CN104013565A - Hair-washing and protecting liquid - Google Patents
Hair-washing and protecting liquid Download PDFInfo
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- CN104013565A CN104013565A CN201410299143.7A CN201410299143A CN104013565A CN 104013565 A CN104013565 A CN 104013565A CN 201410299143 A CN201410299143 A CN 201410299143A CN 104013565 A CN104013565 A CN 104013565A
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Abstract
The invention discloses a hair-washing and protecting liquid containing tea saponin and relates to the technical field of hair-washing articles in chemicals for daily use. The hair-washing and protecting liquid is prepared from the following raw materials in parts by weight: 1-4 parts of caulis spatholobi extracting liquid, 0.5-1.5 parts of peanut oil, 3-5 parts of conditioner, 1-4 parts of centella extracting liquid, 3-5 parts of freshener, 1-3 parts of pseudo-aqueous flavor, 15-25 parts of black hair brightener, 4-6 parts of pumpkin juice, 3-5 parts of soybean juice, 1-3 parts of impatiens balsamina juice and the balance of pure water. The hair-washing and protecting liquid has the characteristics of diminishing inflammation and sterilizing, integrating hair-washing and protection and has a good effect and the like, so that the hair-washing and protecting liquid is suitable for people of all ages.
Description
Technical field
The present invention relates to the hair shampoo article technical field in daily-use chemical industry, particularly a kind of hair protecting shampoo.
Background technology
Current hair shampoo article numerous and complicated on the market, product has dividing of low-medium-high level, although high-grade hair shampoo article effect is better, it is expensive, general population can not consume; Although middle-grade product price can be general population and accepts, its effect allows people become suspicious; Especially some low grade products adopt the composition of chemosynthesis, and improper use meeting makes the undue defat of scalp, cause root of hair pruritus, inflammation, make hair quality impaired.
Tea saponin is the natural surfactant material that daily use chemicals industry is rare as natural product, utilize the surface-active action of tea saponin, can be used to do shampoo, shampoo etc., there is hair-washing hair-care double effects, not only make that hair is glossy, feel is good, the index such as specified elongation elasticity rate and coefficient of friction of hair is also better than like product, has the pharmacological effects such as hair care skin-care effect, anti-inflammatory anti-itch and anti-dandruff effect, and non-stimulated to skin, irritated effect, use safety.Thereby, in the last few years, occurred that some adopted the hair washing product of tea saponin as Main Ingredients and Appearance.As disclosed in Chinese patent (number of patent application is 201210297044.6) " a kind of containing tea saponin shampoo ", comprises tea saponin, tea tree oil, auxiliary agent and water, and the purity of wherein said tea saponin is 90%～99.98%.Of the present invention containing tea saponin shampoo use high-purity tea saponin and natural tea tree oil, greatly reduce the impact of impurity on the anti-dandruff effect that sterilizes such as protein, resin, organic acid, pigment in common tea Saponin, strengthen the shampoo anti-dandruff effect that sterilizes simultaneously, reached All Pure Nature hair washing, nursing effect.
Summary of the invention
The object of the present invention is to provide one to there is antiinflammatory, biocidal efficacies, integrate the good hair shampoo article of hair-washing hair-care and effect.
For achieving the above object, the technical measures that the present invention takes are a kind of hair protecting shampoos of invention, are to be prepared from by the raw material of following weight portion:
Its preparation process is as follows:
(1), pretreatment of raw material:
1., Sucus Cucurbitae moschatae preparation: Fructus Cucurbitae moschatae is cleaned, removed after Semen Cucurbitae, be cut into the Fructus Cucurbitae moschatae sheet that 0.1-0.25cm is thick, then, add the warm water of 1-2 times of weight, 50-65 DEG C, constant temperature soaks 7-12h, and filter pressing, obtains Fructus Cucurbitae moschatae water extraction liquid; Be that 0.55-0.7MPa, temperature are that in the falling film condenser of 40-50 DEG C, to be concentrated into solid content be 0.085-0.175mg/ml by Fructus Cucurbitae moschatae water extraction liquid in vacuum, obtain Fructus Cucurbitae moschatae concentrated solution; ,, at normal temperatures, in Fructus Cucurbitae moschatae concentrated solution, add the glyceryl monostearate that accounts for Fructus Cucurbitae moschatae concentrated solution weight 2.5-4.5% and the Mel that accounts for Fructus Cucurbitae moschatae concentrated solution volume 2.0-5.0% thereafter, stir 0.1-0.3h, transfer in freezer and leave standstill 10-18h, filter, obtain Fructus Cucurbitae moschatae filtrate; Fructus Cucurbitae moschatae filtrate is centrifugal through the centrifuge of 3000-5000r/min, obtain Fructus Cucurbitae moschatae centrifugal liquid, then in Fructus Cucurbitae moschatae centrifugal liquid, add the tea saponin that accounts for Fructus Cucurbitae moschatae centrifugal liquid weight 0.6-1.2%, stir evenly, leave standstill 3-5h, then, by centrifugal through the centrifuge of 10000-15000r/min upper strata Fructus Cucurbitae moschatae solution, obtain Sucus Cucurbitae moschatae, for subsequent use;
