CN107308057A - A kind of submissive nourishing hair and nontoxic soft hair cream and preparation method thereof - Google Patents
A kind of submissive nourishing hair and nontoxic soft hair cream and preparation method thereof Download PDFInfo
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- CN107308057A CN107308057A CN201710606828.5A CN201710606828A CN107308057A CN 107308057 A CN107308057 A CN 107308057A CN 201710606828 A CN201710606828 A CN 201710606828A CN 107308057 A CN107308057 A CN 107308057A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention provides a kind of submissive nourishing hair and nontoxic soft hair cream and preparation method thereof, contain house oil, olive oil, lanolin, isobutyl palmitate, saualane, olive emulsifying agent, general-purpose self-emulsifying mixed emulsifier AC 402, lemon extract, kelp extract, soapberry extract, honey, light-coloured vinegar, red wine, milk, 1% sodium hyaluronate solution, marine alga spirit, pyrrolidines ketone acid carboxylic acid sodium, cocamidopropyl betaine surfactant CAB, amino acid foaming agent ECS 22SB, height bubble powder, lauryl sodium sulfate, the double stearates 638 of Macrogol 6000, sodium alginate, sodium cellulose glycolate, essence, ethylparaben ethanol solution and sodium hydroxide solution.Compared with prior art, this soft hair cream property is gentle, and safe, the method combined using active material in natural plants with gentle surfactant, elimination hair is really up to the mark, and drying is withered and yellow, can moisten moisturizing, make the submissive show of hair bright.
Description
Technical field
The invention belongs to daily necessities field, and in particular to a kind of submissive nourishing hair and nontoxic soft hair cream and its preparation side
Method.
Background technology
Hair is made up of the keratoprotein cell of sulfur-bearing, middle to be connected by cystine linkages such as Cystines, makes hair flexible
And retractility.Hair can show the makings and self-image of people with flying colors, and the hair that we are intended to oneself is pitch-black bright
It is beautiful, it is generous moving, then spend more times, energy and money to be placed on hair washing, on hair care, safeguard that itself is finer with this
Image, shows oneself unique looks and makings.
Elasticity too sufficient hard hair, does moulding not persistently and flexible type, always recovers the apperance of its script quickly, and hair style is not yet
It can produce a desired effect.Close immanent structure can guarantee that hair is shaped for a long time, be a bit very important in hairdressing.Hair number
Why ten thousand radixin matter fibers can closely be gathered, and have benefited from the curing of countless lateral connections between adjacent protein fibre
Key.If hair for a long time with oxygen, UV contact, or hair-waving when, it is one not yet rinse well just use two doses, two can be caused
Sulfide linkage is gradually aoxidized and is broken, and loose symptom will be presented in the structure of hair.Protein, water, disulfide bond and melanin are groups
Into four key elements of hair, four contents number, the elastic, soft bright, close with pitch-black degree of hair is have impact on respectively.
We can solve this too hard problem of hair quality with soft hair cream.Softening is a kind of submissive technical term, for
A kind of beautification nursing means of harder hair quality.However, soft hair agent conventional at present is a kind of excitant very strong liquid medicine, easily damage
Hinder scalp, make hair scalp health problem more severe.
The content of the invention
In order to solve the above technical problems, it is an object of the invention to provide a kind of submissive nourishing hair and nontoxic soft hair
Cream, it is gentle salubrious using a variety of natural component extracts, improve scalp environment, anti-dry hair and hair tip jag promotes scalp
Metabolism, makes hair keep submissive for a long time.
Present invention also offers a kind of submissive preparation method for nourishing hair and nontoxic soft hair cream, composition of raw materials is coordinated to set
Meter, product property is stable.
A kind of submissive nourishing hair and nontoxic soft hair cream that the present invention is provided, contain following raw material components：
Volumes of aqueous ethanol fraction used in 2% ethylparaben ethanol solution is 75%.
The 3%NaOH solution refers to that NaOH solution mass concentration is 3%.
Described lemon extract is prepared by the following method：
Weigh lemon appropriate, 0.15-0.8h is soaked after incision, heating decocts extraction 3 times, the 1st time plus 10-15 times and measured
Water, extracts 1-2h, and the 2nd time plus 8-10 times measure water, extracts 0.5-1.5h, measures water the 3rd time plus 8-10 times, extracts 0.5-1.5h, often
Secondary filtration, merging filtrate, 3-6 times of g/mL of the volume concentration of filtrate to lemon weight, filtering is produced.
Described kelp extract is prepared by the following method：
Weigh Shredded kelp appropriate, heating water boils extraction 3 times, add 8-15 times to measure water for the first time and extract 1-2h, the 2nd time plus 8-10
Times amount water, extracts 1-1.5h, the 3rd time plus 8-10 times measure water, extract 0.5-1.5h, are filtered every time with double gauze, merging filtrate,
The volume concentration of filtrate is to 3-6 times of g/mL of Shredded kelp weight, and filtering produces.
