CN107184406A - One kind is planted extraction without anti-corrosion ginger without silicone oil shampoo and preparation method thereof - Google Patents
One kind is planted extraction without anti-corrosion ginger without silicone oil shampoo and preparation method thereof Download PDFInfo
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- CN107184406A CN107184406A CN201710332913.7A CN201710332913A CN107184406A CN 107184406 A CN107184406 A CN 107184406A CN 201710332913 A CN201710332913 A CN 201710332913A CN 107184406 A CN107184406 A CN 107184406A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/51—Chelating agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
Abstract
Extraction is planted without anti-corrosion ginger without silicone oil shampoo the invention provides one kind, includes the preparing raw material of following weight percentage：Gingerol 0.1~5% and tax fat agent 0.4~6%；It is described to assign the mixture that fat agent is the Octyl Ethers of PPG 3,12~13 carbon alcohol lactates, the propylene glycol oleates of PEG 55 and the glyceryl cocoates of PEG 7.Extraction is planted without preparation method of the anti-corrosion ginger without silicone oil shampoo present invention also offers one kind.Shampoo of the present invention can effectively cleaning and nourishing hair and scalp, strong root of hair, make hair salubrious elegant submissive, be not in that scalp hardly possible is ventilative after hair washing, greasy thick and heavy phenomenon while can increase the gloss of hair again, gives people easily comfortable to feel.
Description
Technical field
The present invention relates to a kind of shampoo, and in particular to one kind is planted extraction without anti-corrosion ginger without silicone oil shampoo and its preparation side
Method.
Background technology
Shampoo refers to a kind of hair products with functions such as cleaning, anti-dandruff, treatment oil.With living standards of the people
Improve, to the quality requirement of shampoo also more and more higher, particularly plus the environmental pollution being on the rise, the fungi on scalp is got over
Come more, cause the various symptom of scalp, such as dandruff is excessive, and hair dries up, alopecia etc..At present, many natural materials have
Good hair-washing hair-care performance, has been used to wash during hair care applies some make up.Returned in modern cosmetics under the trend of the Nature, people
It is highly desirable have a kind of to human hair and scalp safety, and the hair care of washing for having certain effect applies some make up, therefore, will be natural
Material elite stoste is combined with modern chemical industry technology, and the natural hair washing shield cosmetics of exploitation will be natural hair-washing hair-care cosmetics from now on
The direction of development.
In order that hair is submissive in traditional shampoo, add the highly viscous silicon compound of some HMWs and serve as smooth
Agent, they can be adsorbed in each hair surface, form very smooth film.The silicon compound commonly used in current shampoo has poly-
Dimethyl siloxane, amido silicon oil, cyclomethicone etc., in hair-washing hair-care, these silicon-containing compounds can be between hair scale piece
Gap fill up, people can be allowed to think that hair sense of touch is very smooth, but be due to that silicone oil has water insoluble characteristic, be wrapped in head
Silicon on hair and scalp is less susceptible to be cleaned, and enrichment so year in year out, silicone oil can adsorb the meeting on hair
Cause that hair is thicker, hair weight becomes weight, reduce the electrostatic interaction of hair, hair gradually lost elasticity, produced disconnected hair, scalp
Clogging of pores, causes scalp oxygen flow not enough, papilla may gradually atrophy, scalp just start to occur it is withered and yellow, itch, or even alopecia
Phenomenon, and hair dry after generally seem it is flat collapse, it is not fluffy；Easily accumulation is viscous grey, greasy, clouding.And it is used for a long time
Siliceous oils product can be covered because of hair by silicone oil, and the real nutrition subsequently nursed cannot be introduced into and hair quality is deteriorated.
In addition, the use of preservative is extremely common in washing product, but excessive or inappropriate preservative can make table
Chrotoplast developmental immaturity, loosely organized, so that epidermis is thinning, easily by environmental stimuli, phylactic power defensive power declines, can damaging cells
DNA, makes skin follow the string gradually, easily produces relaxation, microgroove, and the Skin Cell damaged by preservative then can continuous defect
Breeding, makes skin quality worse and worse.So using for traditional preservatives is endangered so that existing washing product is badly in need of finding natural anticorrosion
Agent is seted out to no added preservative direction.
The content of the invention
It is an object of the invention to overcome prior art exist weak point and provide one kind plant extraction without anti-corrosion ginger without
Silicone oil shampoo and preparation method thereof.
To achieve the above object, the technical scheme taken of the present invention is：One kind is planted extraction without anti-corrosion ginger without silicone oil shampoo,
Characterized in that, including the preparing raw material of following weight percentage：Gingerol 0.1~5% and tax fat agent 0.4~6%；It is described
It is PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7 glyceryl cocoates to assign fat agent
Mixture.
