CN105878119A - Birch sap toner and preparation method thereof - Google Patents

Birch sap toner and preparation method thereof Download PDF

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Publication number
CN105878119A
CN105878119A CN201610358322.2A CN201610358322A CN105878119A CN 105878119 A CN105878119 A CN 105878119A CN 201610358322 A CN201610358322 A CN 201610358322A CN 105878119 A CN105878119 A CN 105878119A
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China
Prior art keywords
betulae platyphyllae
sucus
sucus betulae
astringent
platyphyllae
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CN201610358322.2A
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CN105878119B (en
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郭德军
刘亚娜
杨华
庞惟俏
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GREATER KHINGAN RANGE CHAOYUE WILD BERRY DEVELOPMENT CO LTD
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Heilongjiang Bayi Agricultural University
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin

Abstract

The invention relates to a birch sap toner and a preparation method thereof. The toner is prepared from the following components in percentage by mass: 8-10 percent of red raspberry distillate, 0.2-0.3 percent of potassium sorbate, 0.05-0.1 percent of vitamin C, 0.03-0.05 percent of hyaluronic acid, 0.02-0.04 percent of lysozyme, 0.01-0.02 percent of jasmine absolute and the balance of birch sap. The birch sap toner is a natural cosmetic, is mild and non-irritant, has an excellent effect of smoothing skin, can be used for removing acnes and freckles on the face of a person with good moistening effect, and can be used in a large area constantly for a long time.

Description

A kind of Sucus Betulae platyphyllae astringent and preparation method thereof
One, technical field
The present invention relates to cosmetic field, be specifically related to a kind of Sucus Betulae platyphyllae astringent and preparation method thereof.
Two, background technology
Astringent is the cosmetics of a kind of transparent liquid, spreads upon the surface of skin, is used for cleaning skin, moisturizing, holding skin Health, is people's requisite articles for use of daily beauty and skin care.Astringent comprises substantial amounts of nutrient substance, can be that skin carries For abundant nutrition, can be with the moisture of conditioning skin and oil point, Glycerin is allowed to more soft, is rich in gloss.
But the most a lot of astringent all contain alcoholic content, two fatal defects so occur.One, ethanol is easily waved Send out, and also can take away the moisture on skin when volatilization, make xerosis cutis.Its two, the ethanol capacity of decomposition that concentration is higher Very strong, while decomposing facial oil, also can destroy the water quality film that skin is own, make skin become fragile sensitive.So, contain Ethanol astringent must not use long lasting for large area.
Three, summary of the invention
It is an object of the present invention to provide a kind of Sucus Betulae platyphyllae astringent, this Sucus Betulae platyphyllae astringent is main with water Raw material, for alcohol-free plant toning lotion, is used for solving the problem that spirituosity astringent can not use long lasting for large area, It is a further object to provide the preparation method of this Sucus Betulae platyphyllae astringent.
To achieve these goals, the concrete technical scheme that the present invention uses is as follows: each group of this Sucus Betulae platyphyllae astringent Divide and calculate according to mass percent, red raspberry fruit distillate 8 ~ 10%, potassium sorbate 0.2 ~ 0.3%, vitamin c 0.05 ~ 0.1%, Hyaluronic acid 0.03 ~ 0.05%, lysozyme 0.02 ~ 0.04%, jasmin essence 0.01 ~ 0.02%, remaining is Sucus Betulae platyphyllae.
In such scheme 70% of content described in Sucus Betulae platyphyllae, the red raspberry fruit distillate of described content, jasmin essence, Pyrusussuriensis Acid potassium, vitamin, lysozyme are proportionally added into, and uniformly after mixing, the rolling gradient ceramic-film machine microfiltration of via hole diameter 1.4 m removes Bacterium, is prepared as microfiltration bacteria-removing liquid;30% of content described in Sucus Betulae platyphyllae adds the hyaluronic acid of described content, carries out high-temperature instantaneous Sterilization, is prepared as the hyaluronic acid solution of sterilizing, microfiltration bacteria-removing liquid and hyaluronic acid solution, obtains described Betula after mix homogeneously Liquid astringent.
