CN107737039A - Containing ginger without silicone oil without sulfate health-care shampoo and its preparation technology - Google Patents

Containing ginger without silicone oil without sulfate health-care shampoo and its preparation technology Download PDF

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CN107737039A
CN107737039A CN201711126848.9A CN201711126848A CN107737039A CN 107737039 A CN107737039 A CN 107737039A CN 201711126848 A CN201711126848 A CN 201711126848A CN 107737039 A CN107737039 A CN 107737039A
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extract
ethanol
shampoo
immersion liquid
ginger
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赵锴
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Guangzhou Peerless Enterprise Group Co Ltd
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Guangzhou Peerless Enterprise Group Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/006Antidandruff preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/008Preparations for oily hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q7/00Preparations for affecting hair growth
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/30Characterized by the absence of a particular group of ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/30Characterized by the absence of a particular group of ingredients
    • A61K2800/34Free of silicones
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/82Preparation or application process involves sonication or ultrasonication

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
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  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
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  • Cosmetics (AREA)

Abstract

Present invention offer is a kind of to be made up of without silicone oil containing ginger without sulfate health-care shampoo and its preparation technology, shampoo 64%~68% shampoo base, 18%~22% ginger-root extract, 2%~4% ginseng root extract, 2%~4% radix-polygoni multiflori extract, 2%~4% purslane extract and 4%~6% Flos Chrysanthemi Indici extract.The Chinese herbal medicine extract contained in shampoo of the present invention, the metabolism of scalp can not only be improved, promote scalp blood circulation, and the effect of being regenerated with promoting blood circulation and removing blood stasis, rich in nutrition, hair follicle stimulating and reaching anti-alopecia-stopping and growing and blacking hair, to seborrhea, dandruff is excessive, and itching of the scalp has certain curative effect, can prevent the scalp allergic phenomena occurred during hair washing, hair-washing hair-care has good oil-control effect, makes hair is more compliant lubricate, be glossy;And ginger and chrysanthemum indicum are thinning with the use of can effectively solve the problems, such as that plant shampoo water becomes sour, it is ensured that shampoo stable system.

Description

Containing ginger without silicone oil without sulfate health-care shampoo and its preparation technology
Technical field
The invention belongs to hair shampoo article technical field, and in particular to be it is a kind of containing ginger without silicone oil without sulfate health care Shampoo and its preparation technology.
Background technology
In the current era of fast development, the work of people and rhythm of life are more and more faster, due to operating pressure, sleep not Good, inherent cause adds the influence of natural environment, it may appear that exiguous human hair, head are itched vigorous dandruff, grease, scalp allergy, hair Phenomena such as withered coarse.Shampoo is the indispensable commodity in people's life, how to possess bright, submissive, high resilience, is easy to The healthy hair combed, turns into standard of perfection of the people to shampoo quality requirement.With the improvement of living standards, keep all over the face Pitch-black dense hair is the common aspiration of people.Consumer also improves constantly to the quality requirements of shampoo, containing silicone oil and The shampoo of dioxane (sulfate surfactant impurities) can not again meet consumer demand, and shampoo will be towards Amino acid surfactant, hair care are taken care of hair, developed without directions such as silicone oil scalp care, medicinal herb componentses nursing, and shampoo is not only There is the effect such as cleaning, smooth, hair care, but also to have and promote natural on-off cycles of hair growth development, relieving itching and removing dandruff, oil-control strengthen the hair, prevent scalp The features such as allergy.At present, the shampoo of the various functions of market sale, typically chemical substance are blended to prepare production, Clean effect is notable, but the side effect of chemical substance is easily caused hair nutrition loss, and hair quality is damaged, and hair becomes increasingly hair It is rough, withered, or even alopecia.So study the shampoo of multiple functions highly significant using the effect of China's Chinese herbal medicine.
Addition of the Chinese herbal medicine extract in daily chemical products can significantly improve the quality and effect performance of product, but Chinese herbal medicine Complicated component, there is very big test to the viscosity of product, acid-base property, corruptibility, color, therefore, it is necessary to study it is a in Without silicone oil without sulfate shampoo the shampoo of chemical composition (be different from be entirely), shampoo will not only have good steady herbal medicine It is qualitative, not thinning discoloration corruption, and have good Chinese herbal medicine hair care hair care, the effect of nursing scalp.
The content of the invention
It is an object of the invention to provide it is a kind of containing ginger without silicone oil without sulfate health-care shampoo, can not only prevent from containing Ginger it is thinning spoiled without sulfate health-care shampoo without silicone oil, and medicinal herb componentses therein can promote natural on-off cycles of hair growth to develop, With relieving itching and removing dandruff, oil-control strengthen the hair, the function of preventing scalp allergy, also there is good hair care hair care, nursing scalp.
It is a further object to provide above-mentioned preparation technology of the no silicone oil without sulfate health-care shampoo.
The technical solution adopted in the present invention is,
By mass percentage, it is made up of containing ginger without silicone oil without sulfate health-care shampoo following component:64%~ 68% shampoo base, 18%~22% ginger-root extract, 2%~4% ginseng root extract, 2%~4% what head Black extract, 2%~4% purslane extract, 4%~6% Flos Chrysanthemi Indici extract, the mass percent of above each component Summation is 100%.
Wherein, shampoo base by mass percentage, is made up of following component:58%~63% Hamposyl L Sodium, 12%~16% Cocoamidopropyl betaine, 13%~17% LAA, 1.5%~4.5% Plant amino acid class, 1%~2% hydrogenating glycerol of polyethylene glycol -200 palm acid ester, 0.1%~1.5% glycerine moon Cinnamic acid ester, 0.1%~1.5% certain herbaceous plants with big flowers of polyglycereol -3 acid esters, 0.1%~1.5% PPG-3 myristic acids ether, 0.1%~ 1.3% palmitamide hydroxypropyltrimonium chloride, 0.4%~1.5% citric acid, 0.1%~0.3% EDTA-2Na, 1%~1.5% preservative, 0.3%~0.7% essential oil, the mass percent summation of above each component is 100%.
Preferred scheme is, containing ginger without silicone oil without sulfate health-care shampoo, by mass percentage, by following component group Into:66% shampoo base, 20% ginger-root extract, 3% ginseng root extract, 3% radix-polygoni multiflori extract, 3% Purslane extract, 5% Flos Chrysanthemi Indici extract;
Wherein, shampoo base by mass percentage, is made up of following component:60.60% sodium lauroyl sarcosine, 13.65% Cocoamidopropyl betaine, 15.15% LAA, 3.05% plant amino acid class, 1.50% hydrogenating glycerol of polyethylene glycol -200 palm acid ester, 0.75% glycerol monolaurate, 0.75% polyglycereol -3 Certain herbaceous plants with big flowers acid esters, 0.75% PPG-3 myristic acids ether, 0.70% palmitamide hydroxypropyltrimonium chloride, 1.05% lemon Acid, 0.15% EDTA-2Na, 1.30% preservative, 0.60% essential oil.
