CN112807251A - Silicone-oil-free shampoo with scalp care effect and preparation process thereof - Google Patents
Silicone-oil-free shampoo with scalp care effect and preparation process thereof Download PDFInfo
- Publication number
- CN112807251A CN112807251A CN202110057472.0A CN202110057472A CN112807251A CN 112807251 A CN112807251 A CN 112807251A CN 202110057472 A CN202110057472 A CN 202110057472A CN 112807251 A CN112807251 A CN 112807251A
- Authority
- CN
- China
- Prior art keywords
- water
- extract
- conditioner containing
- butanediol
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/522—Antioxidants; Radical scavengers
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the technical field of daily cosmetics, in particular to silicone oil-free shampoo with a scalp care effect and a preparation process thereof. The method comprises the following raw materials: water, anionic surfactant, amphoteric surfactant, olive oil PEG-7 esters, polyquaternium-7, PEG-7 glycerol cocoate, decyl glucoside, conditioner, glycerol, PEG-40 hydrogenated castor oil, daily essence, and antiseptic. The silicone-oil-free shampoo prepared by the invention has strong dirt-removing power, is fine and rich in foam, has a good nursing effect on head skin, can nourish the head skin, prevent hair from drying, can promote metabolism of scalp cells, prevent scalp from aging, promote hair growth, strengthen hair roots and make hair soft and smooth.
Description
Technical Field
The invention relates to the technical field of daily cosmetics, in particular to silicone oil-free shampoo with a scalp care effect and a preparation process thereof.
Background
Shampoo is a hair washing product which is most widely used, and is one of the most commonly used hair cosmetics, and is used for washing off human body secreted oil, sweat stain, cells detached from the scalp, foreign dust, microorganisms, residues of styling products, bad smell and the like which are attached to the scalp and hair, and keeping the scalp and hair clean and beautiful. Shampoo in the market appears in various forms, and in recent years, shampoo without silicone oil has higher heat. Silicone-free shampoos are shampoos that are free of silicones (e.g., dimethicone, dimethiconol, amodimethicone, phenyl trimethicone, etc.). Silicone oil deposits on hair, causing collapse of the hair and greatly diminishing the visual effect of the hair volume, which can be avoided by using a silicone oil-free shampoo. For people with little hair, soft hair or easy oil and sensitivity of scalp, the shampoo without silicone oil is recommended, so that the hair can be fluffy, the hair looks more and the scalp can be fresher.
The silicone-free shampoo washes hair to the most original ecology, separates scalp care and hair care, and then uses a care product to care the scalp. In order to solve the problem, a silicone oil-free shampoo with a scalp care effect is needed, which can reduce the number of care steps and can well care the scalp and the hair.
Disclosure of Invention
The first object of the present invention is to provide a silicone-free shampoo having a scalp care effect, which is capable of caring a scalp while cleaning hair. The invention also aims to provide a preparation process of the silicone oil-free shampoo with the scalp care effect.
The silicone oil-free shampoo with the scalp care effect provided by the invention comprises the following raw materials: water, an anionic surfactant, an amphoteric surfactant, olive oil PEG-7 esters, polyquaternium-7, PEG-7 glyceryl cocoate, decyl glucoside, a conditioner containing a calendula extract, a conditioner containing soluble proteoglycan, a conditioner containing a brown algae extract, a conditioner containing hydrolyzed wheat protein, a conditioner containing hydrolyzed keratin, a conditioner containing a lotus flower extract, a conditioner containing a bisque flower extract, a conditioner containing a purslane extract, a conditioner containing chamomile flower water, a conditioner containing lavender flower water, glycerol, PEG-40 hydrogenated castor oil, essence for daily use and a preservative.
Preferably, the conditioning agent containing the calendula extract is a mixture of water, butanediol and the calendula extract, wherein the mass ratio of the water to the butanediol to the calendula extract is 77.5: 20: 2.5-77: 20: 3, more preferably 77.5: 20: 2.5;
the conditioner containing soluble proteoglycan is a mixture of water, butanediol and soluble proteoglycan, wherein the mass ratio of the water to the butanediol to the soluble proteoglycan is 77.5: 20: 2.5-77: 20: 3, more preferably 77.5: 20: 2.5;
the conditioning agent containing the brown algae extract is a mixture of water, butanediol and the brown algae extract, wherein the mass ratio of the water to the butanediol to the brown algae extract is 77.5: 20: 2.5-77: 20: 3, more preferably 77.5: 20: 2.5;
the conditioner containing hydrolyzed wheat protein is a mixture of water, butanediol and hydrolyzed wheat protein, wherein the mass ratio of the water to the butanediol to the hydrolyzed wheat protein is 77.5: 20: 2.5-77: 20: 3, more preferably 77.5: 20: 2.5;
the conditioner containing the hydrolyzed keratin is a mixture of water, butanediol and hydrolyzed keratin, wherein the mass ratio of the water to the butanediol to the hydrolyzed keratin is 77.5: 20: 2.5-77: 20: 3, more preferably 77.5: 20: 2.5;
the conditioning agent containing the lotus extract is a mixture of water, butanediol and the lotus extract, wherein the mass ratio of the water to the butanediol to the lotus extract is 77.5: 20: 2.5-77: 20: 3, more preferably 77.5: 20: 2.5;
the conditioner containing the extract of the vegetarian square flower is a mixture of water, 1, 2-hexanediol, p-hydroxyacetophenone and the extract of the vegetarian square flower, wherein the mass ratio of the water to the 1, 2-hexanediol to the p-hydroxyacetophenone to the extract of the vegetarian square flower is 91.75: 0.75: 0.75: 6.75-91.5: 0.75: 0.75: 7, more preferably 91.75: 0.75: 0.75: 6.75;
the conditioning agent containing the purslane extract is a mixture of water, butanediol, 1, 2-hexanediol and the purslane extract, wherein the mass ratio of the water, the butanediol, the 1, 2-hexanediol and the purslane extract is 58: 10: 2: 30-56: 10: 2: 32, more preferably 58: 10: 2: 30, of a nitrogen-containing gas;
the conditioner containing the water of the chamomile is a mixture of water, butanediol and the water of the chamomile, wherein the mass ratio of the water to the butanediol to the water of the chamomile is 75: 20: 5-73: 20: 7, more preferably 75: 20: 5;
the conditioner containing the lavender flower water is a mixture of water, butanediol and the lavender flower water, wherein the mass ratio of the water to the butanediol to the chamomile flower water is 75: 20: 5-72: 20: 8, more preferably 75: 20: 5.
preferably, the preservative is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium chloride, magnesium nitrate and water, wherein the mass ratio of the methylchloroisothiazolinone, the methylisothiazolinone, the magnesium chloride, the magnesium nitrate and the water is 1.12: 0.36: 0.75: 22.5: 75.27-0.9: 0.3: 0.75: 22.5: 75.55. the invention adopts the methyl chloro isothiazolinone, methyl isothiazolinone, magnesium chloride, magnesium nitrate and water to be mixed as the preservative, has good heat-resisting stability and is safe and reliable in the shampoo without silicone oil.
Preferably, the anionic surfactant is a mixed anionic surfactant of sodium laureth sulfate and water in a mass ratio of 70:30-75:25, more preferably 70: 30; the amphoteric surfactant is prepared by mixing lauramidopropyl betaine and water at a mass ratio of 30:70-35:65, and preferably 30: 70. The lauramidopropyl betaine has excellent performance and extremely low irritation, is compatible with the anionic surfactant sodium lauryl polyether sulfate, has ideal washing, conditioning and antistatic effects, has excellent softness, mild effect on skin, abundant and stable foam, and has good viscosity regulating effect.
Preferably, the feed is prepared from the following raw materials in percentage by mass: 50-60% of water, 15-20% of anionic surfactant, 15-20% of amphoteric surfactant, 5-10% of olive oil PEG-7 esters, 0.0001-5% of polyquaternium-70.0001, 0.0001-5% of PEG-7 glyceryl cocoate, 1-2% of decyl glucoside, 0.0001-1% of conditioning agent containing calendula extract, 0.0001-1% of conditioning agent containing soluble protein polysaccharide, 0.0001-1% of conditioning agent containing brown algae extract, 0.0001-1% of conditioning agent containing hydrolyzed wheat protein, 0.0001-1% of conditioning agent containing hydrolyzed keratin, 0.0001-1% of conditioning agent containing lotus flower extract, 0.0001-1% of conditioning agent containing bisque flower extract, 0.0001-1% of conditioning agent containing purslane extract, 0.0001-1% of conditioning agent containing chamomile water, and the like, 0.0001-1% of conditioner containing lavender flower water, 0.0001-1% of glycerin, 0.0001-1% of PEG-40 hydrogenated castor oil, 0.0001-1% of daily essence and 0.0001-1% of preservative.
The invention provides a preparation process of silicone oil-free shampoo with scalp care effect, which comprises the following steps:
(1) adding water and an anionic surfactant into a reaction kettle, heating, and uniformly stirring;
(2) then adding amphoteric surfactant, stirring well, adding oleum Olivarum PEG-7 esters, polyquaternium-7, PEG-7 glyceryl cocoate, decyl glucoside and glycerol, and stirring well;
(3) cooling, adding uniformly mixed PEG-40 hydrogenated castor oil and daily essence, then adding a conditioner containing a calendula extract, a conditioner containing soluble proteoglycan, a conditioner containing a brown algae extract, a conditioner containing hydrolyzed wheat protein, a conditioner containing hydrolyzed keratin, a conditioner containing a lotus flower extract, a conditioner containing a vegetarian square flower extract, a conditioner containing a purslane extract, a conditioner containing chamomile flower water, a conditioner containing lavender flower water and a preservative, and uniformly stirring;
(4) cooling again, and filtering to obtain the silicone oil-free shampoo with scalp care effect.
Preferably, the temperature of heating in the step (1) is 60-80 ℃.
Preferably, the temperature in the step (3) is reduced to 45-50 ℃.
Preferably, the step (4) is: cooling to 35-40 deg.C, and filtering with 80-100 mesh filter screen to obtain shampoo without silicone oil for caring scalp.
Preferably, the stirring speed in the step (1) is 300-500rpm, and the stirring time is 30-40 minutes; the stirring speed in the step (2) is 300-500rpm, and the stirring time is 20-30 minutes; the stirring speed in the step (3) is 300-500rpm, and the stirring time is 15-20 minutes.
More preferably, the method comprises the following steps:
(1) adding water and an anionic surfactant into a reaction kettle, starting stirring, heating to 70 ℃, and stirring until the water and the anionic surfactant are completely dissolved;
(2) adding the amphoteric surfactant into a reaction kettle, stirring until the amphoteric surfactant is completely dissolved, continuously adding the olive oil PEG-7 esters, the polyquaternium-7, the PEG-7 glyceryl cocoate, the decyl glucoside and the glycerin into the reaction kettle, and stirring until the amphoteric surfactant is completely dissolved;
(3) cooling the reaction kettle to 45 ℃, taking a proper clean container, uniformly mixing PEG-40 hydrogenated castor oil and daily essence, adding the mixture into the reaction kettle, continuously adding a conditioner containing calendula officinalis extract, a conditioner containing soluble proteoglycan, a conditioner containing brown algae extract, a conditioner containing hydrolyzed wheat protein, a conditioner containing hydrolyzed keratin, a conditioner containing lotus flower extract, a conditioner containing vegetarian square flower extract, a conditioner containing purslane extract, a conditioner containing chamomile water, a conditioner containing lavender water and a preservative into the reaction kettle, and stirring until the materials are completely dissolved;
(4) cooling to 37 ℃, sampling, conveying to a product pipe for detection, filtering and discharging by using a 80-100 mesh filter screen after the product pipe is detected to be qualified, and obtaining the silicone oil-free shampoo with the scalp care effect.
In order to increase the softness and smoothness of the hair, olive oil PEG-7 esters are added into the prepared silicone-free shampoo, the olive oil PEG-7 esters have good compatibility, and are compounded with surfactants of lauramidopropyl betaine, sodium laureth sulfate, polyquaternium-7, decyl glucoside and PEG-40 hydrogenated castor oil, so that the hair is softer and smoother.
In order to maintain the oil balance of skin and hair and moisten scalp, PEG-7 glyceryl cocoate is added into the prepared silicone-free shampoo, and the PEG-7 glyceryl cocoate is a hydrophilic emollient ester prepared by the reaction of natural oil and ethylene oxide. The product can maintain oil balance of skin and hair, reduce dryness, increase lubrication feeling of skin and hair, has good skin permeability, and has effects of caring head skin and moistening skin.
In order to enable the prepared silicone-oil-free shampoo to have rich and fine foam, decyl glucoside is added into the shampoo, and the decyl glucoside has the characteristics of stability, nontoxicity, solubility, easiness in biodegradation, low irritation to skin and the like, has an obvious synergistic effect when being compounded with sodium laureth sulfate, lauramidopropyl betaine and PEG-40 hydrogenated castor oil, can increase the surface activity and viscosity of the shampoo, improves the decontamination capability of the silicone-oil-free shampoo, and enables the prepared silicone-oil-free shampoo to have rich, fine and stable foam.
In order to improve the metabolism of the head skin and inhibit the aging of the head skin, a conditioner containing a calendula extract, a conditioner containing a brown algae extract, a conditioner containing a vegetarian square flower extract, a conditioner containing a lotus flower extract and a conditioner containing lavender flower water are added into the prepared silicone-free shampoo, and the conditioners are mixed to remove free radicals in cells, prevent the aging of the head skin, improve the cell activity of the head skin, promote the growth of hair and strengthen hair roots.
In order to better nourish the head skin and prevent the hair from drying, a conditioner containing soluble proteoglycan, a conditioner containing hydrolyzed wheat protein and glycerin are added into the shampoo without silicone oil, and the components are mixed for use, so that water molecules in the air can be adsorbed, a good moisturizing effect can be achieved, the head skin is nourished, the dandruff is reduced, and the hair is prevented from drying.
In order to better care the skin of the head, a conditioner containing a purslane extract and a conditioner containing a chrysanthemum water of the spring white chrysanthemum are added into the prepared silicone-free shampoo, and the conditioner containing the purslane extract and the conditioner containing the chrysanthemum water of the spring white chrysanthemum are mixed with the conditioner containing the calendula extract for use, so that the shampoo has a good sterilization effect, improves the sensitive skin and prevents the inflammation of the skin of the head.
The polyquaternium-7 can greatly improve the modifiability and the conditioning property of hair, the hair can be bright, smooth and easy to comb after being washed, the hair has good wet-processing, dry-combing and entanglement resistance, the compatibility with other components in the silicone oil-free shampoo prepared by the invention is good, and the prepared silicone oil-free shampoo does not generate turbidity, precipitation and layering phenomena.
Therefore, in summary, the present invention has the following advantages:
(1) the silicone-oil-free shampoo prepared by the invention has strong dirt-removing power, is fine and rich in foam, has a good nursing effect on head skin, can nourish the head skin, prevent hair from drying, can promote metabolism of scalp cells, prevent scalp from aging, promote hair growth, strengthen hair roots and make hair soft and smooth.
(2) According to the invention, the olive oil PEG-7 esters added into the silicone-oil-free shampoo are compounded with surfactants of lauramidopropyl betaine, sodium laureth sulfate, decyl glucoside and PEG-40 hydrogenated castor oil, so that the hair is softer and smoother.
(3) The decyl glucoside lauryl polyether sodium sulfate, lauramidopropyl betaine and PEG-40 hydrogenated castor oil added into the silicone oil-free shampoo prepared by the invention are compounded, so that the obvious synergistic effect is achieved, the surface activity and viscosity of the shampoo can be increased, the decontamination capability of the silicone oil-free shampoo is improved, and the foam is rich and fine.
(4) The conditioner containing the calendula extract, the conditioner containing the brown algae extract, the conditioner containing the vegetarian fanghua extract, the conditioner containing the lotus flower extract and the conditioner containing the lavender flower water which are added into the silicone-oil-free shampoo are mixed, so that free radicals in cells can be eliminated, the aging of head skin is prevented, the cell activity of the head skin is improved, the growth of hair is promoted, and hair roots are stronger.
(5) The conditioner containing soluble proteoglycan, the conditioner containing hydrolyzed wheat protein and glycerin which are added into the silicone-oil-free shampoo can better nourish the skin of the head, prevent the hair from drying, play a good role in moisturizing and nourish the skin of the head.
Detailed Description
It should be noted that the following detailed description is exemplary and is intended to provide further explanation of the disclosure. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this application belongs.
It is noted that the terminology used herein is for the purpose of describing particular embodiments only and is not intended to be limiting of example embodiments according to the present application. As used herein, the singular forms also include the plural forms unless the context clearly dictates otherwise, and further, it is understood that when the terms "comprises" and/or "comprising" are used in this specification, they specify the presence of the stated features, steps, operations, devices, components, and/or combinations thereof.
The technical solutions of the present invention will be described clearly and completely with reference to the following embodiments, and it should be understood that the described embodiments are some, but not all, embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The silicone-oil-free shampoo with the scalp care effect comprises the following raw materials in parts by mass: 60% of water, 15% of anionic surfactant, 15% of amphoteric surfactant, 5% of olive oil PEG-7 esters, 70.5% of polyquaternium, 0.5% of PEG-7 glyceryl cocoate, 1% of decyl glucoside, 0.2% of conditioner containing calendula extract, 0.2% of conditioner containing soluble proteoglycan, 0.2% of conditioner containing brown algae extract, 0.2% of conditioner containing hydrolyzed wheat protein, 0.3% of conditioner containing hydrolyzed keratin, 0.2% of conditioner containing lotus extract, 0.2% of conditioner containing vegetarian square flower extract, 0.2% of conditioner containing purslane extract, 0.3% of conditioner containing chamomile water, 0.2% of conditioner containing lavender flower water, 0.2% of glycerol, 0.4% of PEG-40 hydrogenated castor oil, 0.1% of daily essence and 0.1% of preservative. The conditioning agent containing the calendula extract is a mixture of water, butanediol and the calendula extract, wherein the mass ratio of the water to the butanediol to the calendula extract is 77.5: 20: 2.5; the conditioner containing soluble proteoglycan is a mixture of water, butanediol and soluble proteoglycan, wherein the mass ratio of the water to the butanediol to the soluble proteoglycan is 77.5: 20: 2.5; the conditioning agent containing the brown algae extract is a mixture of water, butanediol and the brown algae extract, wherein the mass ratio of the water to the butanediol to the brown algae extract is 77.5: 20: 2.5; the conditioner containing hydrolyzed wheat protein is a mixture of water, butanediol and hydrolyzed wheat protein, wherein the mass ratio of the water to the butanediol to the hydrolyzed wheat protein is 77.5: 20: 2.5; the conditioner containing the hydrolyzed keratin is a mixture of water, butanediol and hydrolyzed keratin, wherein the mass ratio of the water to the butanediol to the hydrolyzed keratin is 77.5: 20: 2.5; the conditioning agent containing the lotus extract is a mixture of water, butanediol and the lotus extract, wherein the mass ratio of the water to the butanediol to the lotus extract is 77.5: 20: 2.5; the conditioner containing the extract of the vegetarian square flower is a mixture of water, 1, 2-hexanediol, p-hydroxyacetophenone and the extract of the vegetarian square flower, wherein the mass ratio of the water to the 1, 2-hexanediol to the p-hydroxyacetophenone to the extract of the vegetarian square flower is 91.75: 0.75: 0.75: 6.75; the conditioning agent containing the purslane extract is a mixture of water, butanediol, 1, 2-hexanediol and the purslane extract, wherein the mass ratio of the water, the butanediol, the 1, 2-hexanediol and the purslane extract is 58: 10: 2: 30, of a nitrogen-containing gas; the conditioner containing the water of the chamomile is a mixture of water, butanediol and the water of the chamomile, wherein the mass ratio of the water to the butanediol to the water of the chamomile is 75: 20: 5; the conditioner containing the lavender flower water is a mixture of water, butanediol and the lavender flower water, wherein the mass ratio of the water to the butanediol to the lavender flower water is 75: 20: 5. the preservative is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium chloride, magnesium nitrate and water, wherein the mass ratio of the methylchloroisothiazolinone, the methylisothiazolinone, the magnesium chloride, the magnesium nitrate and the water is 0.9: 0.3: 0.75: 22.5: 75.55. the anionic surfactant is an anionic surfactant formed by mixing sodium laureth sulfate and water according to a mass ratio of 70:30, and the amphoteric surfactant is an amphoteric surfactant formed by mixing lauramidopropyl betaine and water according to a mass ratio of 30: 70.
A preparation process of silicone oil-free shampoo with a scalp care effect comprises the following steps:
(1) adding water and anionic surfactant into a reaction kettle, heating to 70 ℃, stirring for 30 minutes at 500rmp to completely dissolve the raw materials;
(2) adding an amphoteric surfactant into a reaction pot, stirring for 20 minutes at 500rmp, then continuously adding olive oil PEG-7 esters, polyquaternium-7, PEG-7 glycerol cocoate, decyl glucoside and glycerol into the reaction pot, and stirring for 20 minutes at 500rmp to completely dissolve the raw materials;
(3) cooling the reaction kettle to 45 ℃, taking a proper clean container, uniformly mixing PEG-40 hydrogenated castor oil and daily essence, adding the mixture into the reaction kettle, continuously adding a conditioner containing calendula officinalis extract, a conditioner containing soluble proteoglycan, a conditioner containing brown algae extract, a conditioner containing hydrolyzed wheat protein, a conditioner containing hydrolyzed keratin, a conditioner containing lotus flower extract, a conditioner containing vegetarian fanninghamia extract, a conditioner containing purslane extract, a conditioner containing chamomile water, a conditioner containing lavender water and a preservative into the reaction kettle, and stirring for 15 minutes at 500rmp to completely dissolve the raw materials;
(4) and cooling to 37 ℃, sampling, conveying to a sample tube for detection, filtering and discharging by using a 100-mesh filter screen after the sample tube is detected to be qualified, and thus obtaining the silicone-oil-free shampoo with the scalp care effect.