Red raspberry fruit distillate 10% in such scheme, potassium sorbate 0.3%, vitamin c 0.1%, hyaluronic acid 0.05%, Lysozyme 0.03%, jasmin essence 0.02%, remaining is Sucus Betulae platyphyllae.
The preparation method of Sucus Betulae platyphyllae astringent in such scheme:
(1) ripe red raspberry fruit is crushed, 70 ~ 75 DEG C, decompression distillation under the conditions of vacuum 30-60mbar, collect Rhizophora apiculata Blume Certain kind of berries fruit weight 1/4 distillate, airtight cryopreservation is standby;
(2) Sucus Betulae platyphyllae acquisition time before foliation in early spring, resin is when starting to flow, from Betula in person, from branch soft to Till foliation, i.e. when Daily minimum temperature-5 DEG C is with the highest temperature 10 DEG C, on Betula is dry, bore shallow bore hole, by hollow aluminum pipe and Plastic Drum Collect Sucus Betulae platyphyllae;Within 10-12 hour, collect a Sucus Betulae platyphyllae, collected Sucus Betulae platyphyllae through 120 mesh filter-cloth filtering remove impurity, rapidly-20 DEG C freezen protective;
(3) in formula the 70% of Sucus Betulae platyphyllae content, and the red raspberry fruit distillate of described content, jasmin essence, potassium sorbate, dimension Raw element, lysozyme are proportionally added into, and uniformly after mixing, the rolling gradient ceramic-film machine microfiltration of via hole diameter 1.4 m is degerming, crosses mould Power is 100kPa, cross-flow rate 5m/s, and recoil 10 times/h, and filtration temperature 40 ~ 45 DEG C is prepared as microfiltration bacteria-removing liquid;
(4) formula adds in the 30% of Sucus Betulae platyphyllae content the hyaluronic acid of described content, is heated to 65 ~ 70 DEG C, passes through homogenizer After mix homogeneously, then it is heated to 130 DEG C through heat-exchangers of the plate type and carries out high-temperature instantaneous sterilization in 5 seconds, be prepared as the hyalomitome of sterilizing Acid solution, uses heat-exchangers of the plate type temperature of charge to be down to 40 ~ 45 DEG C, by whole microfiltration bacteria-removing liquids and the sterilizing of above-mentioned preparation All transparent matter acid solution, in material-compound tank after mix homogeneously, carry out aseptic auto-filling, i.e. obtain Sucus Betulae platyphyllae astringent.
Sucus Betulae platyphyllae is a kind of natural activated water, has the laudatory title of healthy Herba Cynomorii in Northern Europe, is usually used in alleviating burn, skin Rash etc.." Chinese medicine voluminous dictionary " recites pine gum alcohol, fatty acid, tannin, polysaccharide, Saponin, protein in birch juice. only have Effects such as coughing, eliminate the phlegm, relieving asthma, be antibacterial, nature and flavor " bitter ", " trembling with fear ".Song dynasty " Kai Baofeng grass " records birch juice " bitter, flat, nontoxic ".According to Data at home and abroad is analyzed, birch juice rich in multiple amino acid needed by human body, various mineral particularly calcium, magnesium, potassium, sodium, phosphorus, Germanium, selenium and other trace elements content are higher, and dry is up to about 1%, and amino acid whose total amount is up to 17579.4mg/L, trace element Total amount reach 160.84mg/L.Sucus Betulae platyphyllae is rich in polysaccharide, aminoacid, essential oil, birch bud alcohol, saponin, nicotinic acid, malic acid and birch The compositions such as skin brain, have skin nourishing and the character of bacteriocidin, be a kind of natural bright and clean skin, has and removes people on the face Acne and effect of freckle.They can supplement moisture and the nutritional labeling of loss in skin, eliminates pachylosis, removes skin antiperspirant Stain, sebum, the effect of sterilizing and itch-relieving.