Ginger is the new fresh quench stem of zingiber, warm-natured, containing gingerol, zingiberene, zingerone, gingerol etc. it is main into
Point, also containing several amino acids such as glutamic acid, asparatate, serine, glycine.For theory of traditional Chinese medical science, ginger is warm-natured,
Inducing diaphoresis is dissipated, and can increase local blood circulation, and hair follicle stimulating is opened, and promotes hair regeneration, therefore be a natural hair washing shield
Send out raw material.Scalp vein is stimulated after being put on the skin outside ginger liquid, strengthens local blood circulation, promotes the growth of hair.Gingerol, zingiberene oil
It can make skin of head blood circulation normalization, promote scalp metabolism, activate hair follicle tissue, it is effective anti-alopecia-stopping, white
Hair, stimulates kainogenesis long, and can suppress scalp pruritus, strengthens root of hair, the effects such as having cleaning scalp, remove dandruff.
The present invention is using PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7 glycerine
Cocounut oil acid esters substitute traditional silicone oil as fat agent is assigned, because traditional silicone oil is not dissolved in surfactant system, make for a long time
On the hair and not easy cleaning with easy absorption, makes hair gradually lose elasticity, produce disconnected hair, scalp clogging of pores is made for a long time
It is not enough into scalp oxygen flow, papilla may gradually atrophy, scalp just start to occur it is withered and yellow, itch, or even alopecia phenomenon, this hair
The bright tax fat agent is completely soluble in the surfactant system of shampoo, and the grease in their structure and skin
Composition all compares approximate, therefore correct leatherware has extraordinary nourish to lubricate, and hair can be made to wash rear salubrious submissive non-greasy, no
Have the gloss of obvious thick and heavy sense, softening hair and increase hair.Gingerol and the addition of cooperation according to the above ratio for assigning fat agent,
So that shampoo of the present invention can not only effectively cleaning and nourishing hair, make hair salubrious elegant submissive, correct pico-ampere completely without
Stimulate, moreover it is possible to strong root of hair, be especially used for a long time, the gloss of hair can be increased, give people easily comfortable sensation.
Preferably, the PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7 glycerine
The weight ratio of cocounut oil acid esters is：PPG-3 Octyl Ethers：12~13 carbon alcohol lactates：PEG-55 propylene glycol oleates：PEG-7 glycerine
Cocounut oil acid esters=1~10:1~10:1~10:1~10.Drawn through inventor's test of many times, tax fat agent of the invention is using above-mentioned
During proportioning, the submissive effect to hair is preferable.
Preferably, the shampoo also includes following preparing raw material：Preservative, hair conditioner, cation opsonizing agent, table
Face activating agent and thickener.
Preferably, the extraction of planting is without in preparing raw material of the anti-corrosion ginger without silicone oil shampoo, the weight hundred of the preservative
Point content is that the weight percentage of 0.01~1.5%, hair conditioner is the weight percent of 0.3~5%, cation opsonizing agent
Content is that the weight percentage of 0.3~3%, surfactant is 22~48% and the weight percentage of thickener is 0.01
~10%.
Preferably, the preservative is the mixing of decoyl hydroximic acid, parahydroxyacet-ophenone, the sad fat of glycerine and butanediol
Thing.
The use of preservative is extremely common in washing product, but excessive or inappropriate preservative can make epidermal cell
Developmental immaturity, loosely organized, so that epidermis is thinning, easily by environmental stimuli, phylactic power defensive power declines, and meeting damaging cells DNA makes skin
Skin is followed the string gradually, easily produces relaxation, microgroove, and the Skin Cell damaged by preservative constantly defect can then be bred, order
Skin quality is worse and worse.Preservative of the present invention is the mixed of decoyl hydroximic acid, parahydroxyacet-ophenone, the sad fat of glycerine and butanediol
Compound, more effective to mould, an unbounded quantity of to require, and excitant is low, and in shampoo of the present invention other raw materials phase
Capacitive is a kind of gentle preservative of efficient natural preferably.In addition, preservative of the present invention also has chelating Ca2+、Fe2+With
Fe3+Effect, it is possible to reduce the concentration of metal ion, reduce the infringement that traditional preservatives are brought to scalp.
Preferably, the hair conditioner is cocoyl glucoside, fibroin, the isostearic acid of dipentaerythritol four
At least one of ester, hydrolyzed wheat protein, Hydrolyzed Collagen and panthenol；It is highly preferred that the hair conditioner is hydrolysis
The mixture of wheat gluten, Hydrolyzed Collagen and panthenol；The weight of the hydrolyzed wheat protein, Hydrolyzed Collagen and panthenol
Than for：Hydrolyzed wheat protein：Hydrolyzed Collagen：Panthenol=1~5:1~5:1~4.
Hydrolyzed wheat protein and Hydrolyzed Collagen can supplement the lac nutrition being lost in for hair, make hair healthy
It is glossy.Application of the panthenol in shampoo, shows as the moisture-keeping functions lasting to hair, and it can wrap up hair, with moisten,
Moisturizing, it is smooth, bifurcated is reduced, prevents hair to be damaged, increases the density of hair, the effect of the gloss of hair quality is improved.Hydrolyzed wheat
Albumen, Hydrolyzed Collagen and panthenol fit applications according to the above ratio, can provide nutrition for hair, non-stimulated to scalp, be
Shampoo synergy of the present invention.