Described soapberry extract is to be prepared by the following method：
Weigh soapberry appropriate, heating decocts extraction 3 times, the 1st time plus 8-15 times and measures 75% ethanol, extracts 0.5-2h, the 2nd
It is secondary plus 8-10 times measure 75% ethanol, extract 0.5-1.5h, measure 75% ethanol the 3rd time plus 8-10 times, extract 0.5-1.5h, every time filter
Cross, merging filtrate, filtrate is concentrated by evaporation to 3-6 times of g/mL of soapberry weight, is produced.
Described essence is Hami melon essence, milk flavour, peach flavor, flavoring rose essence, lemon extract, jasmine perfume
One kind in essence, osmanthus flower fragrance or green cucumber essence.
A kind of submissive preparation method for nourishing hair and nontoxic soft hair cream that the present invention is provided, comprises the following steps：
A) sodium alginate 0.1-2.0g is weighed, is added in 50-100mL distilled water, standing allows it to be fully swelled, sea is formed
Sodium alginate gel liquid, it is standby；
B) sodium carboxymethylcellulose 0.08-1.5g is weighed, is added in 50-100mL distilled water, 40-60 DEG C of heating water bath,
Heat while stirring, standing allows it to be fully swelled, form sodium carboxymethylcellulose lime set, it is standby；
C) the double 0.1-1.5g of stearate 638 of Macrogol 6000 are weighed, is added in 50-100mL distilled water, adds
3%NaOH solution 0.1-0.3mL adjusts its pH value for 7-8, with 60-80 DEG C of heating water bath, heats while stirring, and standing allows it to fill
Divide and be swelled, form the double coagulant liquids of stearate 638 of Macrogol 6000, it is standby；
D) lauryl sodium sulfate 0.1-1.5g, high bubble powder 0.1-1.5g, cocamidopropyl betaine surface are weighed
Activating agent CAB 1-5g, amino acid foaming agent ECS-22SB 1-5g and distilled water 10-50mL are mixed, and are placed in 60-90 DEG C of thermostatted water
Stirring and dissolving in bath, forms solution 1 after being completely dissolved, stand-by；
E) lemon extract 0.1-1.5mL, kelp extract 0.1-1.5mL, soapberry extract 0.1- are taken respectively
1.5mL, honey 0.1-1.5g, light-coloured vinegar 0.1-1.5mL, milk 0.1-1.5mL, red wine 0.1-1.5mL, marine alga spirit 0.1-1.5g,
Pyrrolidines ketone acid carboxylic acid sodium 0.1-1.5g and 1% sodium hyaluronate solution 0.1-3mL, stirs, and forms solution 2, stand-by；
F) house oil 0.5-3g, olive oil 0.5-3g, saualane 0.5-3.5g, lanolin 0.5-3.5g, palmitic acid are weighed different
Monooctyl ester 0.5-3.5g, olive emulsifying agent 1-7g and general-purpose self-emulsifying mixed emulsifier AC-4021-8g, are placed in 60-90 DEG C of water-bath
On, mix, it is stand-by as oil phase；
G) 10-35mL distilled water is measured, is placed in 60-90 DEG C of water-bath, it is stand-by as aqueous phase；
Etc. h) when oil phase reaches mutually synthermal with aqueous phase, aqueous phase is added in oil phase in thread shape, it is stirring while adding, until
Form the fine and smooth uniform emulsion bases of milky；
I) coagulated toward the double stearate coagulant liquids of addition solution 1, solution 2, Macrogol 6000, sodium alginate in emulsion bases
Glue, sodium carboxymethylcellulose lime set, 2% ethylparaben ethanol solution 0.5-3.5mL and essence 0.05-0.3mL, with stirring
Uniformly, submissive nourishing hair and nontoxic soft hair cream are produced.
The made soft hair cream of the present invention is creamy white, and viscosity is suitable, and foam is smooth abundant, and fine and smooth uniform, stretchability is good
Good, it is suitable to feel nice and cool, and stability is good, fragrant.
Various composition in the present invention is as follows：
Contain more citric acid, potassium element and a small amount of sodium element in lemon, can effectively control hair grease hypersecretion,
Soften scalp and decompose dandruff, help dandruff to come off, may also suppress the generation of bacterium, remove the peculiar smell of hair, reach cleaning scalp,
The effect of anti-dandruff and itching-relieving.Also contain substantial amounts of vitamin A in lemon juice, have functions that to nourish scalp, make the bright and clean softness of hair, it is sliding
Along it is glossy, rich in fragrance.