Preservative is Phenoxyethanol and methylisothiazolinone, and the mass ratio of Phenoxyethanol and methylisothiazolinone is 16:1.
Essential oil is Rosa Damascana, ginger essential oil, orchid essential oil, sun flower essential oil or lotus flower essential oil.
The composition of plant amino acid class has:Hydrolyzed vegetable protein, polylysine, Phenoxyethanol and water.
It is above-mentioned as follows without preparation technology of the silicone oil without sulfate health-care shampoo, its concrete operation step containing ginger:
Step 1,
1.1 take fresh race, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the race of crushing Immersion liquid, the race of crushing is immersed in 9~11 hours in immersion liquid, in immersion process, the temperature of immersion liquid 20 DEG C~30 DEG C are maintained always;The immersion liquid is the mixed liquor of deionized water and ethanol, and the mass percent of ethanol is dense Spend for 98%, the volume ratio of deionized water and 98% ethanol is 40:60;Followed by the mixture of race and soak is put Ultrasonic extraction 1.5~2.5 hours is carried out in ultrasonic extractor, the pressure of setting is normal pressure, and temperature is 60~80 DEG C, ultrasound Frequency is 200~400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains race extract;Race extract is passed through again Centrifugal filtration, filtrate recycling ethanol is collected, the filtrate finally given is officinale root extract;
1.2 take fresh ginseng, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the ginseng of crushing Immersion liquid, the ginseng of crushing is immersed in 9~11 hours in immersion liquid, in immersion process, the temperature of immersion liquid 20 DEG C~30 DEG C are maintained always;The immersion liquid is the mixed liquor of deionized water and ethanol, and the mass percent of ethanol is dense Spend for 98%, the volume ratio of deionized water and 98% ethanol is 40:60;Followed by the mixture of ginseng and soak is put Ultrasonic extraction 1.5~2.5 hours is carried out in ultrasonic extractor, the pressure of setting is normal pressure, and temperature is 60~80 DEG C, ultrasound Frequency is 200~400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains ginseng extract;Ginseng extract is passed through again Centrifugal filtration, filtrate recycling ethanol is collected, the filtrate finally given is ginseng root extract;
1.3 take the fresh fleece-flower root, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the fleece-flower root of crushing Immersion liquid, the fleece-flower root of crushing is immersed in 9~11 hours in immersion liquid, in immersion process, the temperature of immersion liquid 20 DEG C~30 DEG C are maintained always;The immersion liquid is the mixed liquor of deionized water and ethanol, and the mass percent of ethanol is dense Spend for 98%, the volume ratio of deionized water and 98% ethanol is 40:60;Followed by the mixture of the fleece-flower root and soak is put Ultrasonic extraction 1.5~2.5 hours is carried out in ultrasonic extractor, the pressure of setting is normal pressure, and temperature is 60~80 DEG C, ultrasound Frequency is 200~400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains fleece-flower root extract;Fleece-flower root extract is passed through again Centrifugal filtration, filtrate recycling ethanol is collected, the filtrate finally given is radix-polygoni multiflori extract;
1.4 take fresh purslane, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the purslane of crushing Immersion liquid, the purslane of crushing is immersed in 9~11 hours in immersion liquid, in immersion process, the temperature of immersion liquid 20 DEG C~30 DEG C are maintained always;The immersion liquid is the mixed liquor of deionized water and ethanol, and the mass percent of ethanol is dense Spend for 98%, the volume ratio of deionized water and 98% ethanol is 40:60;Followed by the mixture of purslane and soak is put Ultrasonic extraction 1.5~2.5 hours is carried out in ultrasonic extractor, the pressure of setting is normal pressure, and temperature is 60~80 DEG C, ultrasound Frequency is 200~400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains purslane extract;Purslane extract is passed through again Centrifugal filtration, filtrate recycling ethanol is collected, the filtrate finally given is purslane extract;
1.5 take fresh chrysanthemum indicum, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the chrysanthemum indicum of crushing Immersion liquid, the chrysanthemum indicum of crushing is immersed in 9~11 hours in immersion liquid, in immersion process, the temperature of immersion liquid 20 DEG C~30 DEG C are maintained always;The immersion liquid is the mixed liquor of deionized water and ethanol, and the mass percent of ethanol is dense Spend for 98%, the volume ratio of deionized water and 98% ethanol is 40:60;Followed by the mixture of chrysanthemum indicum and soak is put Ultrasonic extraction 1.5~2.5 hours is carried out in ultrasonic extractor, the pressure of setting is normal pressure, and temperature is 60~80 DEG C, ultrasound Frequency is 200~400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains chrysanthemum indicum extract;Chrysanthemum indicum extract is passed through again Centrifugal filtration, filtrate recycling ethanol is collected, the filtrate finally given is Flos Chrysanthemi Indici extract;
Step 2,
By mass percentage, 58%~63% sodium lauroyl sarcosine, 12%~16% cocamidopropyl propyl amide is weighed Glycine betaine, 13%~17% LAA, 1.5%~4.5% plant amino acid class, 1%~2% it is poly- The hydrogenating glycerol of ethylene glycol -200 palm acid ester, 0.1%~1.5% glycerol monolaurate, 0.1%~1.5% polyglycereol - 3 certain herbaceous plants with big flowers acid esters, 0.1%~1.5% PPG-3 myristic acids ether, 0.1%~1.3% palmitamide hydroxypropyltrimonium chloride, 0.4%~1.5% citric acid, 0.1%~0.3% EDTA-2Na, 1%~1.5% preservative, 0.3%~0.7% Essential oil, the mass percent summation of above each component is 100%;
Wherein, preservative is the quality of Phenoxyethanol and methylisothiazolinone, Phenoxyethanol and methylisothiazolinone Than for 16:1;
Step 3,
3.1 first by sodium lauroyl sarcosine, Cocoamidopropyl betaine, LAA, plant amino Acids, the hydrogenating glycerol of polyethylene glycol -200 palm acid ester, glycerol monolaurate, the certain herbaceous plants with big flowers of polyglycereol -3 acid esters, PPG-3 myristic acids Ether, palmitamide hydroxypropyltrimonium chloride, citric acid and EDTA-2Na pour into liquid and washed in pot, then heat while stirring, will Liquid wash mixture in pot temperature be heated to 75 DEG C~80 DEG C after maintain the temperature to continue to stir, until the material that liquid is washed in pot is complete Fully dissolved, stop heating and stirring, obtain mixture A;
Mixture A is naturally cooling to 30 DEG C~40 DEG C by 3.2 again, and Phenoxyethanol, methyl-isothiazol are added into mixture A Quinoline ketone and essential oil, stir, and obtain shampoo base;
Step 4,
By mass percentage, weigh 64%~68% shampoo base, 18%~22% ginger-root extract, 2%~ 4% ginseng root extract, 2%~4% radix-polygoni multiflori extract, 2%~4% purslane extract, 4%~6% open country Chrysanthemum extract, the mass percent summation of above each component is 100%;
Step 5,
Ginger-root extract, ginseng root extract, radix-polygoni multiflori extract, purslane extraction are added in most backward shampoo base Thing and Flos Chrysanthemi Indici extract, stir and obtain containing ginger without silicone oil without sulfate health-care shampoo.
