CN102631304A - Shampoo salt emulsion and preparation method thereof - Google Patents
Shampoo salt emulsion and preparation method thereof Download PDFInfo
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- CN102631304A CN102631304A CN2012101428898A CN201210142889A CN102631304A CN 102631304 A CN102631304 A CN 102631304A CN 2012101428898 A CN2012101428898 A CN 2012101428898A CN 201210142889 A CN201210142889 A CN 201210142889A CN 102631304 A CN102631304 A CN 102631304A
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Abstract
The invention discloses a shampoo salt emulsion and a preparation method thereof. The shampoo salt emulsion is characterized by comprising the following components in parts by weight: 10-30 parts of edible salt, 10-40 parts of surfactant, 0.1-5 parts of suspension stabilizer, 1-10 parts of emulsified silicone oil, 0.1-5 parts of thickening agent, 0.1-1.5 parts of anti-dandruff agent, 0.1-3 parts of essential oil extracted from spice, 0.1-4 parts of humectant, 0.1-3 parts of positive ion conditioner, 0-5 parts of nutritive additive and 30-70 parts of deionized water. The invention also relates to a preparation method of the shampoo salt emulsion. Compared with the prior art, the shampoo salt emulsion has the advantages that the shampoo salt emulsion fully plays a synergistic effect of the edible salt and the anti-dandruff agent in the concentration range of 10-30 parts of salt containing amount and 0.1-1.5 parts of anti-dandruff agent; the respective beneficial effect of the edible salt and the anti-dandruff agent can be improved; and in addition, the natural salt can play functions of sterilization and corrosion resistance; and the product safety can be greatly improved.
Description
Technical field
The present invention relates to a kind of hair shampoo article, the invention still further relates to the method for preparing of this hair shampoo article.
Background technology
In cosmetics, the effect of antiseptic is the protection product, makes it to avoid microbial contamination, prolongs the shelf life of product; Guarantee security of products, prevent that consumer from causing possible infection because of use receives the product of microbial contamination.At present, listed regulation was used during 56 kinds of cosmetics were formed antiseptic and the maximum points for attention such as working concentration, the scope of application that allow thereof in 2007 in version " cosmetics health standard ".Classify according to active matter, be divided into be imidazolidinyl urea, in uride, isothiazolone, parabens, quaternary ammonium salt-15, benzoic acid/benzyl alcohol and derivant thereof, iodo propinyl butyl carbamate, triclosan etc.But the influence from the chemical constituent of antiseptic is brought might cause skin abnormality hypertrophy, canceration; Irradiation at daylight issues biochemical variation, makes the people produce photaesthesia, skin rubefaction, blackening, pain; Cause that the people is irritated, symptom red, that itch occurs; Cause the potential risks such as burn of skin, worry the formaldehyde that discharges like DMDMH; Kazon series is chloride, possibly stimulation arranged to some skin matter; IPBC possibly cause taking in the potential risk of known antiseptic such as iodine.Along with the progress of science and technology, the medium material of plant extract quintessence oil or polarity substitutes traditional chemical preservative as effective natural antiseptic agent.
According to statistics, all in various degree puzzlements that receives dandruff of the adult more than 80%, the dandruff problem has become the second largest hair problem that is only second to alopecia and perplexs consumer.To consumer demand, anti-dandruff type hair washing product emerges in an endless stream on the current market, and the anti-dandruff shampoo product that utilizes the characteristic of edible salt bactericidal antiphlogistic to process is less.Discover that the factor that causes dandruff mainly contains three: chlosma, sebum, individual susceptible type.To be that everyone is inherent can't change in wherein individual susceptibility, and modern science and technology also is difficult to accomplish the inhibition fully to sebum secretion, and therefore the most effective at present anti-dandruff method is through using the antifungal effective ingredient to suppress chlosma.There is multiple antifungal effective ingredient available in the market, like salicylic acid, ZPT, OCT, climbazole and ketoconazole etc.According to character own, cost of material and the safety in utilization of raw material, pyrroles's thioketone zinc (ZPT) remains one of the strongest candidate, and climbazole is number two.
A lot of antibiotic anti-dandruff technical literatures are disclosed in the prior art; Be 200710135779.8 be called that if any application number " a kind of antibiotic desquamation compositions and application thereof " and application number are open for the application for a patent for invention that the 201010511385.X name is called " a kind of antibiotic desquamation compositions and application thereof "; A kind of anti-dandruff composition that comprises ZPT (ZPT) is disclosed; Point out that ZPT has killing of brute force and suppresses reproductive effect antibacterial, mycovirus; Can go out by seborrhea, convention amount is harmless to human non-toxic, and life-time service has no side effect; Be widely used in preparation removing scurf and relieving itching shampoo and hair moisturizer, but for reaching the ZPT large usage quantity that effective anti-dandruff effect is used.