Contain more I in sea-tangle, this element is the primary raw material of internal synthetic thyroid element.And the light of hair
Pool is precisely due to the effect that thyroxine is played in vivo." hair quality " and contained cutin composition, be from the albumen of sulfur-bearing
Drawn in matter, and protein is the important substance for making hair produce gloss.In sea-tangle in addition to containing iodine, calcium, element sulphur, also
Contain iron, sodium, magnesium, potassium, cobalt, phosphorus, mannitol and vitamin B1、B2, a variety of nutriments such as C.These nutrients are all big to hairdressing
There is benifit.Therefore, in the present invention, using sea-tangle to the growing of hair, moisten, pitch-black, submissive all there is special effect.
Tartaric acid in soapberry can help skin removed to be deposited in the aging cutin of outer layer, accelerate skin renewal, be used for
Hair washing also can pre- anti-dandruff, have functions that anti-dandruff and itching-relieving, its foaming abundancy, feel is fine and smooth, strong detergency.Soapberry also contains
The a variety of natural nutritions such as amino acid, vitamin conditioning materials, with antibacterial, anti-inflammatory, it is antipruritic the effects such as, and to skin irritatin
It is small, it is safe and reliable.Its also anti-oxidant, removing is freely acted on by base, anticoagulation etc. simultaneously.Its adding in soft hair cream formula
Enter, reduce the use of traditional chemical surfactant, reduce the excitant of chemical surfactant, and can reduce by this class
Potential risks material dioxanes is brought into surfactant, improves the security of soft hair cream.Simultaneously to common soft hair cream
It is significantly increased using the dry comb of rear hair, flexibility, glossiness.
Saualane can suppress the peroxide of lipid as the avirulent marine biomaterial with effect of preventing and curing diseases
Change, be that rare chemical stability is high, the splendid animal fat of use feeling will not cause allergy and stimulation, and can accelerate formula
Middle other active components absorb and permeated, and may also suppress fungus growth, promote microcirculation, form natural diaphragm, assign hair
Fabulous brightness and combing is felt, moistens and non-greasy.
Pyrrolidines ketone acid carboxylic acid sodium is a kind of natural moisture preserving agent, from Pidolidone, can comfortably be moistened to hair carry
Sense.Pyrrolidines ketone acid carboxylic acid sodium also has excellent hygroscopicity, and increase hair is soft while giving hair comfort and moisture feeling
Property and elasticity, help to delay hair aging.
Olive oil is rich in squalene and essential fatty acid, there is beautifying face and moistering lotion.Abundant list contained by it is not
Saturated fatty acid liposoluble vitamin and phenols polyphenoils, it is short-tempered to solve hair, the problems such as color development is obscure, moreover it is possible to hair
Scale supplements the nutrients, and healthy hair is discharged attractive luster again.Also contain vitamin B and E in other olive oil, can pre- anticreep
The appearance of hair, fuel-displaced, dandruff etc., anti-dry hair and hair slightly jag.Olive oil is salubrious oiliness after using, it is easy to absorbs, is one
Plant pure natural safe and reliable cosmetic good merchantable brand.
Marine alga spirit is a kind of high-quality NMF, energy moisture-keeping crease-shedding, while can enhance metabolism, prevents skin senescence, thorn
Swash fibrocyte and manufacture more colloids, elasticin matter and mucopolysaccharide etc., promote epidermal growth, make skin smoother and
It is young.There are promotion scalp metabolism, pre- anti-aging effect simultaneously.
House oil has the effect of nutrient to hair, and the hair after coming to one's autumn and perming easily divides because of nutrient loss
Fork, fracture.The nutrient (vitamin E and leukotrienes) contained in house oil, if being directly applied on scalp, fully massage just can ooze
Enter hair quality layer, hair more thick healthy can be made.
Sodium alginate risen in hair shampoo article it is good thicken, antistatic and barbotage.Shampoo paste sense of touch is soft after addition
It is sliding, and can prevent the viscosity during effect product sterilization from declining phenomenon.Sodium alginate also has film forming, can effectively protect
Hair is injury-free, pins the moisture of hair, the brilliance for making hair radiate the vigour of youth.Further, it is also possible to improve the moisture retention of hair,
Hair is set to keep submissive for a long time.
There is methyl hydroxybenzoate efficient sterilization and anticorrosion to act on, and emulsion can be prevented putrid and deteriorated, improve emulsion quality.