The present invention beneficial functional be,
(1) ginger-root extract, ginseng root extract, radix-polygoni multiflori extract, purslane extract, Flos Chrysanthemi Indici extract compounding Extracts of Chinese herbal medicine mixture, the metabolism of scalp can not only be improved, promote scalp blood circulation, and there is promoting blood circulationization The effect of stasis of blood, rich in nutrition, hair follicle stimulating regenerate and reach anti-alopecia-stopping and growing and blacking hair, it is excessive to seborrhea, dandruff, Itching of the scalp has certain curative effect, can prevent the scalp allergic phenomena occurred during hair washing, and hair-washing hair-care has good oil-control effect Fruit, make hair is more compliant lubricate, be glossy.
(2) ginger-root extract and Flos Chrysanthemi Indici extract are contained in plant formula of the present invention, chrysanthemum indicum has antibacterial action in itself There is certain antiseptic power simultaneously, ginger has well anti-oxidant, antibacterial and antiprotozoan effect;Ginger and chrysanthemum indicum coordinate and made With can effectively solve the problems, such as that plant shampoo water becomes sour thinning discoloration, it is ensured that the stabilization for aqueous systems of having one's hair wash.
(3) refinement of plant extracts of the present invention uses low temperature ultrasonic abstraction technique, and low temperature will not be to plant nutrient substance Damage, and the plant extracts purity extracted is higher, can also retain the fragrance of plant in itself;Make plant extracts Meet natural, safe and healthy requirement.
(4) present invention is used as a no sulfate-free health-care shampoo of silicone oil, does not contain methyl hydroxybenzoate Nipasol, hydroxyl Benzene methyl Nipasol can stimulate skin, influence hormonal balance and alopecia, be easy carcinogenic preservative;Without diglycollic amide class The big surfactant of excitant, diglycollic amide class surfactant can cause scalp scorching, or even allergic reaction;Sulphur is not contained Acid salt surfactant, would not bring dioxanes residue into, and dioxanes has strong carcinogenicity;Mineral oil animal oil oil is not contained Fat;Using gentle amino acid surfactant as principal surfactant, the stimulation to scalp is reduced so as to reduce disturbing for scalp Itch, play a part of nursing scalp;The not special conditioning system of silicate-containing oil, will not block hair follicle pore, not increase to hair Burden will not cause accumulation of the conditioner on hair, and feel is smooth when cleaning hair, wash that rear hair is not clearly withered not to knot, It is a softer and smoother touch.
Embodiment
The present invention provide it is a kind of containing ginger without silicone oil without sulfate health-care shampoo, by mass percentage, by with the following group Part composition:64%~68% shampoo base, 18%~22% ginger-root extract, 2%~4% ginseng root extract, 2%~4% radix-polygoni multiflori extract, 2%~4% purslane extract, 4%~6% Flos Chrysanthemi Indici extract, above each group The mass percent summation of part is 100%;
Wherein, shampoo base by mass percentage, is made up of following component:58%~63% Hamposyl L Sodium, 12%~16% Cocoamidopropyl betaine, 13%~17% LAA, 1.5%~4.5% Plant amino acid class, 1%~2% hydrogenating glycerol of polyethylene glycol -200 palm acid ester, 0.1%~1.5% glycerine moon Cinnamic acid ester, 0.1%~1.5% certain herbaceous plants with big flowers of polyglycereol -3 acid esters, 0.1%~1.5% PPG-3 myristic acids ether, 0.1%~ 1.3% palmitamide hydroxypropyltrimonium chloride, 0.4%~1.5% citric acid, 0.1%~0.3% EDTA-2Na, 1%~1.5% preservative, 0.3%~0.7% essential oil, the mass percent summation of above each component is 100%.
Each material effect in shampoo of the present invention is described below:
Ginger-root extract:Main component is gingerol, protein, fat, dietary fiber, carrotene and trace element; It has significant antibacterial and antiprotozoan effect;For have in cosmetics clearing heat and detoxicating, detumescence, it is anti-oxidant, prevent that decortication is de- Hair, and promote hair epidermis part capillary circulation, wound and other effects is smoothed, also there is very strong oxidation resistance, be A kind of natural the effect of property plant additive.
Ginseng root extract:The telangiectasis on head can be made, the nutrition of hair can be increased, improve the toughness of hair, Alopecia, disconnected hair are reduced, there is protective effect to the hair of damage.With nourishing hair, promote hair growth and other effects.
Radix-polygoni multiflori extract:Have anti-aging, Wu Sifa, happy color, the effect of strengthening the essence blood-nourishing.Promote hair cell newborn, Slow down white hair growth, anti-alopecia-stopping, to seborrhea, dandruff is excessive, and itching of the scalp has certain curative effect.
Purslane extract:Its antiallergy effect is close with " slips extract " and " 10% glycyrrhizic acid diformazan powder ";Horse Bitterroot contains substantial amounts of noradrenalin (containing 0.25% in fresh purslane), neurohormone (has and plays blood vessel Shrink effect, hypotension and the function of reducing tissue bleeding), also containing nutrients, vitamin, amino acid series and biflavone Class liquiritin;Due to there is extraordinary effect in terms of pharmacology containing this composition, burn, cutaneous pain, itch, eczema and purulence are such as treated It is swollen, therefore for having remarkable efficacy as anti-inflammatory, anti-irritant, antianaphylactic bioactive additive in cosmetics.
Flos Chrysanthemi Indici extract:The effect of with antibacterial, antiviral, heat-clearing anti-inflammatory, elimination activity free radical, also with antioxygen Change acts on, and prevents skin senescence.
Sodium lauroyl sarcosine:Moderate performance, skin and eyes are not stimulated, dry skin and degreasing will not be caused, can produced Raw abundant and stable cream-like bubble, is easily adsorbed in scalp surface, delays the volatilization of scalp moisture, making the scalp of user has Soft refreshing, not tight sensation.
Cocoamidopropyl betaine:With foaminess, thickening property and bactericidal properties, compounded with anion surfactant, Material body viscosity can be improved, thickening effect is obvious.
LAA:It is a kind of amphoteric surfactant, there is special mildness and extremely low stimulation Property, good foaminess, foaming abundancy is fine and closely woven, and skin sense is good, can significantly improve the foam state of formula system, easily biological-degradable, Security is good, and it and anion, cation, nonionic surfactant have good compatibility in the range of very wide PH, and Other surfactants (AES etc.) excitant can effectively be reduced.
Plant amino acid class:It is low molecule angulation albumen, its composition is hydrolyzed vegetable protein, polylysine, Phenoxyethanol And water;Hair can be penetrated into, reconstruction hair, makes hair more strong, shows the beautiful outward appearance of health.