Preferably, the cation opsonizing agent is behenyl amido propyl dimethylamine, stearyl trimethyl ammonium chloride, soybean oil
At least one of base trimethyl ammonium chloride, behenyl base trimethyl ammonium chloride, cation guar gum and polyquaternium -7；More preferably
Ground, the cation opsonizing agent is the mixture of behenyl base trimethyl ammonium chloride, cation guar gum and polyquaternium -7；It is described
The weight ratio of behenyl base trimethyl ammonium chloride, cation guar gum and polyquaternium -7 is：Behenyl base trimethyl ammonium chloride：Sun from
Sub- guar gum：Polyquaternium -7=1~3:1~3:1~3.
Preferably, the thickener is in hydroxyethyl cellulose, cetanol, stearyl alcohol, carbomer, coconut oleoyl amine DEA
It is at least one；The surfactant is lauroyl both sexes base diethyl acid disodium, laruyl alcohol sulfosuccinate disodium, tallow fatty acid
At least one of sodium, laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and Cocoamidopropyl betaine；More preferably
Ground, the surfactant is the mixed of laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and Cocoamidopropyl betaine
Compound；The weight ratio of the laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and Cocoamidopropyl betaine is：Bay
Alcohol polyethers sodium sulfovinate：Laruyl alcohol sodium sulfovinate：Cocoamidopropyl betaine=3~5:2~3:1~2.
Surfactant used in the present invention is relatively mild surfactant, can mitigate hair washing to a certain extent
Stimulation of the water to scalp, reduces and hair is injured.
Preferably, the shampoo also includes the raw material of following weight percentage：Essence 0.01~1% and pH adjusting agent
0.1~1%；The pH adjusting agent is citric acid.
Preferably, the preparation method of the gingerol is：Ginger is cleaned, ground, is added in extractor, super face is carried out
Boundary's carbon dioxide abstraction, the temperature of extraction is 33 DEG C, and pressure is 7.52MPa, and extraction time is 10~15 minutes, and extraction terminates
Afterwards, decompression separation obtains gingerol.
At present, the main extracting method of gingerol is that alcohol extracting is followed the example of, and the extraction time that needs are followed the example of in alcohol extracting is relatively long, carries
Take number of times relatively many, and waste organic solvent, the risk of residual solvent, or even pollution environment are there may also be in extract,
Inefficiency.Gingerol is extracted using supercritical carbon dioxide extraction method in the present invention, relative to alcohol extracting and commonly
There is advantages below for water extraction method：1st, carbon dioxide chemistry stability is good, does not have the risk of residual solvent in extract；2、
It is colourless nonpoisonous and tasteless, it is free from environmental pollution；3rd, carbon dioxide can prevent gingerol to be oxidized, and use safety, efficiency high.Using upper
Stating the preparation method of gingerol can make the yield of gingerol reach 86.3%.
Present invention also offers a kind of above-mentioned plant extraction without preparation method of the anti-corrosion ginger without silicone oil shampoo, including following step
Suddenly：
(1) in the deionized water that, surfactant is added to 80~85 DEG C, it is well mixed, adds cation opsonizing agent,
It is well mixed, obtain component A；
(2) component A, is cooled to 55~60 DEG C, gingerol is added thereto, fat agent and cation opsonizing agent is assigned, mixing
Uniformly, component B is obtained；
(3) component B, is cooled to 40~45 DEG C, surfactant, hair conditioner, essence and anti-corrosion are added thereto
Agent, is well mixed, and adjusts pH value, adds thickener, adjusts to target viscosity, produces the extraction of planting and is washed without anti-corrosion ginger without silicone oil
Shampoo.
The beneficial effects of the present invention are：Extraction is planted without anti-corrosion ginger without silicone oil shampoo and its system the invention provides one kind
Preparation Method, shampoo of the present invention is used to have and releived scalp, mitigate the gingerol of scalp irritation and oxidation resistant effect with
Tax fat agent without silicone oil, with the use of raw materials such as non-stimulated preservative, hair conditioner, surfactants, reaches as raw material
To the overall mildness for improving shampoo, excitant of the cleansing to scalp is reduced.Shampoo of the present invention can be effectively
Cleaning and nourishing hair and scalp, strong root of hair make hair salubrious elegant submissive, and being not in that scalp is difficult after having one's hair wash breathes freely, greasy
Thick and heavy phenomenon, while can increase the gloss of hair again, gives people easily comfortable sensation.
Embodiment
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention
It is described further.
Embodiment 1
Extraction of the present invention of planting includes following weight percentage without a kind of embodiment of the anti-corrosion ginger without silicone oil shampoo
Preparing raw material：Gingerol 3%, tax fat agent 3%, preservative 1.2%, hair conditioner 2%, cation opsonizing agent 0.6%, table
Face activating agent 24%, thickener 2%, essence 0.6%, the deionized water of pH adjusting agent 0.1% and surplus；
The tax fat agent is that PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7 are sweet
The mixture of oil palm oleate, the PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7
The weight ratio of glyceryl cocoate is：PPG-3 Octyl Ethers：12~13 carbon alcohol lactates：PEG-55 propylene glycol oleates：PEG-7
Glyceryl cocoate=6:4:3:2.