Beneficial effect:
1, the present invention uses Sucus Betulae platyphyllae as raw material production astringent, Sucus Betulae platyphyllae effect: Sucus Betulae platyphyllae is rich in polysaccharide, aminoacid, perfume (or spice) The compositions such as quintessence oil, birch bud alcohol, saponin, nicotinic acid and birch skin brain, have the character of bacteriocidin, have removing people's acne on the face They can supplement moisture and the nutritional labeling of loss in skin with effect of freckle, eliminates pachylosis, removes skin sweat stain, skin Fat, the effect of sterilizing and itch-relieving.It contains a certain proportion of hyaluronic acid simultaneously, has good moisture-keeping efficacy;Natural gentle nothing Stimulating, bright and clean skin effects is excellent, and not spirituosity can use long lasting for large area.
2, the present invention is when preparing Sucus Betulae platyphyllae astringent, in order to retain the nutritional labeling in Sucus Betulae platyphyllae to greatest extent, takes the lead in Sucus Betulae platyphyllae degerming on employ microfiltration sterilization technique.
3, present invention also offers a kind of simple to operate, Sucus Betulae platyphyllae astringent preparation method that production efficiency is high.
Four, detailed description of the invention
Embodiment 1:
Each component of this Sucus Betulae platyphyllae astringent calculates according to mass percent, red raspberry fruit distillate 8%, potassium sorbate 0.2%, Vitamin c 0.1%, hyaluronic acid 0.03%, lysozyme 0.04%, jasmin essence 0.01%, Sucus Betulae platyphyllae is 91.62%.
The preparation method of Sucus Betulae platyphyllae astringent in such scheme:
(1) ripe red raspberry fruit is crushed, 70 ~ 75 DEG C, decompression distillation under the conditions of vacuum 30-60mbar, collect Rhizophora apiculata Blume Certain kind of berries fruit weight 1/4 distillate, airtight cryopreservation is standby.
(2) Sucus Betulae platyphyllae acquisition time should before foliation in early spring, resin is advisable when starting to flow, generally from Betula in person See, soft to foliation from branch, i.e. when Daily minimum temperature-5 DEG C is with the highest temperature 10 DEG C, on Betula is dry, bores shallow bore hole, presses Hollow aluminum pipe and Plastic Drum collect Sucus Betulae platyphyllae;Within generally 10-12 hour, collecting a Sucus Betulae platyphyllae, collected Sucus Betulae platyphyllae is through 120 mesh Filter-cloth filtering remove impurity ,-20 DEG C of freezen protective, thaw during configuration standby rapidly.
(3) the required tool of production and cosmetic bottle are cleaned up, disinfect standby.
(4) by Sucus Betulae platyphyllae 64.134%(i.e. the 70% of formulation content), and red raspberry fruit distillate 8%, jasmin essence 0.01%, Potassium sorbate 0.2%, vitamin c 0.1%, lysozyme 0.04% add, uniformly after mixing, and the rolling gradient pottery of via hole diameter 1.4 m Porcelain film machine microfiltration is degerming, and crossing film pressure is 100kPa, cross-flow rate 5m/s, and recoil 10 times/h, filtration temperature 40 ~ 45 DEG C, preparation Become microfiltration bacteria-removing liquid.
(5) by Sucus Betulae platyphyllae 27.486%(i.e. the 30% of formulation content) middle addition hyaluronic acid 0.03%, it is heated to 65 ~ 70 DEG C, After homogenizer mix homogeneously, then it is heated to 130 DEG C through heat-exchangers of the plate type and carries out high-temperature instantaneous sterilization in 5 seconds, be prepared as going out The hyaluronic acid solution of bacterium, uses heat-exchangers of the plate type that temperature of charge is down to 40 ~ 45 DEG C, is removed by whole microfiltration of above-mentioned preparation Bacterium solution and all transparent matter acid solution of sterilizing, in material-compound tank after mix homogeneously, carry out aseptic auto-filling, i.e. obtain Betula Liquid astringent.