Example 2
The silicone-oil-free shampoo with the scalp care effect comprises the following raw materials in parts by mass: 50% of water, 20% of anionic surfactant, 15% of amphoteric surfactant, 6% of olive oil PEG-7 esters, 75% of polyquaternary ammonium salt, 1% of PEG-7 glyceryl cocoate, 1.5% of decyl glucoside, 0.1% of a conditioner containing calendula extract, 0.1% of a conditioner containing soluble proteoglycan, 0.1% of a conditioner containing brown algae extract, 0.1% of a conditioner containing hydrolyzed wheat protein, 0.1% of a conditioner containing hydrolyzed keratin, 0.1% of a conditioner containing lotus extract, 0.1% of a conditioner containing vegetarian square flower extract, 0.1% of a conditioner containing purslane extract, 0.1% of a conditioner containing chamomile flower water, 0.1% of a conditioner containing lavender flower water, 0.1% of glycerin, 0.2% of PEG-40 hydrogenated castor oil, 0.1% of daily essence and 0.1% of preservative. The conditioning agent containing the calendula extract is a mixture of water, butanediol and the calendula extract, wherein the mass ratio of the water to the butanediol to the calendula extract is 77: 20: 3; the conditioner containing soluble proteoglycan is a mixture of water, butanediol and soluble proteoglycan, wherein the mass ratio of the water to the butanediol to the soluble proteoglycan is 77: 20: 3; the conditioning agent containing the brown algae extract is a mixture of water, butanediol and the brown algae extract, wherein the mass ratio of the water to the butanediol to the brown algae extract is 77: 20: 3; the conditioner containing hydrolyzed wheat protein is a mixture of water, butanediol and hydrolyzed wheat protein, wherein the mass ratio of the water to the butanediol to the hydrolyzed wheat protein is 77: 20: 3; the conditioner containing the hydrolyzed keratin is a mixture of water, butanediol and hydrolyzed keratin, wherein the mass ratio of the water to the butanediol to the hydrolyzed keratin is 77: 20: 3; the conditioning agent containing the lotus extract is a mixture of water, butanediol and the lotus extract, wherein the mass ratio of the water to the butanediol to the lotus extract is 77: 20: 3; the conditioner containing the extract of the vegetarian square flowers is a mixture of water, 1, 2-hexanediol, p-hydroxyacetophenone and the extract of the vegetarian square flowers, wherein the mass ratio of the water to the 1, 2-hexanediol to the p-hydroxyacetophenone to the extract of the vegetarian square flowers is 91.5: 0.75: 0.75: 7; the conditioning agent containing the purslane extract is a mixture of water, butanediol, 1, 2-hexanediol and the purslane extract, wherein the mass ratio of the water, the butanediol, the 1, 2-hexanediol and the purslane extract is 56: 10: 2: 32, a first step of removing the first layer; the conditioner containing the water of the chamomile is a mixture of water, butanediol and the water of the chamomile, wherein the mass ratio of the water to the butanediol to the water of the chamomile is 73: 20: 7; the conditioner containing the lavender flower water is a mixture of water, butanediol and the lavender flower water, wherein the mass ratio of the water to the butanediol to the lavender flower water is 72: 20: 8. the preservative is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium chloride, magnesium nitrate and water, wherein the mass ratio of the methylchloroisothiazolinone, the methylisothiazolinone, the magnesium chloride, the magnesium nitrate and the water is 1: 0.36: 0.75: 22.5: 75.39. the anionic surfactant is an anionic surfactant formed by mixing sodium laureth sulfate and water according to a mass ratio of 75:25, and the amphoteric surfactant is an amphoteric surfactant formed by mixing lauramidopropyl betaine and water according to a mass ratio of 35: 65.
A preparation process of silicone oil-free shampoo with a scalp care effect comprises the following steps:
(1) adding water and anionic surfactant into a reaction kettle, heating to 60 ℃, and stirring for 40 minutes at 300rmp to completely dissolve the raw materials;
(2) adding an amphoteric surfactant into a reaction pot, stirring for 30 minutes at 300rmp, then continuously adding olive oil PEG-7 esters, polyquaternium-7, PEG-7 glycerol cocoate, decyl glucoside and glycerol into the reaction pot, and stirring for 30 minutes at 300rmp to completely dissolve the raw materials;
(3) cooling the reaction kettle to 50 ℃, taking a proper clean container, uniformly mixing PEG-40 hydrogenated castor oil and daily essence, adding the mixture into the reaction kettle, continuously adding a conditioner containing calendula officinalis extract, a conditioner containing soluble proteoglycan, a conditioner containing brown algae extract, a conditioner containing hydrolyzed wheat protein, a conditioner containing hydrolyzed keratin, a conditioner containing lotus flower extract, a conditioner containing vegetarian fanninghamia extract, a conditioner containing purslane extract, a conditioner containing chamomile water, a conditioner containing lavender water and a preservative into the reaction kettle, and stirring for 20 minutes at 300rmp to completely dissolve the raw materials;
(4) and cooling to 40 ℃, sampling, conveying to a sample tube for detection, and filtering and discharging by using a 80-mesh filter screen after the sample tube is detected to be qualified to obtain the silicone-oil-free shampoo with the scalp care effect.
Example 3
The silicone-oil-free shampoo with the scalp care effect comprises the following raw materials in parts by mass: 52% of water, 16% of anionic surfactant, 20% of amphoteric surfactant, 6% of olive oil PEG-7 esters, 70.5% of polyquaternary ammonium salt, 0.5% of PEG-7 glyceryl cocoate, 2% of decyl glucoside, 1% of conditioner containing calendula extract, 1% of conditioner containing soluble proteoglycan, 0.5% of conditioner containing brown algae extract, 0.03% of conditioner containing hydrolyzed wheat protein, 0.07% of conditioner containing hydrolyzed keratin, 0.04% of conditioner containing lotus extract, 0.06% of conditioner containing vegetarian square flower extract, 0.04% of conditioner containing purslane extract, 0.06% of conditioner containing chamomile flower water, 0.07% of conditioner containing lavender flower water, 0.03% of glycerol, 0.05% of PEG-40 hydrogenated castor oil, 0.03% of daily essence and 0.02% of preservative. The conditioning agent containing the calendula extract is a mixture of water, butanediol and the calendula extract, wherein the mass ratio of the water to the butanediol to the calendula extract is 77.2: 20: 2.8 of; the conditioner containing soluble proteoglycan is a mixture of water, butanediol and soluble proteoglycan, wherein the mass ratio of the water to the butanediol to the soluble proteoglycan is 77.4: 20: 2.6; the conditioning agent containing the brown algae extract is a mixture of water, butanediol and the brown algae extract, wherein the mass ratio of the water to the butanediol to the brown algae extract is 77.3: 20: 2.7; the conditioner containing hydrolyzed wheat protein is a mixture of water, butanediol and hydrolyzed wheat protein, wherein the mass ratio of the water to the butanediol to the hydrolyzed wheat protein is 77.1: 20: 2.9; the conditioner containing the hydrolyzed keratin is a mixture of water, butanediol and hydrolyzed keratin, wherein the mass ratio of the water to the butanediol to the hydrolyzed keratin is 77.3: 20: 2.7; the conditioning agent containing the lotus extract is a mixture of water, butanediol and the lotus extract, wherein the mass ratio of the water to the butanediol to the lotus extract is 77.2: 20: 2.8 of; the conditioner containing the extract of the vegetarian square flowers is a mixture of water, 1, 2-hexanediol, p-hydroxyacetophenone and the extract of the vegetarian square flowers, wherein the mass ratio of the water to the 1, 2-hexanediol to the p-hydroxyacetophenone to the extract of the vegetarian square flowers is 91.6: 0.75: 0.75: 6.9; the conditioning agent containing the purslane extract is a mixture of water, butanediol, 1, 2-hexanediol and the purslane extract, wherein the mass ratio of the water, the butanediol, the 1, 2-hexanediol and the purslane extract is 57: 10: 2: 31; the conditioner containing the water of the chamomile is a mixture of water, butanediol and the water of the chamomile, wherein the mass ratio of the water to the butanediol to the water of the chamomile is 74: 20: 6; the conditioner containing the lavender flower water is a mixture of water, butanediol and the lavender flower water, wherein the mass ratio of the water to the butanediol to the lavender flower water is 74: 20: 6. the preservative is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium chloride, magnesium nitrate and water, wherein the mass ratio of the methylchloroisothiazolinone, the methylisothiazolinone, the magnesium chloride, the magnesium nitrate and the water is 1.1: 0.36: 0.75: 22.5: 75.29. the anionic surfactant is an anionic surfactant formed by mixing sodium laureth sulfate and water according to a mass ratio of 73:27, and the amphoteric surfactant is an amphoteric surfactant formed by mixing lauramidopropyl betaine and water according to a mass ratio of 34: 66.