2., Semen Glycines juice preparation: Semen Glycines is cleaned, dropped in the warm water of 1.5-2.5 times of weight, 40-50 DEG C, be dipped to abundant expansion; Adequately expanded Semen Glycines, through extruder processing, is obtained to Semen Glycines filter liquor and Semen Glycines slag; In Semen Glycines slag, add the ethanol that equivalent weight, volumetric concentration are 45-55%, soak at normal temperatures 1.5-3.0h, filter, obtain Semen Glycines alcohol extract; Semen Glycines alcohol extract is mixed with Semen Glycines filter liquor, obtain Semen Glycines mixed liquor; At normal temperatures, in Semen Glycines mixed liquor, adding the ethylene glycol monostearate that accounts for Semen Glycines mixed liquor weight 1.5-3%, stir evenly, is then that 0.55-0.7MPa, temperature are to be concentrated into without alcohol in the falling film condenser of 40-50 DEG C by it in vacuum, obtains Semen Glycines concentrated solution; In Semen Glycines concentrated solution, add the tea saponin that accounts for Semen Glycines concentrated solution weight 0.2-0.5%, stir evenly, add again and account for Semen Glycines concentrated solution weight 10-15%, 100-200 object neutral silica gel (model is ZC-001), stir along clockwise direction 2-4h, then be transferred to standing 4-8h in freezer, filter, obtain Semen Glycines filtrate; Again that Semen Glycines filtrate is centrifugal through the centrifuge of 10000-15000r/min, obtain Semen Glycines juice, for subsequent use;
3., Caulis Spatholobi extracting solution preparation: Caulis Spatholobi rattan is cleaned, be cut into the Caulis Spatholobi sheet of wide 0.5-1.0cm, long 2.0-4.0cm, then add the ethanol that 2-4 times of weight, volumetric concentration are 40-55% in Caulis Spatholobi sheet, boil and extract 0.6-0.9h, filter, obtain milletol extract; Be that 0.55-0.7MPa, temperature are that in the falling film condenser of 40-50 DEG C, to be concentrated into alcoholic degree be 25-32% by milletol extract in vacuum, obtain Caulis Spatholobi concentrated solution; In Caulis Spatholobi concentrated solution, add the ethylene glycol monostearate that accounts for Caulis Spatholobi concentrated solution weight 5.5-9.5% again, stir 0.1-0.3h, add again the acid active carbon (model is Norit-GC) that accounts for Caulis Spatholobi concentrated solution weight 12-16%, and stir after 0.5-0.8h at 40-50 DEG C, be transferred in freezer, leave standstill 15-20h, filter, obtain Caulis Spatholobi filtrate; Be to filter in the filter membrane device that is 25-35nm of 1.15-2.25Mpa, aperture Caulis Spatholobi filtrate at pressure, collect Caulis Spatholobi pressing filtering liquid; In Caulis Spatholobi pressing filtering liquid, add the tea saponin that accounts for Caulis Spatholobi pressing filtering liquid weight 0.6-1%, stir 0.1-0.3h, then add the ethyl acetate of equal volume, stir at normal temperatures 0.2-0.5h, leave standstill, layering, filtration, obtain the alcohol liquid after Caulis Spatholobi extraction; Then be that 0.55-0.7Mpa, temperature are to be concentrated into without alcohol in the falling film condenser of 40-50 DEG C by the alcohol liquid after Caulis Spatholobi extraction in vacuum, obtain Caulis Spatholobi extraction concentrated solution; Again Caulis Spatholobi is extracted to concentrated solution and be transferred in freezer, leave standstill 10-15h, filter, obtain Caulis Spatholobi extraction concentrated filtrate; Again Caulis Spatholobi is extracted to concentrated filtrate centrifugal through the centrifuge of 10000-15000r/min, obtain Caulis Spatholobi extracting solution, for subsequent use;
4., Herba Centellae extracting solution preparation: Herba Centellae is cleaned, drop into (alkali used is sodium bicarbonate or calcium bicarbonate or sodium dihydrogen phosphate) in the aqueous alkali that 2-3 times of weight, pH value are 7-9, boil and extract 1.5-2.0h, filter, obtain Herba Centellae water extraction liquid; Be that 0.55-0.7MPa, temperature are that in the falling film condenser of 65-75 DEG C, to be concentrated into solid content be 0.45-0.7mg/ml by Herba Centellae water extraction liquid in vacuum again, filter, obtain Herba Centellae concentrated solution; In Herba Centellae concentrated solution, add the ethylene glycol monostearate that accounts for Herba Centellae concentrated solution weight 0.15-0.45% and the Mel that accounts for Herba Centellae concentrated solution volume 2.0-5.0% again, stir 0.1-0.3h, and at normal temperatures leave standstill 10-15h, then, then add the 200-300 order neutral silica gel (model is GF-245) that accounts for Herba Centellae concentrated solution weight 10-15%, and stir in the counterclockwise direction 0.5-0.7h, then, leave standstill at normal temperatures 3-6h, filter, collect upper strata Herba Centellae solution; By centrifugal through the centrifuge of 10000-15000r/min upper strata Herba Centellae solution, obtain Herba Centellae extracting solution again, for subsequent use;
5., Flos Impatientis juice preparation: Flos Impatientis (note: Flos Impatientis petal) is cleaned, dropped in distil container together with the ethanol that is 50-60% with 3-5 times of weight, volumetric concentration, distill 8-12h at 85-100 DEG C, collect Flos Impatientis distillate; Be that 0.55-0.7MPa, temperature are that in the falling film condenser of 40-50 DEG C, to be concentrated into alcoholic degree be 30-40% by Flos Impatientis distillate in vacuum again, filter, obtain Flos Impatientis concentrated solution; In Flos Impatientis concentrated solution, add the ethylene glycol monostearate that accounts for Flos Impatientis concentrated solution weight 1.2-1.75% again, stir in the counterclockwise direction at normal temperatures 0.2-0.4h, leave standstill 2-3h, then, centrifuge through 10000-15000r/min is centrifugal, obtains Flos Impatientis juice, for subsequent use;
, get the raw materials ready: get respectively each raw material by above-mentioned weight portion, for subsequent use;
(3), mix: above-mentioned each raw material for subsequent use is dropped in agitator, is that under 80-100MHz, oscillation treatment, to mix homogeneously, is filtered in frequency, obtains compound, for subsequent use;
(4), sterilizing: compound for subsequent use, through pasteurize, is obtained to hair protecting shampoo of the present invention.
