrated solution again and account for Caulis Spatholobi concentrated solution
The ethylene glycol monostearate of weight 7.5%, stirs 0.2h, adds and account for Caulis Spatholobi concentrated solution weight
The acid activated carbon (model is Norit-GC) of 14%, and at 45 DEG C after stirring 0.6h, transfer
To freezer, stand 18h, filter, obtain Caulis Spatholobi filtrate；By Caulis Spatholobi filtrate pressure be 1.5Mpa,
Aperture be 30nm filter membrane device in filter, collect Caulis Spatholobi pressing filtering liquid；In Caulis Spatholobi pressing filtering liquid
Add the tea saponin accounting for Caulis Spatholobi pressing filtering liquid weight 0.8%, stir 0.2h, add equal volume
Ethyl acetate, stirs 0.4h at normal temperatures, stands, is layered, filters, after obtaining Caulis Spatholobi extraction
Alcohol liquid；Then the alcohol liquid after Caulis Spatholobi being extracted vacuum be 0.6Mpa, temperature be the fall of 45 DEG C
Membrane concentrator is concentrated into without alcohol, obtains Caulis Spatholobi extraction concentrated solution；Again Caulis Spatholobi is extracted concentrated solution to turn
Move in freezer, stand 12h, filter, obtain Caulis Spatholobi extraction concentrated filtrate；Again Caulis Spatholobi is extracted
Take the concentrated filtrate centrifuge through 12000r/min, obtain Caulis Spatholobi extracting solution, standby；
4., prepared by Herba Centellae extracting solution: cleaned by Herba Centellae, puts into 3 times of weight, pH value is 8
Sodium bicarbonate aqueous solution in, boil extraction 1.8h, filter, obtain Herba Centellae Aqueous extracts；Again will be long-pending
Snow grass Aqueous extracts vacuum be 0.6MPa, temperature be the falling film condenser of 70 DEG C in be concentrated into solid
Thing content is 0.55mg/ml, filters, obtains Herba Centellae concentrated solution；Add in Herba Centellae concentrated solution again
Account for the ethylene glycol monostearate of Herba Centellae concentrated solution weight 0.3% and account for Herba Centellae concentrated solution volume
The Mel of 4%, stirs 0.2h, and stands 12h at normal temperatures, then, adds that to account for Herba Centellae dense
The 250 mesh neutral silica gels (model is GF-245) of contracting liquid weight 12%, and stir in the counterclockwise direction
0.6h, then, stands 4h at normal temperatures, filters, and collects upper strata Herba Centellae solution；Again by upper strata
Herba Centellae solution, through the centrifuge of 12000r/min, obtains Herba Centellae extracting solution, standby；
5., prepared by Flos Impatientis juice: is cleaned by Flos Impatientis, is 55% with 4 times of weight, volumetric concentration
Ethanol together put into distillation container in, at 90 DEG C distill 10h, collect Flos Impatientis distillate；Again
By Flos Impatientis distillate vacuum be 0.6MPa, temperature be the falling film condenser of 45 DEG C in be concentrated into
Alcoholic degree is 35% (that is: the volumetric concentration of ethanol is 35%), filters, obtains Flos Impatientis concentrated solution；Again
The ethylene glycol monostearate accounting for Flos Impatientis concentrated solution weight 1.5% is added in Flos Impatientis concentrated solution,
Stir 0.3h the most in the counterclockwise direction, stand 2h, then, being centrifuged through 12000r/min
Machine is centrifuged, and obtains Flos Impatientis juice, standby；
(2), get the raw materials ready: take conditioner 3 parts the most respectively (wherein: octadecyl trimethyl chlorination
Ammonium, three whale METH ammonium chloride and each 1 part of polyquaternary ammonium salt-7), freshener 3 parts (wherein: Herba Menthae
Oil, Oleum Camelliae and each 1 part of Aloe glue), 1 part of water quality essence (wherein: oleum Citri sinensis and Fructus Citri Limoniae oil each 0.5
Part), hair color light agent 15 parts (wherein: cucumber extract, Semen Sesami Nigrum extracting solution fleece-flower root extracting solution
Each 5 parts), Oleum Arachidis hypogaeae semen 1.5 parts, Caulis Spatholobi extracting solution 1 part, Herba Centellae extracting solution 4 parts, Impatientis
Flower juice 1 part, Sucus Cucurbitae moschatae 4 parts, Semen Glycines juice 3 parts, pure water 63.5 parts, standby；
(3), mixing: above-mentioned standby each raw material is put in agitator, shakes under frequency is 90MHz
Swing and process to mix homogeneously, become compound, standby；
(4), sterilizing: (sterilization temperature is 62-65 DEG C, protects through pasteurize by standby compound
Hold 30min), it is the hair protecting shampoo of the present invention.