The soft hair cream that the present invention is provided with the addition of some extracted form natural plant compositions, and this is one kind U.S. for harder hair quality
Hair nursing, can make hair soften, and become submissive, become docile.Each active ingredient complements each other, synergy：Lemonade can be very well
Cleaning-nursing scalp and hair, and quality be gently difficult injure skin.The various trace elements contained in sea-tangle can make head
Hair is moist, pitch-black light；Tartaric acid in soapberry can be with anti-dandruff and itching-relieving, while there is anti-inflammation；Moreover, passing through increase
Thickener, NMF are further nursed and improved to hair；Such as pyrrolidone sodium carboxylate, olive oil, house oil, marine alga spirit
Etc. can effectively anti-alopecia-stopping, it is fuel-displaced, dry and hair the tip bifurcated the problems such as appearance, improve hair moisture retention, make hair long-term
Keep submissive.In these natural extracts and NMF of addition, hair care ingredients are nourished and a variety of important micro containing a large amount of
Element, while effective cleaning, nursing, can promote hair metabolism, pre- anti-aging, while having nutrient work
With making hair more thick healthy.In preparation process, adjusted using sodium hydroxide after pH, heating water bath, moreover, preparing marine alga
During double 638 coagulant liquids of stearate of sour sodium gel liquid, sodium carboxymethylcellulose lime set and Macrogol 6000, using water-bath plus
Heat so that soft hair cream denseness is suitable is fine and smooth uniform.
Compared with prior art, lemon extract and kelp extract in the present invention, quality are gentle, are difficult to injure skin,
To keeping healthy growth, the hair quality of hair are submissive, color and luster is shiny black there is special effect.Soapberry can improve scalp environment, in advance
Anti-dandruff, accelerates skin renewal, makes it fine and smooth salubrious, rich in gloss.This soft hair cream can be by changing the chain link in hair
Tissue, is then rearranged, and reaches the effect of softening hair.The natural moisture preserving agent added in the soft hair cream can strengthen hair
Moisture-retaining capacity, anti-dry hair and hair tip jag promotes scalp metabolism, can supplement nutrition needed for hair scalp, moisture,
Healthy hair is moistened gloss, improve hair and dry up the phenomenon of short-tempered alopecia.Improve scalp blood circulation simultaneously, enhance metabolism,
Gentle nutrition, finally makes hair shiny black submissive.
Embodiment
With reference to embodiment, the present invention will be further described.
Embodiment 1
A kind of submissive nourishing hair and nontoxic soft hair cream, contain following raw material components：
Volumes of aqueous ethanol fraction used in 2% ethylparaben ethanol solution is 75%.
The preparation of 1.1 lemon extracts
Weigh and 0.15h soaked after lemon 50g, incision, heating, which is decocted, extracts 3 times, the 1st time plus 10 times amount water, extracts 1h,
2nd time plus 8 times amount water, extracts 0.5h, and the 3rd time plus 8 times amount water extracts 0.5h, every time filtration, merging filtrate, the volume of filtrate
3 times of g/mL of lemon weight are concentrated into, filtering is produced.
The preparation of 1.2 kelp extracts
Weigh Shredded kelp 100g, heating water boils extraction 3 times, for the first time plus 8 times of amount water extract 1h, the 2nd time plus 8 times amount water,
1h is extracted, the 3rd time plus 8 times amount water extract 0.5h, filtered every time with double gauze, merging filtrate, the volume concentration of filtrate to sea
3 times of g/mL with silk weight, filtering is produced.
The preparation of 1.3 soapberry extracts
Soapberry 200g is weighed, heating, which is decocted, extracts 3 times, the 1st time plus 8 times 75% ethanol of amount, extracts 1h, the 2nd time plus 8 times
75% ethanol is measured, 1h is extracted, the 3rd time plus 8 times 75% ethanol of amount extracts 0.5h, every time filtration, merging filtrate, filtrate is rotated
Evaporimeter is concentrated into 3 times of g/mL of soapberry weight, produces.
