CN100551352C - A kind of emulsified salt type Chinese herbal medicine emulsion used for washing and caring hair and preparation method thereof - Google Patents
A kind of emulsified salt type Chinese herbal medicine emulsion used for washing and caring hair and preparation method thereof Download PDFInfo
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- CN100551352C CN100551352C CNB2007100659841A CN200710065984A CN100551352C CN 100551352 C CN100551352 C CN 100551352C CN B2007100659841 A CNB2007100659841 A CN B2007100659841A CN 200710065984 A CN200710065984 A CN 200710065984A CN 100551352 C CN100551352 C CN 100551352C
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- 241000411851 herbal medicine Species 0.000 title claims abstract description 39
- 150000003839 salts Chemical class 0.000 title claims abstract description 30
- 238000005406 washing Methods 0.000 title claims abstract description 20
- 239000000839 emulsion Substances 0.000 title claims abstract description 16
- 238000002360 preparation method Methods 0.000 title abstract description 6
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 33
- 238000010008 shearing Methods 0.000 claims abstract description 21
- 238000003756 stirring Methods 0.000 claims abstract description 18
- 239000011780 sodium chloride Substances 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000012141 concentrate Substances 0.000 claims abstract description 11
- 239000008367 deionised water Substances 0.000 claims abstract description 11
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 11
- 230000001804 emulsifying effect Effects 0.000 claims abstract description 10
- 150000004676 glycans Chemical class 0.000 claims abstract description 9
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 9
- 239000005017 polysaccharide Substances 0.000 claims abstract description 9
- 239000004094 surface-active agent Substances 0.000 claims abstract description 8
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 7
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 7
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 7
- 239000003945 anionic surfactant Substances 0.000 claims abstract description 7
- 239000003093 cationic surfactant Substances 0.000 claims abstract description 7
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 7
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229920002545 silicone oil Polymers 0.000 claims abstract description 7
- 239000008117 stearic acid Substances 0.000 claims abstract description 7
- 150000005846 sugar alcohols Polymers 0.000 claims abstract description 7
- 239000000080 wetting agent Substances 0.000 claims abstract description 7
- 239000002888 zwitterionic surfactant Substances 0.000 claims abstract description 7
- 229930003270 Vitamin B Natural products 0.000 claims abstract description 6
- 235000019156 vitamin B Nutrition 0.000 claims abstract description 6
- 239000011720 vitamin B Substances 0.000 claims abstract description 6
- 230000032683 aging Effects 0.000 claims abstract description 4
- 239000000047 product Substances 0.000 claims description 23
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 13
- 241000628997 Flos Species 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 10
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 9
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 6
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 claims description 6
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 claims description 6
- 150000001768 cations Chemical class 0.000 claims description 6
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 6
- ILRSCQWREDREME-UHFFFAOYSA-N dodecanamide Chemical compound CCCCCCCCCCCC(N)=O ILRSCQWREDREME-UHFFFAOYSA-N 0.000 claims description 6
- QCCKPZOPTXCJPL-UHFFFAOYSA-N dodecyl(dimethyl)azanium;hydroxide Chemical compound [OH-].CCCCCCCCCCCC[NH+](C)C QCCKPZOPTXCJPL-UHFFFAOYSA-N 0.000 claims description 6
- 239000000194 fatty acid Substances 0.000 claims description 6
- 229930195729 fatty acid Natural products 0.000 claims description 6
- 239000000706 filtrate Substances 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 239000003292 glue Substances 0.000 claims description 6
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 claims description 6
- 241001643642 Viticis Species 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 5
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 claims description 5
- MMBILEWCGWTAOV-UHFFFAOYSA-N N-(2-Hydroxypropyl)dodecanamide Chemical compound CCCCCCCCCCCC(=O)NCC(C)O MMBILEWCGWTAOV-UHFFFAOYSA-N 0.000 claims description 4
- 238000004458 analytical method Methods 0.000 claims description 4
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 claims description 3
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 3
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 3
- DHHFDKNIEVKVKS-FMOSSLLZSA-N Betanin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC(C(=C1)O)=CC(C[C@H]2C([O-])=O)=C1[N+]2=C\C=C\1C=C(C(O)=O)N[C@H](C(O)=O)C/1 DHHFDKNIEVKVKS-FMOSSLLZSA-N 0.000 claims description 3
- DHHFDKNIEVKVKS-MVUYWVKGSA-N Betanin Natural products O=C(O)[C@@H]1NC(C(=O)O)=C/C(=C\C=[N+]/2\[C@@H](C(=O)[O-])Cc3c\2cc(O)c(O[C@H]2[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O2)c3)/C1 DHHFDKNIEVKVKS-MVUYWVKGSA-N 0.000 claims description 3
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 3
- VBIIFPGSPJYLRR-UHFFFAOYSA-M Stearyltrimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCCCC[N+](C)(C)C VBIIFPGSPJYLRR-UHFFFAOYSA-M 0.000 claims description 3
- 125000000217 alkyl group Chemical group 0.000 claims description 3
- 150000001408 amides Chemical class 0.000 claims description 3
- 235000012677 beetroot red Nutrition 0.000 claims description 3
- 239000001654 beetroot red Substances 0.000 claims description 3
- 235000002185 betanin Nutrition 0.000 claims description 3
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims description 3
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims description 3
- 235000019864 coconut oil Nutrition 0.000 claims description 3
- 239000003240 coconut oil Substances 0.000 claims description 3
- 150000001991 dicarboxylic acids Chemical class 0.000 claims description 3
- 238000009826 distribution Methods 0.000 claims description 3
- SYELZBGXAIXKHU-UHFFFAOYSA-N dodecyldimethylamine N-oxide Chemical compound CCCCCCCCCCCC[N+](C)(C)[O-] SYELZBGXAIXKHU-UHFFFAOYSA-N 0.000 claims description 3
- -1 fatty acid alkyl alcohol amide Chemical class 0.000 claims description 3
- 150000004665 fatty acids Chemical class 0.000 claims description 3
- 229940075507 glyceryl monostearate Drugs 0.000 claims description 3
- 229920002674 hyaluronan Polymers 0.000 claims description 3
- 229960003160 hyaluronic acid Drugs 0.000 claims description 3
- 125000000400 lauroyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 3
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 claims description 3
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 claims description 3
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 3
- 230000001105 regulatory effect Effects 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 239000000661 sodium alginate Substances 0.000 claims description 3
- 235000010413 sodium alginate Nutrition 0.000 claims description 3
- 229940005550 sodium alginate Drugs 0.000 claims description 3
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 3
- 235000011152 sodium sulphate Nutrition 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- 239000000600 sorbitol Substances 0.000 claims description 3
- 229940032094 squalane Drugs 0.000 claims description 3
- 238000001291 vacuum drying Methods 0.000 claims description 3
- 238000010792 warming Methods 0.000 claims description 3
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 2
- 230000008030 elimination Effects 0.000 claims description 2
- 238000003379 elimination reaction Methods 0.000 claims description 2
- 244000241257 Cucumis melo Species 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 10
- 239000006260 foam Substances 0.000 abstract description 6
- 208000001840 Dandruff Diseases 0.000 abstract description 5
- 230000001139 anti-pruritic effect Effects 0.000 abstract description 3
- 239000003908 antipruritic agent Substances 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 3
- 210000004761 scalp Anatomy 0.000 abstract description 3
- 238000003475 lamination Methods 0.000 abstract description 2
- 235000002639 sodium chloride Nutrition 0.000 description 34
- 241000219112 Cucumis Species 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 208000003251 Pruritus Diseases 0.000 description 3
- 238000005303 weighing Methods 0.000 description 3
- MYXLAFOWZCKBBV-UHFFFAOYSA-N C=C.C(CCCCCCCCCCC)[O] Chemical group C=C.C(CCCCCCCCCCC)[O] MYXLAFOWZCKBBV-UHFFFAOYSA-N 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 230000007803 itching Effects 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 2
- 201000004384 Alopecia Diseases 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 231100000360 alopecia Toxicity 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 230000003648 hair appearance Effects 0.000 description 1
- 230000035876 healing Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000005185 salting out Methods 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
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- Cosmetics (AREA)
Abstract
The invention discloses a kind of emulsified salt type emulsion used for washing and caring hair and preparation method thereof, with polyhydric alcohol dissolving lanoline and wetting agent; In deionized water, add anion surfactant, non-ionic surface active agent, zwitterionic surfactant and cationic surfactant; Merge gains and add emulsified silicone oil, stearic acid and acrylic resin, place homogeneous emulsifying machine constant temperature to stir; Add sodium chloride again, the setting shearing force is 600rpm～1200rpm, makes sodium chloride emulsifying and homogenizing; Add to remove Chinese herbal medicine extract, Pearl Concentrate, vitamin B, emulsified silicone oil and the essence of polysaccharide at last, regulate pH value after quietly obtain product to ageing.The present invention can give full play to the beneficial functional of salt and Chinese herbal medicine, the problem that product viscosity is poor, foam is low when efficiently solving the coexistence of the lamination problem of salt and salt and Chinese herbal medicine extract.Have effects such as hair washing, hair care, anti-dandruff, antipruritic, anticreep, non-stimulated to scalp, market application foreground is good.