The hair protecting shampoo of the present invention, its using method is identical with commercially available shampoo.
Embodiment two
The hair protecting shampoo containing tea saponin of the present embodiment, its preparation process is as follows:
(1), pretreatment of raw material: identical with embodiment one；
(2), get the raw materials ready: take conditioner 5 parts the most respectively (wherein: octadecyl trimethyl chlorination
Ammonium 3 parts, three whale METH ammonium chloride 2 parts), freshener 5 parts (wherein: Oleum menthae 2 parts, reed
3 parts of luxuriant growth glue), 3 parts of water quality essence (wherein: oleum Citri sinensis and each 1.5 parts of Fructus Citri Limoniae oil), hair color light
Agent 25 parts (wherein: cucumber extract 12 parts, Radix Polygoni Multiflori extracting solution 13 parts), Caulis Spatholobi extracting solution 4
Part, Herba Centellae extracting solution 1 part, Flos Impatientis juice 3 parts, Oleum Arachidis hypogaeae semen 0.5 part, Sucus Cucurbitae moschatae 6 parts,
Semen Glycines juice 5 parts, pure water 42.5 parts, standby；
Other step is identical with embodiment one.
Embodiment three
The hair protecting shampoo containing tea saponin of the present embodiment, its preparation process is as follows:
(1), pretreatment of raw material: identical with embodiment one；
(2), get the raw materials ready: take 4 parts of (octadecyl trimethyl ammonium chloride 4 of conditioner the most respectively
Part), glyceryl monostearate 1 part, freshener 4 parts (wherein: Oleum Camelliae and each 2 parts of Aloe glue),
2 parts of water quality essence (wherein: oleum Citri sinensis and each 1 part of Fructus Citri Limoniae oil), hair color light agent 20 parts (wherein:
Each 5 parts of cucumber extract, Semen Sesami Nigrum extracting solution, Radix Polygoni Multiflori extracting solution, green tea extractive liquor), Caulis Spatholobi
Extracting solution 3 parts, Herba Centellae extracting solution 3 parts, Flos Impatientis juice 2 parts, Oleum Arachidis hypogaeae semen 1 part, Sucus Cucurbitae moschatae
5 parts, Semen Glycines juice 4 parts, pure water 48 parts, standby；
Other step is identical with embodiment one.
The hair protecting shampoo of the present invention, is suitable for the crowd at each age of men and women, old and young and uses.