The preparation method of 1.4 soft hair cream：
A) sodium alginate 0.1g is weighed, is added in the beaker equipped with 50mL distilled water, standing allows it to be fully swelled 12h,
Sodium alginate gel liquid is formed, it is standby；
B) sodium carboxymethylcellulose 0.08g is weighed, is added in the beaker equipped with 50mL distilled water, 40 DEG C of heating water baths,
Heat while stirring, standing allows it to be fully swelled, form sodium carboxymethylcellulose lime set, it is standby；
C) the double 0.1g of stearate 638 of Macrogol 6000 are weighed, are added in the beaker equipped with 50mL distilled water, plus
It is 7.1 to enter 3%NaOH solution 0.1mL to adjust its pH value, with 60 DEG C of heating water baths, is heated while stirring, standing makes it fully molten
It is swollen, the double stearate coagulant liquids of Macrogol 6000 are formed, it is standby；
D) lauryl sodium sulfate 0.1g, high bubble powder 0.1g, cocamidopropyl betaine surfactant CAB are weighed
1g, amino acid foaming agent ECS-22SB 1g, distilled water 10mL are placed in stirring and dissolving in 60 DEG C of thermostat water baths in beaker 1,
Solution 1 is formed after being completely dissolved, it is stand-by；
E) take lemon extract 0.1mL respectively, it is kelp extract 0.1mL, soapberry extract 0.1mL, honey 0.1g, white
Vinegar 0.1mL, milk 0.1mL, red wine 0.1mL, marine alga spirit 0.1g, pyrrolidines ketone acid carboxylic acid sodium 0.1g and 1% Sodium Hyaluronate are molten
Liquid 0.1mL, stirs, and forms solution 2, stand-by；
F) house oil 0.5g, olive oil 0.5g, saualane 0.5g, lanolin 0.5g, isobutyl palmitate 0.5g, olive are weighed
Emulsifying agent 1g, general-purpose self-emulsifying mixed emulsifier AC-402 1g, it is placed in 60 DEG C of water-baths, it is stand-by as oil phase；
G) 10mL distilled water is measured, is placed in 60 DEG C of water-baths, it is stand-by as aqueous phase；
Etc. h) when oil phase reaches mutually synthermal with aqueous phase, aqueous phase is added in oil phase in thread shape, it is stirring while adding, until
Form the fine and smooth uniform emulsion bases of milky；
I) coagulated toward the double stearate coagulant liquids of addition solution 1, solution 2, Macrogol 6000, sodium alginate in emulsion bases
Glue, sodium carboxymethylcellulose lime set, the ethanol solution 0.5mL of 2% ethylparaben 75%, flavoring rose essence 0.05mL, use glass
Rod, which stirs, produces submissive nourishing hair and nontoxic soft hair cream.
Embodiment 2
A kind of submissive nourishing hair and nontoxic soft hair cream, contain following raw material components：
Volumes of aqueous ethanol fraction used in 2% ethylparaben ethanol solution is 75%.
The preparation of 2.1 lemon extracts
Weigh and 0.4h is soaked after lemon 100g, incision, heating, which is decocted, extracts 3 times, the 1st time plus 12 times amount water, extracts
1.5h, the 2nd time plus 9 times amount water extracts 1h, and the 3rd time plus 9 times amount water extracts 1h, every time filtration, merging filtrate, the volume of filtrate
4 times of g/mL of lemon weight are concentrated into, filtering is produced.
The preparation of 2.2 kelp extracts
Shredded kelp 150g is weighed, heating water boils extraction 3 times, add 12 times of amount water to extract 1.5h, the 2nd time plus 9 times amount for the first time
Water, extracts 1.2h, and the 3rd time plus 9 times amount water extracts 1h, filtered every time with double gauze, merging filtrate, the volume concentration of filtrate
To 4 times of g/mL of Shredded kelp weight, filtering is produced.
The preparation of 2.3 soapberry extracts
Weigh soapberry 200g, heating, which is decocted, extracts 3 times, the 1st time plus 12 times 75% ethanol of amount, extracts 1h, Jia 9 the 2nd time
75% ethanol of amount, extracts 1h again, and the 3rd time plus 9 times 75% ethanol of amount, extraction 1h, filtration every time, merging filtrate, filtrate is rotated
Evaporimeter is concentrated into 4 times of g/mL of soapberry weight, produces.
The preparation of 2.4 soft hair cream
A) sodium alginate 0.8g is weighed, is added in the beaker equipped with 80mL distilled water, standing allows it to be fully swelled 12h,
Sodium alginate gel liquid is formed, it is standby；
B) sodium carboxymethylcellulose 0.8g is weighed, is added in the beaker equipped with 80mL distilled water, 50 DEG C of heating water baths, side
Side stirring is heated, standing allows it to be fully swelled, form sodium carboxymethylcellulose lime set, it is standby；
C) the double 0.8g of stearate 638 of Macrogol 6000 are weighed, are added in the beaker equipped with 80mL distilled water, plus
It is 7.2 to enter 3%NaOH solution 0.2mL to adjust its pH value, with 70 DEG C of heating water baths, is heated while stirring, standing makes it fully molten
It is swollen, the double stearate coagulant liquids of Macrogol 6000 are formed, it is standby；
D) lauryl sodium sulfate 0.8g, high bubble powder 0.8g, cocamidopropyl betaine surfactant CAB are weighed
2g, amino acid foaming agent ECS-22SB 2g, distilled water 20mL are placed in stirring and dissolving in 70 DEG C of thermostat water baths in beaker 1,
Solution 1 is formed after being completely dissolved, it is stand-by；
E) take lemon extract 0.8mL respectively, it is kelp extract 0.8mL, soapberry extract 0.8mL, honey 0.8g, white
Vinegar 0.8mL, milk 0.8mL, red wine 0.8mL, marine alga spirit 0.8g, pyrrolidines ketone acid carboxylic acid sodium 0.8g, 1% sodium hyaluronate solution
1mL, stirs, and forms solution 2, stand-by；
F) weigh house oil 1g, olive oil 1g, saualane 1g, lanolin 1g, isobutyl palmitate 1g, olive emulsifying agent 3g,
General-purpose self-emulsifying mixed emulsifier AC-402 3g, are placed in 70 DEG C of water-baths, stand-by as oil phase；
G) 25mL distilled water is measured, is placed in 70 DEG C of water-baths, it is stand-by as aqueous phase；
Etc. h) when oil phase reaches mutually synthermal with aqueous phase, aqueous phase is added in oil phase in thread shape, it is stirring while adding, until
Form the fine and smooth uniform emulsion bases of milky；
I) coagulated toward the double stearate coagulant liquids of addition solution 1, solution 2, Macrogol 6000, sodium alginate in emulsion bases
Glue, sodium carboxymethylcellulose lime set, the ethanol solution 1.5mL of 2% ethylparaben 75%, green cucumber essence 0.15mL, use glass
Rod, which stirs, produces submissive nourishing hair and nontoxic soft hair cream.