Summary of the invention
Technical problem to be solved by this invention is to the above-mentioned state of the art a kind of have sterilizing and itch-relieving and anti-dandruff function to be provided, and can guarantee that product does not receive contamination by micro, safe and reliable hair washing salt breast.
Another technical problem to be solved by this invention provides the method for preparing of a kind of technology hair washing salt breast simple, easy to make.
The present invention solves the problems of the technologies described above the technical scheme that is adopted: a kind of hair washing salt breast is characterized in that comprising following component and weight proportion thereof:
10 ~ 30 parts of edible salts, 10 ~ 40 parts in surfactant, 0.1 ~ 5 part of suspension stabilizer; 1 ~ 10 part of emulsified silicone oil, 0.1 ~ 5 part of thickening agent, anti-dandruff dose 0.1 ~ 1.5 part; Spice extracts 0.1 ~ 3 part of quintessence oil, 0.1 ~ 4 part of wetting agent, 0.1 ~ 3 part of cation opsonizing agent; 0 ~ 5 part of nourishing additive agent, 30 ~ 70 parts of deionized waters.
Described surfactant is at least a in sodium laureth sulfate, laureth ammonium sulfate, sodium lauryl sulfate, ammonium lauryl sulfate, dodecanamide propyl hydroxy sulfo lycine, cocamido propyl betaine, lauryl glucoside, lauryl alcohol phosphate ester potassium, coconut oil single ethanol amide sulfosuccinic acid monoesters disodium, coconut oil single ethanol amide, the sodium lauroyl sarcosine;
Described edible salt is at least a in sea salt, well mine salt or the lake salt;
Described suspension stabilizer is two phthalic acid amide;
Described anti-dandruff dose is ZPT;
Described wetting agent is at least a in glycerol, propylene glycol, the butanediol;
Described cation opsonizing agent is at least a in guar gum hydroxypropyl-trimethyl ammonium chloride, cationic cellulose, polyquaternary ammonium salt, the cation high molecular protein peptide;
Described emulsified silicone oil is at least a in polydimethylsiloxane, the dimethiconol;
Described thickening agent is at least a in xanthan gum, hydroxyethyl-cellulose, the cithrol;
Described nourishing additive agent is at least a in Jojoba oil, Aloe extract, pantothenylol, vitamins, amino acids, olive oil, hyaluronate sodium, the sodium lactate.
As preferably, comprise following component and weight proportion thereof:
12 ~ 26 parts of edible salts, 10 ~ 40 parts in surfactant, 0.3 ~ 3 part of suspension stabilizer; 2 ~ 6 parts of emulsified silicone oils, 0.1 ~ 3 part of thickening agent, anti-dandruff dose 0.5 ~ 1 part; Spice extracts 0.1 ~ 2 part of quintessence oil, 0.3 ~ 2 part of wetting agent, 0.2 ~ 2 part of cation opsonizing agent; 0.3 ~ 4 part of nourishing additive agent, 30 ~ 70 parts of deionized waters.
A kind of method for preparing of the salt breast of having one's hair wash is characterized in that comprising the steps;
1. place reaction pot to be heated to 50 ~ 60 ℃ in water, will be added to the water together with thickening agent with the scattered cation opsonizing agent of wetting agent stirs again;
2. adding surfactant and suspension stabilizer then stirs and is incubated (with 60 ℃ for good);
3. said mixture is evacuated and when lowering the temperature (45 ℃ for good), adds emulsified silicone oil and anti-dandruff dose, stir; Or add emulsified silicone oil, anti-dandruff dose and nourishing additive agent, stir;
4. add edible salt and spice at last and extract quintessence oil, stir, cooling (be good with 35 ℃) discharging afterwards is finished product, detects to change filling machine over to after qualified and carry out fill.