Described conditioner refers to one or more in octadecyl trimethyl ammonium chloride, three whale METH ammonium chloride, polyquaternary ammonium salt-7, in the time being two or more, weight portion or other ratio such as the ratio of each component is.
Described freshener is one or more in Oleum menthae, Oleum Camelliae, Aloe glue, in the time being two or more, weight portion or other ratio such as the ratio of each component is.
Described water quality essence is a kind of in oleum Citri sinensis, Fructus Citri Limoniae oil or two kinds, in the time being two kinds, weight portion or other ratio such as the ratio of each component is.
Described hair color light agent is one or more in cucumber extract, Semen Sesami Nigrum extracting solution, Radix Polygoni Multiflori extracting solution, green tea extractive liquor, in the time being two or more, weight portion or other ratio such as the ratio of each component is.
The technical scheme one of its optimization is to be prepared from by the raw material of following weight portion:
The technical scheme two of its optimization is to be prepared from by the raw material of following weight portion:
The technical scheme three of its optimization is to be prepared from by the raw material of following weight portion:
Hair protecting shampoo of the present invention, its primary raw material comprises conditioner, freshener, water quality essence, the agent of hair color light, Sucus Cucurbitae moschatae, Semen Glycines juice, Caulis Spatholobi extracting solution, Herba Centellae extracting solution, Oleum Arachidis hypogaeae semen, Flos Impatientis juice and pure water, also include the ethylene glycol monostearate being added in Flos Impatientis juice, Herba Centellae extracting solution, Caulis Spatholobi extracting solution, Semen Glycines juice, be added on Mel in Herba Centellae extracting solution, be added on the tea saponin in Caulis Spatholobi extracting solution, Semen Glycines juice, Sucus Cucurbitae moschatae, be added on the glyceryl monostearate in Sucus Cucurbitae moschatae.
Ethylene glycol monostearate [molecular formula: CH
3(CH
2)
16cOOCH
2cH
2oH)] in liquid scrubbing product, use and can produce obvious pearl effect, and can increase the viscosity of product, also there is skin care, hair care hair care and antistatic property; Meanwhile, good with the surfactant intermiscibility of other type, and can embody its stable pearl effect and thickening conditioning functions; And non-stimulated to skin, to hair not damaged.Be mainly used in shampoo, body lotion, skin lotion and high-grade liquid detergent etc.
Tea saponin (Tea Saponin) is a kind of natural nonionic surfactant of function admirable, and it has foaming, emulsifying, dispersion, the performance such as gentle, and has the pharmacological action of the aspects such as impervious, antiinflammatory, analgesia.Tea saponin wash my hair has loose, smooth, the anti-dandruff of sending out, the advantage such as antipruritic, has effect of clean hair care.
Glyceryl monostearate (molecular formula: C
42h
84o
8) in cosmetics as emulsifying agent and surfactant.
Conditioner comprises octadecyl trimethyl ammonium chloride, three whale METH ammonium chloride, polyquaternary ammonium salt-7.Wherein: octadecyl trimethyl ammonium chloride (molecular formula: C
21h
46clN) be a kind of softening agent, can make hair bulk, soft, be commonly used for the raw material of hair conditioner.Three whale METH ammonium chloride (model: VARISOFT TC90) are a kind of cationic surfactants, are applicable to manufacture hair conditioner, shampoo with treatment.Polyquaternary ammonium salt-7 (molecular formula: C
11h
21clN
2o) be a kind of cation opsonizing agent, for shampoo, bath gel, the emulsion that shaves, sizing water, also can be used as hair ornamenting conditioner, shampoo, hair conditioner, setting agent, skin moistening skin protectant, cold wave, the cosmetics such as emulsion, bath foam that shave, green grass or young crops has sterilization, sterilization and antisepsis.
Freshener comprises Oleum menthae, Oleum Camelliae, Aloe glue, wherein: Oleum menthae [Mentha arvensis oil (Mint oil; Cornmint oil)] pungent to disperse, cool to heat clearing away, clear light cool loose, after using, can produce refrigerant sense.In Oleum Camelliae (Camellia oleifera Abel), be rich in oleic acid, linoleic acid, there is skin care, black hair effect, can ultraviolet light, and antibacterial, kill germ; Meanwhile, in Oleum Camelliae, both contained tea saponin, also contain the multiple beneficial such as tea polyphenols active substance, can make shampoo and hair conditioner and use, can prevent tinea capitis, alopecia, scurf (Dandruff) and antipruritic.Aloe glue includes abundant vitamin, aminoacid, fatty acid, polysaccharose substance; There is natural antiinflammatory, antibiotic effect, also there is moisturizing, the function such as sun-proof, can protect hair not to be subject to ultraviolet infringement.
Water quality essence comprises oleum Citri sinensis, Fructus Citri Limoniae oil, wherein: Fructus Citri sinensis (skin) oil has special orange scent and gentle fragrant flavour.Fructus Citri Limoniae oil has strong citris aromas, can refreshment.
The agent of hair color light comprises commercially available cucumber extract, Semen Sesami Nigrum extracting solution, Radix Polygoni Multiflori extracting solution, green tea extractive liquor, wherein: Fructus Cucumidis sativi (Cucumis sativus Linn) extracting solution has antipyretic and antidote functions, can make hair surface form smooth hygroscopic mem-brane, increase the water content of hair.Semen Sesami Nigrum (Sesamum indicum L.) extracting solution contains antioxidant, vitamin E, sesamol, Semen Sesami melanin and trace element, being mainly used in the cosmetics such as shampoo, hair care, skin protection, is a kind of desirable natural cosmetics additive.In the Radix Polygoni Multiflori (Polygonum multiflorum Thunb.) extracting solution, contain the nutritions such as phospholipid, energy hairy root nourishing, hair black pigment is generated, can make hair more black, can also become hair nutrition conditioner, for hair care, the cosmetics of hair care or hair growth promoting, can make hair be easy to combing, pitch-black light, has good therapeutical effect for juvenile poliosis disease.Green tea (greentea) extracting solution contains the benefit materials such as tea polyphenols, caffeine, lipopolysaccharide, theanine, has the pharmacological actions such as moisturizing, antiinflammatory, sterilization, washing, hair care, fat-reducing, has good hair washing, hair care effect.
Sucus Cucurbitae moschatae adopts Fructus Cucurbitae moschatae preparation, in Fructus Cucurbitae moschatae (Cucurbita moschata), contain the multiple composition useful to human body, as polysaccharide, aminoacid, activated protein carotenoid and various trace elements etc., especially the pectin including has good adsorptivity, can bond and eliminate dirt and bacteriotoxin and other harmful substances on hair.
Semen Glycines juice adopts Semen Glycines preparation, Semen Glycines (Glycine max) contains the beneficiating ingredients such as multiple human body essential amino acid, and important Nutrition is played in human tissue cell, both can improve immune function of human body, also can improve skin aging, hair is had to good maintenance action.
Caulis Spatholobi extracting solution adopts Caulis Spatholobi preparation, and Caulis Spatholobi (Millettia dielsiana) has effect of relaxing muscles and tendons to promote blood circulation, nourishing blood for regulating menstruation, can unfold scalp meridians and blood vessel, increases scalp blood flow, plays the effect of hair care hair care.
Herba Centellae extracting solution adopts Herba Centellae preparation, and Herba Centellae (Centellaasiatica) can heat-clearing and toxic substances removing, inducing diuresis and reducing edema, also can refresh oneself by beneficial brain, and replacement that can scalp irritation deep skin cell, plays the effect of hair care hair care.
Flos Impatientis juice adopts Flos Impatientis preparation, and Flos Impatientis (Impatiens balsamina) has blood circulation promoting and blood stasis dispelling, the deep effect of stimulating the menstrual flow, and its pollen can effectively improve the blood circulation of scalp and hair follicle to strengthen scalp and hair follicle activity.
Semen arachidis hypogaeae (Arachishypogaea) oil, containing the glyceride of multiple fatty acid, has good lubrication to hair; Also contain multiple defying age composition, have the effect that delays brain function aging.
Mel (Apis cerana Fabr or Apis mellifera L.) contains the indispensable trace element of multiple human body and vitamin, is natural cosmetic health product.
Pure water, not containing any harmful substance and antibacterial, can supplement moisture content to human body in effective and safe ground, has very strong dissolubility, therefore very strong with human body cell affinity, has the effect enhancing metabolism.
Therefore, hair protecting shampoo of the present invention, has antiinflammatory, biocidal efficacies, meanwhile, contains the multiple active ingredient useful to hair, can hair care take care of hair, and clean result is better.
The hair protecting shampoo that contains tea saponin of the present invention, once carried out Anti-hair loss test:
50 of subjects, the age, between 20-40 year, is divided into test group (30 people) and matched group (20 people) at random, and test group personnel, use the hair protecting shampoo that contains tea saponin of the present invention; Matched group personnel, use commercially available shampoo (middle-grade product on the upper side) as reference.Once, 3 combing hairs of every natural gift morning, noon and afternoon, collect the hair that comes off and also record radical in hair washing in every 3 days, get its integer after obtaining meansigma methods.Test starts from early autumn, and the product that test is used, is the hair protecting shampoo that contain tea saponin prepared by embodiment tri-.
After the test of 60 days, statistical data, it the results are shown in table 1 below.
Table 1 Anti-hair loss statistical effect
From the data in table 1 above, through Anti-hair loss test, the improve significantly effect of alopecia of hair protecting shampoo of the present invention.Thereby hair protecting shampoo of the present invention possesses good hair care effect.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.Explanation is below the mode exemplifying, but protection scope of the present invention is not limited to this.
Embodiment mono-
The hair protecting shampoo that contains tea saponin of the present embodiment, its preparation process is as follows:
(1), pretreatment of raw material:
1., Sucus Cucurbitae moschatae preparation: Fructus Cucurbitae moschatae is cleaned, removed after Semen Cucurbitae, be cut into the Fructus Cucurbitae moschatae sheet that 0.15cm is thick (length uniformity), then, add 2 times of weight, the warm water of 60 DEG C, constant temperature soaks 10h, and filter pressing, obtains Fructus Cucurbitae moschatae water extraction liquid; Be that 0.6MPa, temperature are that in the falling film condenser of 45 DEG C, to be concentrated into solid content be 0.125mg/ml by Fructus Cucurbitae moschatae water extraction liquid in vacuum, obtain Fructus Cucurbitae moschatae concentrated solution; , at normal temperatures, to Fructus Cucurbitae moschatae concentrated solution in add the glyceryl monostearate that account for Fructus Cucurbitae moschatae concentrated solution weight 3.5% and the Mel that accounts for Fructus Cucurbitae moschatae concentrated solution volume 4%, stir 0.2h, transfer in freezer and leave standstill 15h, filter, obtain Fructus Cucurbitae moschatae filtrate thereafter; Fructus Cucurbitae moschatae filtrate is centrifugal through the centrifuge of 4000r/min, obtain Fructus Cucurbitae moschatae centrifugal liquid, then in Fructus Cucurbitae moschatae centrifugal liquid, add the tea saponin that accounts for Fructus Cucurbitae moschatae centrifugal liquid weight 0.9%, stir evenly, leave standstill 4h, then, by centrifugal through the centrifuge of 12000r/min upper strata Fructus Cucurbitae moschatae solution, obtain Sucus Cucurbitae moschatae, for subsequent use;
2., Semen Glycines juice preparation: Semen Glycines is cleaned, dropped in 2 times of weight, the warm water of 45 DEG C, be dipped to abundant expansion; Adequately expanded Semen Glycines, through extruder processing, is obtained to Semen Glycines filter liquor and Semen Glycines slag; In Semen Glycines slag, add the ethanol that equivalent weight, volumetric concentration are 50%, soak at normal temperatures 2h, filter, obtain Semen Glycines alcohol extract; Semen Glycines alcohol extract is mixed with Semen Glycines filter liquor, obtain Semen Glycines mixed liquor; At normal temperatures, in Semen Glycines mixed liquor, adding the ethylene glycol monostearate that accounts for Semen Glycines mixed liquor weight 2.2%, stir evenly, is then that 0.6MPa, temperature are to be concentrated into without alcohol in the falling film condenser of 45 DEG C by it in vacuum, obtains Semen Glycines concentrated solution; In Semen Glycines concentrated solution, add the tea saponin that accounts for Semen Glycines concentrated solution weight 0.35%, stir evenly, add again and account for Semen Glycines concentrated solution weight 12%, 150 object neutral silica gels (model is ZC-001), stir along clockwise direction 3h, then be transferred to standing 6h in freezer, filter, obtain Semen Glycines filtrate; Again that Semen Glycines filtrate is centrifugal through the centrifuge of 12000r/min, obtain Semen Glycines juice, for subsequent use;
3., Caulis Spatholobi extracting solution preparation: Caulis Spatholobi rattan is cleaned, be cut into the Caulis Spatholobi sheet of wide 0.8cm, long 3cm, then add the ethanol that 3 times of weight, volumetric concentration are 50% in Caulis Spatholobi sheet, boil and extract 0.8h, filter, obtain milletol extract; Be that 0.6MPa, temperature are that in the falling film condenser of 45 DEG C, to be concentrated into alcoholic degree be 30% (that is: the volumetric concentration of ethanol is 30%) by milletol extract in vacuum, obtain Caulis Spatholobi concentrated solution; In Caulis Spatholobi concentrated solution, add the ethylene glycol monostearate that accounts for Caulis Spatholobi concentrated solution weight 7.5% again, stir 0.2h, add again the acid active carbon (model is Norit-GC) that accounts for Caulis Spatholobi concentrated solution weight 14%, and stir after 0.6h at 45 DEG C, be transferred in freezer, leave standstill 18h, filter, obtain Caulis Spatholobi filtrate; Be to filter in the filter membrane device that is 30nm of 1.5Mpa, aperture Caulis Spatholobi filtrate at pressure, collect Caulis Spatholobi pressing filtering liquid; In Caulis Spatholobi pressing filtering liquid, add the tea saponin that accounts for Caulis Spatholobi pressing filtering liquid weight 0.8%, stir 0.2h, then add the ethyl acetate of equal volume, stir at normal temperatures 0.4h, leave standstill, layering, filtration, obtain the alcohol liquid after Caulis Spatholobi extraction; Then be that 0.6Mpa, temperature are to be concentrated into without alcohol in the falling film condenser of 45 DEG C by the alcohol liquid after Caulis Spatholobi extraction in vacuum, obtain Caulis Spatholobi extraction concentrated solution; Again Caulis Spatholobi is extracted to concentrated solution and be transferred in freezer, leave standstill 12h, filter, obtain Caulis Spatholobi extraction concentrated filtrate; Again Caulis Spatholobi is extracted to concentrated filtrate centrifugal through the centrifuge of 12000r/min, obtain Caulis Spatholobi extracting solution, for subsequent use;
4., Herba Centellae extracting solution preparation: Herba Centellae is cleaned, dropped in the sodium bicarbonate aqueous solution that 3 times of weight, pH value are 8, boil and extract 1.8h, filter, obtain Herba Centellae water extraction liquid; Be that 0.6MPa, temperature are that in the falling film condenser of 70 DEG C, to be concentrated into solid content be 0.55mg/ml by Herba Centellae water extraction liquid in vacuum again, filter, obtain Herba Centellae concentrated solution; In Herba Centellae concentrated solution, add the ethylene glycol monostearate that accounts for Herba Centellae concentrated solution weight 0.3% and the Mel that accounts for Herba Centellae concentrated solution volume 4% again, stir 0.2h, and at normal temperatures leave standstill 12h, then, then add the 250 order neutral silica gels (model is GF-245) that account for Herba Centellae concentrated solution weight 12%, and stir in the counterclockwise direction 0.6h, then, leave standstill at normal temperatures 4h, filter, collect upper strata Herba Centellae solution; By centrifugal through the centrifuge of 12000r/min upper strata Herba Centellae solution, obtain Herba Centellae extracting solution again, for subsequent use;
5., Flos Impatientis juice preparation: Flos Impatientis is cleaned, dropped in distil container together with the ethanol that is 55% with 4 times of weight, volumetric concentration, distill 10h at 90 DEG C, collect Flos Impatientis distillate; Be that 0.6MPa, temperature are that in the falling film condenser of 45 DEG C, to be concentrated into alcoholic degree be 35% (that is: the volumetric concentration of ethanol is 35%) by Flos Impatientis distillate in vacuum again, filter, obtain Flos Impatientis concentrated solution; In Flos Impatientis concentrated solution, add the ethylene glycol monostearate that accounts for Flos Impatientis concentrated solution weight 1.5% again, stir in the counterclockwise direction at normal temperatures 0.3h, leave standstill 2h, then, centrifugal through the centrifuge of 12000r/min, obtain Flos Impatientis juice, for subsequent use;
(2), get the raw materials ready: get respectively by weight 3 parts of conditioners (wherein: octadecyl trimethyl ammonium chloride, each 1 part of three whale METH ammonium chloride and polyquaternary ammonium salt-7), 3 parts of fresheners (wherein: Oleum menthae, each 1 part of Oleum Camelliae and Aloe glue), 1 part, water quality essence (wherein: each 0.5 part of oleum Citri sinensis and Fructus Citri Limoniae oil), 15 parts of hair color light agent (wherein: cucumber extract, each 5 parts of Semen Sesami Nigrum extracting solution fleece-flower root extracting solution), 1.5 parts of Oleum Arachidis hypogaeae semen, 1 part of Caulis Spatholobi extracting solution, 4 parts of Herba Centellae extracting solution, 1 part of Flos Impatientis juice, 4 parts of Sucus Cucurbitae moschatae, 3 parts of Semen Glycines juice, 63.5 parts of pure water, for subsequent use,
(3), mix: above-mentioned each raw material for subsequent use is dropped in agitator, is that under 90MHz, oscillation treatment, to mix homogeneously, becomes compound in frequency, for subsequent use;
(4), sterilizing: compound for subsequent use, through pasteurize (sterilization temperature is 62-65 DEG C, keeps 30min), is to hair protecting shampoo of the present invention.
Hair protecting shampoo of the present invention, its using method is identical with commercially available shampoo.
Embodiment bis-
The hair protecting shampoo that contains tea saponin of the present embodiment, its preparation process is as follows:
(1), pretreatment of raw material: identical with embodiment mono-;
, get the raw materials ready: get respectively by weight 5 parts of conditioners (wherein: 3 parts of octadecyl trimethyl ammonium chloride, 2 parts of three whale METH ammonium chloride), freshener 5 parts of (wherein: 2 parts of Oleum menthae, 3 parts of Aloe glues), water quality essence 3 parts of (wherein: each 1.5 parts of oleum Citri sinensis and Fructus Citri Limoniae oil), the agent of hair color light 25 parts of (wherein: 12 parts of cucumber extracts, 13 parts of Radix Polygoni Multiflori extracting solution), 4 parts of Caulis Spatholobi extracting solution, 1 part of Herba Centellae extracting solution, 3 parts of Flos Impatientis juice, 0.5 part of Oleum Arachidis hypogaeae semen, 6 parts of Sucus Cucurbitae moschatae, 5 parts of Semen Glycines juice, 42.5 parts of pure water, for subsequent use;
Other step is identical with embodiment mono-.
Embodiment tri-
The hair protecting shampoo that contains tea saponin of the present embodiment, its preparation process is as follows:
(1), pretreatment of raw material: identical with embodiment mono-;
(2), get the raw materials ready: get respectively by weight 4 parts of conditioners (4 parts of octadecyl trimethyl ammonium chloride), 1 part of glyceryl monostearate, 4 parts of fresheners (wherein: each 2 parts of Oleum Camelliae and Aloe glue), 2 parts, water quality essence (wherein: each 1 part of oleum Citri sinensis and Fructus Citri Limoniae oil), 20 parts of hair color light agent (wherein: cucumber extract, Semen Sesami Nigrum extracting solution, Radix Polygoni Multiflori extracting solution, each 5 parts of green tea extractive liquor), 3 parts of Caulis Spatholobi extracting solution, 3 parts of Herba Centellae extracting solution, 2 parts of Flos Impatientis juice, 1 part of Oleum Arachidis hypogaeae semen, 5 parts of Sucus Cucurbitae moschatae, 4 parts of Semen Glycines juice, 48 parts of pure water, for subsequent use,
Other step is identical with embodiment mono-.
Hair protecting shampoo of the present invention, the crowd who is applicable to each age of men and women, old and young uses.
Claims (8)
1. a hair protecting shampoo, it is characterized in that being prepared from by the raw material of following weight portion:
Its preparation process is as follows:
(1), pretreatment of raw material:
1., Sucus Cucurbitae moschatae preparation: Fructus Cucurbitae moschatae is cleaned, removed after Semen Cucurbitae, be cut into the Fructus Cucurbitae moschatae sheet that 0.1-0.25cm is thick, then, add the warm water of 1-2 times of weight, 50-65 DEG C, constant temperature soaks 7-12h, and filter pressing, obtains Fructus Cucurbitae moschatae water extraction liquid; Be that 0.55-0.7MPa, temperature are that in the falling film condenser of 40-50 DEG C, to be concentrated into solid content be 0.085-0.175mg/ml by Fructus Cucurbitae moschatae water extraction liquid in vacuum, obtain Fructus Cucurbitae moschatae concentrated solution; ,, at normal temperatures, in Fructus Cucurbitae moschatae concentrated solution, add the glyceryl monostearate that accounts for Fructus Cucurbitae moschatae concentrated solution weight 2.5-4.5% and the Mel that accounts for Fructus Cucurbitae moschatae concentrated solution volume 2.0-5.0% thereafter, stir 0.1-0.3h, transfer in freezer and leave standstill 10-18h, filter, obtain Fructus Cucurbitae moschatae filtrate; Fructus Cucurbitae moschatae filtrate is centrifugal through the centrifuge of 3000-5000r/min, obtain Fructus Cucurbitae moschatae centrifugal liquid, then in Fructus Cucurbitae moschatae centrifugal liquid, add the tea saponin that accounts for Fructus Cucurbitae moschatae centrifugal liquid weight 0.6-1.2%, stir evenly, leave standstill 3-5h, then, by centrifugal through the centrifuge of 10000-15000r/min upper strata Fructus Cucurbitae moschatae solution, obtain Sucus Cucurbitae moschatae, for subsequent use;
2., Semen Glycines juice preparation: Semen Glycines is cleaned, dropped in the warm water of 1.5-2.5 times of weight, 40-50 DEG C, be dipped to abundant expansion; Adequately expanded Semen Glycines, through extruder processing, is obtained to Semen Glycines filter liquor and Semen Glycines slag; In Semen Glycines slag, add the ethanol that equivalent weight, volumetric concentration are 45-55%, soak at normal temperatures 1.5-3.0h, filter, obtain Semen Glycines alcohol extract; Semen Glycines alcohol extract is mixed with Semen Glycines filter liquor, obtain Semen Glycines mixed liquor; At normal temperatures, in Semen Glycines mixed liquor, adding the ethylene glycol monostearate that accounts for Semen Glycines mixed liquor weight 1.5-3%, stir evenly, is then that 0.55-0.7MPa, temperature are to be concentrated into without alcohol in the falling film condenser of 40-50 DEG C by it in vacuum, obtains Semen Glycines concentrated solution; In Semen Glycines concentrated solution, add the tea saponin that accounts for Semen Glycines concentrated solution weight 0.2-0.5%, stir evenly, then add and account for Semen Glycines concentrated solution weight 10-15%, 100-200 object neutral silica gel, stir along clockwise direction 2-4h, then be transferred in freezer and leave standstill 4-8h, filter, obtain Semen Glycines filtrate; Again that Semen Glycines filtrate is centrifugal through the centrifuge of 10000-15000r/min, obtain Semen Glycines juice, for subsequent use;
3., Caulis Spatholobi extracting solution preparation: Caulis Spatholobi rattan is cleaned, be cut into the Caulis Spatholobi sheet of wide 0.5-1.0cm, long 2.0-4.0cm, then add the ethanol that 2-4 times of weight, volumetric concentration are 40-55% in Caulis Spatholobi sheet, boil and extract 0.6-0.9h, filter, obtain milletol extract; Be that 0.55-0.7MPa, temperature are that in the falling film condenser of 40-50 DEG C, to be concentrated into alcoholic degree be 25-32% by milletol extract in vacuum, obtain Caulis Spatholobi concentrated solution; In Caulis Spatholobi concentrated solution, add the ethylene glycol monostearate that accounts for Caulis Spatholobi concentrated solution weight 5.5-9.5% again, stir 0.1-0.3h, add again the acid active carbon that accounts for Caulis Spatholobi concentrated solution weight 12-16%, and stir after 0.5-0.8h at 40-50 DEG C, be transferred in freezer, leave standstill 15-20h, filter, obtain Caulis Spatholobi