Embodiment 3
A kind of submissive nourishing hair and nontoxic soft hair cream, contain following raw material components：
Volumes of aqueous ethanol fraction used in 2% ethylparaben ethanol solution is 75%.
The preparation of 3.1 lemon extracts
Weigh and 0.8h soaked after lemon 90g, incision, heating, which is decocted, extracts 3 times, the 1st time plus 15 times amount water, extracts 2h,
2nd time plus 10 times amount water, extracts 1.5h, and the 3rd time plus 10 times amount water extracts 1.5h, every time filtration, merging filtrate, the body of filtrate
Product is concentrated into 6 times of g/mL of lemon weight, and filtering is produced.
The preparation of 3.2 kelp extracts
Weigh Shredded kelp 90g, heating water boils extraction 3 times, for the first time plus 15 times of amount water extract 2h, the 2nd time plus 10 times amount water,
1.5h is extracted, the 3rd time plus 10 times amount water extracts 1.5h, filtered every time with double gauze, merging filtrate, the volume concentration of filtrate
To 6 times of g/mL of Shredded kelp weight, filtering is produced.
The preparation of 3.3 soapberry extracts
Weigh soapberry 80g, heating, which is decocted, extracts 3 times, the 1st time plus 15 times 75% ethanol of amount, extracts 2h, Jia 10 the 2nd time
75% ethanol of amount, extracts 1.5h, the 3rd time plus 10 times 75% ethanol of amount, extraction 1.5h, every time filtration, merging filtrate, filtrate warp again
Rotary Evaporators are concentrated into 6 times of g/mL of soapberry weight, produce.
The preparation of 3.4 soft hair cream
A) sodium alginate 2.0g is weighed, is added in the beaker equipped with 100mL distilled water, standing allows it to be fully swelled 12h,
Sodium alginate gel liquid is formed, it is standby；
B) sodium carboxymethylcellulose 1.5g is weighed, is added in the beaker equipped with 100mL distilled water, 60 DEG C of heating water baths,
Heat while stirring, standing allows it to be fully swelled, form sodium carboxymethylcellulose lime set, it is standby；
C) the double 1.5g of stearate 638 of Macrogol 6000 are weighed, are added in the beaker equipped with 100mL distilled water, plus
It is 77.3 to enter 3%NaOH solution 0.3mL to adjust its pH value, with 80 DEG C of heating water baths, is heated while stirring, standing makes it fully molten
It is swollen, the double stearate coagulant liquids of Macrogol 6000 are formed, it is standby；
D) lauryl sodium sulfate 1.5g, high bubble powder 1.5g, cocamidopropyl betaine surfactant CAB are weighed
5g, amino acid foaming agent ECS-22SB 5g, distilled water 50mL are placed in stirring and dissolving in 90 DEG C of thermostat water baths in beaker 1,
Solution 1 is formed after being completely dissolved, it is stand-by；
E) take lemon extract 1.5mL respectively, it is kelp extract 1.5mL, soapberry extract 1.5mL, honey 1.5g, white
Vinegar 1.5mL, milk 1.5mL, red wine 1.5mL, marine alga spirit 1.5g, pyrrolidines ketone acid carboxylic acid sodium 1.5g, 1% sodium hyaluronate solution
3mL, stirs, and forms solution 2, stand-by；
F) house oil 3g, olive oil 3g, saualane 3.5g, lanolin 3.5g, isobutyl palmitate 3.5g, olive emulsification are weighed
Agent 7g, general-purpose self-emulsifying mixed emulsifier AC-402 8g, are placed in 90 DEG C of water-baths, stand-by as oil phase；
G) 35mL distilled water is measured, is placed in 90 DEG C of water-baths, it is stand-by as aqueous phase；
Etc. h) when oil phase reaches mutually synthermal with aqueous phase, aqueous phase is added in oil phase in thread shape, it is stirring while adding, until
Form the fine and smooth uniform emulsion bases of milky；
I) coagulated toward the double stearate coagulant liquids of addition solution 1, solution 2, Macrogol 6000, sodium alginate in emulsion bases
Glue, sodium carboxymethylcellulose lime set, the ethanol solution 3.5mL of 2% ethylparaben 75%, milk flavour 0.3mL, use glass bar
Stir and produce submissive nourishing hair and nontoxic soft hair cream.