The preservative is the mixture of decoyl hydroximic acid, parahydroxyacet-ophenone, the sad fat of glycerine and butanediol.
The hair conditioner is the mixture of hydrolyzed wheat protein, Hydrolyzed Collagen and panthenol；The hydrolyzed wheat
The weight ratio of albumen, Hydrolyzed Collagen and panthenol is：Hydrolyzed wheat protein：Hydrolyzed Collagen：Panthenol=1:1:2.
The cation opsonizing agent is the mixing of behenyl base trimethyl ammonium chloride, cation guar gum and polyquaternium -7
Thing；The weight ratio of the behenyl base trimethyl ammonium chloride, cation guar gum and polyquaternium -7 is：Behenyl base trimethyl ammonia chloride
Ammonium：Cation guar gum：Polyquaternium -7=1:1:1.
The surfactant is laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and cocamidopropyl propyl amide beet
Alkali；The weight ratio of the laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and Cocoamidopropyl betaine is：Laruyl alcohol
Polyethers sodium sulfovinate：Laruyl alcohol sodium sulfovinate：Cocoamidopropyl betaine=3:2:1；
The thickener is coconut oleoyl amine DEA；The pH adjusting agent is citric acid.
The preparation method of gingerol described in the present embodiment is：Ginger is cleaned, ground, is added in extractor, is surpassed
Critical carbon dioxide is extracted, and the temperature of extraction is 33 DEG C, and pressure is 7.52MPa, and extraction time is 10~15 minutes, and extraction terminates
Afterwards, decompression separation obtains gingerol.
Extraction is planted described in the present embodiment without preparation method of the anti-corrosion ginger without silicone oil shampoo, is comprised the following steps：
(1), laureth sodium sulfovinate and laruyl alcohol sodium sulfovinate are added in 80~85 DEG C of deionized water, mixing
Uniformly, behenyl base trimethyl ammonium chloride and cation guar gum are added, is well mixed, obtains component A；
(2) component A, is cooled to 55~60 DEG C, gingerol, PPG-3 Octyl Ethers, C12-13 alcohol lactic acid are added thereto
Ester, PEG-55 propylene glycol oleates, PEG-7 glyceryl cocoates and polyquaternium -7, are well mixed, obtain component B；
(3) component B, is cooled to 40~45 DEG C, thereto add Cocoamidopropyl betaine, hydrolyzed wheat protein,
Hydrolytic collagen, panthenol, essence and preservative, are well mixed, and adjust pH value, add thickener, adjust to target viscosity, produce institute
Plant extraction is stated without anti-corrosion ginger without silicone oil shampoo.
Embodiment 2
Extraction of the present invention of planting includes following weight percentage without a kind of embodiment of the anti-corrosion ginger without silicone oil shampoo
Preparing raw material：Gingerol 3%, tax fat agent 3%, preservative 1.2%, hair conditioner 2%, cation opsonizing agent 0.6%, table
Face activating agent 24%, thickener 2%, essence 0.6%, the deionized water of pH adjusting agent 0.1% and surplus；
The tax fat agent is that PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7 are sweet
The mixture of oil palm oleate, the PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7
The weight ratio of glyceryl cocoate is：PPG-3 Octyl Ethers：12~13 carbon alcohol lactates：PEG-55 propylene glycol oleates：PEG-7
Glyceryl cocoate=3:6:6:3.
The preservative is the mixture of decoyl hydroximic acid, parahydroxyacet-ophenone, the sad fat of glycerine and butanediol.
The hair conditioner is the mixture of hydrolyzed wheat protein, Hydrolyzed Collagen and panthenol；The hydrolyzed wheat
The weight ratio of albumen, Hydrolyzed Collagen and panthenol is：Hydrolyzed wheat protein：Hydrolyzed Collagen：Panthenol=1:1:2.
The cation opsonizing agent is the mixing of behenyl base trimethyl ammonium chloride, cation guar gum and polyquaternium -7
Thing；The weight ratio of the behenyl base trimethyl ammonium chloride, cation guar gum and polyquaternium -7 is：Behenyl base trimethyl ammonia chloride
Ammonium：Cation guar gum：Polyquaternium -7=1:1:1.
The surfactant is laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and cocamidopropyl propyl amide beet
Alkali；The weight ratio of the laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and Cocoamidopropyl betaine is：Laruyl alcohol
Polyethers sodium sulfovinate：Laruyl alcohol sodium sulfovinate：Cocoamidopropyl betaine=3:2:1；
The thickener is coconut oleoyl amine DEA；The pH adjusting agent is citric acid.
The preparation method of gingerol described in the present embodiment and plant extraction are without preparation side of the anti-corrosion ginger without silicone oil shampoo
Method is same as Example 1.
Embodiment 3
Extraction of the present invention of planting includes following weight percentage without a kind of embodiment of the anti-corrosion ginger without silicone oil shampoo
Preparing raw material：Gingerol 3%, tax fat agent 3%, preservative 1.2%, hair conditioner 2%, cation opsonizing agent 0.6%, table
Face activating agent 24%, thickener 2%, essence 0.6%, the deionized water of pH adjusting agent 0.1% and surplus；
The tax fat agent is that PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7 are sweet
The mixture of oil palm oleate, the PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7
The weight ratio of glyceryl cocoate is：PPG-3 Octyl Ethers：12~13 carbon alcohol lactates：PEG-55 propylene glycol oleates：PEG-7
Glyceryl cocoate=1:3:5:6.
The preservative is the mixture of decoyl hydroximic acid, parahydroxyacet-ophenone, the sad fat of glycerine and butanediol.
The hair conditioner is the mixture of hydrolyzed wheat protein, Hydrolyzed Collagen and panthenol；The hydrolyzed wheat
The weight ratio of albumen, Hydrolyzed Collagen and panthenol is：Hydrolyzed wheat protein：Hydrolyzed Collagen：Panthenol=1:1:2.
The cation opsonizing agent is the mixing of behenyl base trimethyl ammonium chloride, cation guar gum and polyquaternium -7
Thing；The weight ratio of the behenyl base trimethyl ammonium chloride, cation guar gum and polyquaternium -7 is：Behenyl base trimethyl ammonia chloride
Ammonium：Cation guar gum：Polyquaternium -7=1:1:1.
The surfactant is laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and cocamidopropyl propyl amide beet
Alkali；The weight ratio of the laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and Cocoamidopropyl betaine is：Laruyl alcohol
Polyethers sodium sulfovinate：Laruyl alcohol sodium sulfovinate：Cocoamidopropyl betaine=3:2:1；
The thickener is coconut oleoyl amine DEA；The pH adjusting agent is citric acid.
The preparation method of gingerol described in the present embodiment and plant extraction are without preparation side of the anti-corrosion ginger without silicone oil shampoo
Method is same as Example 1.
Embodiment 4
Extraction of the present invention of planting includes following weight percentage without a kind of embodiment of the anti-corrosion ginger without silicone oil shampoo
Preparing raw material：Gingerol 0.1%, tax fat agent 6%, preservative 0.01%, hair conditioner 0.3%, cation opsonizing agent
0.3%th, the deionized water of surfactant 48%, thickener 10%, essence 0.01%, pH adjusting agent 0.1% and surplus；
The tax fat agent is that PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7 are sweet
The mixture of oil palm oleate, the PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7
The weight ratio of glyceryl cocoate is：PPG-3 Octyl Ethers：12~13 carbon alcohol lactates：PEG-55 propylene glycol oleates：PEG-7
Glyceryl cocoate=4:1:1:1.
The preservative is the mixture of decoyl hydroximic acid, parahydroxyacet-ophenone, the sad fat of glycerine and butanediol.
The hair conditioner is the mixture of hydrolyzed wheat protein, Hydrolyzed Collagen and panthenol；The hydrolyzed wheat
The weight ratio of albumen, Hydrolyzed Collagen and panthenol is：Hydrolyzed wheat protein：Hydrolyzed Collagen：Panthenol=1:5:4.
The cation opsonizing agent is the mixing of behenyl base trimethyl ammonium chloride, cation guar gum and polyquaternium -7
Thing；The weight ratio of the behenyl base trimethyl ammonium chloride, cation guar gum and polyquaternium -7 is：Behenyl base trimethyl ammonia chloride
Ammonium：Cation guar gum：Polyquaternium -7=3:1:1.
The surfactant is laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and cocamidopropyl propyl amide beet
Alkali；The weight ratio of the laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and Cocoamidopropyl betaine is：Laruyl alcohol
Polyethers sodium sulfovinate：Laruyl alcohol sodium sulfovinate：Cocoamidopropyl betaine=5:3:2；
The thickener is coconut oleoyl amine DEA；The pH adjusting agent is citric acid.
The preparation method of gingerol described in the present embodiment and plant extraction are without preparation side of the anti-corrosion ginger without silicone oil shampoo
Method is same as Example 1.
Embodiment 5
Extraction of the present invention of planting includes following weight percentage without a kind of embodiment of the anti-corrosion ginger without silicone oil shampoo
Preparing raw material：Gingerol 5%, tax fat agent 0.4%, preservative 1.5%, hair conditioner 5%, cation opsonizing agent 3%, table
Face activating agent 22%, thickener 0.01%, essence 1%, the deionized water of pH adjusting agent 1% and surplus；
The tax fat agent is that PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7 are sweet
The mixture of oil palm oleate, the PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7
The weight ratio of glyceryl cocoate is：PPG-3 Octyl Ethers：12~13 carbon alcohol lactates：PEG-55 propylene glycol oleates：PEG-7
Glyceryl cocoate=10:1:1:1.
The preservative is the mixture of decoyl hydroximic acid, parahydroxyacet-ophenone, the sad fat of glycerine and butanediol.
The hair conditioner is the mixture of hydrolyzed wheat protein, Hydrolyzed Collagen and panthenol；The hydrolyzed wheat
The weight ratio of albumen, Hydrolyzed Collagen and panthenol is：Hydrolyzed wheat protein：Hydrolyzed Collagen：Panthenol=4:1:4.
The cation opsonizing agent is the mixing of behenyl base trimethyl ammonium chloride, cation guar gum and polyquaternium -7
Thing；The weight ratio of the behenyl base trimethyl ammonium chloride, cation guar gum and polyquaternium -7 is：Behenyl base trimethyl ammonia chloride
Ammonium：Cation guar gum：Polyquaternium -7=3:1:3.
The surfactant is laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and cocamidopropyl propyl amide beet
Alkali；The weight ratio of the laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and Cocoamidopropyl betaine is：Laruyl alcohol
Polyethers sodium sulfovinate：Laruyl alcohol sodium sulfovinate：Cocoamidopropyl betaine=5:2:2；
The thickener is coconut oleoyl amine DEA；The pH adjusting agent is citric acid.
The preparation method of gingerol described in the present embodiment and plant extraction are without preparation side of the anti-corrosion ginger without silicone oil shampoo
Method is same as Example 1.
Embodiment 6
Extraction of the present invention of planting includes following weight percentage without a kind of embodiment of the anti-corrosion ginger without silicone oil shampoo
Preparing raw material：Gingerol 4%, tax fat agent 0.4~6%, preservative 1%, hair conditioner 4%, cation opsonizing agent
0.5%th, the deionized water of surfactant 30%, thickener 5%, essence 0.5%, pH adjusting agent 0.1% and surplus；
The tax fat agent is that PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7 are sweet
The mixture of oil palm oleate, the PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7
The weight ratio of glyceryl cocoate is：PPG-3 Octyl Ethers：12~13 carbon alcohol lactates：PEG-55 propylene glycol oleates：PEG-7
Glyceryl cocoate=1~10:1~10:1~10:1~10.
The preservative is the mixture of decoyl hydroximic acid, parahydroxyacet-ophenone, the sad fat of glycerine and butanediol.
The hair conditioner is cocoyl glucoside.
The cation opsonizing agent is behenyl amido propyl dimethylamine.
The surfactant is laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and cocamidopropyl propyl amide beet
Alkali；The weight ratio of the laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate and Cocoamidopropyl betaine is：Laruyl alcohol
Polyethers sodium sulfovinate：Laruyl alcohol sodium sulfovinate：Cocoamidopropyl betaine=3:3:1；
The thickener is coconut oleoyl amine DEA；The pH adjusting agent is citric acid.
The preparation method of gingerol described in the present embodiment and plant extraction are without preparation side of the anti-corrosion ginger without silicone oil shampoo
Method is same as Example 1.
Embodiment 7
Extraction of the present invention of planting includes following weight percentage without a kind of embodiment of the anti-corrosion ginger without silicone oil shampoo
Preparing raw material：Gingerol 3%, tax fat agent 3%, preservative 1.2%, hair conditioner 2%, cation opsonizing agent 0.6%, table
Face activating agent 24%, thickener 2%, essence 0.6%, the deionized water of pH adjusting agent 0.1% and surplus；
The tax fat agent is that PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7 are sweet
The mixture of oil palm oleate, the PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7
The weight ratio of glyceryl cocoate is：PPG-3 Octyl Ethers：12~13 carbon alcohol lactates：PEG-55 propylene glycol oleates：PEG-7
Glyceryl cocoate=3:6:6:3.
The preservative is the mixture of decoyl hydroximic acid, parahydroxyacet-ophenone, the sad fat of glycerine and butanediol.
The hair conditioner is fibroin.
The cation opsonizing agent is stearyl trimethyl ammonium chloride.
The surfactant is lauroyl both sexes base diethyl acid disodium.
The thickener is hydroxyethyl cellulose；The pH adjusting agent is citric acid.
The preparation method of gingerol described in the present embodiment and plant extraction are without preparation side of the anti-corrosion ginger without silicone oil shampoo
Method is same as Example 1.
Embodiment 8
Plant in described in embodiment 1~7 is extracted without anti-corrosion ginger without silicone oil shampoo progress Physico-chemical tests, gained detection refers to
Mark is as follows：
1st, character is detected
It is that viscosity is suitable without silicone oil shampoo that extraction is planted described in embodiment 1~7 without anti-corrosion ginger, is had good stability, smell
Fragrance is charming, and silk profit is smooth, fine and smooth uniform ginger-colored shampoo.
2nd, pH value is detected
To planting extraction described in embodiment 1~7 without anti-corrosion ginger without silicone oil hair washing water sampling, determined with pH meter, measuring pH value is
5.5~6.5.
3rd, viscosity number is detected
To planting extraction described in embodiment 1~7 without anti-corrosion ginger without silicone oil hair washing water sampling, determined with viscosimeter, measure viscosity
Value 10000~12000.
4th, Detection of Stability
To planting extraction described in embodiment 1~7 without anti-corrosion ginger without silicone oil hair washing water sampling, it is encapsulated in transparence cosmetic bottle
In, be respectively placed in quartz lamp illumination, -15 DEG C, 5 DEG C, 25 DEG C, under 48 DEG C of experiment conditions, to outward appearance, fragrance, pH value, viscosity and
Sundry item carries out the continuance test of 3 months by a definite date, sees whether to occur bleed, layering, separation, precipitation, discoloration, peculiar smell, breaks
The bad phenomenons such as breast, testing result shows that the bad result of the above does not appear in the test of shampoo described in embodiment 1~7
Cheng Zhong, illustrates that it has good stability.
5th, centrifugation detection
To planting extraction described in embodiment 1~7 without anti-corrosion ginger without silicone oil hair washing water sampling, it is encapsulated in centrifuge tube
30min is centrifuged under 3000r/min, sees whether not dispersion component occur, testing result shows, shampoo described in embodiment 1~7
Do not occur not dispersion component, illustrate that its Combination is good.
6th, anaphylaxis is stimulated to detect
To planting extraction described in embodiment 1~7 without anti-corrosion ginger without silicone oil hair washing water sampling, it is applied to 30 age brackets in right amount
On 18-58 Sui volunteer's the back of the hand, to observe 30min, see whether it the phenomenons such as redness, dermexanthesis, foaming occurs, observe result table
Bright, all volunteers do not occur above-mentioned ill symptomses in 30min, and illustrating that this product will not be produced to skin stimulates and anaphylaxis
Problem.
7th, comprehensive using effect detection
Using opinion poll point system, the sample of six case study on implementation is tried out respectively by asking volunteer, and fill on probation
Table carrys out overall merit its using effect.Every group of embodiment sample chooses 100 (age levels of volunteer in all ages and classes stage
The volunteer 50 of volunteer 50 and 38~58 age levels for 18-38) as object on probation, wash hair once within every two days,
It is continuous to use three months, fill in table on probation after trying out and scored.Every using effect total score is 5 points in grade form：5 points are most
High score, is represented very satisfied；4 points are preferable, are relatively satisfied with；3 points are to receive；Less than 3 points cannot receive
Scope, every using effect average situation is as shown in table 1.
Extraction is planted described in the embodiment 1~7 of table 1 without anti-corrosion ginger without the every using effect average situation of silicone oil shampoo
Test result as shown in table 1, as a result shows：Shampoo of the ginger without silicone oil is not only stingless described in embodiment 1~7
Swash, and foaming abundancy, with deep clean, hair is lubricated, effect of scalp is takeed good care of, long-term use can cause hair clearly soft
Slided along silk, gloss is beautiful, and the use feedback effects of wherein embodiment 1 are optimal.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than the present invention is protected
The limitation of scope is protected, although being explained in detail with reference to preferred embodiment to the present invention, one of ordinary skill in the art should
Understand, technical scheme can be modified or equivalent substitution, without departing from the essence of technical solution of the present invention
And scope.
Claims (10)
1. one kind is planted extraction without anti-corrosion ginger without silicone oil shampoo, it is characterised in that the preparation comprising following weight percentage is former
Material：Gingerol 0.1~5% and tax fat agent 0.4~6%；The tax fat agent be PPG-3 Octyl Ethers, 12~13 carbon alcohol lactates,
The mixture of PEG-55 propylene glycol oleates and PEG-7 glyceryl cocoates.
2. extraction is planted as claimed in claim 1 without anti-corrosion ginger without silicone oil shampoo, it is characterised in that the PPG-3 Octyl Ethers, 12
The weight ratio of~13 carbon alcohol lactates, PEG-55 propylene glycol oleates and PEG-7 glyceryl cocoates is：PPG-3 Octyl Ethers：12
~13 carbon alcohol lactates：PEG-55 propylene glycol oleates：PEG-7 glyceryl cocoate=1~10:1~10:1~10:1~10.
3. extraction is planted as claimed in claim 1 or 2 without anti-corrosion ginger without silicone oil shampoo, it is characterised in that the shampoo is also wrapped
Containing following preparing raw material：Preservative, hair conditioner, cation opsonizing agent, surfactant and thickener.
4. extraction is planted as claimed in claim 3 without anti-corrosion ginger without silicone oil shampoo, it is characterised in that the plant extraction is without anti-corrosion ginger
In preparing raw material without silicone oil shampoo, the weight percentage of the preservative is 0.01~1.5%, hair conditioner
Weight percentage in the feed is that 0.3~5%, weight percentage of the cation opsonizing agent is 0.3~3%, institute
The weight percentage for stating surfactant is 22~48% and the weight percentage of the thickener is 0.01~10%.