The hydrogenating glycerol palm acid ester of polyethylene glycol -200:Extremely gentle efficient thickeners, plant origin, property temperature With recommend, for baby products and other sensitive skin gentle hair washing and skin-protection products, there is rich lipid.
Glycerol monolaurate:The food-grade of natural origin is without EO raw materials, washing system hydrophobic thickener, viscosity stabiliser, Or good bactericide, and preservative synergy antiseptic effect can be helped.
The certain herbaceous plants with big flowers acid esters of polyglycereol -3:Superfatting agent without polyethylene glycol, there is the thickening power of brilliance, there is provided comfortable skin sense.
PPG-3 myristic acid ethers:It is the stronger emollient of polarity, lubricity is good, no greasy feeling.
Palmitamide hydroxypropyltrimonium chloride:It is the cationic surfactant of plant origin, in shampoo and hair care A softer and smoother touch feel is provided in element for hair, antistatic effect high with the compatibility of hair and skin, remarkable, surface-active Remarkable thickener in agent system.
Citric acid:With very strong bactericidal action, and the faint scent of shampoo can be increased, citric acid can also improve in addition The performance of surfactant, and be a kind of excellent intercalating agent, poisonous metal can be removed.
EDTA-2Na:For complexing agent, the metal ion that can be complexed in shampoo, stabilization is played to shampoo.
Essential oil:With antibacterial, anti-oxidant, antiallergic sense, moisturizing, promote the effect of cytothesis, washed it can in addition contain increase The fragrance of shampoo.
With reference to specific embodiment, the present invention is described in detail.
Embodiment 1
It is as follows without preparation technology of the silicone oil without sulfate health-care shampoo, its concrete operation step containing ginger:
Step 1,
1.1 take fresh race, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the race of crushing Immersion liquid (immersion liquid weight is 8 times of race weight), the race of crushing is immersed in 10 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 25 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by by life The mixture of race and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 2 hours, and the pressure of setting is normal pressure, temperature For 70 DEG C, supersonic frequency 300HZ;After ultrasonic extraction, supernatant liquor is taken, obtains race extract;Race is extracted again Liquid passes through centrifugal filtration, collects filtrate recycling ethanol, the filtrate finally given is officinale root extract;
1.2 take fresh ginseng, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the ginseng of crushing Immersion liquid (immersion liquid weight is 8 times of ginseng weight), the ginseng of crushing is immersed in 10 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 25 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by by people The mixture of ginseng root and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 2 hours, and the pressure of setting is normal pressure, temperature For 70 DEG C, supersonic frequency 300HZ;After ultrasonic extraction, supernatant liquor is taken, obtains ginseng extract;Ginseng is extracted again Liquid passes through centrifugal filtration, collects filtrate recycling ethanol, the filtrate finally given is ginseng root extract;
1.3 take the fresh fleece-flower root, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the fleece-flower root of crushing Immersion liquid (immersion liquid weight is 8 times of fleece-flower root weight), the fleece-flower root of crushing is immersed in 10 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 25 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by, by what The mixture of the tuber of multiflower knotweed and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 2 hours, and the pressure of setting is normal pressure, temperature For 70 DEG C, supersonic frequency 300HZ;After ultrasonic extraction, supernatant liquor is taken, obtains fleece-flower root extract;The fleece-flower root is extracted again Liquid passes through centrifugal filtration, collects filtrate recycling ethanol, the filtrate finally given is radix-polygoni multiflori extract;
1.4 take fresh purslane, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the purslane of crushing Immersion liquid (immersion liquid weight is 8 times of purslane weight), the purslane of crushing is immersed in 10 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 25 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by by horse The mixture of bitterroot and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 2 hours, and the pressure of setting is normal pressure, temperature For 70 DEG C, supersonic frequency 300HZ;After ultrasonic extraction, supernatant liquor is taken, obtains purslane extract;Purslane is extracted again Liquid passes through centrifugal filtration, collects filtrate recycling ethanol, the filtrate finally given is purslane extract;
1.5 take fresh chrysanthemum indicum, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the chrysanthemum indicum of crushing Immersion liquid (immersion liquid weight is 8 times of chrysanthemum indicum weight), the chrysanthemum indicum of crushing is immersed in 10 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 25 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by by open country The mixture of chrysanthemum and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 2 hours, and the pressure of setting is normal pressure, temperature For 70 DEG C, supersonic frequency 300HZ;After ultrasonic extraction, supernatant liquor is taken, obtains chrysanthemum indicum extract;Chrysanthemum indicum is extracted again Liquid passes through centrifugal filtration, collects filtrate recycling ethanol, the filtrate finally given is Flos Chrysanthemi Indici extract;
Step 2,
By mass percentage, weigh 60.60% sodium lauroyl sarcosine, 13.65% Cocoamidopropyl betaine, 15.15% LAA, 3.05% plant amino acid class, 1.50% hydrogenating glycerol of polyethylene glycol -200 Palm acid ester, 0.75% glycerol monolaurate, 0.75% certain herbaceous plants with big flowers of polyglycereol -3 acid esters, 0.75% PPG-3 myristic acids Ether, 0.70% palmitamide hydroxypropyltrimonium chloride, 1.05% citric acid, 0.15% EDTA-2Na, 1.30% Preservative, 0.60% ginger essential oil;Above each component quality summation is 10kg;
Wherein, preservative is the quality of Phenoxyethanol and methylisothiazolinone, Phenoxyethanol and methylisothiazolinone Than for 16:1;
Plant amino acid class (Hydrolyzed vegetable protein) is bought in Foshan used by the present embodiment He De new materials Co., Ltd;
Step 3,
3.1 first by sodium lauroyl sarcosine, Cocoamidopropyl betaine, LAA, plant amino Acids, the hydrogenating glycerol of polyethylene glycol -200 palm acid ester, glycerol monolaurate, the certain herbaceous plants with big flowers of polyglycereol -3 acid esters, PPG-3 myristic acids Ether, palmitamide hydroxypropyltrimonium chloride, citric acid and EDTA-2Na pour into liquid and washed in pot, then heat while stirring, will Liquid wash mixture in pot temperature be heated to 78 DEG C after maintain the temperature to continue to stir, until the material that liquid is washed in pot is completely molten Solution, stop heating and stirring, obtain mixture A;
Mixture A is naturally cooling to 35 DEG C by 3.2 again, into mixture A add Phenoxyethanol, methylisothiazolinone and Ginger essential oil, stir, obtain shampoo base;
Step 4,
6.6kg shampoo base, 2kg ginger-root extract, 0.3kg ginseng root extract, 0.3kg what head weighed The Flos Chrysanthemi Indici extract of black extract, 0.3kg purslane extract and 0.5kg;
Step 5,
Ginger-root extract, ginseng root extract, radix-polygoni multiflori extract, purslane extraction are added in most backward shampoo base Thing and Flos Chrysanthemi Indici extract, stir and obtain containing ginger without silicone oil without sulfate health-care shampoo A.