Claims (6)
1. a hair protecting shampoo, it is characterised in that be to be prepared from by the raw material of following weight portion:
Described hair color light agent is cucumber extract, Semen Sesami Nigrum extracting solution, Radix Polygoni Multiflori extracting solution, green tea
The mixed liquor of extracting solution, weight portion or other ratio such as the ratio of each component is；
Its preparation process is as follows:
(1), pretreatment of raw material:
1., prepared by Sucus Cucurbitae moschatae: is cleaned by Fructus Cucurbitae moschatae, after removing Semen Cucurbitae, is cut into 0.1-0.25cm thick
Pumpkin slice, then, add 1-2 times of weight, the warm water of 50-65 DEG C, constant temperature soaks 7-12h, pressure
Filter, obtains Fructus Cucurbitae moschatae Aqueous extracts；By Fructus Cucurbitae moschatae Aqueous extracts vacuum be 0.55-0.7MPa, temperature be
Being concentrated into solid content in the falling film condenser of 40-50 DEG C is 0.085-0.175mg/ml, obtains Fructus Cucurbitae moschatae
Concentrated solution；Thereafter, at normal temperatures, in Fructus Cucurbitae moschatae concentrated solution, addition accounts for Fructus Cucurbitae moschatae concentrated solution weight
The glyceryl monostearate of 2.5-4.5% and the Mel accounting for Fructus Cucurbitae moschatae concentrated solution volume 2.0-5.0%, stirring
0.1-0.3h, transfers to stand in freezer 10-18h, filters, obtain Fructus Cucurbitae moschatae filtrate；Fructus Cucurbitae moschatae is filtered
Liquid, through the centrifuge of 3000-5000r/min, obtains Fructus Cucurbitae moschatae centrifugal liquid, then in Fructus Cucurbitae moschatae centrifugal liquid
Add the tea saponin accounting for Fructus Cucurbitae moschatae centrifugal liquid weight 0.6-1.2%, stir evenly, stand 3-5h, then, by upper
Layer Fructus Cucurbitae moschatae solution, through the centrifuge of 10000-15000r/min, obtains Sucus Cucurbitae moschatae, standby；
2., prepared by Semen Glycines juice: is cleaned by Semen Glycines, puts into 1.5-2.5 times of weight, the temperature of 40-50 DEG C
In water, it is dipped to fully expand；Adequately expanded Semen Glycines is processed through extruder, obtains Semen Glycines filter liquor
With Semen Glycines slag；Add equivalent weight in Semen Glycines slag, volumetric concentration is the ethanol of 45-55%, often
Soak 1.5-3.0h under temperature, filter, obtain Semen Glycines alcohol extract；By Semen Glycines alcohol extract and Semen Glycines filter liquor
Mixing, obtains Semen Glycines mixed liquor；At normal temperatures, in Semen Glycines mixed liquor, addition accounts for Semen Glycines mixed liquor weight
Amount 1.5-3% ethylene glycol monostearate, stir evenly, then by its vacuum be 0.55-0.7MPa,
Temperature is to be concentrated into without alcohol in the falling film condenser of 40-50 DEG C, obtains Semen Glycines concentrated solution；Concentrate to Semen Glycines
Liquid adds the tea saponin accounting for Semen Glycines concentrated solution weight 0.2-0.5%, stirs evenly, add and account for Semen Glycines concentration
Liquid weight 10-15%, the neutral silica gel of 100-200 mesh, stir 2-4h, then along clockwise direction
It is transferred in freezer stand 4-8h, filters, obtain Semen Glycines filtrate；Again by Semen Glycines filtrate warp
The centrifuge of 10000-15000r/min, obtains Semen Glycines juice, standby；
3., prepared by Caulis Spatholobi extracting solution: is cleaned by Caulis Spatholobi rattan, is cut into wide 0.5-1.0cm, length
The Caulis Spatholobi sheet of 2.0-4.0cm, then addition 2-4 times of weight, volumetric concentration are in Caulis Spatholobi sheet
The ethanol of 40-55%, boils extraction 0.6-0.9h, filters, obtain milletol extract；By Caulis Spatholobi
Alcohol extract vacuum be 0.55-0.7MPa, temperature be the falling film condenser of 40-50 DEG C in be concentrated into
The volumetric concentration of ethanol is 25-32%, obtains Caulis Spatholobi concentrated solution；Add in Caulis Spatholobi concentrated solution again
Account for the ethylene glycol monostearate of Caulis Spatholobi concentrated solution weight 5.5-9.5%, stir 0.1-0.3h, then
Add the acid activated carbon accounting for Caulis Spatholobi concentrated solution weight 12-16%, and stir at 40-50 DEG C
After 0.5-0.8h, it is transferred in freezer, stands 15-20h, filter, obtain Caulis Spatholobi filtrate；By chicken