Embodiment 2:
Each component of this Sucus Betulae platyphyllae astringent calculates according to mass percent, red raspberry fruit distillate 10%, potassium sorbate 0.3%, vitamin c 0.1%, hyaluronic acid 0.05%, lysozyme 0.03%, jasmin essence 0.02%, Sucus Betulae platyphyllae is 89.5%.
The preparation method of Sucus Betulae platyphyllae astringent in such scheme:
(1) ripe red raspberry fruit is crushed, 70 ~ 75 DEG C, decompression distillation under the conditions of vacuum 30-60mbar, collect Rhizophora apiculata Blume Certain kind of berries fruit weight 1/4 distillate, airtight cryopreservation is standby.
(2) Sucus Betulae platyphyllae acquisition time should before foliation in early spring, resin is advisable when starting to flow, generally from Betula in person See, soft to foliation from branch, i.e. when Daily minimum temperature-5 DEG C is with the highest temperature 10 DEG C, on Betula is dry, bores shallow bore hole, presses Hollow aluminum pipe and Plastic Drum collect Sucus Betulae platyphyllae;Within generally 10-12 hour, collecting a Sucus Betulae platyphyllae, collected Sucus Betulae platyphyllae is through 120 mesh Filter-cloth filtering remove impurity ,-20 DEG C of freezen protective, thaw during configuration standby rapidly.
(3) the required tool of production and cosmetic bottle are cleaned up, disinfect standby.
(4) by Sucus Betulae platyphyllae 62.65%(i.e. the 70% of formulation content), red raspberry fruit distillate 10%, jasmin essence 0.02%, mountain Potassium sorbate 0.3%, vitamin 0.1%, lysozyme 0.03% add, uniformly after mixing, and the rolling gradient ceramic-film of via hole diameter 1.4 m Machine microfiltration is degerming, and crossing film pressure is 100kPa, cross-flow rate 5m/s, and recoil 10 times/h, and filtration temperature 40 ~ 45 DEG C is prepared as micro- Filter bacterium solution.
(5) by Sucus Betulae platyphyllae 26.85%(i.e. the 30% of formulation content) middle addition hyaluronic acid 0.05%, it is heated to 65 ~ 70 DEG C, After homogenizer mix homogeneously, then it is heated to 130 DEG C through heat-exchangers of the plate type and carries out high-temperature instantaneous sterilization in 5 seconds, be prepared as going out The hyaluronic acid solution of bacterium, uses heat-exchangers of the plate type that temperature of charge is down to 40 ~ 45 DEG C, is removed by whole microfiltration of above-mentioned preparation Bacterium solution and all transparent matter acid solution of sterilizing, in material-compound tank after mix homogeneously, carry out aseptic auto-filling, i.e. obtain Betula Liquid astringent.
Embodiment 3:
Each component of this Sucus Betulae platyphyllae astringent calculates according to mass percent, red raspberry fruit distillate 9%, potassium sorbate 0.2%, Vitamin c 0.05%, hyaluronic acid 0.04%, lysozyme 0.02%, jasmin essence 0.01%, Sucus Betulae platyphyllae is 90.68%.
The preparation method of Sucus Betulae platyphyllae astringent in such scheme:
(1) ripe red raspberry fruit is crushed, 70 ~ 75 DEG C, decompression distillation under the conditions of vacuum 30-60mbar, collect Rhizophora apiculata Blume Certain kind of berries fruit weight 1/4 distillate, airtight cryopreservation is standby.