Embodiment 2
It is as follows without preparation technology of the silicone oil without sulfate health-care shampoo, its concrete operation step containing ginger:
Step 1,
1.1 take fresh race, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the race of crushing Immersion liquid (immersion liquid weight is 8 times of race weight), the race of crushing is immersed in 9 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 20 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by by life The mixture of race and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 2.5 hours, and the pressure of setting is normal pressure, temperature Spend for 80 DEG C, supersonic frequency 200HZ;After ultrasonic extraction, supernatant liquor is taken, obtains race extract;Race is extracted again Take liquid to pass through centrifugal filtration, collect filtrate recycling ethanol, the filtrate finally given is officinale root extract;
1.2 take fresh ginseng, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the ginseng of crushing Immersion liquid (immersion liquid weight is 8 times of ginseng weight), the ginseng of crushing is immersed in 9 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 20 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by by people The mixture of ginseng root and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 2.5 hours, and the pressure of setting is normal pressure, temperature Spend for 80 DEG C, supersonic frequency 200HZ;After ultrasonic extraction, supernatant liquor is taken, obtains ginseng extract;Ginseng is extracted again Take liquid to pass through centrifugal filtration, collect filtrate recycling ethanol, the filtrate finally given is ginseng root extract;
1.3 take the fresh fleece-flower root, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the fleece-flower root of crushing Immersion liquid (immersion liquid weight is 8 times of fleece-flower root weight), the fleece-flower root of crushing is immersed in 9 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 20 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by, by what The mixture of the tuber of multiflower knotweed and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 2.5 hours, and the pressure of setting is normal pressure, temperature Spend for 80 DEG C, supersonic frequency 200HZ;After ultrasonic extraction, supernatant liquor is taken, obtains fleece-flower root extract;The fleece-flower root is extracted again Take liquid to pass through centrifugal filtration, collect filtrate recycling ethanol, the filtrate finally given is radix-polygoni multiflori extract;
1.4 take fresh purslane, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the purslane of crushing Immersion liquid (immersion liquid weight is 8 times of purslane weight), the purslane of crushing is immersed in 9 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 20 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by by horse The mixture of bitterroot and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 2.5 hours, and the pressure of setting is normal pressure, temperature Spend for 80 DEG C, supersonic frequency 200HZ;After ultrasonic extraction, supernatant liquor is taken, obtains purslane extract;Purslane is extracted again Take liquid to pass through centrifugal filtration, collect filtrate recycling ethanol, the filtrate finally given is purslane extract;
1.5 take fresh chrysanthemum indicum, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the chrysanthemum indicum of crushing Immersion liquid (immersion liquid weight is 8 times of chrysanthemum indicum weight), the chrysanthemum indicum of crushing is immersed in 9 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 20 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by by open country The mixture of chrysanthemum and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 2.5 hours, and the pressure of setting is normal pressure, temperature Spend for 80 DEG C, supersonic frequency 200HZ;After ultrasonic extraction, supernatant liquor is taken, obtains chrysanthemum indicum extract;Chrysanthemum indicum is extracted again Take liquid to pass through centrifugal filtration, collect filtrate recycling ethanol, the filtrate finally given is Flos Chrysanthemi Indici extract;
Step 2,
By mass percentage, weigh 58.00% sodium lauroyl sarcosine, 16.00% Cocoamidopropyl betaine, 13.00% LAA, 4.50% plant amino acid class, 2.00% hydrogenating glycerol of polyethylene glycol -200 Palm acid ester, 1.50% glycerol monolaurate, 0.10% certain herbaceous plants with big flowers of polyglycereol -3 acid esters, 1.50% PPG-3 myristic acids Ether, 0.10% palmitamide hydroxypropyltrimonium chloride, 1.50% citric acid, 0.10% EDTA-2Na, 1.00% Preservative and 0.70% ginger essential oil;Above each component quality summation is 10kg;
Wherein, preservative is the quality of Phenoxyethanol and methylisothiazolinone, Phenoxyethanol and methylisothiazolinone Than for 16:1;
Plant amino acid class (Hydrolyzed vegetable protein) is bought in Foshan used by the present embodiment He De new materials Co., Ltd;
Step 3,
3.1 first by sodium lauroyl sarcosine, Cocoamidopropyl betaine, LAA, plant amino Acids, the hydrogenating glycerol of polyethylene glycol -200 palm acid ester, glycerol monolaurate, the certain herbaceous plants with big flowers of polyglycereol -3 acid esters, PPG-3 myristic acids Ether, palmitamide hydroxypropyltrimonium chloride, citric acid and EDTA-2Na pour into liquid and washed in pot, then heat while stirring, will Liquid wash mixture in pot temperature be heated to 75 DEG C after maintain the temperature to continue to stir, until the material that liquid is washed in pot is completely molten Solution, stop heating and stirring, obtain mixture A;
Mixture A is naturally cooling to 30 DEG C by 3.2 again, into mixture A add Phenoxyethanol, methylisothiazolinone and Ginger essential oil, stir, obtain shampoo base;
Step 4,
Weigh 6.4kg shampoo base, 2.2kg ginger-root extract, 0.2kg ginseng root extract, 0.4kg what The Flos Chrysanthemi Indici extract of tuber of multiflower knotweed extract, 0.4kg purslane extract and 0.4kg;
Step 5,
Ginger-root extract, ginseng root extract, radix-polygoni multiflori extract, purslane extraction are added in most backward shampoo base Thing and Flos Chrysanthemi Indici extract, stir and obtain containing ginger without silicone oil without sulfate health-care shampoo B.