Caulis seu Radix Schisandrae Henryi filtrate pressure be 1.15-2.25Mpa, aperture be 25-35nm filter membrane device in filter,
Collect Caulis Spatholobi pressing filtering liquid；Add in Caulis Spatholobi pressing filtering liquid and account for Caulis Spatholobi pressing filtering liquid weight 0.6-1%
Tea saponin, stir 0.1-0.3h, add the ethyl acetate of equal volume, stir at normal temperatures
0.2-0.5h, stands, is layered, filters, and obtains the alcohol liquid after Caulis Spatholobi extraction；Then Caulis Spatholobi is extracted
Alcohol liquid after taking vacuum be 0.55-0.7Mpa, temperature be the falling film condenser of 40-50 DEG C in dense
It is reduced to without alcohol, obtains Caulis Spatholobi extraction concentrated solution；Caulis Spatholobi extracts concentrated solution again be transferred in freezer,
Stand 10-15h, filter, obtain Caulis Spatholobi extraction concentrated filtrate；Again Caulis Spatholobi is extracted concentrated
Filtrate, through the centrifuge of 10000-15000r/min, obtains Caulis Spatholobi extracting solution, standby；
4., prepared by Herba Centellae extracting solution: cleaned by Herba Centellae, puts into 2-3 times of weight, pH value is
In the aqueous alkali of 7-9, boil extraction 1.5-2.0h, filter, obtain Herba Centellae Aqueous extracts；Again will be long-pending
Snow grass Aqueous extracts vacuum be 0.55-0.7MPa, temperature be the falling film condenser of 65-75 DEG C in dense
Being reduced to solid content is 0.45-0.7mg/ml, filters, obtains Herba Centellae concentrated solution；Again to Herba Centellae
Concentrated solution adds and accounts for the ethylene glycol monostearate of Herba Centellae concentrated solution weight 0.15-0.45% and account for
The Mel of Herba Centellae concentrated solution volume 2.0-5.0%, stirs 0.1-0.3h, and stands at normal temperatures
10-15h, then, adds the 200-300 mesh neutrality silicon accounting for Herba Centellae concentrated solution weight 10-15%
Glue, and stir 0.5-0.7h in the counterclockwise direction, then, stand 3-6h at normal temperatures, filter,
Collect upper strata Herba Centellae solution；Again by upper strata Herba Centellae solution being centrifuged through 10000-15000r/min
Machine is centrifuged, and obtains Herba Centellae extracting solution, standby；
5., prepared by Flos Impatientis juice: is cleaned by Flos Impatientis, with 3-5 times of weight, volumetric concentration is
The ethanol of 50-60% puts in distillation container together, distills 8-12h, collect Impatientis at 85-100 DEG C
Flower distillate；Again by Flos Impatientis distillate vacuum be 0.55-0.7MPa, temperature be 40-50 DEG C
Falling film condenser in be concentrated into the volumetric concentration of ethanol be 30-40%, filter, obtain Flos Impatientis and concentrate
Liquid；The ethylene glycol list accounting for Flos Impatientis concentrated solution weight 1.2-1.75% is added again in Flos Impatientis concentrated solution
Stearate, stirs 0.2-0.4h the most in the counterclockwise direction, stands 2-3h, then, warp
The centrifuge of 10000-15000r/min, obtains Flos Impatientis juice, standby；
(2), get the raw materials ready: take each raw material respectively by above-mentioned weight portion, standby；
(3), mixing: above-mentioned standby each raw material is put in agitator, is 80-100MHz in frequency
Lower oscillation treatment, to mix homogeneously, filters, obtains compound, standby；
(4), sterilizing: by standby compound through pasteurize, obtain hair protecting shampoo.
Hair protecting shampoo the most according to claim 1, it is characterised in that: described conditioner
Refer to the one in octadecyl trimethyl ammonium chloride, three whale METH ammonium chloride, polyquaternary ammonium salt-7
Or multiple, when for time two or more, weight portion or other ratio such as the ratio of each component is.
Hair protecting shampoo the most according to claim 1 and 2, it is characterised in that: described is clear
Cool dose is one or more in Oleum menthae, Oleum Camelliae, Aloe glue, when for time two or more, and each component
Proportioning for waiting weight portion or other ratio.
Hair protecting shampoo the most according to claim 3, it is characterised in that: described water quality is fragrant
Essence is the one in oleum Citri sinensis, Fructus Citri Limoniae oil or two kinds, when for two kinds, the weight such as the ratio of each component is
Amount part or other ratio.