Description
Technical field
The invention belongs to the hair cosmetic technical field, be specifically related to a kind of Chinese herbal medicine emulsion used for washing and caring hair that contains emulsifying salt.Simultaneously, the invention still further relates to the preparation method of this emulsion used for washing and caring hair.
Background technology
In the market hair washing, hair products are of a great variety, in order to reach hair washing, hair care, anti-dandruff, itching relieving effect, need to use various chemical addition agents.Life-time service is not only unhelpful to human body, nor is beneficial to environmental protection.And natural salt not only have sterilization, sterilization, antipruritic, invigorate blood circulation and the effect of skin moistening, and skin had preserve moisture well and restrain effect, its application in the beauty and skin care product is approved by masses.But hair washing, hair products belong to emulsion system more, and a kind of exactly strong demulsifier of salt, if it is added in the into existing product system simply, must cause the emulsion system breakdown of emulsion to be disintegrated or make product some composition wherein lose use value because of salting-out effect.Therefore, how under the prerequisite that keeps constant product quality, bring into play the good characteristic of salt as much as possible, become the hot issue of technical research in this field.
The inventor at salt the application in daily chemical products carried out years of researches, aspect skin-cleaning articles, obtained breakthrough, application has also obtained multinomial Chinese patent, for example " a kind of emulsified salt type skin-cleaning articles and preparation method thereof " (patent No.: 200410022594.2).And have one's hair wash, though hair products have a lot of similar parts with clean skin product, different instructions for uses has determined them to have many difference on raw materials for production and preparation method.Particularly in order to strengthen effect, all added Chinese herbal medicine extract in now many hair washings, the hair products, the adding of salt not only can cause existing product system instability, easily layering, and the coexistence of salt and Chinese herbal medicine also can make the product foam reduce rapidly, the influence use.How salt (content is greater than 5%) and Chinese herbal medicine are applied to the product of defending the doctrine of having one's hair wash simultaneously, and the system that reaches is stable, foam enriches, is easy to combing, removing scurf and relieving itching, effect such as a softer and smoother touch, glossy, no matter is prior art or all not on the books in first to file.
Summary of the invention
The objective of the invention is at the deficiencies in the prior art, provide that a kind of to be difficult for layering, in stable condition, collection hair washing, hair care, hair care be the emulsified salt type Chinese herbal medicine emulsion used for washing and caring hair of one.
Another object of the present invention provides a kind of method for preparing above-mentioned emulsion used for washing and caring hair.
Purpose of the present invention is achieved by the following technical programs.
A kind of emulsified salt type Chinese herbal medicine emulsion used for washing and caring hair, this emulsion used for washing and caring hair is made by the raw material of following weight parts: anion surfactant 5～25, non-ionic surface active agent 5～20, zwitterionic surfactant 3～12, cationic surfactant 1～8, sodium chloride 5～30, Chinese herbal medicine extract 0.5～5.0, emulsified silicone oil 0.5～5.0, stearic acid 0.2～10, acrylic resin 0.2～20, polyhydric alcohol 20～100, wetting agent 0.2～30, lanoline 1～10, Pearl Concentrate 1～5, vitamin B 0.1～2, deionized water 25～60, essence 0.01～0.3.
Described anion surfactant is selected from a kind of in dodecyl sodium sulfate, polyoxyethylenated alcohol sodium sulfate, sodium lauroyl sarcosine, dodecyl oxygen ethylene (3) ether phosphate sodium or the ten dicarboxylic acids sodium.
Described non-ionic surface active agent is selected from a kind of in lauroyl diglycollic amide, alkyl polyglycoside, fatty acid distribution of coconut oil monoethanolamine, fatty acid alkyl alcohol amide, lauroyl isopropanol amide or the glyceryl monostearate.
Described zwitterionic surfactant is selected from a kind of in dodecanamide propyl betanin, cocamidopropyl betaine or the dodecyldimethylammonium hydroxide inner salt.
Described cationic surfactant is selected from a kind of in dimethyl dodecyl amine oxide, octadecyl trimethyl ammonium chloride or the cation melon glue.
Described polyhydric alcohol is selected from a kind of in glycerol, propylene glycol or the sorbitol.
Described wetting agent is selected from a kind of in squalane, hyaluronic acid, sodium alginate or the sun caul-fat.
Described sodium chloride is a kind of of deep-well salt or sea salt.
Described Chinese herbal medicine extract need be removed polysaccharide.
Described Chinese herbal medicine extract is preferably made by the raw material of following weight portion: Radix Sophorae Flavescentis 1～5, Herba Artemisiae Scopariae 1～5, Fructus Viticis 1～3, Radix Polygoni Multiflori 2～10, Cortex Dictamni 1～5, Cortex Mori 1～5, Herba Taraxaci 1～3, Flos Lonicerae 1～3, Fructus Chebulae 1～5, Rhizoma Chuanxiong 2～10, Herba Asari 1～5, Rhizoma Zingiberis Recens 5～15, Cortex Phellodendri 1～5, Radix Angelicae Sinensis 1～5, Radix Scutellariae 1～5, Radix Glycyrrhizae 1～5, Galla Chinensis 1～5, Flos Chrysanthemi 1～5.
A kind of method for preparing above-mentioned emulsified salt type Chinese herbal medicine emulsion used for washing and caring hair, this method comprises the step of following order:
(1) with polyhydric alcohol dissolving lanoline and wetting agent;
(2) in deionized water, add anion surfactant, non-ionic surface active agent, zwitterionic surfactant, cationic surfactant respectively, and stir;
(3) step (1) and (2) gains are placed the agitator tank of homogeneous emulsifying machine, add emulsified silicone oil, stearic acid, acrylic resin, settings shearing force is 600rpm～1200rpm, is warming up to 50～75 ℃, constant temperature stirring 5～25min;
(4) add sodium chloride, be cooled to 60 ℃～45 ℃, the setting shearing force is 600rpm～1200rpm, and mixing time 5～25min makes sodium chloride fully dissolve and reach emulsifying and homogenizing under strong shear action;
(5) add Chinese herbal medicine extract and Pearl Concentrate, temperature, shearing force are constant, mixing time 5～25min;
(6) add vitamin B, essence, the reduction shearing force is 600rpm～1000rpm, progressively is cooled to room temperature;
(7) regulating pH value is 6.0～8.0;
(8) step (7) gains are evacuated to the finished product jar, quiet to ageing 20～28 hours, promptly get product.
Wherein, described Chinese herbal medicine extract is made by following method: Chinese herbal medicine is clean, dried and crushed to 20～40 orders, with water is to extract solvent, liquid-solid ratio 3: 1, ebuillition of heated 30min after-filtration, filtering residue repeats to extract 3 times, merging filtrate concentrates filtrate, and concentrated solution carries out alcohol with 4～5 times of amount 95% ethanol and analyses, cross the elimination polysaccharide, concentrate, be required Chinese herbal medicine extract behind the vacuum drying.
Compared with prior art, the present invention has following outstanding advantage: by the synergism stable prod system of stearic acid and acrylic resin, and reach and improve foamy purpose by adding complexed surfactant and removing technological means such as polysaccharide in the Chinese herbal medicine extract.Can in the concentration range of salinity 5%～30%, Chinese herbal medicine extract 0.5～5.0%, give full play to the beneficial functional of salt and Chinese herbal medicine, the problem that product viscosity is poor, foam is low when having solved the coexistence of the lamination problem of salt and salt and Chinese herbal medicine extract effectively.Have suitable viscosity, and viscosity can be adjusted at 4000mPas～80000mPas; Suitable foam height, and foam height can adjust between 90mm～130mm has effects such as hair washing, hair care, anti-dandruff, antipruritic, anticreep, and is non-stimulated to scalp, has market application foreground well.
The specific embodiment
By specific embodiment given below and typical Application Example, can further be well understood to the present invention, but they not limitation of the invention.
Embodiment 1
(1) with 96g glycerol dissolving 16.7g lanoline, 4.5g squalane;
(2) in the 350g deionized water, add polyoxyethylenated alcohol sodium sulfate 50g, lauroyl diglycollic amide 30g, dodecanamide propyl betanin 30g respectively, dimethyl dodecyl amine oxide 15g, and stir;
(3) step (1) and (2) gains are placed the agitator tank of homogeneous emulsifying machine, add emulsified silicone oil 7.2g, stearic acid 4.0g, acrylic resin 5.0g, settings shearing force is 900rpm, is warming up to 55 ℃, constant temperature stirring 20min;
(4) add sodium chloride 100g, be cooled to 45 ℃, open the shear agitation function of homogeneous emulsifying machine, the setting shearing force is 1000rpm, and mixing time 20min makes sodium chloride fully dissolve and reach emulsifying and homogenizing under strong shear action;
(5) add Chinese herbal medicine extract 6.6g, Pearl Concentrate 10g, temperature, shearing force are constant, stir 15min;
(6) add vitamin B 5g, essence 2g, the setting shearing force is 800rpm, progressively is cooled to room temperature;
(7) regulating pH value is 6.5;
(8) step (7) gains are evacuated to the finished product jar, quiet to ageing 20～28 hours, promptly get product.
Wherein said Chinese herbal medicine extract is made by following method: it is standby to take by weighing Radix Sophorae Flavescentis 10g, Herba Artemisiae Scopariae 10g, Fructus Viticis 10g, Radix Polygoni Multiflori 20g, Cortex Dictamni 10g, Cortex Mori 10g, Herba Taraxaci 10g, Flos Lonicerae 10g, Fructus Chebulae 10g, Rhizoma Chuanxiong 20g, Herba Asari 10g, Rhizoma Zingiberis Recens 50g, Cortex Phellodendri 10g, Radix Angelicae Sinensis 10g, Radix Scutellariae 10g, Radix Glycyrrhizae 10g, Galla Chinensis 10g and Flos Chrysanthemi 10g.Said herbal medicine is clean, dried and crushed to 20 order, with water is to extract solvent, liquid-solid ratio 3: 1, ebuillition of heated 30mi n after-filtration, filtering residue repeats to extract 3 times, merging filtrate, filtrate is concentrated, concentrated solution carries out alcohol and analyses with 4 times of amount 95% ethanol, removes by filter polysaccharide, concentrates, is required Chinese herbal medicine extract behind the vacuum drying.
Embodiment 2
Repeat embodiment 1, following difference is arranged: in the step (1), with propylene glycol 90g dissolving 15g lanoline, 4.5g sodium alginate; In the step (2), in the 300g deionized water, add sodium lauroyl sarcosine 32g, alkyl polyglycoside 22g, cocamidopropyl betaine 14g, cation melon glue 8g respectively, and stir; In the step (3), temperature is 65 ℃, stirs 15min, and in the step (4), the sodium chloride of adding is 90g, and temperature is 55 ℃, and the setting shearing force is 900rpm, mixing time 15min.
Wherein said Chinese herbal medicine extract is made by following method: it is standby to take by weighing Radix Sophorae Flavescentis 30g, Herba Artemisiae Scopariae 30g, Fructus Viticis 20g, Radix Polygoni Multiflori 60g, Cortex Dictamni 30g, Cortex Mori 30g, Herba Taraxaci 20g, Flos Lonicerae 20g, Fructus Chebulae 30g, Rhizoma Chuanxiong 60g, Herba Asari 30g, Rhizoma Zingiberis Recens 10g, Cortex Phellodendri 30g, Radix Angelicae Sinensis 30g, Radix Scutellariae 30g, Radix Glycyrrhizae 30g, Galla Chinensis 30g and Flos Chrysanthemi 30g.Said herbal medicine is clean, dried and crushed to 30 order.Concentrated solution carries out alcohol with 5 times of amount 95% ethanol analyses, and removes by filter polysaccharide.
Embodiment 3
Repeat embodiment 1, following difference is arranged: in the step (1), with 96g glycerol dissolving 15g lanoline, 5g sun caul-fat; In the step (2), in the 280g deionized water, add sodium lauroyl sarcosine 32g, fatty acid distribution of coconut oil monoethanolamine 20g, dodecyldimethylammonium hydroxide inner salt 16g respectively, octadecyl trimethyl ammonium chloride 15g, and stir; In the step (3), temperature is 50 ℃, stirs 25min; In the step (4), the sodium chloride of adding is 85g, and temperature is 40 ℃, and the setting shearing force is 1000rpm, mixing time 20min.