A preparation process of silicone oil-free shampoo with a scalp care effect comprises the following steps:
(1) adding water and an anionic surfactant into a reaction kettle, heating to 80 ℃, and stirring for 35 minutes at 400rmp to completely dissolve the raw materials;
(2) adding an amphoteric surfactant into a reaction pot, stirring for 25 minutes at 400rmp, then continuously adding olive oil PEG-7 esters, polyquaternium-7, PEG-7 glycerol cocoate, decyl glucoside and glycerol into the reaction pot, and stirring for 25 minutes at 300rmp to completely dissolve the raw materials;
(3) cooling the reaction kettle to 48 ℃, taking a proper clean container, uniformly mixing PEG-40 hydrogenated castor oil and daily essence, adding the mixture into the reaction kettle, continuously adding a conditioner containing calendula officinalis extract, a conditioner containing soluble proteoglycan, a conditioner containing brown algae extract, a conditioner containing hydrolyzed wheat protein, a conditioner containing hydrolyzed keratin, a conditioner containing lotus flower extract, a conditioner containing vegetarian fanninghamia extract, a conditioner containing purslane extract, a conditioner containing chamomile water, a conditioner containing lavender water and a preservative into the reaction kettle, and stirring for 18 minutes at 400rmp to completely dissolve the raw materials;
(4) and cooling to 40 ℃, sampling, conveying to a sample tube for detection, and filtering and discharging by using a 80-mesh filter screen after the sample tube is detected to be qualified to obtain the silicone-oil-free shampoo with the scalp care effect.
Comparative example
The technical scheme of the shampoo without silicone oil is basically the same as that of the shampoo in the embodiment 1, and the shampoo is characterized by only comprising the following raw materials in percentage by mass: 60% of water, 15% of anionic surfactant, 15% of amphoteric surfactant, 5% of olive oil PEG-7 esters, 71% of polyquaternary ammonium salt, 1% of PEG-7 glyceryl cocoate, 1% of glycerol, 1% of PEG-40 hydrogenated castor oil, 0.5% of daily essence and 0.5% of preservative. The preservative is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium chloride, magnesium nitrate and water, wherein the mass ratio of the methylchloroisothiazolinone, the methylisothiazolinone, the magnesium chloride, the magnesium nitrate and the water is 0.9: 0.3: 0.75: 22.5: 75.55. the anionic surfactant is an anionic surfactant formed by mixing sodium laureth sulfate and water according to a mass ratio of 70:30, and the amphoteric surfactant is an amphoteric surfactant formed by mixing lauramidopropyl betaine and water according to a mass ratio of 30: 70.
Hazard identification analysis is carried out on the silicone oil-free shampoo prepared in the embodiment 1 of the invention, because risk substances possibly brought in raw materials and possibly generated or brought in a production process are provided, and a hazard identification table of cosmetic safety risk substances is provided, which shows that the silicone oil-free shampoo prepared in the invention does not have safety risk substances harmful to human health.
TABLE 1 safety risk substance detection table in silicone oil-free shampoo
As can be seen from table 1, the physicochemical raw materials in the silicone oil-free shampoo prepared in example 1 of the present invention are stable, no risk substance is generated after the raw materials are mixed, no substances other than the formula and possible risk substances are entrained in the product, no safety risk substance exists, and the shampoo meets the requirements of "technical standards for cosmetic safety".
Randomly selecting 100 18-25 years old women to evaluate the using effect of the shampoo, wherein 50 people have long hair and 50 people have short hair, and the hair is washed once every three days for one month continuously. Of these, 25 short-haired women and 25 long-haired women used the silicone-free shampoo prepared in example 1, and the remaining 25 short-haired women and 25 long-haired women used the silicone-free shampoo prepared in the comparative example, and the test data are shown in table 2.
TABLE 2 evaluation table for shampoo without silicone oil
As can be seen from the data in Table 2, the shampoo without silicone oil prepared in the embodiment 1 of the invention has better using effect than the shampoo prepared in a comparative example, can obviously improve the dryness of hair, obviously reduce hair loss, reduce dandruff and has good decontamination effect. Therefore, the silicone oil-free shampoo provided by the invention can enhance hair roots, reduce hair loss, improve hair dryness, enable hair to be more smooth, nourish head skin, reduce dandruff and simultaneously have a good decontamination effect.
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; while the invention has been described in detail and with reference to the foregoing embodiments, it will be understood by those skilled in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; and the modifications or the substitutions do not make the essence of the corresponding technical solutions depart from the scope of the technical solutions of the embodiments of the present invention.
Claims (10)
1. The silicone-oil-free shampoo with the scalp care effect is characterized by comprising the following raw materials: water, an anionic surfactant, an amphoteric surfactant, olive oil PEG-7 esters, polyquaternium-7, PEG-7 glyceryl cocoate, decyl glucoside, a conditioner containing a calendula extract, a conditioner containing soluble proteoglycan, a conditioner containing a brown algae extract, a conditioner containing hydrolyzed wheat protein, a conditioner containing hydrolyzed keratin, a conditioner containing a lotus flower extract, a conditioner containing a bisque flower extract, a conditioner containing a purslane extract, a conditioner containing chamomile flower water, a conditioner containing lavender flower water, glycerol, PEG-40 hydrogenated castor oil, essence for daily use and a preservative.
2. The silicone-oil-free shampoo with the scalp care effect as claimed in claim 1, wherein the silicone-oil-free shampoo comprises the following components in percentage by weight:
the conditioning agent containing the calendula extract is a mixture of water, butanediol and the calendula extract, wherein the mass ratio of the water to the butanediol to the calendula extract is 77.5: 20: 2.5-77: 20: 3;
the conditioner containing soluble proteoglycan is a mixture of water, butanediol and soluble proteoglycan, wherein the mass ratio of the water to the butanediol to the soluble proteoglycan is 77.5: 20: 2.5-77: 20: 3;
the conditioning agent containing the brown algae extract is a mixture of water, butanediol and the brown algae extract, wherein the mass ratio of the water to the butanediol to the brown algae extract is 77.5: 20: 2.5-77: 20: 3;
the conditioner containing hydrolyzed wheat protein is a mixture of water, butanediol and hydrolyzed wheat protein, wherein the mass ratio of the water to the butanediol to the hydrolyzed wheat protein is 77.5: 20: 2.5-77: 20: 3;
the conditioner containing the hydrolyzed keratin is a mixture of water, butanediol and hydrolyzed keratin, wherein the mass ratio of the water to the butanediol to the hydrolyzed keratin is 77.5: 20: 2.5-77: 20: 3;
the conditioning agent containing the lotus extract is a mixture of water, butanediol and the lotus extract, wherein the mass ratio of the water to the butanediol to the lotus extract is 77.5: 20: 2.5-77: 20: 3;
the conditioner containing the extract of the vegetarian square flower is a mixture of water, 1, 2-hexanediol, p-hydroxyacetophenone and the extract of the vegetarian square flower, wherein the mass ratio of the water to the 1, 2-hexanediol to the p-hydroxyacetophenone to the extract of the vegetarian square flower is 91.75: 0.75: 0.75: 6.75-91.5: 0.75: 0.75: 7;
the conditioning agent containing the purslane extract is a mixture of water, butanediol, 1, 2-hexanediol and the purslane extract, wherein the mass ratio of the water, the butanediol, the 1, 2-hexanediol and the purslane extract is 58: 10: 2: 30-56: 10: 2: 32, a first step of removing the first layer;
the conditioner containing the water of the chamomile is a mixture of water, butanediol and the water of the chamomile, wherein the mass ratio of the water to the butanediol to the water of the chamomile is 75: 20: 5-73: 20: 7;
the conditioner containing the lavender flower water is a mixture of water, butanediol and the lavender flower water, wherein the mass ratio of the water to the butanediol to the lavender flower water is 75: 20: 5-72: 20: 8.
3. the silicone-oil-free shampoo with the scalp care effect as claimed in claim 1, wherein the silicone-oil-free shampoo comprises the following components in percentage by weight: the preservative is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium chloride, magnesium nitrate and water, wherein the mass ratio of the methylchloroisothiazolinone, the methylisothiazolinone, the magnesium chloride, the magnesium nitrate and the water is 1.12: 0.36: 0.75: 22.5: 75.27-0.9: 0.3: 0.75: 22.5: 75.55.
4. the silicone-oil-free shampoo with the scalp care effect as claimed in claim 1, wherein the silicone-oil-free shampoo comprises the following components in percentage by weight: the anionic surfactant is a mixed anionic surfactant of sodium laureth sulfate and water according to the mass ratio of 70:30-75:25, and the amphoteric surfactant is a mixed amphoteric surfactant of lauramidopropyl betaine and water according to the mass ratio of 30:70-35: 65.
5. The silicone-oil-free shampoo with the scalp care effect as claimed in claim 1 is characterized by comprising the following raw materials in percentage by mass: 50-60% of water, 15-20% of anionic surfactant, 15-20% of amphoteric surfactant, 5-10% of olive oil PEG-7 esters, 0.0001-5% of polyquaternium-70.0001, 0.0001-5% of PEG-7 glyceryl cocoate, 1-2% of decyl glucoside, 0.0001-1% of conditioning agent containing calendula extract, 0.0001-1% of conditioning agent containing soluble protein polysaccharide, 0.0001-1% of conditioning agent containing brown algae extract, 0.0001-1% of conditioning agent containing hydrolyzed wheat protein, 0.0001-1% of conditioning agent containing hydrolyzed keratin, 0.0001-1% of conditioning agent containing lotus flower extract, 0.0001-1% of conditioning agent containing bisque flower extract, 0.0001-1% of conditioning agent containing purslane extract, 0.0001-1% of conditioning agent containing chamomile water, and the like, 0.0001-1% of conditioner containing lavender flower water, 0.0001-1% of glycerin, 0.0001-1% of PEG-40 hydrogenated castor oil, 0.0001-1% of daily essence and 0.0001-1% of preservative.
6. A process for preparing the silicone oil-free shampoo with scalp care effect as claimed in any one of claims 1 to 5, which comprises the following steps:
(1) adding water and an anionic surfactant into a reaction kettle, heating, and uniformly stirring;
(2) then adding amphoteric surfactant, stirring well, adding oleum Olivarum PEG-7 esters, polyquaternium-7, PEG-7 glyceryl cocoate, decyl glucoside and glycerol, and stirring well;
(3) cooling, adding uniformly mixed PEG-40 hydrogenated castor oil and daily essence, then adding a conditioner containing a calendula extract, a conditioner containing soluble proteoglycan, a conditioner containing a brown algae extract, a conditioner containing hydrolyzed wheat protein, a conditioner containing hydrolyzed keratin, a conditioner containing a lotus flower extract, a conditioner containing a vegetarian square flower extract, a conditioner containing a purslane extract, a conditioner containing chamomile flower water, a conditioner containing lavender flower water and a preservative, and uniformly stirring;
(4) cooling again, and filtering to obtain the silicone oil-free shampoo with scalp care effect.