Hair protecting shampoo the most according to claim 4, it is characterised in that be by following weight portion
Raw material be prepared from:
Hair protecting shampoo the most according to claim 4, it is characterised in that be by following weight portion
Raw material be prepared from:
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410299143.7A CN104013565B (en) | 2014-06-28 | 2014-06-28 | A kind of hair protecting shampoo |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410299143.7A CN104013565B (en) | 2014-06-28 | 2014-06-28 | A kind of hair protecting shampoo |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104013565A CN104013565A (en) | 2014-09-03 |
| CN104013565B true CN104013565B (en) | 2016-09-14 |
Family
ID=51430757
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410299143.7A Expired - Fee Related CN104013565B (en) | 2014-06-28 | 2014-06-28 | A kind of hair protecting shampoo |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104013565B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104274376B (en) * | 2014-10-27 | 2016-11-23 | 南通市巨力弹簧吊架有限公司 | A kind of green pollution-removing disinfecting handwashing liquid and preparation method thereof |
| CN105012206A (en) * | 2015-09-03 | 2015-11-04 | 哈尔滨泉兴科技有限公司 | Green tea shampoo formula |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102007036499A1 (en) * | 2007-08-01 | 2009-02-05 | Henkel Ag & Co. Kgaa | Natural cosmetic hair treatment agent |
| CN103371956A (en) * | 2012-04-18 | 2013-10-30 | 赵艳姝 | Novel honey moistening liquid shampoo |
| CN102836097B (en) * | 2012-08-21 | 2014-09-03 | 伊国群 | Liquid shampoo containing tea saponin |
| CN103816093B (en) * | 2014-03-20 | 2015-12-30 | 宁波亿拍客网络科技有限公司 | -kind of Oleum Camelliae Fructus Cucurbitae moschatae cold cream and processing method |
-
2014
- 2014-06-28 CN CN201410299143.7A patent/CN104013565B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN104013565A (en) | 2014-09-03 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102860976B (en) | Nourishing hair-care liquid shampoo and preparation method thereof | |
| CN102614102B (en) | Dandruff-removing medicinal composition and preparation method thereof | |
| CN105078850A (en) | Liquid shampoo and preparation method thereof | |
| CN104490678B (en) | A kind of rosemary hydrosol toner and preparation method thereof | |
| CN108245455A (en) | Loss preventing plant sends out agent and its purposes in daily chemical product | |
| CN104606106A (en) | Natural plant nano-emulsion bath lotion | |
| CN107496317B (en) | Repairing and nursing shampoo containing periplaneta americana active ingredient | |
| CN105125472B (en) | A kind of nourishing black hair hair cream containing natural extract and preparation method thereof | |
| CN102846503A (en) | Refreshing, anti-dandruff, nourishing and healthful shampoo and preparation method thereof | |
| CN104161718A (en) | Loofah skin moisturizer and preparation method thereof | |
| CN103263373A (en) | Crocus sativus bath cream and preparation method thereof | |
| CN104434698B (en) | A kind of antistatic, radiation proof hair cream and preparation method thereof | |
| CN105853300A (en) | Degreasing, dandruff removing, itching relieving and moistening cream shampoo and preparation method thereof | |
| CN102258453A (en) | Natural hair and skin beautifying nursing agent and using method thereof | |
| CN104825361A (en) | Natural shampoo containing camellia saponin | |
| CN108464961B (en) | Natural plant shampoo and preparation method thereof | |
| CN104013565B (en) | A kind of hair protecting shampoo | |
| CN103462855B (en) | Cosmetic containing American ginseng and longan and preparation method thereof | |
| CN109700732A (en) | Botanical hair shampoo and preparation method thereof | |
| CN110613663A (en) | Skin repairing composition, skin care product and preparation method thereof | |
| CN105560151A (en) | Salt for hair care, and preparation method thereof | |
| CN105168041A (en) | Anti-dandruff antipruritic shampoo and preparation method thereof | |
| CN101987078A (en) | Lucid ganoderma-mint shampoo and preparation method thereof | |
| CN113583768A (en) | Dandruff-removing, itching-relieving, smooth, bright and anti-alopecia shampoo soap and preparation method thereof | |
| CN113278477A (en) | Whitening, moisturizing, moistening and bacteriostatic bath soap and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160914 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |