CN105534795A - Mild anti-dandruff hair washing salt and preparation method thereof - Google Patents
Mild anti-dandruff hair washing salt and preparation method thereof Download PDFInfo
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- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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Abstract
The invention disclosesamild anti-dandruff hair washing salt which is prepared from the following main raw materials in parts by mass: 13-20 parts of bamboo salt, 60-85 parts of deionized water, 3-4 parts of betaine, 10-12 parts of grecian laurel fruit, 8-10 parts of cortex mori, 7-9 parts of spina gleditsiae, 6-9 parts of szechwan chinaberry fruit, 5-7 parts of hamamelis mollis oliver, 2-5 parts of herb of alligator alternanthera, 3-6 parts of hairyvein agrimonia herb and bud, 4-6 parts of liquorice, 0.6-1.2 parts of couch grass essential oil, 0.5-0.7 part of sorbitol, 0.4-0.6 part of sodium dodecyl sulfate, 0.5-0.7 part of silicone oil and 0.4-0.6 part of zinc pyrithione. The hair washing salt disclosed by the invention has powerful effects of sterilization, bacteria inhibiting, dandruff removal and itching relieving and can prevent seborrhea; and due to the permeability of salt in hair washing, the hair washing salt goes deep into the skin, promotes blood circulation and skin metabolism and removes redundant fat and cuticle.
Description
Technical field
The present invention relates to field of medical materials, especially relate to the hair washing Salt And Preparation Method of energy moderately removing dandruff.
Background technology
Dandruff is the horn cell that scalp comes off, and under normal circumstances, horn cell comes off seldom, very slow, can not be seen significantly.But under certain stimulates, jejune horn cell produces in a large number, luming comes off, and forms flying or fluttering in profusion " snowflake " phenomenon, the dandruff be namely commonly called as.Dandruff causes primarily of dandruff pityrosporion ovale, majority's scalp has dandruff pityrosporion ovale, and what have does not produce symptom.Dandruff pityrosporion ovale affects by interior extrinsic factor, breeds in a large number, destroys the homergy of scalp, and this is the main cause that dandruff produces.Be deficient in vitamin in health B
12, vitaminF, vitamin B
6, dandruff also can be caused many.The dandruff is general skin dirt, and namely the horny layer of epidermis face of constantly peeling off produces, and be also metabolic result, the dandruff is divided into the physiological dandruff and the pathologic dandruff.The physiological dandruff is generally grown up common for dryness scurf, and in bran shape, linen little phosphine bits are dispersed between hair.Another kind of is oiliness scurf, and scalp and hair contain the sensation of greasy glutinous cunning, above the attached thick crust having thickness to differ, this clear condition is common especially with newborn child.The pathologic dandruff refers to that scalp is because of bacteriological infection, fungal infection, or other physics, chemical injury cause the inflammation of scalp.Generally show as the dandruff too much, pore is blocked, just causes hair weak state, easy bacterial multiplication, and chafe produces head pruritus problem.
The food of dandruff sporeformer is exactly scalp pomade, and dandruff sporeformer in fact each number of people has, and just because food is deficient, breeding is slowly.Once food is abundant, rapidly, dandruff just can see in growth.So anti-dandruff method has two: one to be deoil, two is Antifungis.General Antifungi product has: cave health azoles (universal, side effect is large, easy alopecia), arsenic sulfur cave zinc (pure import formula, side effect is little).
In the method for existing shampoo salt, publication number CN102631304A(application number 201210142889.8) patent discloses a kind of shampoo salt emulsion and preparation method thereof, comprise following component and weight proportion thereof: edible salt 10-30 part, surfactant 10-40 part, suspension stabilizer 0.1-5 part, emulsified silicone oil 1-10 part, thickening agent 0.1-5 part, anti-dandruff agent 0.1-1.5 part, spice extracts quintessence oil 0.1-3 part, wetting agent 0.1-4 part, cation opsonizing agent 0.1-3 part, nourishing additive agent 0-5 part, deionized water 30-70 part.Publication number CN103536487A(application number 201310491164.4) patent discloses a kind of dandruff control shampoo containing, be made up of the raw material of following parts by weight: edible white vinegar 12-30 part, medicated beer 20-50 part, Radix Paeoniae Rubra 22-28 part, Fructus Xanthii 20-30 part, Semen Sesami Nigrum 15-50 part.Publication number CN105055203A(application number 201510442004.X) patent discloses a kind of antidandruff and antipruritic shampoo, be made up of the raw material of following parts by weight: edible white vinegar 2-30 part, medicated beer 2-50 part, Radix Angelicae Sinensis 2-30 part, Fructus Forsythiae 10-30 part, Semen Sesami Nigrum 5-50 part, Rhizoma Cimicifugae 1-15 part, Radix Polygoni Multiflori 1-20 part, Rhizoma Zingiberis Recens 1-10 part, Cortex Acanthopancis 2-8 part.
Traditional therapy is that local uses 17-hydroxy-11-dehydrocorticosterone or the medicine such as coal tar, Xi Ersheng liquid, though dandruff can be removed to a certain extent, but because of the reason such as toxic and side effects and dosage, life-time service can produce injury to scalp, patient often not easily accepts, can not life-time service, and easily cause capitis pityriasis and dandruff dermatitis for a long time more not or recurrent exerbation.Not only can not nourish scalp, can decompose on the contrary and peel off those dry, loose skin, the situation that the dandruff is come off is aggravated.
Summary of the invention
For the deficiencies in the prior art, an object of the present invention is the shampoo salt providing energy moderately removing dandruff, there is the powerful effect with anti-bacteria breeding, removing scurf and relieving itching of killing, anti-sebum can overflow, utilize the permeability of salt during hair washing, go deep into skin, blood circulation promoting, promote skin metabolism, deep layer cleaning skin, remove excess oil and horny layer.Another object is just to provide the preparation method of the shampoo salt of above-mentioned energy moderately removing dandruff.
Above-mentioned purpose of the present invention is achieved through the following technical solutions:
The shampoo salt of energy moderately removing dandruff, takes off the primary raw material stating quality proportioning and is prepared from: bamboo salt 13-20 part; Deionized water 60-85 part; Betanin 3-4 part; Fructus Lauri nobilis 10-12 part; Cortex Mori 8-10 part; Spina Gleditsiae 7-9 part; Fructus Toosendan 6-9 part; Radix Hamamelidis Mollis 5-7 part; Alternanthera philoxeroides 2-5 part; Herba Agrimoniae 3-6 part; Radix Glycyrrhizae 4-6 part; Rhizoma Imperatae quintessence oil 0.6-1.2 part; Sorbitol 0.5-0.7 part; Sodium lauryl sulphate 0.4-0.6 part; Silicone oil 0.5-0.7 part; Zinc Pyrithione 0.4-0.6 part.
The shampoo salt of energy moderately removing dandruff, preferred scheme is, takes off the primary raw material stating quality proportioning and is prepared from: bamboo salt 16-18 part; Deionized water 65-80 part; Betanin 3.3-3.7 part; Fructus Lauri nobilis 10.5-11.5 part; Cortex Mori 8.5-9.5 part; Spina Gleditsiae 7.5-8.5 part; Fructus Toosendan 7-8 part; Radix Hamamelidis Mollis 5.5-6.5 part; Alternanthera philoxeroides 3-4 part; Herba Agrimoniae 4-5 part; Radix Glycyrrhizae 4.5-5.5 part; Rhizoma Imperatae quintessence oil 0.8-1.0 part; Sorbitol 0.55-0.65 part; Sodium lauryl sulphate 0.45-0.55 part; Silicone oil 0.55-0.65 part; Zinc Pyrithione 0.45-0.55 part.
The shampoo salt of energy moderately removing dandruff, the scheme be more preferably is, takes off the primary raw material stating quality proportioning and is prepared from: bamboo salt 17 parts; Deionized water 72 parts; Betanin 3.5 parts; Fructus Lauri nobilis 11 parts; Cortex Mori 9 parts; Spina Gleditsiae 8 parts; Fructus Toosendan 7.5 parts; Radix Hamamelidis Mollis 6 parts; Alternanthera philoxeroides 3.5 parts; Herba Agrimoniae 4.5 parts; 5 parts, Radix Glycyrrhizae; Rhizoma Imperatae quintessence oil 0.9 part; Sorbitol 0.6 part; Sodium lauryl sulphate 0.5 part; Silicone oil 0.6 part; Zinc Pyrithione 0.5 part.
The preparation method of the shampoo salt of above-mentioned energy moderately removing dandruff, step is as follows:
(1) Fructus Lauri nobilis and Fructus Toosendan rice wine is soaked 2-3 days, take out, moderate heat stir-fries 30-40 minute, dries, pulverizes, cross 120-160 mesh sieve;
(2) Cortex Mori, Alternanthera philoxeroides, Herba Agrimoniae and Radix Glycyrrhizae are smashed, be placed in multi-function extractor, add water, extract twice, each extraction 40-50 minute, merge extractive liquid;
(3) be placed in marmite by Spina Gleditsiae and Radix Hamamelidis Mollis, soak 20-30 minute, add white vinegar, decoct twice, each decoction 30-40 minute, collecting decoction, obtains medicinal liquid;
(4) by step (2) gained extracting solution and step (3) gained medicinal liquid mix homogeneously, be concentrated into 1/2 of original volume, add step (1) gained powder, fully stir, room temperature places 40-60 minute;
(5) by bamboo salt and betanin mixing, be placed in heatproof glass container, add deionized water, (preferable temperature controls as 60-70 DEG C in heating while stirring, be more preferably temperature to control to be 65 DEG C), continue to be stirred to and dissolve completely, when being cooled to 30-40 DEG C, add Sorbitol, sodium lauryl sulphate and Zinc Pyrithione, stir 30-40 minute;
(6) step (4) gained end product is joined in step (5) gained end product, mix homogeneously, be concentrated into the thick liquid that relative density is 1.05-1.10, add citric acid, regulate Ph value to be 5-6, add Rhizoma Imperatae quintessence oil and silicone oil, stir, sterilize 20-30 minute at 120-140 DEG C of temperature, is placed in degassing tank vacuum outgas, discharging after cooling, encapsulates with plastic packing soft tube.
The preparation method of the shampoo salt of above-mentioned energy moderately removing dandruff, preferred scheme is: the consumption of the preferred rice wine of step (1) is 3-5 times of Fructus Lauri nobilis and Fructus Toosendan quality, and the consumption being more preferably rice wine is Fructus Lauri nobilis and Fructus Toosendan quality 4 times.
The preparation method of the shampoo salt of above-mentioned energy moderately removing dandruff, preferred scheme is: step (1) is preferred crosses 130-150 mesh sieve, is more preferably 140 mesh sieves.
The preparation method of the shampoo salt of above-mentioned energy moderately removing dandruff, preferred scheme is: step (2) is preferably each extracts 43-47 minute, more seriously extracts 45 minutes at every turn.
The preparation method of the shampoo salt of above-mentioned energy moderately removing dandruff, preferred scheme is: the consumption of the preferred white vinegar of step (3) is the 15%-20% of Spina Gleditsiae and Radix Hamamelidis Mollis quality, and the consumption being more preferably white vinegar is 18% of Spina Gleditsiae and Radix Hamamelidis Mollis quality.
The preparation method of the shampoo salt of above-mentioned energy moderately removing dandruff, preferred scheme is: step (6) preferably regulates Ph value to be 5.3-5.7, is more preferably and regulates Ph value to be 5.5.
Above-mentioned can the preparation method of shampoo salt of moderately removing dandruff, preferred scheme is: step (6) preferably sterilizes 23-27 minute at 125-135 DEG C of temperature, to be more preferably at 130 DEG C of temperature sterilization 25 minutes.
Using method: after being drenched by hair, gets appropriate shampoo salt and is placed in turn round after the palm of the hand crumples out a little foam again and sends out, clean after 1-2 minute with clear water.
Beneficial effect of the present invention is mainly reflected in:
1, shampoo salt of the present invention has powerful bactericidal, the effect of removing scurf and relieving itching, anti-sebum can overflow, utilizes the permeability of salt, go deep into skin, blood circulation promoting during hair washing, promote skin metabolism, remove excess oil and horny layer.
2, shampoo salt of the present invention is compared with existing dandruff control shampoo containing, and have better removing scurf and relieving itching function, convention amount is harmless to human non-toxic, safe without toxic side effect, is applicable to long term consumer and uses.
3, shampoo salt of the present invention utilizes the scrub of salt to remove the cutin of skin surface, and come off the skin that thirst smoothly, delay skin aging, can secondary skin or hair.
4, the anti-inflammation and sterilization effect of shampoo salt of the present invention is better, can reduce the infection sending out skin and root of hair.
Detailed description of the invention
Describe technical scheme of the present invention in detail below in conjunction with embodiment and experimental example, but protection domain is not by this restriction.
Embodiment 1 can the shampoo salt of moderately removing dandruff, takes off to state primary raw material and be prepared from (getting 80g for every part): bamboo salt 13 parts; Deionized water 60 parts; Betanin 3 parts; Fructus Lauri nobilis 10 parts; Cortex Mori 8 parts; Spina Gleditsiae 7 parts; Fructus Toosendan 6 parts; Radix Hamamelidis Mollis 5 parts; Alternanthera philoxeroides 2 parts; Herba Agrimoniae 3 parts; 4 parts, Radix Glycyrrhizae; Rhizoma Imperatae quintessence oil 0.6 part; Sorbitol 0.5 part; Sodium lauryl sulphate 0.4 part; Silicone oil 0.5 part; Zinc Pyrithione 0.4 part.
The preparation process of the shampoo salt of energy moderately removing dandruff is as follows:
(1) Fructus Lauri nobilis and Fructus Toosendan rice wine (consumption is 3 times of Fructus Lauri nobilis and Fructus Toosendan quality) are soaked 2 days, take out, moderate heat stir-fries 30 minutes, dries, and pulverizes, and crosses 120 mesh sieves;
(2) Cortex Mori, Alternanthera philoxeroides, Herba Agrimoniae and Radix Glycyrrhizae are smashed, be placed in multi-function extractor, add water, extract twice, each extraction 40 minutes, merge extractive liquid;
(3) be placed in marmite by Spina Gleditsiae and Radix Hamamelidis Mollis, soak 20 minutes, add white vinegar (consumption is 15% of Spina Gleditsiae and Radix Hamamelidis Mollis quality), decoct twice, each decoction 30 minutes, collecting decoction, obtains medicinal liquid;
(4) by step (2) gained extracting solution and step (3) gained medicinal liquid mix homogeneously, be concentrated into 1/2 of original volume, add step (1) gained powder, fully stir, room temperature places 40 minutes;
(5) by bamboo salt and betanin mixing, be placed in heatproof glass container, add deionized water, heat while stirring (it is 60 DEG C that temperature controls), continue to be stirred to and dissolve completely, when being cooled to 30 DEG C, add Sorbitol, sodium lauryl sulphate and Zinc Pyrithione, stir 30 minutes;
(6) step (4) gained end product is joined in step (5) gained end product, mix homogeneously, be concentrated into the thick liquid that relative density is 1.05, add citric acid, regulate Ph value to be 5, add Rhizoma Imperatae quintessence oil and silicone oil, stir, sterilize 20 minutes at 120 DEG C of temperature, be placed in degassing tank vacuum outgas, discharging after cooling, encapsulates with plastic packing soft tube.
Using method: after being drenched by hair, gets appropriate shampoo salt and is placed in turn round after the palm of the hand crumples out a little foam again and sends out, clean after 1-2 minute with clear water.
Embodiment 2 can the shampoo salt of moderately removing dandruff, takes off to state primary raw material and be prepared from (getting 20g for every part): bamboo salt 20 parts; Deionized water 85 parts; Betanin 4 parts; Fructus Lauri nobilis 12 parts; Cortex Mori 10 parts; Spina Gleditsiae 9 parts; Fructus Toosendan 9 parts; Radix Hamamelidis Mollis 7 parts; Alternanthera philoxeroides 5 parts; Herba Agrimoniae 6 parts; 6 parts, Radix Glycyrrhizae; Rhizoma Imperatae quintessence oil 1.2 parts; Sorbitol 0.7 part; Sodium lauryl sulphate 0.6 part; Silicone oil 0.7 part; Zinc Pyrithione 0.6 part.
The preparation process of the shampoo salt of energy moderately removing dandruff is as follows:
(1) Fructus Lauri nobilis and Fructus Toosendan rice wine (consumption is 5 times of Fructus Lauri nobilis and Fructus Toosendan quality) are soaked 3 days, take out, moderate heat stir-fries 40 minutes, dries, and pulverizes, and crosses 160 mesh sieves;
(2) Cortex Mori, Alternanthera philoxeroides, Herba Agrimoniae and Radix Glycyrrhizae are smashed, be placed in multi-function extractor, add water, extract twice, each extraction 50 minutes, merge extractive liquid;
(3) be placed in marmite by Spina Gleditsiae and Radix Hamamelidis Mollis, soak 30 minutes, add white vinegar (consumption is 20% of Spina Gleditsiae and Radix Hamamelidis Mollis quality), decoct twice, each decoction 40 minutes, collecting decoction, obtains medicinal liquid;
(4) by step (2) gained extracting solution and step (3) gained medicinal liquid mix homogeneously, be concentrated into 1/2 of original volume, add step (1) gained powder, fully stir, room temperature places 60 minutes;
(5) by bamboo salt and betanin mixing, be placed in heatproof glass container, add deionized water, heat while stirring (it is 70 DEG C that temperature controls), continue to be stirred to and dissolve completely, when being cooled to 40 DEG C, add Sorbitol, sodium lauryl sulphate and Zinc Pyrithione, stir 40 minutes;
(6) step (4) gained end product is joined in step (5) gained end product, mix homogeneously, be concentrated into the thick liquid that relative density is 1.10, add citric acid, regulate Ph value to be 6, add Rhizoma Imperatae quintessence oil and silicone oil, stir, sterilize 30 minutes at 140 DEG C of temperature, be placed in degassing tank vacuum outgas, discharging after cooling, encapsulates with plastic packing soft tube.
Using method: after being drenched by hair, gets appropriate shampoo salt and is placed in turn round after the palm of the hand crumples out a little foam again and sends out, clean after 1-2 minute with clear water.
Model case one gold medal XX, man, 31 years old, people from Liaocheng of Shandong Province.More dandruff is there is in Mr. Jin without under obvious inducement, and head is itched, a lot of with dandruff after hands scratching, attempted multiple dandruff control shampoo containing, as Head&Shoulders, overlord etc., but effect is all not obvious, also makes some inquiries about anti-dandruff folk prescription, such as with the washing water of rice etc. after vinegar, fermentation, be all not improved.Use the present invention to treat the shampoo salt (embodiment 2) of dandruff, after hair is drenched, get appropriate shampoo salt and be placed in turn round again after the palm of the hand crumples out a little foam and send out, clean with clear water after 1-2 minute, once, within 4 days, find that dandruff obviously reduces afterwards, head pruritus phenomenon disappears in hair washing every day.Continue use after one week, dandruff disappears substantially.
Embodiment 3 can the shampoo salt of moderately removing dandruff, takes off to state primary raw material and be prepared from (getting 50g for every part): bamboo salt 16 parts; Deionized water 65 parts; Betanin 3.3 parts; Fructus Lauri nobilis 10.5 parts; Cortex Mori 8.5 parts; Spina Gleditsiae 7.5 parts; Fructus Toosendan 7 parts; Radix Hamamelidis Mollis 5.5 parts; Alternanthera philoxeroides 3 parts; Herba Agrimoniae 4 parts; 4.5 parts, Radix Glycyrrhizae; Rhizoma Imperatae quintessence oil 0.8 part; Sorbitol 0.55 part; Sodium lauryl sulphate 0.45 part; Silicone oil 0.55 part; Zinc Pyrithione 0.45 part.
The preparation process of the shampoo salt of energy moderately removing dandruff is as follows:
(1) Fructus Lauri nobilis and Fructus Toosendan rice wine (consumption is 3 times of Fructus Lauri nobilis and Fructus Toosendan quality) are soaked 2 days, take out, moderate heat stir-fries 33 minutes, dries, and pulverizes, and crosses 130 mesh sieves;
(2) Cortex Mori, Alternanthera philoxeroides, Herba Agrimoniae and Radix Glycyrrhizae are smashed, be placed in multi-function extractor, add water, extract twice, each extraction 43 minutes, merge extractive liquid;
(3) be placed in marmite by Spina Gleditsiae and Radix Hamamelidis Mollis, soak 23 minutes, add white vinegar (consumption is 17% of Spina Gleditsiae and Radix Hamamelidis Mollis quality), decoct twice, each decoction 33 minutes, collecting decoction, obtains medicinal liquid;
(4) by step (2) gained extracting solution and step (3) gained medicinal liquid mix homogeneously, be concentrated into 1/2 of original volume, add step (1) gained powder, fully stir, room temperature places 45 minutes;
(5) by bamboo salt and betanin mixing, be placed in heatproof glass container, add deionized water, heat while stirring (it is 63 DEG C that temperature controls), continue to be stirred to and dissolve completely, when being cooled to 33 DEG C, add Sorbitol, sodium lauryl sulphate and Zinc Pyrithione, stir 33 minutes;
(6) step (4) gained end product is joined in step (5) gained end product, mix homogeneously, be concentrated into the thick liquid that relative density is 1.07, add citric acid, regulate Ph value to be 5.3, add Rhizoma Imperatae quintessence oil and silicone oil, stir, sterilize 23 minutes at 125 DEG C of temperature, be placed in degassing tank vacuum outgas, discharging after cooling, encapsulates with plastic packing soft tube.
Using method: after being drenched by hair, gets appropriate shampoo salt and is placed in turn round after the palm of the hand crumples out a little foam again and sends out, clean after 1-2 minute with clear water.
Embodiment 4 can the shampoo salt of moderately removing dandruff, takes off to state primary raw material and be prepared from (getting 30g for every part): bamboo salt 18 parts; Deionized water 80 parts; Betanin 3.7 parts; Fructus Lauri nobilis 11.5 parts; Cortex Mori 9.5 parts; Spina Gleditsiae 8.5 parts; Fructus Toosendan 8 parts; Radix Hamamelidis Mollis 6.5 parts; Alternanthera philoxeroides 4 parts; Herba Agrimoniae 4-5 part; 5.5 parts, Radix Glycyrrhizae; Rhizoma Imperatae quintessence oil 1.0 parts; Sorbitol 0.65 part; Sodium lauryl sulphate 0.55 part; Silicone oil 0.65 part; Zinc Pyrithione 0.55 part.
The preparation process of the shampoo salt of energy moderately removing dandruff is as follows:
(1) Fructus Lauri nobilis and Fructus Toosendan rice wine (consumption is 5 times of Fructus Lauri nobilis and Fructus Toosendan quality) are soaked 3 days, take out, moderate heat stir-fries 37 minutes, dries, and pulverizes, and crosses 150 mesh sieves;
(2) Cortex Mori, Alternanthera philoxeroides, Herba Agrimoniae and Radix Glycyrrhizae are smashed, be placed in multi-function extractor, add water, extract twice, each extraction 47 minutes, merge extractive liquid;
(3) be placed in marmite by Spina Gleditsiae and Radix Hamamelidis Mollis, soak 27 minutes, add white vinegar (consumption is 19% of Spina Gleditsiae and Radix Hamamelidis Mollis quality), decoct twice, each decoction 37 minutes, collecting decoction, obtains medicinal liquid;
(4) by step (2) gained extracting solution and step (3) gained medicinal liquid mix homogeneously, be concentrated into 1/2 of original volume, add step (1) gained powder, fully stir, room temperature places 55 minutes;
(5) by bamboo salt and betanin mixing, be placed in heatproof glass container, add deionized water, heat while stirring (it is 67 DEG C that temperature controls), continue to be stirred to and dissolve completely, when being cooled to 37 DEG C, add Sorbitol, sodium lauryl sulphate and Zinc Pyrithione, stir 37 minutes;
(6) step (4) gained end product is joined in step (5) gained end product, mix homogeneously, be concentrated into the thick liquid that relative density is 1.09, add citric acid, regulate Ph value to be 5.7, add Rhizoma Imperatae quintessence oil and silicone oil, stir, sterilize 27 minutes at 135 DEG C of temperature, be placed in degassing tank vacuum outgas, discharging after cooling, encapsulates with plastic packing soft tube.
Using method: after being drenched by hair, gets appropriate shampoo salt and is placed in turn round after the palm of the hand crumples out a little foam again and sends out, clean after 1-2 minute with clear water.
What XX of model case two, female, 18 years old, people from Linyi.Mrs He was a student of high two at that time, and learning pressure is comparatively large, and the time is relatively tighter, and Mrs He washes hair substantially relatively more hasty at every turn, many times rinsed not thorough, and normal residual more shampoo, the time has been grown and just occurred a lot of dandruff.Just start Mrs He also very irritated, so recruitment hair washing frequency, washed to be adjusted to by original 3 days one and wash for 2 days one, adhere to the time of one month nearly, just hair washing dandruff on the same day obviously reduces, but second day dandruff is still a lot, uses special dandruff control shampoo containing to be also not improved.Used the shampoo salt (embodiment 4) that the present invention treats dandruff afterwards instead, after being drenched by hair, get appropriate shampoo salt and be placed in turn round after the palm of the hand crumples out a little foam again and send out, clean with clear water after 1-2 minute, hair washing every day once, finds that dandruff obviously reduces for 5 days afterwards.Continue use after one week, dandruff disappears substantially.Later stage visits and learns that effect is better, seldom has dandruff.