Hair washing salt breast of the present invention, described surfactant is respectively: sodium laureth sulfate (content is 70%), consumption are about 5 parts to about 25 parts, are preferably about 6 parts to about 22 parts, more preferably about 7 parts to about 19 parts; Laureth ammonium sulfate (purity is 70%) is about 5 parts to 30 parts, is preferably about 6 parts to about 25 parts, more preferably about 7 parts to about 20 parts; Sodium lauryl sulfate (content is >=92%) is about 0.1 part to about 10 parts, is preferably about 0.5 part to about 8 parts, more preferably about 1 part to about 6 parts; Ammonium lauryl sulfate (purity is 70%) is about 0.1 part to about 10 parts, is preferably about 0.5 part to about 8 parts, more preferably about 1.0 parts to about 6 parts; Dodecanamide propyl hydroxy sulfo lycine (content is 30%) consumption is about 1 part to about 15 parts, is preferably about 2 parts to about 13 parts, more preferably about 3 parts to about 10 parts; Cocamido propyl betaine (purity is 30%) is about 2 parts to 16 parts, is preferably about 3 parts to about 14 parts, more preferably about 4 parts to about 12 parts; Lauryl glucoside (purity is 50%) is about 0.5 part to about 6 parts, is preferably about 0.8 part to about 5 parts, more preferably about 1 part to about 4 parts; Sodium lauroyl sarcosine (purity is 30%) is about 0.5 part to about 6 parts, is preferably about 0.8 part to about 5 parts, more preferably about 1 part to about 4 parts; Lauryl alcohol phosphate ester potassium (purity is 50%) is about 0.5 part to about 6 parts, is preferably about 0.8 part to about 5 parts, more preferably about 1 part to about 4 parts; Coconut oil single ethanol amide sulfosuccinic acid monoesters disodium (purity is 40%) is about 0.5 part to about 6 parts, is preferably about 0.8 part to about 5 parts, more preferably about 1 part to about 4 parts; Coconut oil single ethanol amide (content is >=92%) consumption quality percentage composition is about 0.1 part to about 5 parts, is preferably about 0.2 part to about 4 parts, more preferably about 0.5 part to about 3 parts;
Above-mentioned edible salt (purity is >=91.0%) is about 10 parts to about 30 parts; Be preferably about 11 parts to about 28 parts; More preferably about 12 parts to about 26 parts, even the Exposure to Sunlight sea salt (purity for >=91.0 parts) that more preferably is rich in the natural minerals elite is about 12 parts to about 26 parts.
Above-mentioned wetting agent is that glycerol (content is >=98.5%) consumption is about 0.1 part to about 5 parts, preferred about 0.2 part to about 4 parts, and more preferably from about 0.3 part to about 3 parts; Propylene glycol (content is >=98.5%) consumption is about 0.1 part to about 5 parts, preferred about 0.2 part to about 4 parts, and more preferably from about 0.3 part to about 3 parts; Butanediol (content is >=98.5%) consumption is about 0.1 part to about 5 parts, preferred about 0.2 part to about 4 parts, and more preferably from about 0.3 part to about 3 parts;
Above-mentioned suspension stabilizer is that two (hydrogenated-tallow group) phthalic acid amide (content is >=98.0%) consumption is about 0.1 part to about 5 parts, preferred about 0.2 part to about 4 parts, and more preferably from about 0.3 part to about 3 parts;
Above-mentioned thickening agent be respectively xanthan gum (viscosity for >=600mPas) consumption is about 0.1 part to about 3 parts, preferably about 0.1 part to about 2 parts, more preferably from about 0.1 part to about 1 part; 16 octadecanol (content is >=99%) consumption is about 0.1 part to about 4 parts, preferred about 0.1 part to about 3 parts, and more preferably from about 0.1 part to about 2 parts; Hydroxyethyl-cellulose (content is >=87%) consumption is about 0.1 part to about 3 parts, preferred about 0.1 part to about 2.5 parts, and more preferably from about 0.1 part to about 2 parts;
Above-mentioned cation opsonizing agent be respectively the guar gum hydroxypropyl-trimethyl ammonium chloride (viscosity for >=2500mPas) consumption is about 0.1 part to about 3 parts, is preferably about 0.1 part to about 2 parts, more preferably about 0.1 part to about 1 part; Cationic cellulose (viscosity is that 50 ~ 60000mPas) consumptions are about 0.1 part to about 3 parts, preferred about 0.1 part to about 2 parts, and more preferably from about 0.1 part to about 1 part;
It is about 0.1 part to about 10 parts that above-mentioned emulsified silicone oil is respectively small particle diameter emulsified silicone oil (particle size range is≤2 μ m) consumption, preferred about 0.5 part to about 8 parts, and more preferably from about 1.0 parts to about 6 parts; Big particle diameter emulsified silicone oil (particle size range is D5015.0 ~ 35.0 μ m) consumption is about 0.1 part to about 5 parts, is preferably about 0.2 part to about 4 parts, more preferably about 0.3 part to about 3 parts;
Above-mentioned anti-dandruff dose is that ZPT (content is >=95%) consumption is about 0.1 part to about 1 part, preferred about 0.3 part to about 1 part, and more preferably from about 0.5 part to about 1 part;
It is Fructus Citri Limoniae quintessence oil, Flos Rosae Rugosae quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil etc. that above-mentioned natural perfume material extracts quintessence oil, and its consumption is about 0.1 part to about 3 parts, preferred about 0.1 part to about 2.5 parts, and more preferably from about 0.1 part to about 2 parts;
Above-mentioned nourishing additive agent is D-panthenol, zinc oxide, Jojoba oil, Aloe extract, pantothenylol, vitamins, amino acids, olive oil, hyaluronate sodium, sodium lactate etc.; Its consumption is about 0.1 part to about 6 parts; Preferred about 0.2 part to about 5 parts, more preferably from about 0.3 part to about 4 parts.
Compared with prior art, the invention has the advantages that: be rich in pure natural salt frosted microgranule and famous and precious plant extract elite in the prescription, during hair washing; The sodium ion that sodium chloride ionization in the salt goes out can get into and destroy its body fluid balance and ph balancing in the bacterial body; Make the bacterial cell dehydration dead, have the function of stronger disinfection, thereby guarantee to avoid contamination by micro; And can sodium chloride concentration be diluted behind the chance water; Thereby can not cause the phenomenon of human body skin dehydration,, a good basis environment is provided for the anti-dandruff dose of effectiveness that performance is maximum.Edible salt ability softening skin cutin promotes the circulation of health blood effectively, improves metabolism; Sterilizing and itch-relieving; Keep the moisture of skin, anti-dandruff dose has antifungic action, can reduce the generation of the dandruff; Cooperate with edible salt to can further improve sterilizing and itch-relieving and anti-dandruff effect, be beneficial to the maximum sterilizing function of edible salt performance.In the concentration range of rational salinity and anti-dandruff dose, give full play to the synergism of edible salt and anti-dandruff dose, improve both beneficial effects separately, and constant product quality, foam is abundant.In addition, the method for preparing technology among the present invention is simple, easy to operate, and safety is higher, easily operation.
For guaranteeing that the anti-dandruff effect of effective antibacterial reduces anti-dandruff dose of consumption simultaneously, adopt anti-dandruff dose to be used with edible salt, this product need not use antiseptic simultaneously, has effectively guaranteed the safety in utilization of product.
The specific embodiment
Below in conjunction with embodiment the present invention is described in further detail.
Embodiment one: the prescription of present embodiment basic composition is:
30 parts in sea salt, 13 parts of sodium laureth sulfate (purity is 70%), 6 parts of dodecanamide propyl hydroxy sulfo lycines (purity is 30%), 5 parts of sodium lauryl sulfates (purity is 92%), 1.0 parts of coconut oil single ethanol amides (purity is 92%), 0.5 part of two phthalic acid amide (purity is 98%), 0.5 part of ZPT suspension (purity is 50%), 2 parts of polydimethylsiloxane, 0.6 part of Fructus Citri Limoniae quintessence oil, 0.4 part of propylene glycol, 0.5 part of guar gum hydroxypropyl-trimethyl ammonium chloride, 0.5 part of xanthan gum, 0.8 part of D-panthenol, 39.2 parts in water, above-mentioned is parts by weight.
Method for preparing includes following steps:
One, places reaction pot to be heated to 60 ℃ distilled water, will join in the distilled water with scattered xanthan gum of propylene glycol and guar gum hydroxypropyl-trimethyl ammonium chloride again and stir;
Two, then, adding sodium laureth sulfate, dodecanamide propyl hydroxy sulfo lycine, sodium lauryl sulfate, coconut oil single ethanol amide and two phthalic acid amide stir and are incubated;
Three, then, after the mixture that stirs is evacuated, add polydimethylsiloxane, ZPT suspension and D-panthenol, be stirred to and be uniformly dispersed;
Four, last, add sea salt and Fructus Citri Limoniae quintessence oil, and stir, cooling back discharging is finished product.
Embodiment two: the prescription of present embodiment basic composition is:
25 parts in sea salt, 16 parts of sodium laureth sulfate (purity is 70%), 4 parts of dodecanamide propyl hydroxy sulfo lycines (purity is 30%), 2 parts of sodium lauryl sulfates (purity is 92%), 1.5 parts of coconut oil single ethanol amides (purity is 92%), 1.0 parts of two phthalic acid amide (purity is 98%), 1.0 parts of ZPT suspensions (purity is 50%), 3 parts of polydimethylsiloxane, 1 part of dimethiconol, 0.3 part of Flos Rosae Rugosae quintessence oil, 1 part of glycerol, 0.5 part of cationic cellulose, 0.4 part of xanthan gum, 0.5 part of 16 octadecanol, 0.3 part of D-panthenol, 0.5 part of vitamin E, 42 parts in water, above-mentioned is mass percent.