(2) Sucus Betulae platyphyllae acquisition time should before foliation in early spring, resin is advisable when starting to flow, generally from Betula in person See, soft to foliation from branch, i.e. when Daily minimum temperature-5 DEG C is with the highest temperature 10 DEG C, on Betula is dry, bores shallow bore hole, presses Hollow aluminum pipe and Plastic Drum collect Sucus Betulae platyphyllae;Within generally 10-12 hour, collecting a Sucus Betulae platyphyllae, collected Sucus Betulae platyphyllae is through 120 mesh Filter-cloth filtering remove impurity ,-20 DEG C of freezen protective, thaw during configuration standby rapidly.
(3) the required tool of production and cosmetic bottle are cleaned up, disinfect standby.
(4) by Sucus Betulae platyphyllae 63.476%(i.e. the 70% of formulation content), red raspberry fruit distillate 9%, jasmin essence 0.01%, mountain Potassium sorbate 0.2%, vitamin 0.05%, lysozyme 0.02% add, uniformly after mixing, and the rolling gradient ceramic-film of via hole diameter 1.4 m Machine microfiltration is degerming, and crossing film pressure is 100kPa, cross-flow rate 5m/s, and recoil 10 times/h, and filtration temperature 40 ~ 45 DEG C is prepared as micro- Filter bacterium solution.
(5) by Sucus Betulae platyphyllae 27.204%(i.e. the 30% of formulation content) middle addition hyaluronic acid 0.04%, it is heated to 65 ~ 70 DEG C, After homogenizer mix homogeneously, then it is heated to 130 DEG C through heat-exchangers of the plate type and carries out high-temperature instantaneous sterilization in 5 seconds, be prepared as going out The hyaluronic acid solution of bacterium, uses heat-exchangers of the plate type that temperature of charge is down to 40 ~ 45 DEG C, is removed by whole microfiltration of above-mentioned preparation Bacterium solution and all transparent matter acid solution of sterilizing, in material-compound tank after mix homogeneously, carry out aseptic auto-filling, i.e. obtain Betula Liquid astringent.

Claims (4)

1. a Sucus Betulae platyphyllae astringent, it is characterised in that: each component of this Sucus Betulae platyphyllae astringent calculates according to mass percent, Red raspberry fruit distillate 8 ~ 10%, potassium sorbate 0.2 ~ 0.3%, vitamin c 0.05 ~ 0.1%, hyaluronic acid 0.03 ~ 0.05%, molten Bacterium enzyme 0.02 ~ 0.04%, jasmin essence 0.01 ~ 0.02%, remaining is Sucus Betulae platyphyllae.
Sucus Betulae platyphyllae astringent the most according to claim 1, it is characterised in that: the 70% of described Sucus Betulae platyphyllae content, described contain The red raspberry fruit distillate of amount, jasmin essence, potassium sorbate, vitamin, lysozyme are proportionally added into, uniformly after mixing, through hole The rolling gradient ceramic-film machine microfiltration of footpath 1.4 m is degerming, is prepared as microfiltration bacteria-removing liquid;The 30% of described Sucus Betulae platyphyllae content adds The hyaluronic acid of described content, carries out high-temperature instantaneous sterilization, is prepared as the hyaluronic acid solution of sterilizing, and microfiltration bacteria-removing liquid is with transparent After matter acid solution mix homogeneously, obtain described Sucus Betulae platyphyllae astringent.
Sucus Betulae platyphyllae astringent the most according to claim 1, it is characterised in that: described red raspberry fruit distillate 10%, Pyrusussuriensis Acid potassium 0.3%, vitamin c 0.1%, hyaluronic acid 0.05%, lysozyme 0.03%, jasmin essence 0.02%, remaining is Sucus Betulae platyphyllae.