Embodiment 3
It is as follows without preparation technology of the silicone oil without sulfate health-care shampoo, its concrete operation step containing ginger:
Step 1,
1.1 take fresh race, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the race of crushing Immersion liquid (immersion liquid weight is 8 times of race weight), the race of crushing is immersed in 11 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 30 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by by life The mixture of race and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 1.5 hours, and the pressure of setting is normal pressure, temperature Spend for 60 DEG C, supersonic frequency 400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains race extract;Race is extracted again Take liquid to pass through centrifugal filtration, collect filtrate recycling ethanol, the filtrate finally given is officinale root extract;
1.2 take fresh ginseng, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the ginseng of crushing Immersion liquid (immersion liquid weight is 8 times of ginseng weight), the ginseng of crushing is immersed in 11 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 30 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by by people The mixture of ginseng root and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 1.5 hours, and the pressure of setting is normal pressure, temperature Spend for 60 DEG C, supersonic frequency 400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains ginseng extract;Ginseng is extracted again Take liquid to pass through centrifugal filtration, collect filtrate recycling ethanol, the filtrate finally given is ginseng root extract;
1.3 take the fresh fleece-flower root, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the fleece-flower root of crushing Immersion liquid (immersion liquid weight is 8 times of fleece-flower root weight), the fleece-flower root of crushing is immersed in 11 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 30 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by, by what The mixture of the tuber of multiflower knotweed and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 1.5 hours, and the pressure of setting is normal pressure, temperature Spend for 60 DEG C, supersonic frequency 400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains fleece-flower root extract;The fleece-flower root is extracted again Take liquid to pass through centrifugal filtration, collect filtrate recycling ethanol, the filtrate finally given is radix-polygoni multiflori extract;
1.4 take fresh purslane, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the purslane of crushing Immersion liquid (immersion liquid weight is 8 times of purslane weight), the purslane of crushing is immersed in 11 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 30 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by by horse The mixture of bitterroot and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 1.5 hours, and the pressure of setting is normal pressure, temperature Spend for 60 DEG C, supersonic frequency 400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains purslane extract;Purslane is extracted again Take liquid to pass through centrifugal filtration, collect filtrate recycling ethanol, the filtrate finally given is purslane extract;
1.5 take fresh chrysanthemum indicum, clean, and crush, and cross 40 mesh sieves;Then 8 times of amounts of addition into the chrysanthemum indicum of crushing Immersion liquid (immersion liquid weight is 8 times of chrysanthemum indicum weight), the chrysanthemum indicum of crushing is immersed in 11 small in immersion liquid When, in immersion process, the temperature of immersion liquid maintains 30 DEG C always;The immersion liquid is deionized water and ethanol (ethanol Mass percent concentration be mixed liquor 98%), the volume ratio of deionized water and 98% ethanol is 40:60;Followed by by open country The mixture of chrysanthemum and soak, which is placed in ultrasonic extractor, carries out ultrasonic extraction 1.5 hours, and the pressure of setting is normal pressure, temperature Spend for 60 DEG C, supersonic frequency 400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains chrysanthemum indicum extract;Chrysanthemum indicum is extracted again Take liquid to pass through centrifugal filtration, collect filtrate recycling ethanol, the filtrate finally given is Flos Chrysanthemi Indici extract;
Step 2,
By mass percentage, weigh 63.00% sodium lauroyl sarcosine, 12.00% Cocoamidopropyl betaine, 17.00% LAA, 1.50% plant amino acid class, 1.00% hydrogenating glycerol of polyethylene glycol -200 Palm acid ester, 0.10% glycerol monolaurate, 1.50% certain herbaceous plants with big flowers of polyglycereol -3 acid esters, 0.10% PPG-3 myristic acids Ether, 1.30% palmitamide hydroxypropyltrimonium chloride, 0.40% citric acid, 0.30% EDTA-2Na, 1.50% Preservative and 0.30% ginger essential oil;Above each component quality summation is 10kg;
Wherein, preservative is the quality of Phenoxyethanol and methylisothiazolinone, Phenoxyethanol and methylisothiazolinone Than for 16:1;
Plant amino acid class (Hydrolyzed vegetable protein) is bought in Foshan used by the present embodiment He De new materials Co., Ltd;
Step 3,
3.1 first by sodium lauroyl sarcosine, Cocoamidopropyl betaine, LAA, plant amino Acids, the hydrogenating glycerol of polyethylene glycol -200 palm acid ester, glycerol monolaurate, the certain herbaceous plants with big flowers of polyglycereol -3 acid esters, PPG-3 myristic acids Ether, palmitamide hydroxypropyltrimonium chloride, citric acid and EDTA-2Na pour into liquid and washed in pot, then heat while stirring, will Liquid wash mixture in pot temperature be heated to 80 DEG C after maintain the temperature to continue to stir, until the material that liquid is washed in pot is completely molten Solution, stop heating and stirring, obtain mixture A;
Mixture A is naturally cooling to 40 DEG C by 3.2 again, into mixture A add Phenoxyethanol, methylisothiazolinone and Ginger essential oil, stir, obtain shampoo base;
Step 4,
Weigh 6.8kg shampoo base, 1.8kg ginger-root extract, 0.4kg ginseng root extract, 0.2kg what The Flos Chrysanthemi Indici extract of tuber of multiflower knotweed extract, 0.2kg purslane extract and 0.6kg;
Step 5,
Ginger-root extract, ginseng root extract, radix-polygoni multiflori extract, purslane extraction are added in most backward shampoo base Thing and Flos Chrysanthemi Indici extract, stir and obtain containing ginger without silicone oil without sulfate health-care shampoo C.
The effect of ginger shampoo of the present invention, is described in further detail with reference to experiment:
Test group I:The shampoo A prepared for the embodiment of the present invention 1.
Test group II:The shampoo B prepared for the embodiment of the present invention 2.
Test group III:The shampoo C prepared for the embodiment of the present invention 3.
Contrast groups I:The content of step 4 as different from Example 1, remaining is same as Example 1;
The particular content of step 4 is:
Weigh 7.2kg shampoo base, 1.6kg ginger-root extract, 0.3kg ginseng root extract, 0.3kg what The Flos Chrysanthemi Indici extract of tuber of multiflower knotweed extract, 0.3kg purslane extract and 0.3kg.
Ginger-root extract, ginseng root extract, radix-polygoni multiflori extract, purslane extract, Flos Chrysanthemi Indici extract and hair washing The preparation method of liquid base material is consistent with embodiment 1.
Contrast groups II:The content of step 4 as different from Example 1, remaining is same as Example 1;
The particular content of step 4 is:
Weigh 7.6kg shampoo base, 1.4kg ginger-root extract, 0.3kg ginseng root extract, 0.3kg what The Flos Chrysanthemi Indici extract of tuber of multiflower knotweed extract, 0.3kg purslane extract and 0.1kg.
Ginger-root extract, ginseng root extract, radix-polygoni multiflori extract, purslane extract, Flos Chrysanthemi Indici extract and hair washing The preparation method of liquid base material is consistent with embodiment 1.
Test for the first time, the sample that greenhouse has just been made:The viscosity of the sample of test group I is 4000mPa.s, free from extraneous odour; The viscosity of the sample of test group II is 4000mPa.s, free from extraneous odour;The viscosity of the sample of test group III is 4000mPa.s, is no different Taste;The viscosity of the sample of contrast groups I is 4000mPa.s, free from extraneous odour;The viscosity of the sample of contrast groups II is 4000mPa.s, is no different Taste.
Second of test, 40 DEG C of insulating boxs place the sample of 24 hours:The viscosity of the sample of test group I is 3800mPa.s, Free from extraneous odour;The viscosity of the sample of test group II is 3800mPa.s, free from extraneous odour;The viscosity of the sample of test group III is 3800mPa.s free from extraneous odour;The viscosity of the sample of contrast groups I is 3500mPa.s, slightly peculiar smell;The viscosity of the sample of contrast groups II is 3300mPa.s, there is peculiar smell, and peculiar smell slightly weighs than contrast groups I.
Third time is tested, and 40 DEG C of insulating boxs place the sample of 10 days:The viscosity of the sample of test group I is 3800mPa.s, nothing Peculiar smell;The viscosity of the sample of test group II is 3800mPa.s, free from extraneous odour;The viscosity of the sample of test group III is 3800mPa.s, Free from extraneous odour;The viscosity of the sample of contrast groups I is 3000mPa.s, there is stink;The viscosity of the sample of contrast groups II is 2600mPa.s, There is stink.