7. The preparation process of the silicone-oil-free shampoo with the scalp care effect as claimed in claim 6, characterized in that: the heating temperature in the step (1) is 60-80 ℃.
8. The preparation process of the silicone-oil-free shampoo with the scalp care effect as claimed in claim 6, characterized in that: and (4) cooling to 45-50 ℃ in the step (3).
9. The preparation process of the silicone-oil-free shampoo with the scalp care effect as claimed in claim 6, wherein the step (4) is: cooling to 35-40 deg.C, and filtering with 80-100 mesh filter screen to obtain shampoo without silicone oil for caring scalp.
10. The preparation process of the silicone-oil-free shampoo with the scalp care effect as claimed in claim 6, characterized in that: the stirring speed in the step (1) is 300-500rpm, and the stirring time is 30-40 minutes; the stirring speed in the step (2) is 300-500rpm, and the stirring time is 20-30 minutes; the stirring speed in the step (3) is 300-500rpm, and the stirring time is 15-20 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110057472.0A CN112807251A (en) | 2021-01-15 | 2021-01-15 | Silicone-oil-free shampoo with scalp care effect and preparation process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110057472.0A CN112807251A (en) | 2021-01-15 | 2021-01-15 | Silicone-oil-free shampoo with scalp care effect and preparation process thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112807251A true CN112807251A (en) | 2021-05-18 |
Family
ID=75869584
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202110057472.0A Pending CN112807251A (en) | 2021-01-15 | 2021-01-15 | Silicone-oil-free shampoo with scalp care effect and preparation process thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112807251A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114569527A (en) * | 2022-03-08 | 2022-06-03 | 杨卓涛 | Multi-effect repairing shampoo |
| CN115369648A (en) * | 2021-10-21 | 2022-11-22 | 青岛融美发制品集团有限公司 | Silicone-oil-free wig post-treatment agent and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107184406A (en) * | 2017-05-11 | 2017-09-22 | 曾万祥 | One kind is planted extraction without anti-corrosion ginger without silicone oil shampoo and preparation method thereof |
| CN107375053A (en) * | 2017-06-16 | 2017-11-24 | 曾万祥 | A kind of ginseng and Chinese angelica root is without silicone oil shampoo and preparation method thereof |
-
2021
- 2021-01-15 CN CN202110057472.0A patent/CN112807251A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107184406A (en) * | 2017-05-11 | 2017-09-22 | 曾万祥 | One kind is planted extraction without anti-corrosion ginger without silicone oil shampoo and preparation method thereof |
| CN107375053A (en) * | 2017-06-16 | 2017-11-24 | 曾万祥 | A kind of ginseng and Chinese angelica root is without silicone oil shampoo and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 杭州心悦化妆品有限公司: "《http://ftba.nmpa.gov.cn:8181/ftban/itownet/hzp_ba/fw/pz.jsp?processid=20200107131514c2ri3&nid=20200107131514c2ri3》", 20 January 2020, 国产非特殊用途化妆品备案信息服务平台 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115369648A (en) * | 2021-10-21 | 2022-11-22 | 青岛融美发制品集团有限公司 | Silicone-oil-free wig post-treatment agent and preparation method thereof |
| CN115369648B (en) * | 2021-10-21 | 2024-03-08 | 青岛海森林发制品集团股份有限公司 | Silicone oil-free wig post-treatment agent and preparation method thereof |
| CN114569527A (en) * | 2022-03-08 | 2022-06-03 | 杨卓涛 | Multi-effect repairing shampoo |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106038330B (en) | A kind of mildy wash and preparation method thereof | |
| CN108096173A (en) | Mild amino acid shampoo of a kind of green and preparation method thereof | |
| CN107496317B (en) | Repairing and nursing shampoo containing periplaneta americana active ingredient | |
| CN112807251A (en) | Silicone-oil-free shampoo with scalp care effect and preparation process thereof | |
| CN107737039A (en) | Containing ginger without silicone oil without sulfate health-care shampoo and its preparation technology | |
| WO2019205086A1 (en) | A hair cleansing composition containing natural oils | |
| CN108721177A (en) | Camellia amino acid shampoo | |
| CN113876672A (en) | Amino acid mild tear-free natural plant shampoo and preparation method thereof | |
| DE10128799A1 (en) | Aqueous cosmetic agent, for use in e.g. shampoos, conditioners and liquid soaps, comprises anionic, nonionic and amphoteric surfactant, polymer and copolymer, starch derivatives, thickener and additives in acceptable medium | |
| CN112515995A (en) | Shampoo bath lotion containing tea seed oil and preparation method thereof | |
| CN114366680A (en) | Shampoo composition for maintaining scalp health, preventing alopecia and strengthening hair and preparation method thereof | |
| CN108158921A (en) | A kind of plant composition comprising tea bran and rosemary and its preparation method and application | |
| CN109498520A (en) | Desquamation compositions, shampoo and preparation method thereof | |
| CN115444766A (en) | Double-component shampoo with scalp nourishing effect and preparation method thereof | |
| CN114366693A (en) | Shampoo shower gel for infants and children | |
| CN111096917B (en) | Long-acting anti-dandruff itching-relieving composition and application thereof | |
| CN113693976A (en) | Sericin stock solution shampoo and preparation method thereof | |
| CN113648261A (en) | Ginger shampoo with scalp care effect and preparation method thereof | |
| CN113893196A (en) | A bath product containing natural plant extract | |
| CN110090168B (en) | Washing and caring product with hair growth promoting and hair strengthening effects | |
| CN112515986A (en) | Shampoo containing camphor oil component and preparation method thereof | |
| CN110946787A (en) | Non-irritating aloe hair conditioner | |
| KR101534342B1 (en) | Scalp-care Composition for Enhanced Scalp-Safety and anti-dandruff effect | |
| KR100414538B1 (en) | Hair cosmetic composition | |
| CN108721198A (en) | A kind of shampoo and preparation method thereof with moisture-keeping efficacy |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20210518 |