Embodiment 4
The physical and chemical index of embodiment 1,2,3 is as follows：
4.1 character
This product is that viscosity is suitable, and foam is smooth abundant, fine and smooth uniform, the soft hair cream of the good milky of stretchability.
4.2 pH value inspections
A small amount of soft hair cream is dipped with the pH test paper of wetting, pH is 6-7.
4.3 caloric test
Soft hair cream is packaged in transparence cosmetic bottle, in 4 DEG C of refrigerator cold-storage observations in one week or so without lamination.In
24h in 55 DEG C of insulating box, soap lye emulsifies the phenomenon such as spoiled without layering.
4.4 centrifugal test
Soft hair cream is packaged in 3000r/min in tool plug test tube and centrifuges 20min, no lamination.
4.5 irritation tests, anaphylaxis experiment
Small white mouse back cuts off hair, the soft hair cream prepared by embodiment 1,2,3 is smeared respectively in cutting plucked position, and do not have
Apply position to be compared, as a result without excitant and allergic reaction.
Take 1 gram in kind to be applied in volunteer (20-60 Sui, 80 people) gesture and facial expression, observation after spending 30 minutes, do not occur it is rubescent,
Dermexanthesis, foaming phenomena.
4.6 room temperatures place experiment
The made soft hair cream of embodiment 1,2,3 is placed in emulsifiable paste bottle, investigation 6 months is stored at room temperature, no lamination is used
After feel unchanged, smell is unchanged.
4.7 soft hair effects
Volunteer's (20-60 Sui, 80 people) is chosen, obtained soft hair cream is used for volunteer's hair, it is mixed with a small amount of water
Merging is washed by rubbing with the hands repeatedly, finds foaming abundancy, and volunteers generally feel smooth comfortable, and feel is preferable.The no matter dry comb of hair or
Wet comb property is all good.After being eluted with water, hair submissive such as silk, fluffy non-greasy, moistening effect preferably, are washed rear hair and clearly relaxed
It is suitable, it is smooth submissive, and without sense of discomfort, no allergic reaction.Through one month continuously use, hair was substantially glossy, soft, hair
Matter phenomenon really up to the mark is significantly reduced.
Embodiment 5
The soft hair cream resultant effect is investigated
Feel to evaluate the effect for the soft hair cream that embodiment 1,2,3 is produced following with probation.Commented using opinion poll
Point-score, chooses the women of 90 20-60 Sui age brackets as object on probation, three groups is arbitrarily divided into, respectively with embodiment 1,2,3
The soft hair cream wash my hair prepared.Weekly using twice, use time is two months.Every using effect total score is 5 points：5 points are
Best result, represents fine, very satisfied；4 points are preferable；3 points are to receive；Less than 3 points are bad, it is impossible to received.Below
For every average.It the results are shown in Table 1：
The resultant effect of table 1 is investigated
In summary, made soft hair cream foaming abundancy of the present invention, has good compliance, moisture retention, alimentary, wet
Comb property, feels salubrious comfortable when using, good with rear hair elasticity, has submissive, moisturizing, nourishes the effect of profit hair.
Claims (6)
1. a kind of submissive nourishing hair and nontoxic soft hair cream, it is characterised in that the submissive nourishing hair and nontoxic soft hair
Cream contains following raw material components：
2. submissive nourishing hair according to claim 1 and nontoxic soft hair cream, it is characterised in that described lemon is extracted
Liquid is prepared by the following method：
Weigh lemon appropriate, 0.15-0.8h is soaked after incision, heating decocts extraction 3 times, the 1st time plus 10-15 times and measures water, carries
Take 1-2h, measure water the 2nd time plus 8-10 times, extract 0.5-1.5h, measure water the 3rd time plus 8-10 times, extract 0.5-1.5h, every time filter
Cross, merging filtrate, 3-6 times of g/mL of the volume concentration of filtrate to lemon weight, filtering is produced.
3. submissive nourishing hair according to claim 1 or 2 and nontoxic soft hair cream, it is characterised in that described sea-tangle
Extract solution is prepared by the following method：
Weigh Shredded kelp appropriate, heating water boils extraction 3 times, for the first time plus 8-15 times is measured water and extract 1-2h, measure for the 2nd time plus 8-10 times
Water, extracts 1-1.5h, and the 3rd time plus 8-10 times measure water, extract 0.5-1.5h, are filtered every time with double gauze, merging filtrate, filtrate
Volume concentration to 3-6 times of g/mL of Shredded kelp weight, filtering produces.