After shampoo wash my hair of the present invention, the salubriouser non-greasy of scalp, hair soft;After continuous use two months There is no dandruff, oil-control positive effect, alopecia significantly reduces, and hair is shiny black.It is several Consumer's Experiences below, to verify that the present invention washes The hair-washing hair-care effect of shampoo.
1. Guangzhou Baiyun District Mr. Wang, male, 44 years old;Operating pressure is big, and exiguous human hair is matt, and hair loss is serious;Use within two days The hair to drop of combing one's hair of being got up daily once after shampoo of the present invention, after one month is constantly reduced, hair become more blackening, it is submissive, It is glossy;After three months, combing hair of getting up morning, for the hair to come off substantially at 5~30, hair becomes more, shiny black to have Gloss, per week use more than once is adhered to later.
2. Guangzhou Fanyu District labor, female, 25 years old;Often hair dyeing, hair is lackluster, dry up, frangibility, and head itch, Dandruff is serious;After shampoo of the present invention, using once, one month takes effect, and dandruff tails off, and itching of the scalp subtracts within least two days Gently;After three months, dandruff and itching of the scalp disappear substantially, and hair is naturally submissive, glossy, easily comb, and hair fractures point The phenomenon of fork disappears.
3. Guangzhou Huangpu District Zhu, female, 55 years old;Hair is not greasy, mixed and disorderly, no elastic, submissive, hair quality jaundice, hair Often fracture, hair slightly more bifurcated;Hair quality improves, the submissive glossy, hair of hair breaks after used shampoo of the present invention 2 months The situation for splitting bifurcated has also taken a turn for the better.Hold on using shampoo of the present invention after 1 month, her hair healthy, it is submissive, have light Pool, hair are not broken and flexible, and hair scalp is no longer greasy, and hair scalp moistens salubrious.

Claims (8)

1. containing ginger without silicone oil without sulfate health-care shampoo, it is characterised in that by mass percentage, by following component group Into:64%~68% shampoo base, 18%~22% ginger-root extract, 2%~4% ginseng root extract, 2%~ 4% radix-polygoni multiflori extract, 2%~4% purslane extract, 4%~6% Flos Chrysanthemi Indici extract, above each component Mass percent summation is 100%.
2. according to claim 1 containing ginger without silicone oil without sulfate health-care shampoo, it is characterised in that:The shampoo Base-material by mass percentage, is made up of following component:58%~63% sodium lauroyl sarcosine, 12%~16% cocounut oil acyl Amine CAB, 13%~17% LAA, 1.5%~4.5% plant amino acid class, 1%~ 2% hydrogenating glycerol of polyethylene glycol -200 palm acid ester, 0.1%~1.5% glycerol monolaurate, 0.1%~1.5% The certain herbaceous plants with big flowers of polyglycereol -3 acid esters, 0.1%~1.5% PPG-3 myristic acids ether, 0.1%~1.3% palmitamide oxypropyl trimethyl Ammonium chloride, 0.4%~1.5% citric acid, 0.1%~0.3% EDTA-2Na, 1%~1.5% preservative, 0.3%~ 0.7% essential oil, the mass percent summation of above each component is 100%.
3. according to claim 2 containing ginger without silicone oil without sulfate health-care shampoo, it is characterised in that:The no silicone oil Without sulfate health-care shampoo, by mass percentage, it is made up of following component:66% shampoo base, 20% race carry Take thing, 3% ginseng root extract, 3% radix-polygoni multiflori extract, 3% purslane extract, 5% Flos Chrysanthemi Indici extract;
Wherein, shampoo base by mass percentage, is made up of following component:60.60% sodium lauroyl sarcosine, 13.65% Cocoamidopropyl betaine, 15.15% LAA, 3.05% plant amino acid class, 1.50% hydrogenating glycerol of polyethylene glycol -200 palm acid ester, 0.75% glycerol monolaurate, 0.75% polyglycereol -3 Certain herbaceous plants with big flowers acid esters, 0.75% PPG-3 myristic acids ether, 0.70% palmitamide hydroxypropyltrimonium chloride, 1.05% lemon Acid, 0.15% EDTA-2Na, 1.30% preservative, 0.60% essential oil.
4. according to Claims 2 or 3 containing ginger without silicone oil without sulfate health-care shampoo, it is characterised in that:It is described anti- Rotten agent is Phenoxyethanol and methylisothiazolinone, and the mass ratio of Phenoxyethanol and methylisothiazolinone is 16:1.
5. according to Claims 2 or 3 containing ginger without silicone oil without sulfate health-care shampoo, it is characterised in that:The essence Oil is Rosa Damascana, ginger essential oil, orchid essential oil, sun flower essential oil or lotus flower essential oil.
6. according to Claims 2 or 3 containing ginger without silicone oil without sulfate health-care shampoo, it is characterised in that:The plant The composition of thing amino acids has:Hydrolyzed vegetable protein, polylysine, Phenoxyethanol and water.
7. described in claim 2 containing ginger without preparation technology of the silicone oil without sulfate health-care shampoo, it is characterised in that its have Body operating procedure is as follows:
Step 1,
1.1 take fresh race, clean, and crush, and cross 40 mesh sieves;Then the immersion of 8 times of amounts is added into the race of crushing Liquid, the race of crushing is immersed in 9~11 hours in immersion liquid, in immersion process, the temperature of immersion liquid is always Maintain 20 DEG C~30 DEG C;The immersion liquid is the mixed liquor of deionized water and ethanol, and the mass percent concentration of ethanol is 98%, the volume ratio of deionized water and 98% ethanol is 40:60;Followed by the mixture of race and soak being placed in super Ultrasonic extraction 1.5~2.5 hours is carried out in sound wave extractor, the pressure of setting is normal pressure, and temperature is 60~80 DEG C, supersonic frequency For 200~400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains race extract;Again by race extract by centrifuging Filtering, filtrate recycling ethanol is collected, the filtrate finally given is officinale root extract;
1.2 take fresh ginseng, clean, and crush, and cross 40 mesh sieves;Then the immersion of 8 times of amounts is added into the ginseng of crushing Liquid, the ginseng of crushing is immersed in 9~11 hours in immersion liquid, in immersion process, the temperature of immersion liquid is always Maintain 20 DEG C~30 DEG C;The immersion liquid is the mixed liquor of deionized water and ethanol, and the mass percent concentration of ethanol is 98%, the volume ratio of deionized water and 98% ethanol is 40:60;Followed by the mixture of ginseng and soak being placed in super Ultrasonic extraction 1.5~2.5 hours is carried out in sound wave extractor, the pressure of setting is normal pressure, and temperature is 60~80 DEG C, supersonic frequency For 200~400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains ginseng extract;Again by ginseng extract by centrifuging Filtering, filtrate recycling ethanol is collected, the filtrate finally given is ginseng root extract;