4. the Sucus Betulae platyphyllae astringent preparation method described in a claim 1 or 2, it is characterised in that: described Sucus Betulae platyphyllae is made up Water preparation method:
(1) ripe red raspberry fruit is crushed, 70 ~ 75 DEG C, decompression distillation under the conditions of vacuum 30-60mbar, collect Rhizophora apiculata Blume Certain kind of berries fruit weight 1/4 distillate, airtight cryopreservation is standby;
(2) Sucus Betulae platyphyllae acquisition time before foliation in early spring, resin is when starting to flow, from Betula in person, from branch soft to Till foliation, i.e. when Daily minimum temperature-5 DEG C is with the highest temperature 10 DEG C, on Betula is dry, bore shallow bore hole, by hollow aluminum pipe and Plastic Drum Collect Sucus Betulae platyphyllae;Within 10-12 hour, collect a Sucus Betulae platyphyllae, collected Sucus Betulae platyphyllae through 120 mesh filter-cloth filtering remove impurity, rapidly-20 DEG C freezen protective;
(3) in formula the 70% of Sucus Betulae platyphyllae content, and the red raspberry fruit distillate of described content, jasmin essence, potassium sorbate, dimension Raw element, lysozyme are proportionally added into, and uniformly after mixing, the rolling gradient ceramic-film machine microfiltration of via hole diameter 1.4 m is degerming, crosses mould Power is 100kPa, cross-flow rate 5m/s, and recoil 10 times/h, and filtration temperature 40 ~ 45 DEG C is prepared as microfiltration bacteria-removing liquid;
(4) formula adds in the 30% of Sucus Betulae platyphyllae content the hyaluronic acid of described content, is heated to 65 ~ 70 DEG C, passes through homogenizer After mix homogeneously, then it is heated to 130 DEG C through heat-exchangers of the plate type and carries out high-temperature instantaneous sterilization in 5 seconds, be prepared as the hyalomitome of sterilizing Acid solution, uses heat-exchangers of the plate type temperature of charge to be down to 40 ~ 45 DEG C, by whole microfiltration bacteria-removing liquids and the sterilizing of above-mentioned preparation All transparent matter acid solution, in material-compound tank after mix homogeneously, carry out aseptic auto-filling, i.e. obtain Sucus Betulae platyphyllae astringent.
CN201610358322.2A 2016-05-26 2016-05-26 A kind of japanese white birch juice toner and preparation method thereof Active CN105878119B (en)

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CN106974860A (en) * 2017-04-05 2017-07-25 中国科学院西北高原生物研究所 A kind of skin care compositions containing raspberry and emulsion
EP4062900A3 (en) * 2017-04-27 2023-08-09 Yang Sheng Tang (Shanghai) Cosmetic R&D Co., Ltd. Skin care cosmetic composition
CN107019660A (en) * 2017-04-27 2017-08-08 养生堂(上海)化妆品研发有限公司 Moisture-keeping cosmetics composition
CN107049865A (en) * 2017-04-27 2017-08-18 养生堂(上海)化妆品研发有限公司 Skin care cosmetic compositions
CN107019660B (en) * 2017-04-27 2018-05-11 养生堂(上海)化妆品研发有限公司 Moisture-keeping cosmetics composition
WO2018196481A1 (en) * 2017-04-27 2018-11-01 养生堂(上海)化妆品研发有限公司 Moisturizing cosmetics composition
WO2018196482A1 (en) * 2017-04-27 2018-11-01 养生堂(上海)化妆品研发有限公司 Skin care cosmetic composition
EP3510993A4 (en) * 2017-04-27 2020-06-03 Yang Sheng Tang (Shanghai) Cosmetic R&D Co., Ltd. Skin care cosmetic composition
US10799445B2 (en) 2017-04-27 2020-10-13 Yang Sheng Tang (Shanghai) Cosmetic R&D Co., Ltd. Moisturizing cosmetic composition
CN107354009A (en) * 2017-08-08 2017-11-17 湖北瑞晟生物有限责任公司 A kind of production method of hydrosol
CN108653190A (en) * 2018-07-09 2018-10-16 广州丽彦妆生物科技有限公司 A kind of multiple-effect of edible lysozyme repairs toner and preparation method thereof
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CN110731923B (en) * 2019-07-30 2022-08-02 浙江养生堂天然药物研究所有限公司 Enhanced moisturizing cosmetic compositions
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