5. extraction is planted as claimed in claim 4 without anti-corrosion ginger without silicone oil shampoo, it is characterised in that the preservative is decoyl hydroxyl
The mixture of the sad fat of oxime acid, parahydroxyacet-ophenone, glycerine and butanediol.
6. extraction is planted as claimed in claim 4 without anti-corrosion ginger without silicone oil shampoo, it is characterised in that the hair conditioner is coconut palm
Oil base glucoside, fibroin, dipentaerythritol pentaerythritol tetraisostearate, hydrolyzed wheat protein, Hydrolyzed Collagen and panthenol
At least one of；Preferably, the hair conditioner is the mixture of hydrolyzed wheat protein, Hydrolyzed Collagen and panthenol；
The weight ratio of the hydrolyzed wheat protein, Hydrolyzed Collagen and panthenol is：Hydrolyzed wheat protein：Hydrolyzed Collagen：Panthenol
=1~5:1~5:1~4.
7. extraction is planted as claimed in claim 4 without anti-corrosion ginger without silicone oil shampoo, it is characterised in that the cation opsonizing agent is
Behenyl amido propyl dimethylamine, stearyl trimethyl ammonium chloride, soybean oil base trimethyl ammonium chloride, behenyl base trimethyl ammonia chloride
At least one of ammonium, cation guar gum and polyquaternium -7；Preferably, the cation opsonizing agent is behenyl base trimethyl
The mixture of ammonium chloride, cation guar gum and polyquaternium -7；The behenyl base trimethyl ammonium chloride, cation guar gum and
The weight ratio of polyquaternium -7 is：Behenyl base trimethyl ammonium chloride：Cation guar gum：Polyquaternium -7=1~3:1~3:1
~3.
8. extraction is planted as claimed in claim 4 without anti-corrosion ginger without silicone oil shampoo, it is characterised in that the thickener is ethoxy
At least one of cellulose, cetanol, stearyl alcohol, carbomer, coconut oleoyl amine DEA；The surfactant is lauroyl two
Property base diethyl acid disodium, laruyl alcohol sulfosuccinate disodium, tallow fatty acid sodium, laureth sodium sulfovinate, laruyl alcohol sulfuric acid
At least one of ester sodium and Cocoamidopropyl betaine；Preferably, the surfactant is laureth sulfuric ester
The mixture of sodium, laruyl alcohol sodium sulfovinate and Cocoamidopropyl betaine；The laureth sodium sulfovinate, laruyl alcohol sulphur
The weight ratio of acid esters sodium and Cocoamidopropyl betaine is：Laureth sodium sulfovinate：Laruyl alcohol sodium sulfovinate：Cocounut oil acyl
Amine CAB=3~5:2~3:1~2.
9. extraction is planted as claimed in claim 1 without anti-corrosion ginger without silicone oil shampoo, it is characterised in that the preparation side of the gingerol
Method is：Ginger is cleaned, ground, is added in extractor, supercritical carbon dioxide extracting is carried out, the temperature of extraction is 33 DEG C,
Pressure is 7.52MPa, and extraction time is 10~15 minutes, and after extraction terminates, decompression separation obtains gingerol.
10. a kind of planted as any one of claim 1~9 extracts without preparation method of the anti-corrosion ginger without silicone oil shampoo, its
It is characterised by, comprises the following steps：
(1) in the deionized water that, surfactant is added to 80~85 DEG C, it is well mixed, adds cation opsonizing agent, mixes
Uniformly, component A is obtained；
(2) component A, is cooled to 55~60 DEG C, gingerol is added thereto, fat agent and cation opsonizing agent is assigned, is well mixed,
Obtain component B；
(3) component B, is cooled to 40~45 DEG C, surfactant, hair conditioner, essence and preservative are added thereto, is mixed
Close uniformly, adjust pH value, add thickener, adjust to target viscosity, produce described plant and extract without anti-corrosion ginger without silicone oil shampoo.
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| CN201710332913.7A CN107184406A (en) | 2017-05-11 | 2017-05-11 | One kind is planted extraction without anti-corrosion ginger without silicone oil shampoo and preparation method thereof |
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| CN108685810A (en) * | 2018-06-26 | 2018-10-23 | 深圳黛盛贸易有限公司 | A kind of pure ginger maintenance leaves shampoo and its manufacture craft |
| CN112807251A (en) * | 2021-01-15 | 2021-05-18 | 杭州心悦化妆品有限公司 | Silicone-oil-free shampoo with scalp care effect and preparation process thereof |
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| CN108685810A (en) * | 2018-06-26 | 2018-10-23 | 深圳黛盛贸易有限公司 | A kind of pure ginger maintenance leaves shampoo and its manufacture craft |
| CN112807251A (en) * | 2021-01-15 | 2021-05-18 | 杭州心悦化妆品有限公司 | Silicone-oil-free shampoo with scalp care effect and preparation process thereof |
| WO2023232366A1 (en) * | 2022-06-01 | 2023-12-07 | Beiersdorf Ag | Emulsion with glyceryl caprylate and at least one ppg alkyl ether |
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Application publication date: 20170922 |