1.3 take the fresh fleece-flower root, clean, and crush, and cross 40 mesh sieves;Then the immersion of 8 times of amounts is added into the fleece-flower root of crushing Liquid, the fleece-flower root of crushing is immersed in 9~11 hours in immersion liquid, in immersion process, the temperature of immersion liquid is always Maintain 20 DEG C~30 DEG C;The immersion liquid is the mixed liquor of deionized water and ethanol, and the mass percent concentration of ethanol is 98%, the volume ratio of deionized water and 98% ethanol is 40:60;Followed by the mixture of the fleece-flower root and soak being placed in super Ultrasonic extraction 1.5~2.5 hours is carried out in sound wave extractor, the pressure of setting is normal pressure, and temperature is 60~80 DEG C, supersonic frequency For 200~400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains fleece-flower root extract;Again by fleece-flower root extract by centrifuging Filtering, filtrate recycling ethanol is collected, the filtrate finally given is radix-polygoni multiflori extract;
1.4 take fresh purslane, clean, and crush, and cross 40 mesh sieves;Then the immersion of 8 times of amounts is added into the purslane of crushing Liquid, the purslane of crushing is immersed in 9~11 hours in immersion liquid, in immersion process, the temperature of immersion liquid is always Maintain 20 DEG C~30 DEG C;The immersion liquid is the mixed liquor of deionized water and ethanol, and the mass percent concentration of ethanol is 98%, the volume ratio of deionized water and 98% ethanol is 40:60;Followed by the mixture of purslane and soak being placed in super Ultrasonic extraction 1.5~2.5 hours is carried out in sound wave extractor, the pressure of setting is normal pressure, and temperature is 60~80 DEG C, supersonic frequency For 200~400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains purslane extract;Again by purslane extract by centrifuging Filtering, filtrate recycling ethanol is collected, the filtrate finally given is purslane extract;
1.5 take fresh chrysanthemum indicum, clean, and crush, and cross 40 mesh sieves;Then the immersion of 8 times of amounts is added into the chrysanthemum indicum of crushing Liquid, the chrysanthemum indicum of crushing is immersed in 9~11 hours in immersion liquid, in immersion process, the temperature of immersion liquid is always Maintain 20 DEG C~30 DEG C;The immersion liquid is the mixed liquor of deionized water and ethanol, and the mass percent concentration of ethanol is 98%, the volume ratio of deionized water and 98% ethanol is 40:60;Followed by the mixture of chrysanthemum indicum and soak being placed in super Ultrasonic extraction 1.5~2.5 hours is carried out in sound wave extractor, the pressure of setting is normal pressure, and temperature is 60~80 DEG C, supersonic frequency For 200~400HZ;After ultrasonic extraction, supernatant liquor is taken, obtains chrysanthemum indicum extract;Again by chrysanthemum indicum extract by centrifuging Filtering, filtrate recycling ethanol is collected, the filtrate finally given is Flos Chrysanthemi Indici extract;
Step 2,
By mass percentage, 58%~63% sodium lauroyl sarcosine, 12%~16% cocamidopropyl propyl amide beet is weighed Alkali, 13%~17% LAA, 1.5%~4.5% plant amino acid class, 1%~2% poly- second two The hydrogenating glycerol of alcohol -200 palm acid ester, 0.1%~1.5% glycerol monolaurate, 0.1%~1.5% certain herbaceous plants with big flowers of polyglycereol -3 Acid esters, 0.1%~1.5% PPG-3 myristic acids ether, 0.1%~1.3% palmitamide hydroxypropyltrimonium chloride, 0.4%~1.5% citric acid, 0.1%~0.3% EDTA-2Na, 1%~1.5% preservative, 0.3%~0.7% Essential oil, the mass percent summation of above each component is 100%;
Wherein, preservative is Phenoxyethanol and methylisothiazolinone, and the mass ratio of Phenoxyethanol and methylisothiazolinone is 16:1;
Step 3,
3.1 first by sodium lauroyl sarcosine, Cocoamidopropyl betaine, LAA, plant amino acid class, The hydrogenating glycerol of polyethylene glycol -200 palm acid ester, glycerol monolaurate, the certain herbaceous plants with big flowers of polyglycereol -3 acid esters, PPG-3 myristic acids ether, palm fibre Palmitic acid amidopropyltrimonium chloride, citric acid and EDTA-2Na pour into liquid and washed in pot, then heat while stirring, and liquid is washed into pot The temperature of interior mixture maintains the temperature to continue to stir after being heated to 75 DEG C~80 DEG C, until the material that liquid is washed in pot is completely molten Solution, stop heating and stirring, obtain mixture A;
Mixture A is naturally cooling to 30 DEG C~40 DEG C by 3.2 again, and Phenoxyethanol, methylisothiazolinone are added into mixture A And essential oil, stir, obtain shampoo base;
Step 4,
By mass percentage, weigh 64%~68% shampoo base, 18%~22% ginger-root extract, 2%~4% Ginseng root extract, 2%~4% radix-polygoni multiflori extract, 2%~4% purslane extract, 4%~6% chrysanthemum indicum carry Thing is taken, the mass percent summation of above each component is 100%;
Step 5,
In most backward shampoo base add ginger-root extract, ginseng root extract, radix-polygoni multiflori extract, purslane extract and Flos Chrysanthemi Indici extract, stir and obtain containing ginger without silicone oil without sulfate health-care shampoo.
8. according to claim 7 containing ginger without preparation technology of the silicone oil without sulfate health-care shampoo, it is characterised in that: The essential oil is Rosa Damascana, ginger essential oil, orchid essential oil, sun flower essential oil or lotus flower essential oil.
CN201711126848.9A 2017-11-15 2017-11-15 Containing ginger without silicone oil without sulfate health-care shampoo and its preparation technology Pending CN107737039A (en)

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CN110960476A (en) * 2019-12-31 2020-04-07 娇时日化(杭州)股份有限公司 Mousse for hair and hair of dry-cleaning shampoo with rich moisture and comfort and preparation method thereof
CN111759790A (en) * 2020-06-15 2020-10-13 深圳前海创新工场健康产业有限公司 Shampoo containing turmeric extract ginseng stem cell material and preparation method thereof
CN111956522A (en) * 2020-09-22 2020-11-20 福建省梦娇兰日用化学品有限公司 Infant shampoo without silicone oil and preparation method thereof
CN115487127A (en) * 2022-07-13 2022-12-20 广东嘉丹婷日用品有限公司 Anti-hair loss oil-control silicone-oil-free shampoo and preparation method thereof

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CN110960476A (en) * 2019-12-31 2020-04-07 娇时日化(杭州)股份有限公司 Mousse for hair and hair of dry-cleaning shampoo with rich moisture and comfort and preparation method thereof
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CN111759790A (en) * 2020-06-15 2020-10-13 深圳前海创新工场健康产业有限公司 Shampoo containing turmeric extract ginseng stem cell material and preparation method thereof
CN111956522A (en) * 2020-09-22 2020-11-20 福建省梦娇兰日用化学品有限公司 Infant shampoo without silicone oil and preparation method thereof
CN115487127A (en) * 2022-07-13 2022-12-20 广东嘉丹婷日用品有限公司 Anti-hair loss oil-control silicone-oil-free shampoo and preparation method thereof

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