CN102631304B - Preparation method of shampoo salt emulsion - Google Patents
Preparation method of shampoo salt emulsion Download PDFInfo
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- CN102631304B CN102631304B CN2012101428898A CN201210142889A CN102631304B CN 102631304 B CN102631304 B CN 102631304B CN 2012101428898 A CN2012101428898 A CN 2012101428898A CN 201210142889 A CN201210142889 A CN 201210142889A CN 102631304 B CN102631304 B CN 102631304B
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Abstract
The invention discloses a shampoo salt emulsion and a preparation method thereof. The shampoo salt emulsion is characterized by comprising the following components in parts by weight: 10-30 parts of edible salt, 10-40 parts of surfactant, 0.1-5 parts of suspension stabilizer, 1-10 parts of emulsified silicone oil, 0.1-5 parts of thickening agent, 0.1-1.5 parts of anti-dandruff agent, 0.1-3 parts of essential oil extracted from spice, 0.1-4 parts of humectant, 0.1-3 parts of positive ion conditioner, 0-5 parts of nutritive additive and 30-70 parts of deionized water. The invention also relates to a preparation method of the shampoo salt emulsion. Compared with the prior art, the shampoo salt emulsion has the advantages that the shampoo salt emulsion fully plays a synergistic effect of the edible salt and the anti-dandruff agent in the concentration range of 10-30 parts of salt containing amount and 0.1-1.5 parts of anti-dandruff agent; the respective beneficial effect of the edible salt and the anti-dandruff agent can be improved; and in addition, the natural salt can play functions of sterilization and corrosion resistance; and the product safety can be greatly improved.
Description
Technical field
The present invention relates to a kind of hair shampoo article, the invention still further relates to the preparation method of this hair shampoo article.
Background technology
In cosmetics, the effect of antiseptic is the protection product, makes it to avoid microbial contamination, prolongs the shelf life of product; Guarantee the safety of product, prevent that consumer from causing possible infection because use is subjected to the product of microbial contamination.At present, listed regulation was used during 56 kinds of cosmetics formed antiseptic and the maximum points for attention such as working concentration, the scope of application that allow thereof in 2007 in version " cosmetics health standard ".Classify according to active matter, be divided into be imidazolidinyl urea, in uride, isothiazolone, parabens, quaternary ammonium salt-15, benzoic acid/benzyl alcohol and derivant thereof, IPBC, triclosan etc.But the impact from the chemical composition of antiseptic is brought might cause skin abnormality hypertrophy, canceration; Irradiation at daylight issues biochemical variation, makes the people produce photaesthesia, skin rubefaction, blackening, pain; Cause that the people is irritated, symptom red, that itch occurs; Cause the potential risks such as burn of skin, worry the formaldehyde that discharges such as DMDMH; Kazon series is chloride, may stimulation be arranged to some skin quality; IPBC may cause taking in the potential risk of the known antiseptic such as iodine.Along with the progress of science and technology, the medium material of plant extract quintessence oil or polarity substitutes traditional chemical preservative as effective natural antiseptic agent.
According to statistics, all in various degree puzzlements that is subject to dandruff of the adult more than 80%, the dandruff problem has become the second largest hair problem that is only second to alopecia and perplexs consumer.For consumer demand, anti-dandruff class hair washing product emerges in an endless stream on the Vehicles Collected from Market, and the anti-dandruff shampoo product that utilizes the characteristic of edible salt bactericidal antiphlogistic to make is less.Research is found to cause the factor of dandruff to mainly contain three: chlosma, sebum, individual susceptible type.Wherein individual susceptibility is everyone intrinsic can't changing, and modern science and technology also is difficult to accomplish the fully inhibition to sebum secretion, and therefore the most effective anti-dandruff method is by using the antifungal effective ingredient to suppress chlosma at present.There is in the market multiple antifungal effective ingredient available, such as salicylic acid, ZPT, OCT, climbazole and ketoconazole etc.According to nature, cost of material and the safety in utilization of raw material, Zinc pyrithione (ZPT) remains one of the strongest candidate, and climbazole is number two.
A lot of antibiotic anti-dandruff technical literatures are disclosed in the prior art, be 200710135779.8 be called that if any application number " a kind of antibiotic desquamation compositions and application thereof " and application number are that the 201010511385.X name is called the application for a patent for invention of " a kind of antibiotic desquamation compositions and application thereof " open, a kind of anti-dandruff composition that comprises Zinc Pyrithione (ZPT) is disclosed, point out that ZPT is to antibacterial, mycovirus has powerful killing and the inhibition effect, can go out by seborrhea, convention amount is nontoxic to human body, life-time service has no side effect, be widely used in preparation removing scurf and relieving itching shampoo and hair moisturizer, but the ZPT large usage quantity of using for reaching effective anti-dandruff effect.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of have sterilizing and itch-relieving and anti-dandruff function for the above-mentioned state of the art, and can guarantee that product is not subjected to the pollution of microorganism, safe and reliable hair washing salt breast.
Another technical problem to be solved by this invention provides the preparation method of a kind of technique hair washing salt breast simple, easy to make.
The present invention solves the problems of the technologies described above the technical scheme that adopts: a kind of hair washing salt breast is characterized in that comprising following component and weight proportion thereof:
10 ~ 30 parts of edible salts, 10 ~ 40 parts in surfactant, 0.1 ~ 5 part of suspension stabilizer, 1 ~ 10 part of emulsified silicone oil, 0.1 ~ 5 part of thickening agent, anti-dandruff dose 0.1 ~ 1.5 part, spice extracts 0.1 ~ 3 part of quintessence oil, 0.1 ~ 4 part of wetting agent, 0.1 ~ 3 part of cation opsonizing agent, 0 ~ 5 part of nourishing additive agent, 30 ~ 70 parts of deionized waters.
Described surfactant is at least a in sodium laureth sulfate, laureth ammonium sulfate, sodium lauryl sulfate, ammonium lauryl sulfate, dodecanamide propyl hydroxy sulfo lycine, cocamido propyl betaine, lauryl glucoside, lauryl alcohol phosphate ester potassium, Coconut Fatty Acid Monoethanolamide sulfosuccinic acid monoesters disodium, Coconut Fatty Acid Monoethanolamide, the sodium lauroyl sarcosine;
Described edible salt is at least a in sea salt, well mine salt or the lake salt;
Described suspension stabilizer is two phthalic acid amide;
Described anti-dandruff dose is Zinc Pyrithione;
Described wetting agent is at least a in glycerol, propylene glycol, the butanediol;
Described cation opsonizing agent is at least a in guar gum hydroxypropyl-trimethyl ammonium chloride, cationic cellulose, polyquaternary ammonium salt, the cation high molecular protein peptide;
Described emulsified silicone oil is at least a in polydimethylsiloxane, the dimethiconol;
Described thickening agent is at least a in xanthan gum, hydroxyethyl-cellulose, the cithrol;
Described nourishing additive agent is at least a in Jojoba oil, Aloe extract, pantothenylol, vitamins, amino acids, olive oil, hyaluronate sodium, the sodium lactate.
As preferably, comprise following component and weight proportion thereof:
12 ~ 26 parts of edible salts, 10 ~ 40 parts in surfactant, 0.3 ~ 3 part of suspension stabilizer, 2 ~ 6 parts of emulsified silicone oils, 0.1 ~ 3 part of thickening agent, anti-dandruff dose 0.5 ~ 1 part, spice extracts 0.1 ~ 2 part of quintessence oil, 0.3 ~ 2 part of wetting agent, 0.2 ~ 2 part of cation opsonizing agent, 0.3 ~ 4 part of nourishing additive agent, 30 ~ 70 parts of deionized waters.
A kind of preparation method of the salt breast of having one's hair wash is characterized in that comprising the steps;
1. water is placed reaction pot to be heated to 50 ~ 60 ℃, will be added to the water together with thickening agent with the scattered cation opsonizing agent of wetting agent stirs again;
2. then adding surfactant and suspension stabilizer stirs and is incubated (take 60 ℃ as good);
3. said mixture is evacuated and when lowering the temperature (45 ℃ for good), adds emulsified silicone oil and anti-dandruff dose, stir; Or add emulsified silicone oil, anti-dandruff dose and nourishing additive agent, stir;
4. add at last edible salt and spice and extract quintessence oil, stir, afterwards discharging of cooling (take 35 ℃ as good) is finished product, detects to change filling machine over to after qualified and carry out fill.
Hair washing salt of the present invention breast, described surfactant is respectively: sodium laureth sulfate (content is 70%), consumption are approximately 5 parts to approximately 25 parts, are preferably approximately 6 parts to approximately 22 parts, more preferably approximately 7 parts to approximately 19 parts; Laureth ammonium sulfate (purity is 70%) is approximately 5 parts to 30 parts, is preferably approximately 6 parts to approximately 25 parts, more preferably approximately 7 parts to approximately 20 parts; Sodium lauryl sulfate (content is 〉=92%) is approximately 0.1 part to approximately 10 parts, is preferably approximately 0.5 part to approximately 8 parts, more preferably approximately 1 part to approximately 6 parts; Ammonium lauryl sulfate (purity is 70%) is approximately 0.1 part to approximately 10 parts, is preferably approximately 0.5 part to approximately 8 parts, more preferably approximately 1.0 parts to approximately 6 parts; Dodecanamide propyl hydroxy sulfo lycine (content is 30%) consumption is approximately 1 part to approximately 15 parts, is preferably approximately 2 parts to approximately 13 parts, more preferably approximately 3 parts to approximately 10 parts; Cocamido propyl betaine (purity is 30%) is approximately 2 parts to 16 parts, is preferably approximately 3 parts to approximately 14 parts, more preferably approximately 4 parts to approximately 12 parts; Lauryl glucoside (purity is 50%) is approximately 0.5 part to approximately 6 parts, is preferably approximately 0.8 part to approximately 5 parts, more preferably approximately 1 part to approximately 4 parts; Sodium lauroyl sarcosine (purity is 30%) is approximately 0.5 part to approximately 6 parts, is preferably approximately 0.8 part to approximately 5 parts, more preferably approximately 1 part to approximately 4 parts; Lauryl alcohol phosphate ester potassium (purity is 50%) is approximately 0.5 part to approximately 6 parts, is preferably approximately 0.8 part to approximately 5 parts, more preferably approximately 1 part to approximately 4 parts; Coconut Fatty Acid Monoethanolamide sulfosuccinic acid monoesters disodium (purity is 40%) is approximately 0.5 part to approximately 6 parts, is preferably approximately 0.8 part to approximately 5 parts, more preferably approximately 1 part to approximately 4 parts; Coconut Fatty Acid Monoethanolamide (content for 〉=92%) consumption quality percentage composition is approximately 0.1 part to approximately 5 parts, is preferably approximately 0.2 part to approximately 4 parts, more preferably approximately 0.5 part to approximately 3 parts;
Above-mentioned edible salt (purity is 〉=91.0%) is approximately 10 parts to approximately 30 parts, be preferably approximately 11 parts to approximately 28 parts, more preferably approximately 12 parts to approximately 26 parts, even the Exposure to Sunlight sea salt (purity is 〉=91.0 parts) that more preferably is rich in the natural minerals elite is approximately 12 parts to approximately 26 parts.
Above-mentioned wetting agent is that glycerol (content is 〉=98.5%) consumption is approximately 0.1 part to approximately 5 parts, preferred approximately 0.2 part to approximately 4 parts, and more preferably from about 0.3 part to approximately 3 parts; Propylene glycol (content is 〉=98.5%) consumption is approximately 0.1 part to approximately 5 parts, preferred approximately 0.2 part to approximately 4 parts, and more preferably from about 0.3 part to approximately 3 parts; Butanediol (content is 〉=98.5%) consumption is approximately 0.1 part to approximately 5 parts, preferred approximately 0.2 part to approximately 4 parts, and more preferably from about 0.3 part to approximately 3 parts;
Above-mentioned suspension stabilizer is that two (hydrogenated-tallow group) phthalic acid amide (content is 〉=98.0%) consumption is approximately 0.1 part to approximately 5 parts, preferred approximately 0.2 part to approximately 4 parts, and more preferably from about 0.3 part to approximately 3 parts;
Above-mentioned thickening agent be respectively xanthan gum (viscosity for 〉=600mPas) consumption is approximately 0.1 part to approximately 3 parts, preferably approximately 0.1 part to approximately 2 parts, more preferably from about 0.1 part to approximately 1 part; Cetostearyl alcohol (content is 〉=99%) consumption is approximately 0.1 part to approximately 4 parts, preferred approximately 0.1 part to approximately 3 parts, and more preferably from about 0.1 part to approximately 2 parts; Hydroxyethyl-cellulose (content is 〉=87%) consumption is approximately 0.1 part to approximately 3 parts, preferred approximately 0.1 part to approximately 2.5 parts, and more preferably from about 0.1 part to approximately 2 parts;
Above-mentioned cation opsonizing agent be respectively the guar gum hydroxypropyl-trimethyl ammonium chloride (viscosity for 〉=2500mPas) consumption is approximately 0.1 part to approximately 3 parts, is preferably approximately 0.1 part to approximately 2 parts, more preferably approximately 0.1 part to approximately 1 part; Cationic cellulose (viscosity is that 50 ~ 60000mPas) consumptions are approximately 0.1 part to approximately 3 parts, preferred approximately 0.1 part to approximately 2 parts, and more preferably from about 0.1 part to approximately 1 part;
It is approximately 0.1 part to approximately 10 parts that above-mentioned emulsified silicone oil is respectively small particle diameter emulsified silicone oil (particle size range is≤2 μ m) consumption, preferred approximately 0.5 part to approximately 8 parts, and more preferably from about 1.0 parts to approximately 6 parts; (particle size range is D to large particle diameter emulsified silicone oil
5015.0 ~ 35.0 μ m) consumption is approximately 0.1 part to approximately 5 parts, is preferably approximately 0.2 part to approximately 4 parts, more preferably approximately 0.3 part to approximately 3 parts;
Above-mentioned anti-dandruff dose is that Zinc Pyrithione (content is 〉=95%) consumption is approximately 0.1 part to approximately 1 part, preferred approximately 0.3 part to approximately 1 part, and more preferably from about 0.5 part to approximately 1 part;
It is Fructus Citri Limoniae quintessence oil, Flos Rosae Rugosae quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil etc. that above-mentioned natural perfume material extracts quintessence oil, and its consumption is approximately 0.1 part to approximately 3 parts, preferred approximately 0.1 part to approximately 2.5 parts, and more preferably from about 0.1 part to approximately 2 parts;
Above-mentioned nourishing additive agent is D-panthenol, zinc oxide, Jojoba oil, Aloe extract, pantothenylol, vitamins, amino acids, olive oil, hyaluronate sodium, sodium lactate etc., its consumption is approximately 0.1 part to approximately 6 parts, preferred approximately 0.2 part to approximately 5 parts, more preferably from about 0.3 part to approximately 4 parts.
Compared with prior art, the invention has the advantages that: be rich in pure natural salt frosted microgranule and famous and precious plant extract elite in the prescription, during hair washing, the sodium ion that sodium chloride in the salt ionizes out can enter and destroy its body fluid balance and ph balancing in the bacterial body, make the bacterial cell dehydration dead, function with stronger disinfection, thereby guarantee to avoid the pollution of microorganism, and sodium chloride concentration can be diluted behind the chance water, thereby can not cause the phenomenon of human body skin dehydration, for the anti-dandruff dose of effectiveness that performance is maximum, provide a good basic environment.Edible salt energy softening skin cutin, effectively promote the circulation of health blood, improve metabolism, sterilizing and itch-relieving, keep the moisture of skin, anti-dandruff dose has antifungic action, can reduce the generation of the dandruff, cooperate with edible salt to can further improve sterilizing and itch-relieving and anti-dandruff effect, be beneficial to the maximum sterilizing function of edible salt performance.In the concentration range of rational salinity and anti-dandruff dose, give full play to the synergism of edible salt and anti-dandruff dose, improve both beneficial effects separately, and constant product quality, foam is abundant.In addition, the preparation method technique among the present invention is simple, easy to operate, and safety is higher, easily operation.
For the anti-dandruff effect that guarantees effectively to sterilize reduces anti-dandruff dose of consumption simultaneously, adopt anti-dandruff dose and edible salt to be used in conjunction with, this product need not use antiseptic simultaneously, has effectively guaranteed the safety in utilization of product.
The specific embodiment
Below in conjunction with embodiment the present invention is described in further detail.
Embodiment one: the prescription of the present embodiment basic composition is:
30 parts in sea salt, 13 parts of sodium laureth sulfate (purity is 70%), 6 parts of dodecanamide propyl hydroxy sulfo lycines (purity is 30%), 5 parts of sodium lauryl sulfates (purity is 92%), 10 parts of Coconut Fatty Acid Monoethanolamides (purity is 92%), 0.5 part of two phthalic acid amide (purity is 98%), 0.5 part of Zinc Pyrithione suspension (purity is 50%), 2 parts of polydimethylsiloxane, 0.6 part of Fructus Citri Limoniae quintessence oil, 0.4 part of propylene glycol, 0.5 part of guar gum hydroxypropyl-trimethyl ammonium chloride, 0.5 part of xanthan gum, 0.8 part of D-panthenol, 39.2 parts in water, above-mentioned is parts by weight.
Preparation method includes following steps:
One, distilled water is placed reaction pot be heated to 60 ℃, will join in the distilled water with the scattered xanthan gum of propylene glycol and guar gum hydroxypropyl-trimethyl ammonium chloride again and stir;
Two, then, adding sodium laureth sulfate, dodecanamide propyl hydroxy sulfo lycine, sodium lauryl sulfate, Coconut Fatty Acid Monoethanolamide and two phthalic acid amide stir and are incubated;
Three, then, after the mixture that stirs is evacuated, add polydimethylsiloxane, Zinc Pyrithione suspension and D-panthenol, be stirred to and be uniformly dispersed;
Four, last, add sea salt and Fructus Citri Limoniae quintessence oil, and stir, discharging after the cooling is finished product.
Embodiment two: the prescription of the present embodiment basic composition is:
25 parts in sea salt, 16 parts of sodium laureth sulfate (purity is 70%), 4 parts of dodecanamide propyl hydroxy sulfo lycines (purity is 30%), 2 parts of sodium lauryl sulfates (purity is 92%), 15 parts of Coconut Fatty Acid Monoethanolamides (purity is 92%), 1.0 parts of two phthalic acid amide (purity is 98%), 1.0 parts of Zinc Pyrithione suspensions (purity is 50%), 3 parts of polydimethylsiloxane, 1 part of dimethiconol, 0.3 part of Flos Rosae Rugosae quintessence oil, 1 part of glycerol, 0.5 part of cationic cellulose, 0.4 part of xanthan gum, 0.5 part of cetostearyl alcohol, 0.3 part of D-panthenol, 0.5 part of vitamin E, 42 parts in water, above-mentioned is mass percent.
Preparation method includes following steps:
One, distilled water is placed reaction pot be heated to 60 ℃, will join in the distilled water with the scattered xanthan gum of glycerol and cationic cellulose again and stir;
Two, then, add sodium laureth sulfate, dodecanamide propyl hydroxy sulfo lycine, sodium lauryl sulfate, Coconut Fatty Acid Monoethanolamide and two phthalic acid amide, cetostearyl alcohol stirs and be incubated;
Three, then, after the mixture that stirs is evacuated, add polydimethylsiloxane, dimethiconol, Zinc Pyrithione suspension, D-panthenol and vitamin E, be stirred to and be uniformly dispersed;
Four, last, add sea salt and Flos Rosae Rugosae quintessence oil, and stir, discharging after the cooling is finished product.
Embodiment three: the present embodiment prescription basic composition is:
20 parts in sea salt, 17 parts in laureth ammonium sulfate (purity is 70%), 4 parts of dodecanamide propyl hydroxy sulfo lycines (purity is 30%), 4 parts of ammonium lauryl sulfate (purity is 70%), 2 parts of Coconut Fatty Acid Monoethanolamides (purity is 92%), 1 part of two phthalic acid amide (purity is 98%), 1 part of Zinc Pyrithione suspension (purity is 50%), 5 parts of polydimethylsiloxane, 0.3 part of Flos Rosae Rugosae quintessence oil, 1.0 parts of glycerol, 0.3 part of cationic cellulose, 0.3 part of guar gum hydroxypropyl-trimethyl ammonium chloride, 0.4 part of xanthan gum, 0.5 part of hydroxyethyl-cellulose, 0.3 part of D-panthenol, 0.5 part of fibroin, 42.4 parts in water, above-mentioned is mass percent.
Preparation method includes following steps:
One, distilled water is placed reaction pot be heated to 60 ℃, will join in the distilled water and stir with the scattered xanthan gum of glycerol, hydroxyethyl-cellulose, cationic cellulose, guar gum hydroxypropyl-trimethyl ammonium chloride again;
Two, then, adding laureth ammonium sulfate, dodecanamide propyl hydroxy sulfo lycine, ammonium lauryl sulfate, Coconut Fatty Acid Monoethanolamide and two phthalic acid amide stir and are incubated;
Three, then, after the mixture that stirs is evacuated, add polydimethylsiloxane, Zinc Pyrithione suspension, D-panthenol and fibroin, be stirred to and be uniformly dispersed;
Four, last, add sea salt and Flos Rosae Rugosae quintessence oil, and stir, discharging after the cooling is finished product.
Embodiment four: the present embodiment prescription basic composition is:
15 parts in sea salt, 12 parts of sodium laureth sulfate (purity is 70%), 6 parts of cocamido propyl betaine (purity is 30%), 3 parts of sodium lauroyl sarcosines (purity is 50%), 15 parts of Coconut Fatty Acid Monoethanolamides (purity is 92%), 1.5 parts of two phthalic acid amide (purity is 98%), 1.5 parts of Zinc Pyrithione suspensions (purity is 50%), 3 parts of dimethiconols, 0.5 part of Herba Lysimachiae foenum-graeci quintessence oil, 0.8 part of glycerol, 0.1 part of cationic cellulose, 0.1 part of guar gum hydroxypropyl-trimethyl ammonium chloride, 0.5 part of xanthan gum, 0.3 part of vitamin B5,0.5 part of fibroin, 53.7 parts in water, above-mentioned is mass percent.
Preparation method includes following steps:
One, distilled water is placed reaction pot be heated to 60 ℃, will join in the distilled water and stir with the scattered xanthan gum of glycerol, cationic cellulose, guar gum hydroxypropyl-trimethyl ammonium chloride again;
Two, then, adding sodium laureth sulfate, cocamido propyl betaine, sodium lauroyl sarcosine, Coconut Fatty Acid Monoethanolamide and two phthalic acid amide stir and are incubated;
Three, then, after the mixture that stirs is evacuated, add dimethiconol, Zinc Pyrithione suspension, vitamin B5 and fibroin, be stirred to and be uniformly dispersed;
Four, last, add sea salt and Herba Lysimachiae foenum-graeci quintessence oil, and stir, discharging after the cooling is finished product.
Embodiment five: the present embodiment prescription basic composition is:
10 parts in sea salt, 16 parts of sodium laureth sulfate (purity is 70%), 5 parts of cocamido propyl betaine (purity is 30%), 2 parts of sodium lauroyl sarcosines (purity is 50%), 2 parts of Coconut Fatty Acid Monoethanolamides (purity is 92%), 1 part of lauryl glucoside (purity is 50%), 1 part of two phthalic acid amide (purity is 98%), 2 parts of Zinc Pyrithione suspensions (purity is 50%), 3 parts of polydimethylsiloxane, 0.3 part of Herba Lysimachiae foenum-graeci quintessence oil, 1.2 parts of glycerol, 0.4 part of guar gum hydroxypropyl-trimethyl ammonium chloride, 0.6 part of xanthan gum, 1.5 parts of Aloe extraction solution, 0.5 part of fibroin, 53.5 parts in water, above-mentioned is mass percent.
Preparation method includes following steps:
One, distilled water is placed reaction pot be heated to 60 ℃, will join in the distilled water and stir with the scattered xanthan gum of glycerol, guar gum hydroxypropyl-trimethyl ammonium chloride again;
Two, then, adding sodium laureth sulfate, cocamido propyl betaine, sodium lauroyl sarcosine, Coconut Fatty Acid Monoethanolamide, lauryl glucoside and two phthalic acid amide stir and are incubated;
Three, then, after the mixture that stirs is evacuated, add polydimethylsiloxane, climbazole, vitamin B5, Aloe extraction solution and fibroin, be stirred to and be uniformly dispersed;
Four, last, add sea salt and Herba Lysimachiae foenum-graeci quintessence oil, and stir, discharging after the cooling is finished product.
Application Example:
Object of study: the anti-dandruff effect assessment of product
Research method: the antibacterial ring test in-vitro evaluation method that adopts the anti-dandruff effect of product
Implementation step:
1, the collection of chlosma, separation, cultivation
Gather: employing is scraped the bits method and is drawn materials at the normal person's head with dandruff;
Isolation identification: be inoculated in Leeming ﹠amp; In the Notman culture medium flat plate, 32 ℃ of lower cultivations about 10 days, the various chlosmas of gained are isolated single bacterium colony in same culture medium flat plate line, identify according to the authentication method in the document " classification of Malassezia and in several dermopathic distribution situations ".
2, the antibacterial ring test of product
1. the preparation of test specimen: choose anti-dandruff effect preferably commercially available anti-dandruff shampoo 1 and shampoo 2
The proportion of composing of sample sea salt and anti-dandruff dose:
| Numbering | Sea salt content | Anti-dandruff dose of (Zinc Pyrithione) content |
| 1 | 10 parts | 0.8 part |
| 2 | 12.5 part | 0.8 part |
| 3 | 15 parts | 0.8 part |
| 4 | 17.5 part | 0.8 part |
| 5 | 20 parts | 0.8 part |
2. the preparation of coupons: get qualitative filter paper of Xinhua, break into diameter 5mm circular filter paper sheet with card punch, through pressuresteam sterilization, the coupons of getting the sterilization treatment post-drying is some, dip respectively shampoo Xiao Xu to be checked on coupons with aseptic nipper, coupons is smeared evenly as far as possible.
3. dull and stereotyped preparation: will activate the bacteria suspension that good Malassezia furfur is mixed with 106cfu/ml ~ 107cfu/ml, and get the Leeming﹠amp that bacteria suspension 0.3ml is applied in 12cm; On the Notman culture medium flat plate.With above-mentioned contain the dull and stereotyped 10min of placement of bacterium after, in aseptic superclean bench, open flat plate cover, dry up flat board (approximately 20min) with sterile wind.
4. the mensuration of fungistatic effect: be placed with 1 test print in each flat board, 1 negative control (not containing test hair washing sample) print, totally 2.After being placed with, gently press print with aseptic paster, make it be close to planar surface.Build plate, put to be inverted in 32 ℃ of constant incubators and cultivated 7 days, with the diameter of vernier caliper measurement record inhibition zone.
Antibacterial ring test result:
As a kind of natural antiseptic agent, the protection product is avoided microbial contamination within the shelf-life with pure natural sea salt elite.Main component sodium chloride physicochemical properties are stable in the sea salt in addition, can not cause raw material rotten and make skin occur irritated or stimulate because of illumination or with other substance reactions in the product, simultaneously itself also can not discharge poisonous and harmful substance, this antiseptic is a kind of natural, safe cosmetics preservative.Sea salt can also be assisted cleaning skin or hair, utilizes the permeability of salt during hair washing, gos deep into skin, and blood circulation promoting enhances metabolism, and takes moisture unnecessary in the pore and fine material, fat etc. out of, plays the effect of weight-reducing; Utilize the scrub of salt, remove the cutin of skin surface, the skin that thirst smoothly comes off, delay skin aging plays the effect of body building and beauty treatment, and life-time service can promote skin metabolism, the deep layer cleaning skin, unnecessary oils and fats and horny layer are removed in antiinflammatory, sterilization, antipruritic.During hair washing, utilize sea salt and the anti-dandruff dose of bactericidal action to hair, can reduce the infection of sending out skin and root of hair, replenish simultaneously the mineral of hair, remove the greasy of hair, suppress the dandruff growth, have in addition much to studies show that the effect that anticreep is arranged with the salt hair washing.
Sea salt in the various embodiments described above also can adopt well mine salt or lake salt to substitute, and effect is very nearly the same, is not providing embodiment here.
Claims (6)
1. preparation method of salt breast of having one's hair wash is characterized in that this hair washing salt breast comprises following component and weight proportion thereof:
10 ~ 30 parts of edible salts, 10 ~ 40 parts in surfactant, 0.1 ~ 5 part of suspension stabilizer, 1 ~ 10 part of emulsified silicone oil, 0.1 ~ 5 part of thickening agent, anti-dandruff dose 0.1 ~ 1.5 part, spice extracts 0.1 ~ 3 part of quintessence oil, 0.1 ~ 4 part of wetting agent, 0.1 ~ 3 part of cation opsonizing agent, 0 ~ 5 part of nourishing additive agent, 30 ~ 70 parts of deionized waters;
Described thickening agent is at least a in xanthan gum, hydroxyethyl-cellulose, the cithrol;
Described anti-dandruff dose is Zinc Pyrithione;
Described cation opsonizing agent is at least a in guar gum hydroxypropyl-trimethyl ammonium chloride, cationic cellulose, polyquaternary ammonium salt, the cation high molecular protein peptide;
The method comprises the steps;
1. water is placed reaction pot to be heated to 50 ~ 60 ℃, will be added to the water together with thickening agent with the scattered cation opsonizing agent of wetting agent stirs again;
2. then adding surfactant and suspension stabilizer stirs and is incubated;
3. the mixture after the above-mentioned insulation is evacuated, adds emulsified silicone oil and anti-dandruff dose, stir; Or add emulsified silicone oil, anti-dandruff dose and nourishing additive agent, stir;
4. add at last edible salt and spice and extract quintessence oil, stir, discharging after the cooling is finished product.
2. preparation method according to claim 1 is characterized in that described surfactant is at least a in sodium laureth sulfate, laureth ammonium sulfate, sodium lauryl sulfate, ammonium lauryl sulfate, dodecanamide propyl hydroxy sulfo lycine, cocamido propyl betaine, lauryl glucoside, lauryl alcohol phosphate ester potassium, Coconut Fatty Acid Monoethanolamide sulfosuccinic acid monoesters disodium, Coconut Fatty Acid Monoethanolamide, the sodium lauroyl sarcosine.
3. preparation method according to claim 1 is characterized in that described edible salt is at least a in sea salt, well mine salt or the lake salt.
4. preparation method according to claim 1 is characterized in that described suspension stabilizer is two phthalic acid amide.
5. preparation method according to claim 1 is characterized in that described wetting agent is at least a in glycerol, propylene glycol, the butanediol.
6. preparation method according to claim 1 is characterized in that described emulsified silicone oil is at least a in polydimethylsiloxane, the dimethiconol; Described thickening agent is at least a in xanthan gum, hydroxyethyl-cellulose, the cithrol; Described nourishing additive agent is at least a in Jojoba oil, Aloe extract, pantothenylol, vitamins, amino acids, olive oil, hyaluronate sodium, the sodium lactate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101428898A CN102631304B (en) | 2012-05-10 | 2012-05-10 | Preparation method of shampoo salt emulsion |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101428898A CN102631304B (en) | 2012-05-10 | 2012-05-10 | Preparation method of shampoo salt emulsion |
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| CN108186439A (en) * | 2018-02-09 | 2018-06-22 | 广州御延堂生物科技有限公司 | A kind of sea salt nourishes hair cream and preparation method thereof |
| CN109646352A (en) * | 2019-01-10 | 2019-04-19 | 澳宝化妆品（惠州）有限公司 | A kind of hair-washing composition with anti-dandruff performance containing pomegranate rind extract |
| CN113842331A (en) * | 2021-11-17 | 2021-12-28 | 广州宝丝捷生物科技有限公司 | Novel soothing, nursing, refreshing and anti-dandruff shampoo and preparation method thereof |
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| JPS5682897A (en) * | 1979-12-11 | 1981-07-06 | Sanyo Chemical Ind Ltd | Shampoo composition |
| US5104645A (en) * | 1990-02-02 | 1992-04-14 | The Proctor & Gamble Company | Antidandruff shampoo compositions |
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| CN101084870A (en) * | 2007-06-22 | 2007-12-12 | 昆明理工大学 | Emulsifying salt type traditional Chinese herbs emulsion used for washing and caring hair and preparation method thereof |
| CN101249058A (en) * | 2008-02-26 | 2008-08-27 | 昆明理工大学 | Anti-dandruff relieve itching hair washing cream liquid containing inorganic salt and Chinese medicine and preparation thereof |
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| JP昭56-82897A 1981.07.06 |
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