Embodiment 5 can the shampoo salt of moderately removing dandruff, takes off to state primary raw material and be prepared from (getting 50g for every part): bamboo salt 17 parts; Deionized water 72 parts; Betanin 3.5 parts; Fructus Lauri nobilis 11 parts; Cortex Mori 9 parts; Spina Gleditsiae 8 parts; Fructus Toosendan 7.5 parts; Radix Hamamelidis Mollis 6 parts; Alternanthera philoxeroides 3.5 parts; Herba Agrimoniae 4.5 parts; 5 parts, Radix Glycyrrhizae; Rhizoma Imperatae quintessence oil 0.9 part; Sorbitol 0.6 part; Sodium lauryl sulphate 0.5 part; Silicone oil 0.6 part; Zinc Pyrithione 0.5 part.
The preparation process of the shampoo salt of energy moderately removing dandruff is as follows:
(1) Fructus Lauri nobilis and Fructus Toosendan rice wine (consumption is 4 times of Fructus Lauri nobilis and Fructus Toosendan quality) are soaked 3 days, take out, moderate heat stir-fries 35 minutes, dries, and pulverizes, and crosses 140 mesh sieves;
(2) Cortex Mori, Alternanthera philoxeroides, Herba Agrimoniae and Radix Glycyrrhizae are smashed, be placed in multi-function extractor, add water, extract twice, each extraction 45 minutes, merge extractive liquid;
(3) be placed in marmite by Spina Gleditsiae and Radix Hamamelidis Mollis, soak 25 minutes, add white vinegar (consumption is 18% of Spina Gleditsiae and Radix Hamamelidis Mollis quality), decoct twice, each decoction 35 minutes, collecting decoction, obtains medicinal liquid;
(4) by step (2) gained extracting solution and step (3) gained medicinal liquid mix homogeneously, be concentrated into 1/2 of original volume, add step (1) gained powder, fully stir, room temperature places 50 minutes;
(5) by bamboo salt and betanin mixing, be placed in heatproof glass container, add deionized water, heat while stirring (it is 65 DEG C that temperature controls), continue to be stirred to and dissolve completely, when being cooled to 35 DEG C, add Sorbitol, sodium lauryl sulphate and Zinc Pyrithione, stir 35 minutes;
(6) step (4) gained end product is joined in step (5) gained end product, mix homogeneously, be concentrated into the thick liquid that relative density is 1.08, add citric acid, regulate Ph value to be 5.5, add Rhizoma Imperatae quintessence oil and silicone oil, stir, sterilize 25 minutes at 130 DEG C of temperature, be placed in degassing tank vacuum outgas, discharging after cooling, encapsulates with plastic packing soft tube.
Using method: after being drenched by hair, gets appropriate shampoo salt and is placed in turn round after the palm of the hand crumples out a little foam again and sends out, clean after 1-2 minute with clear water.
The pharmacological effect of each crude drug is respectively:
Bamboo salt: be day is evaporated brine load in triennial QINGZHU, two ends are sealed with natural loess, take pinaster as fuel, the material extract after 1000 DEG C of-1500 DEG C of high-temperature calcinations, make the mineral in bamboo salt and trace element still keep original crudeness, remain that the Nature gives, that ecosystem mineral is originally initial balanced structure intactly.Main component is NaCl, separately containing micro-calcium, potassium, copper, ferrum, zinc etc. and other trace element, helps human body overall absorption especially.Very huge balanced action can be played to human body, and reach spontaneous recovery and the rehabilitation of human body by this balance and adjustment.Bamboo salt also has the function of strengthening osmotic pressure, has recovered the metabolism order of human body, aid digestion, help excretion, help nutrition to input, and have activated the vitality of people.
Deionized water: refer to and eliminate the pure water after in ionic species impurity." deionization " that International Organization for Standardization ISO/TC147 specifies is defined as: " deionized water removes ionic species completely or by halves, mainly refers to adopt ion exchange resin treatment method." ion in water is generally the electrolyte of dissolving, comprise as aniones such as the cationes such as calcium, magnesium, potassium, sodium and carbonate, sulfate radical, chlorate anions, these electrolytical existence can affect the product quality in production technology, therefore each processing method need be adopted to remove.Effect and range of application: 1, scientific research institution, business unit's use for laboratory water; 2, the deionized water needed for electronics industry production technology, high deionized water is produced; 3, chemical industry production technology water, deionized water is used widely as Conventional solvents, as chemical reaction cooling water, chemical agent, chemical fertilizer and fine chemistry industry, cosmetics manufacture process technique deionized water; 4, bio-pharmaceuticals, water for injection, medicinal preparation for oral administration and hemodialysis's deionized water; 5, beverage industry water, drinks brewing water uses deionized water with blending; 6, electroplating industry deionized water; 7, battery industry deionized water; 8, deionized water needed for heating power, thermal power plant's steam.
Betanin: active ingredient is trimethyl glycine; can extract from the root of natural plants, stem, leaf and fruit or adopt trimethylamine and monoxone to be raw material chemosynthesis; be a kind of alkaline matter, there is strong moisture pick-up properties, so often anti-caking agent process can be used in processing technology.Being widely used in middle-and-high-ranking shampoo, bath foam, handwashing liquid, foam clean agent etc. with in the preparation of household detergent, is the main component of the gentle shampoo for baby of preparation, baby's foam bath, baby skin protection product; A kind of excellent softening amendment in hair care and skin care formula; Also can be used as detergent, wetting agent, thickening agent, antistatic additive and antibacterial etc.
Fructus Lauri nobilis: acrid in the mouth, warm in nature.Return lung meridian.For the fruit of canella Laurel.There is wind-damp dispelling, removing toxic substances, effect of parasite killing.For rheumatic arthralgia, fugu poisoning, scabies, right retroauricular carbuncle.
Cortex Mori: sweet in the mouth, cold in nature.Return lung meridian.For the dry root bark of moraceae plants Mulberry.There is eliminating pathogen from the lung for relieving asthma, effect of inducing diuresis to remove edema.For dyspnea and cough due to lung-heat, edema distension oliguria, appearance skin edema.
Spina Gleditsiae: acrid in the mouth, warm in nature.Return liver, stomach warp.For the dry Spina jujubae of leguminous plant Fructus Gleditsia.There is detumescence poison holding, evacuation of pus, effect of parasite killing.For carbuncle from the beginning of or difficulty in discharging of pus; External treatment scabies leprosy.
Fructus Toosendan: bitter in the mouth, cold in nature.Return liver, small intestinal, urinary bladder channel.Another name is Fructus Toosendan, Fructus Toosendan, Fructus Toosendan are real.For the dry mature fruit of Meliaceae plant Fructus Toosendan, primary medicinal component is Fructus Toosendan element, alkaloid etc.There are soothing liver-QI promoting the circulation of QI to relieve pain, effect of anthelmintic.For the breast side of body, abdominal distention, colic, abdominal pain due to worm stagnation.Bitter cold is fallen and is let out, can clearing away liver-fire, let out hot and suffocating, promoting the circulation of QI to relieve pain.
Radix Hamamelidis Mollis: sweet in the mouth, property is put down.Return spleen channel.For the root of Hamamelidaceae Plants Radix Hamamelidis Mollis.Containing nimbecetin, Quercetin, astragalin etc.There is effect of QI invigorating.Weak for impairment caused by overstrain.
Alternanthera philoxeroides: bitter in the mouth, sweet, cold in nature.For the herb of Amaranthaceae Alternanthera plant Alternanthera philoxeroides.There is clearing away heat and promoting diuresis, effect of removing pathogenic heat from blood and toxic substance from the body.For encephalitis b, influenza initial stage, hemoptysis of pulmonary tuberculosis; Eczema is controlled in external, herpes zoster, furuncle, venom, epidemic hemorrhagic conjunctivitis.
Herba Agrimoniae: bitter in the mouth, puckery, property is put down.GUIXIN, Liver Channel.For the dry aerial parts of rosaceous plant Agrimony.There is astringing to arrest bleeding, preventing the attack (or recurrence) of malaria, dysentery relieving, effect of removing toxic substances.For spitting of blood, spit blood, metrostaxis, malaria, dysentery, de-power impairment caused by overstrain, carbuncle sore tumefacting virus, pudendal pruritus leukorrhagia.
Radix Glycyrrhizae: sweet in the mouth, property is put down.GUIXIN.Lung, spleen, stomach warp.For the dry root and rhizome of glycyrrhizic legume, Glycyrrhiza inflata Bat. or Glycyrrhiza glabra L..There is invigorating the spleen and replenishing QI, heat-clearing and toxic substances removing, expelling phlegm for arresting cough, relieving spasm to stop pain, effect of coordinating the actions of various ingredients in a prescription.For weakness of the spleen and stomach, fatigue and weakness, shortness of breath and palpitation, cough with copious phlegm, the anxious pain of institute's abdomen, extremity contraction, carbuncle sore tumefacting virus, cushion toxicity.
Rhizoma Imperatae quintessence oil: distribute a kind of pure and fresh, light lemon, there is sterilization, softening skin, Meadowsweet Extract, belong to open country hay-scented, vivaciously brisk.Irritatedly gently can feel, strengthen healthy hair cleaning effect.Effective activation blood circulation, helpful to rheumatic pain; Can anthelmintic, house pet also can be helped to drive away parasite, flea etc.
Sorbitol: another name sorbitol, is white hygroscopic powder or crystalline powder, lamellar or granule, is slightly soluble in ethanol and acetic acid.Have good performance of keeping humidity, the moisture that food can be made to keep certain, prevents drying, also can prevent sugar, the crystallizations such as salt, can keep sweet, acid, the balance of bitterness intensity, strengthen the local flavor of food, because it is nonvolatile polyhydric alcohol, so also have the function keeping food aroma.
Sodium lauryl sulphate: be a kind of white or faint yellow micro-sticky thing, soluble in water, be slightly soluble in ethanol, be dissolved in chloroform, ether and V.M.. naphtha hardly.Acid, alkali and hard water are stablized.Industrially be usually used in detergent and textile industry, belong to anion surfactant, compatibility is good again with anion, nonionic, there is good emulsifying, foaming, infiltration, decontamination and dispersive property, be widely used in toothpaste, shampoo, hair cream, shampoo, detergent, liquid washed, cosmetics and the plastics demoulding, the industries such as lubrication and pharmacy, papermaking, building materials, chemical industry.
Silicone oil: the polysiloxane being a kind of different polymerization degree chain structure, added water by dimethyldichlorosilane to be hydrolyzed obtained first minification polycyclic body, ring body obtains low ring body through cracking, rectification, then ring body, closure agent, catalyst are put together the mixture telomerizing and just can obtain various different polymerization degree, just can obtain silicone oil through distilling under reduced pressure removing low-boiling-point substance.Be commonly used for senior lubricant, shockproof oil, insulating oil, defoamer, releasing agent, polish and vacuum diffusion pump wet goods.In various silicone oil, applying the most extensive with methyl-silicone oil, is most important kind in silicone oil, is secondly methyl phenyl silicone oil.Mainly being applied as of silicone oil and derivant thereof: remover, damping oil, dielectric oil, hydraulic oil, heat trnasfer oil, diffusion pump oil, defoamer, lubricant, water-repelling agent, oil paint additive, polishing agent, cosmetics and daily living article additive, surfactant, granule and fibre finish, silicone grease, flocculating agent.
Zinc Pyrithione: for shampoo dandruff, can suppress the growth of Gram-positive, negative bacteria and mycete.Can hair conditioning effectively, delay the aging of hair, control the generation of poliosis and alopecia.Zinc Pyrithione and cation and non-ionic surface active agent form insoluble precipitate, to light and oxidant unstable, unstable to bronsted lowry acids and bases bronsted lowry during higher temperatures.It and EDTA are incompatible, and non-ionic surface active agent can make its part inactivation.When heavy metal exists, chelating or anti-chelation can occur, and these chelates are insoluble in water.Zinc Pyrithione is a kind of chelate, is effectively anti-mildew and antibacterial compound.Its anti-dandruff activity is very strong.
Test example 1: in order to whether the shampoo salt measuring energy moderately removing dandruff of the present invention meets relevant national standard, we have done determination experiment, randomly draws and carries out test experience from the shampoo salt of energy moderately removing dandruff of the present invention.
Relevant regulations according to about shampoo (cream) in huge industry standard QB/T1974-2004 of the light mouth of the People's Republic of China (PRC): outward appearance foreign; Color and luster conforms with the regulations color pool; Fragrance conforms with the regulations odor type; Heat-resisting (40 ± l) DEG C keeps 24h, returns to after room temperature without segregation phenomenon; Cold-resistant-5 DEG C-10 DEG C keep 24h, without dividing a separating water phenomenon after returning to room temperature; PH4.0-8.0; Working substance content (%)>=10.0; Active matter content is (with 100%K
12meter)/%>=8.0 etc.
This detection experiment measures mainly for working substance content: 1 total solid.1.1 instruments: thermometer (precision 0.2 DEG C), analytical balance (precision 0.0002g), constant temperature oven (precision ± 1 DEG C), beaker (250mL), exsiccator.1.2 operations: take sample (being accurate to 0.0002g) in the beaker of drying constant weight, dry 3h in (105 ± 1) DEG C constant temperature oven, and taking-up is put into exsiccator and is cooled to room temperature, claims its quality (being accurate to 0.0002g).1.3 results: the content of total solid, numerical value represents with %, total solids content (%)=(m
3-m
1)/(m
2-m
1) * 100, wherein m
1the quality of-empty beaker, unit is gram (g); m
2the quality of sample and beaker before-oven dry, unit is gram (g); m
3the quality of residue and beaker after-oven dry, unit is gram (g).2. inorganic salt (alcohol-insoluble substance).2.1 instruments: thermometer (precision 0.2 DEG C), analytical balance (precision 0.0002g), thermostatic drying chamber (precision ± 2 DEG C), water-bath heater, Gooch pincers misfortune (30mL), taper bottle,suction (500mL), nutsch filter or minipump, graduated cylinder (100mL), exsiccator.2.2 reagent: 95% neutral alcohol (chemical pure): get appropriate 95% ethanol, add several phenolphthalein indicators, be titrated to blush with 0.1mol/L sodium hydroxide solution.2.3 operations: utilize the sample of drying in 1.2, add 90% neutral alcohol 100mL, be heated to micro-boiling in a water bath, take out.Stir gently, sample is dissolved as far as possible.After staticly settling, supernatant liquid is poured into constant weight and the Gooch being covered with filtering layer increases in misfortune, be filtered in bottle,suction with nutsch filter, as far as possible solid insoluble stayed in beaker, and with appropriate 95% neutral alcohol washing beaker secondary.The Gooch Citrus chachiensis Hort. that cleaning mixture moves into constant weight together with precipitation is collapsed inner filtration, and filtrate is in same bottle,suction.Gooch is increased the baking oven exhausting and put into (105 ± 1) DEG C, constant temperature 3h, take out to put into after exsiccator is cooled to room temperature and weigh (being accurate to 0.0002g).2.4 results: inorganic salt content, numerical value represents with %, inorganic salt content (%)=m/m
0* 100, wherein m-Gooch increases sedimentary quality in pot, unit is gram (g); m
0the quality of-sample, unit is gram (g).3. nitride.3.1 instruments: brown acid buret.3.2 reagent: Neutral potassium chromate (analytical pure): 5%; 0.1mol/L silver nitrate standard solution: take analytical pure silver nitrate 16.989g, moves in the brown volumetric flask of 1L with water dissolution, is diluted to scale, shakes up.Demarcate by the method in QB/T2470.3.3 operations: in the filtrate of filtering in 2.3, instill several phenolphthalein indicators, regulate with acid-base solution and make solution be blush, then add 5% Neutral potassium chromate 2mL-3mL, being titrated to redness with 0.1mol/L silver nitrate standard solution slowly to take off, is terminal when being finally orange.3.4 results: chloride content (in sodium chloride), numerical value represents with %, chloride content (%)=(c*V*0.0585)/m
0* 100, the wherein concentration of c-silver nitrate standard solution, unit is mole often liter (mol/L); The volume of the silver nitrate standard solution consumed during V-titration sample, unit is milliliter (mL); 0.0585-with 1.00mL silver nitrate standard solution [c (AgN0
3)=1.0000mol/L] quality of the suitable sodium chloride represented with gram (g), unit is gram every mM (g/mmol); The quality of m-sample, unit is gram (g).4. working substance content.Working substance content, numerical value represents with %, working substance content (%)=total solids content (%)-inorganic salt content (%)-chloride content (%).
Table 1 total solids content (%), inorganic salt content (%), chloride content and corresponding working substance content
Then average effective thing content (%)=(17.7+16.9+17.8+16.6+17.8+16.7+17.0+17.4+17.2+16.6)/10=17.17, meets the regulation of working substance content (%) >=10.0 completely.
Test example 2: in order to verify the curative effect of the shampoo salt (embodiment 5) of energy moderately removing dandruff of the present invention: in March, 2011, in JIUYUE ,-2011 did contrast test, screening dandruff patient 200 people, all there is typical symptom,, pruritus slightly red with naked eyes visible lamellar white scurfy squama, substrate, greasy etc. is made a definite diagnosis in conjunction with clinical symptoms, obtain patient to agree to, partner treatment.Wherein male 86 example, women 114 example; Age 13-40 year, the course of disease 15 days-3 years.All patients did not use external used medicine in nearly 2 weeks, non-Oral Ketoconazole and other antifungal drugs in 1 month; Eliminating object is anemia of pregnant woman, nursing women, serious hepatorenal disease patient, skin of head secondary infection person.Be divided into matched group and experimental group randomly, wherein experimental group has 140 people, and matched group has 60 people.
Experimental group: use the present invention to treat the shampoo salt of dandruff, after being drenched by hair, gets appropriate shampoo salt and is placed in turn round after the palm of the hand crumples out a little foam again and sends out, clean, 2-3 time weekly after 1-2 minute with clear water.Matched group first uses the moistening hair of warm water, and rear use 2% TPIATOP hair washing, rubs after bubbling and retain 2 minutes, wash away, 2-3 time weekly with clear water.Observe therapeutic effect after being used in conjunction 2 weeks, and follow up a case by regular visits to 3 months.
After using 2 weeks, experimental group has 80%(112 people) patient's dandruff and scurf disappear completely, erythema disappear, skin without greasy, without gargalesthesia; Only have 2.14%(3 people) the dandruff situation of patient without obvious alleviation; All the other 17.86%(25 people) patient have alleviation in various degree.And matched group only has 48.33%(29 people) patient's dandruff and scurf disappear completely, erythema disappear, skin without greasy, without gargalesthesia; But have up to 21.67%(13 people) the dandruff situation of patient without obvious alleviation.And in following up a case by regular visits to after 3 months, the shampoo salt using the present invention to treat dandruff does not all produce untoward reaction phenomenon, and have no side effect, safety is good.So the shampoo salt that the present invention treats dandruff is not only clean but also easy to use, curative effect is more remarkable, is better than traditional Therapeutic Method, clinic extensive use.
Finally it should be noted that, embodiment is the detailed description of the invention of optimum of the present invention, be not limited to the present invention, although with reference to previous embodiment to invention has been detailed description, for a person skilled in the art, it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature.Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (10)
1. the shampoo salt of energy moderately removing dandruff, is characterized in that, take off the primary raw material stating quality proportioning and be prepared from: bamboo salt 13-20 part; Deionized water 60-85 part; Betanin 3-4 part; Fructus Lauri nobilis 10-12 part; Cortex Mori 8-10 part; Spina Gleditsiae 7-9 part; Fructus Toosendan 6-9 part; Radix Hamamelidis Mollis 5-7 part; Alternanthera philoxeroides 2-5 part; Herba Agrimoniae 3-6 part; Radix Glycyrrhizae 4-6 part; Rhizoma Imperatae quintessence oil 0.6-1.2 part; Sorbitol 0.5-0.7 part; Sodium lauryl sulphate 0.4-0.6 part; Silicone oil 0.5-0.7 part; Zinc Pyrithione 0.4-0.6 part.
2. shampoo salt according to claim 1, is characterized in that, takes off the primary raw material stating quality proportioning and is prepared from: bamboo salt 16-18 part; Deionized water 65-80 part; Betanin 3.3-3.7 part; Fructus Lauri nobilis 10.5-11.5 part; Cortex Mori 8.5-9.5 part; Spina Gleditsiae 7.5-8.5 part; Fructus Toosendan 7-8 part; Radix Hamamelidis Mollis 5.5-6.5 part; Alternanthera philoxeroides 3-4 part; Herba Agrimoniae 4-5 part; Radix Glycyrrhizae 4.5-5.5 part; Rhizoma Imperatae quintessence oil 0.8-1.0 part; Sorbitol 0.55-0.65 part; Sodium lauryl sulphate 0.45-0.55 part; Silicone oil 0.55-0.65 part; Zinc Pyrithione 0.45-0.55 part.
3. shampoo salt according to claim 1, is characterized in that, takes off the primary raw material stating quality proportioning and is prepared from: bamboo salt 17 parts; Deionized water 72 parts; Betanin 3.5 parts; Fructus Lauri nobilis 11 parts; Cortex Mori 9 parts; Spina Gleditsiae 8 parts; Fructus Toosendan 7.5 parts; Radix Hamamelidis Mollis 6 parts; Alternanthera philoxeroides 3.5 parts; Herba Agrimoniae 4.5 parts; 5 parts, Radix Glycyrrhizae; Rhizoma Imperatae quintessence oil 0.9 part; Sorbitol 0.6 part; Sodium lauryl sulphate 0.5 part; Silicone oil 0.6 part; Zinc Pyrithione 0.5 part.
4., according to the preparation method of the arbitrary described shampoo salt of claim 1-3, it is characterized in that, step is as follows:
(1) Fructus Lauri nobilis and Fructus Toosendan rice wine is soaked 2-3 days, take out, moderate heat stir-fries 30-40 minute, dries, pulverizes, cross 120-160 mesh sieve;
(2) Cortex Mori, Alternanthera philoxeroides, Herba Agrimoniae and Radix Glycyrrhizae are smashed, be placed in multi-function extractor, add water, extract twice, each extraction 40-50 minute, merge extractive liquid;
(3) be placed in marmite by Spina Gleditsiae and Radix Hamamelidis Mollis, soak 20-30 minute, add white vinegar, decoct twice, each decoction 30-40 minute, collecting decoction, obtains medicinal liquid;
(4) by step (2) gained extracting solution and step (3) gained medicinal liquid mix homogeneously, be concentrated into 1/2 of original volume, add step (1) gained powder, fully stir, room temperature places 40-60 minute;
(5) by bamboo salt and betanin mixing, be placed in heatproof glass container, add deionized water, (preferable temperature controls as 60-70 DEG C in heating while stirring, be more preferably temperature to control to be 65 DEG C), continue to be stirred to and dissolve completely, when being cooled to 30-40 DEG C, add Sorbitol, sodium lauryl sulphate and Zinc Pyrithione, stir 30-40 minute;
(6) step (4) gained end product is joined in step (5) gained end product, mix homogeneously, be concentrated into the thick liquid that relative density is 1.05-1.10, add citric acid, regulate Ph value to be 5-6, add Rhizoma Imperatae quintessence oil and silicone oil, stir, sterilize 20-30 minute at 120-140 DEG C of temperature, is placed in degassing tank vacuum outgas, discharging after cooling, encapsulates with plastic packing soft tube.
5. preparation method according to claim 4, is characterized in that: the consumption of the preferred rice wine of step (1) is 3-5 times of Fructus Lauri nobilis and Fructus Toosendan quality, and the consumption being more preferably rice wine is Fructus Lauri nobilis and Fructus Toosendan quality 4 times.
6. preparation method according to claim 4, is characterized in that: step (1) is preferred crosses 130-150 mesh sieve, is more preferably 140 mesh sieves.
7. preparation method according to claim 4, is characterized in that: step (2) is preferably each extracts 43-47 minute, more seriously extracts 45 minutes at every turn.
8. preparation method according to claim 4, is characterized in that: the consumption of the preferred white vinegar of step (3) is the 15%-20% of Spina Gleditsiae and Radix Hamamelidis Mollis quality, and the consumption being more preferably white vinegar is 18% of Spina Gleditsiae and Radix Hamamelidis Mollis quality.
9. preparation method according to claim 4, is characterized in that: step (6) preferably regulates Ph value to be 5.3-5.7, is more preferably and regulates Ph value to be 5.5.
10. preparation method according to claim 4, is characterized in that: step (6) preferably sterilizes 23-27 minute at 125-135 DEG C of temperature, to be more preferably at 130 DEG C of temperature sterilization 25 minutes.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107519104A (en) * | 2016-06-17 | 2017-12-29 | 自然解决方案园区有限公司 | Improve functional cosmetic composition and preparation method thereof containing the anti-oxidant of rice washing water fermentation culture medium, anti-wrinkle and moisturizing |
| CN111888292A (en) * | 2020-08-18 | 2020-11-06 | 成都天河农业旅游发展有限公司 | Antibacterial and antiallergic shampoo based on spina gleditsiae and preparation method thereof |
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| CN104382797A (en) * | 2014-11-27 | 2015-03-04 | 青岛市市南区隆德中医药研究所 | Shampoo for inhibiting bacteria and removing dandruff |
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| CN103536487A (en) * | 2013-10-18 | 2014-01-29 | 桂林雪芙莲日化有限公司 | Anti-dandruff shampo |
| CN104382797A (en) * | 2014-11-27 | 2015-03-04 | 青岛市市南区隆德中医药研究所 | Shampoo for inhibiting bacteria and removing dandruff |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107519104A (en) * | 2016-06-17 | 2017-12-29 | 自然解决方案园区有限公司 | Improve functional cosmetic composition and preparation method thereof containing the anti-oxidant of rice washing water fermentation culture medium, anti-wrinkle and moisturizing |
| CN111888292A (en) * | 2020-08-18 | 2020-11-06 | 成都天河农业旅游发展有限公司 | Antibacterial and antiallergic shampoo based on spina gleditsiae and preparation method thereof |
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