Wherein said Chinese herbal medicine extract is made by following method: it is standby to take by weighing Radix Sophorae Flavescentis 50g, Herba Artemisiae Scopariae 50g, Fructus Viticis 30g, Radix Polygoni Multiflori 100g, Cortex Dictamni 50g, Cortex Mori 50g, Herba Taraxaci 30g, Flos Lonicerae 30g, Fructus Chebulae 50g, Rhizoma Chuanxiong 100g, Herba Asari 50g, Rhizoma Zingiberis Recens 150g, Cortex Phellodendri 50g, Radix Angelicae Sinensis 50g, Radix Scutellariae 50g, Radix Glycyrrhizae 50g, Galla Chinensis 50g and Flos Chrysanthemi 50g.Said herbal medicine is crushed to 40 orders.
Embodiment 4
Repeat embodiment 1, following difference is arranged: in the step (1), with 90g sorbitol dissolving 15g lanoline, 5g sun caul-fat; In the step (2), in the 250g deionized water, add dodecyl oxygen ethylene (3) ether phosphate sodium 30g, fatty acid alkyl alcohol amide 20g, dodecyldimethylammonium hydroxide inner salt 16g respectively, cation melon glue 15g, and stir; In the step (3), temperature is 70 ℃, stirs 8min, and the setting shearing force is 1200rpm; In the step (4), the sodium chloride of adding is 80g, and temperature is 60 ℃, and the setting shearing force is 900rpm, mixing time 10min.
Embodiment 5
Repeat embodiment 1, following difference is arranged: in the step (1), with 90g glycerol dissolving 7g lanoline, 4g hyaluronic acid; In the step (2), in the 230g deionized water, add sodium lauroyl sarcosine 30g, lauroyl isopropanol amide 20g, dodecyldimethylammonium hydroxide inner salt 14g respectively, cation melon glue 15g, and stir; Temperature is 55 ℃ in the step (3), stirs 18min, and the setting shearing force is 800rpm; In the step (4), the sodium chloride of adding is 75g, and temperature is 45 ℃, and the setting shearing force is 800rpm, mixing time 15min.
Embodiment 6
Repeat embodiment 1, following difference is arranged: in the step (1), with 90g glycerol dissolving 7g lanoline, 5g sun caul-fat; In the step (2), in the 230g deionized water, add ten dicarboxylic acids sodium 50g, glyceryl monostearate 30g, lauroyl isopropanol amide 15g, dodecyldimethylammonium hydroxide inner salt 14g respectively, cation melon glue 10g, and stir; Temperature is 55 ℃ in the step (3), stirs 18min, and the setting shearing force is 1000rpm; In the step (4), the sodium chloride of adding is 75g, and temperature is 45 ℃, and the setting shearing force is 1000rpm, mixing time 15min.
Application Example 1
Object of study: dandruff is many, scalp itch patient, weight person, 20 examples.
Using method: clean hair with embodiment 1 products obtained therefrom, used once, and used for 5 weeks continuously in per three days.
Experimental result: healing person's 12 examples, produce effects person's 6 examples, responder's 2 examples.
Application Example 2
Object of study: alopecia is serious, 20 examples.
Using method: clean hair with embodiment 2 products obtained therefroms, used once, and used for 5 weeks continuously in per three days.
Experimental result: produce effects person's 10 examples, responder's 4 examples.
Application Example 3
Object of study: general hair quality 40 examples.
Using method: clean hair with embodiment 3 products obtained therefroms, used once, and used for 5 weeks continuously in per three days.
Experimental result: feel comfortable person's 35 examples, sensation general person 5 examples.