filtrate; Be to filter in the filter membrane device that is 25-35nm of 1.15-2.25Mpa, aperture Caulis Spatholobi filtrate at pressure, collect Caulis Spatholobi pressing filtering liquid; In Caulis Spatholobi pressing filtering liquid, add the tea saponin that accounts for Caulis Spatholobi pressing filtering liquid weight 0.6-1%, stir 0.1-0.3h, then add the ethyl acetate of equal volume, stir at normal temperatures 0.2-0.5h, leave standstill, layering, filtration, obtain the alcohol liquid after Caulis Spatholobi extraction; Then be that 0.55-0.7Mpa, temperature are to be concentrated into without alcohol in the falling film condenser of 40-50 DEG C by the alcohol liquid after Caulis Spatholobi extraction in vacuum, obtain Caulis Spatholobi extraction concentrated solution; Again Caulis Spatholobi is extracted to concentrated solution and be transferred in freezer, leave standstill 10-15h, filter, obtain Caulis Spatholobi extraction concentrated filtrate; Again Caulis Spatholobi is extracted to concentrated filtrate centrifugal through the centrifuge of 10000-15000r/min, obtain Caulis Spatholobi extracting solution, for subsequent use;
4., Herba Centellae extracting solution preparation: Herba Centellae is cleaned, dropped in the aqueous alkali that 2-3 times of weight, pH value are 7-9, boil and extract 1.5-2.0h, filter, obtain Herba Centellae water extraction liquid; Be that 0.55-0.7MPa, temperature are that in the falling film condenser of 65-75 DEG C, to be concentrated into solid content be 0.45-0.7mg/ml by Herba Centellae water extraction liquid in vacuum again, filter, obtain Herba Centellae concentrated solution; In Herba Centellae concentrated solution, add the ethylene glycol monostearate that accounts for Herba Centellae concentrated solution weight 0.15-0.45% and the Mel that accounts for Herba Centellae concentrated solution volume 2.0-5.0% again, stir 0.1-0.3h, and at normal temperatures leave standstill 10-15h, then, then add the 200-300 order neutral silica gel that accounts for Herba Centellae concentrated solution weight 10-15%, and stir in the counterclockwise direction 0.5-0.7h, then, leave standstill at normal temperatures 3-6h, filter, collect upper strata Herba Centellae solution; By centrifugal through the centrifuge of 10000-15000r/min upper strata Herba Centellae solution, obtain Herba Centellae extracting solution again, for subsequent use;
5., Flos Impatientis juice preparation: Flos Impatientis is cleaned, dropped in distil container together with the ethanol that is 50-60% with 3-5 times of weight, volumetric concentration, distill 8-12h at 85-100 DEG C, collect Flos Impatientis distillate; Be that 0.55-0.7MPa, temperature are that in the falling film condenser of 40-50 DEG C, to be concentrated into alcoholic degree be 30-40% by Flos Impatientis distillate in vacuum again, filter, obtain Flos Impatientis concentrated solution; In Flos Impatientis concentrated solution, add the ethylene glycol monostearate that accounts for Flos Impatientis concentrated solution weight 1.2-1.75% again, stir in the counterclockwise direction at normal temperatures 0.2-0.4h, leave standstill 2-3h, then, centrifuge through 10000-15000r/min is centrifugal, obtains Flos Impatientis juice, for subsequent use;
, get the raw materials ready: get respectively each raw material by above-mentioned weight portion, for subsequent use;
(3), mix: above-mentioned each raw material for subsequent use is dropped in agitator, is that under 80-100MHz, oscillation treatment, to mix homogeneously, is filtered in frequency, obtains compound, for subsequent use;
(4), sterilizing: compound for subsequent use, through pasteurize, is obtained to hair protecting shampoo of the present invention.
2. hair protecting shampoo according to claim 1, it is characterized in that: described conditioner refers to one or more in octadecyl trimethyl ammonium chloride, three whale METH ammonium chloride, polyquaternary ammonium salt-7, in the time being two or more, weight portion or other ratio such as the ratio of each component is.
3. hair protecting shampoo according to claim 1 and 2, is characterized in that: described freshener is one or more in Oleum menthae, Oleum Camelliae, Aloe glue, in the time being two or more, weight portion or other ratio such as the ratio of each component is.
4. hair protecting shampoo according to claim 3, is characterized in that: described water quality essence is a kind of in oleum Citri sinensis, Fructus Citri Limoniae oil or two kinds, in the time being two kinds, weight portion or other ratio such as the ratio of each component is.
5. hair protecting shampoo according to claim 4, it is characterized in that: described hair color light agent is one or more in cucumber extract, Semen Sesami Nigrum extracting solution, Radix Polygoni Multiflori extracting solution, green tea extractive liquor, in the time being two or more, weight portion or other ratio such as the ratio of each component is.
6. hair protecting shampoo according to claim 5, it is characterized in that being prepared from by the raw material of following weight portion:
7. hair protecting shampoo according to claim 5, it is characterized in that being prepared from by the raw material of following weight portion:
8. hair protecting shampoo according to claim 5, it is characterized in that being prepared from by the raw material of following weight portion:
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