4. submissive nourishing hair and nontoxic soft hair cream according to claim any one of 1-3, it is characterised in that described
Soapberry extract is to be prepared by the following method：
Weigh soapberry appropriate, heating, which is decocted, extracts 3 times, the 1st time plus 8-15 times and measure 75% ethanol, extract 0.5-2h, the 2nd time plus
8-10 times is measured 75% ethanol, extracts 0.5-1.5h, measures 75% ethanol the 3rd time plus 8-10 times, extracts 0.5-1.5h, every time filtration,
Merging filtrate, filtrate is concentrated by evaporation to 3-6 times of g/mL of soapberry weight, is produced.
5. submissive nourishing hair and nontoxic soft hair cream according to claim any one of 1-3, it is characterised in that described
Essence is Hami melon essence, milk flavour, peach flavor, flavoring rose essence, lemon extract, cream jasmin france, osmanthus flower fragrance or green grass or young crops
One kind in melon essence.
6. the preparation method of a kind of submissive nourishing hair described in any one of claim 1-5 and nontoxic soft hair cream, its feature
It is, the preparation method comprises the following steps：
A) sodium alginate 0.1-2.0g is weighed, is added in 50-100mL distilled water, standing allows it to be fully swelled, alginic acid is formed
Sodium gel liquid, it is standby；
B) sodium carboxymethylcellulose 0.08-1.5g is weighed, is added in 50-100mL distilled water, 40-60 DEG C of heating water bath, Bian Jia
Hot side stirring, standing allows it to be fully swelled, and forms sodium carboxymethylcellulose lime set, standby；
C) the double 0.1-1.5g of stearate 638 of Macrogol 6000 are weighed, is added in 50-100mL distilled water, adds 3%
NaOH solution 0.1-0.3mL adjusts its pH value for 7-8, with 60-80 DEG C of heating water bath, heats while stirring, and standing makes its abundant
It is swelled, forms the double coagulant liquids of stearate 638 of Macrogol 6000, it is standby；
D) lauryl sodium sulfate 0.1-1.5g, high bubble powder 0.1-1.5g, cocamidopropyl betaine surface-active are weighed
Agent CAB 1-5g, amino acid foaming agent ECS-22SB 1-5g and distilled water 10-50mL are mixed, and are placed in 60-90 DEG C of thermostat water bath
Middle stirring and dissolving, forms solution 1 after being completely dissolved, stand-by；
E) lemon extract 0.1-1.5mL, kelp extract 0.1-1.5mL, soapberry extract 0.1-1.5mL, honeybee are taken respectively
Sweet 0.1-1.5g, light-coloured vinegar 0.1-1.5mL, milk 0.1-1.5mL, red wine 0.1-1.5mL, marine alga spirit 0.1-1.5g, pyrrolidones
Sour carboxylic acid sodium 0.1-1.5g and 1% sodium hyaluronate solution 0.1-3mL, stirs, and forms solution 2, stand-by；
F) house oil 0.5-3g, olive oil 0.5-3g, saualane 0.5-3.5g, lanolin 0.5-3.5g, isobutyl palmitate are weighed
0.5-3.5g, olive emulsifying agent 1-7g and general-purpose self-emulsifying mixed emulsifier AC-4021-8g, are placed in 60-90 DEG C of water-bath,
Mix, it is stand-by as oil phase；
G) 10-35mL distilled water is measured, is placed in 60-90 DEG C of water-bath, it is stand-by as aqueous phase；
Etc. h) when oil phase reaches mutually synthermal with aqueous phase, aqueous phase is added in oil phase in thread shape, it is stirring while adding, until being formed
The fine and smooth uniform emulsion bases of milky；
I) toward the double stearate coagulant liquids of addition solution 1, solution 2, Macrogol 6000, sodium alginate gel in emulsion bases
Liquid, sodium carboxymethylcellulose lime set, 2% ethylparaben ethanol solution 0.5-3.5mL and essence 0.05-0.3mL, it is equal with stirring
It is even, produce submissive nourishing hair and nontoxic soft hair cream.
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| CN110664674A (en) * | 2019-08-15 | 2020-01-10 | 广州欧盛化妆品有限公司 | Beard care oil |
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| CN115569076A (en) * | 2022-09-26 | 2023-01-06 | 华东理工大学 | Liquid crystal hair mask and preparation method thereof |
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| CN115569076A (en) * | 2022-09-26 | 2023-01-06 | 华东理工大学 | Liquid crystal hair mask and preparation method thereof |
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