Claims (2)
1, a kind of emulsified salt type Chinese herbal medicine emulsion used for washing and caring hair, this emulsion used for washing and caring hair is made by the raw material of following weight parts: anion surfactant 5～25, non-ionic surface active agent 5～20, zwitterionic surfactant 3～12, cationic surfactant 1～8, sodium chloride 5～30, the Chinese herbal medicine extract 0.5～5.0 of removal polysaccharide, emulsified silicone oil 0.5～5.0, stearic acid 0.2～10, acrylic resin 0.2～20, polyhydric alcohol 20～100, wetting agent 0.2～30, lanoline 1～10, Pearl Concentrate 1～5, vitamin B 0.1～2, deionized water 25～60, essence 0.01～0.3;
Wherein, described anion surfactant is selected from a kind of in dodecyl sodium sulfate, polyoxyethylenated alcohol sodium sulfate, sodium lauroyl sarcosine or the ten dicarboxylic acids sodium;
Described non-ionic surface active agent is selected from a kind of in lauroyl diglycollic amide, alkyl polyglycoside, fatty acid distribution of coconut oil monoethanolamine, fatty acid alkyl alcohol amide, lauroyl isopropanol amide or the glyceryl monostearate;
Described zwitterionic surfactant is selected from a kind of in dodecanamide propyl betanin, cocamidopropyl betaine or the dodecyldimethylammonium hydroxide inner salt;
Described cationic surfactant is selected from a kind of in dimethyl dodecyl amine oxide, octadecyl trimethyl ammonium chloride or the cation melon glue;
Described polyhydric alcohol is selected from a kind of in glycerol, propylene glycol or the sorbitol;
Described wetting agent is selected from a kind of in squalane, hyaluronic acid, sodium alginate or the sun caul-fat;
The Chinese herbal medicine extract of described removal polysaccharide is made by the raw material of following weight portion: Radix Sophorae Flavescentis 1～5, Herba Artemisiae Scopariae 1～5, Fructus Viticis 1～3, Radix Polygoni Multiflori 2～10, Cortex Dictamni 1～5, Cortex Mori 1～5, Herba Taraxaci 1～3, Flos Lonicerae 1～3, Fructus Chebulae 1～5, Rhizoma Chuanxiong 2～10, Herba Asari 1～5, Rhizoma Zingiberis Recens 5～15, Cortex Phellodendri 1～5, Radix Angelicae Sinensis 1～5, Radix Scutellariae 1～5, Radix Glycyrrhizae 1～5, Galla Chinensis 1～5 and Flos Chrysanthemi 1～5.
2, a kind of method for preparing the described emulsified salt type Chinese herbal medicine of claim 1 emulsion used for washing and caring hair, this method comprises the step of following order:
(1) with polyhydric alcohol dissolving lanoline and wetting agent;
(2) in deionized water, add anion surfactant, non-ionic surface active agent, zwitterionic surfactant, cationic surfactant respectively, and stir;
(3) step (1) and (2) gains are placed the agitator tank of homogeneous emulsifying machine, add emulsified silicone oil, stearic acid, acrylic resin, settings shearing force is 600rpm～1200rpm, is warming up to 50～75 ℃, constant temperature stirring 5～25min;
(4) add sodium chloride, be cooled to 60 ℃～45 ℃, the setting shearing force is 600rpm～1200rpm, and mixing time 5～25min makes sodium chloride fully dissolve and reach emulsifying and homogenizing under strong shear action;
(5) add Chinese herbal medicine extract and Pearl Concentrate, temperature, shearing force are constant, mixing time 5～25min;
(6) add vitamin B, essence, the reduction shearing force is 600rpm～1000rpm, progressively is cooled to room temperature;
(7) regulating pH value is 6.0～8.0;
(8) step (7) gains are evacuated to the finished product jar, quiet to ageing 20～28 hours, promptly get product;
Wherein, described Chinese herbal medicine extract is made by following method: Chinese herbal medicine is clean, dried and crushed to 20～40 orders, with water is to extract solvent, liquid-solid ratio 3: 1, ebuillition of heated 30min after-filtration, filtering residue repeats to extract 3 times, merging filtrate concentrates filtrate, and concentrated solution carries out alcohol with 4～5 times of amount 95% ethanol and analyses, cross the elimination polysaccharide, concentrate, be required Chinese herbal medicine extract behind the vacuum drying.
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Address after: 650118 No. 235, Wuhua, Kunming District, Yunnan, Jianshe Road Co-patentee after: YUNNAN PROVINCIAL ENERGY INVESTMENT CO.,LTD. Patentee after: Kunming University of Science and Technology Address before: 650118 Kunming University of Science and Technology, Kunming, Yunnan Co-patentee before: YUNNAN SALT & SALT CHEMICAL CO.,LTD. Patentee before: Kunming University of Science and Technology |
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