Method for preparing includes following steps:
One, places reaction pot to be heated to 60 ℃ distilled water, will join in the distilled water with scattered xanthan gum of glycerol and cationic cellulose again and stir;
Two, then, adding sodium laureth sulfate, dodecanamide propyl hydroxy sulfo lycine, sodium lauryl sulfate, coconut oil single ethanol amide and two phthalic acid amide, 16 octadecanol stir and are incubated;
Three, then, after the mixture that stirs is evacuated, add polydimethylsiloxane, dimethiconol, ZPT suspension, D-panthenol and vitamin E, be stirred to and be uniformly dispersed;
Four, last, add sea salt and Flos Rosae Rugosae quintessence oil, and stir, cooling back discharging is finished product.
Embodiment three: the present embodiment prescription basic composition is:
20 parts in sea salt, 17 parts in laureth ammonium sulfate (purity is 70%), 4 parts of dodecanamide propyl hydroxy sulfo lycines (purity is 30%), 4 parts of ammonium lauryl sulfate (purity is 70%), 2 parts of coconut oil single ethanol amides (purity is 92%), 1 part of two phthalic acid amide (purity is 98%), 1 part of ZPT suspension (purity is 50%), 5 parts of polydimethylsiloxane, 0.3 part of Flos Rosae Rugosae quintessence oil, 1.0 parts of glycerol, 0.3 part of cationic cellulose, 0.3 part of guar gum hydroxypropyl-trimethyl ammonium chloride, 0.4 part of xanthan gum, 0.5 part of hydroxyethyl-cellulose, 0.3 part of D-panthenol, 0.5 part of fibroin, 42.4 parts in water, above-mentioned is mass percent.
Method for preparing includes following steps:
One, places reaction pot to be heated to 60 ℃ distilled water, will join in the distilled water and stir with the scattered xanthan gum of glycerol, hydroxyethyl-cellulose, cationic cellulose, guar gum hydroxypropyl-trimethyl ammonium chloride again;
Two, then, adding laureth ammonium sulfate, dodecanamide propyl hydroxy sulfo lycine, ammonium lauryl sulfate, coconut oil single ethanol amide and two phthalic acid amide stir and are incubated;
Three, then, after the mixture that stirs is evacuated, add polydimethylsiloxane, ZPT suspension, D-panthenol and fibroin, be stirred to and be uniformly dispersed;
Four, last, add sea salt and Flos Rosae Rugosae quintessence oil, and stir, cooling back discharging is finished product.
Embodiment four: the present embodiment prescription basic composition is:
15 parts in sea salt, 12 parts of sodium laureth sulfate (purity is 70%), 6 parts of cocamido propyl betaine (purity is 30%), 3 parts of sodium lauroyl sarcosines (purity is 50%), 1.5 parts of coconut oil single ethanol amides (purity is 92%), 1.5 parts of two phthalic acid amide (purity is 98%), 1.5 parts of ZPT suspensions (purity is 50%), 3 parts of dimethiconols, 0.5 part of Herba Lysimachiae foenum-graeci quintessence oil, 0.8 part of glycerol, 0.1 part of cationic cellulose, 0.1 part of guar gum hydroxypropyl-trimethyl ammonium chloride, 0.5 part of xanthan gum, 0.3 part of vitamin B5,0.5 part of fibroin, 53.7 parts in water, above-mentioned is mass percent.
Method for preparing includes following steps:
One, places reaction pot to be heated to 60 ℃ distilled water, will join in the distilled water and stir with the scattered xanthan gum of glycerol, cationic cellulose, guar gum hydroxypropyl-trimethyl ammonium chloride again;
Two, then, adding sodium laureth sulfate, cocamido propyl betaine, sodium lauroyl sarcosine, coconut oil single ethanol amide and two phthalic acid amide stir and are incubated;
Three, then, after the mixture that stirs is evacuated, add dimethiconol, ZPT suspension, vitamin B5 and fibroin, be stirred to and be uniformly dispersed;
Four, last, add sea salt and Herba Lysimachiae foenum-graeci quintessence oil, and stir, cooling back discharging is finished product.
Embodiment five: the present embodiment prescription basic composition is:
10 parts in sea salt, 16 parts of sodium laureth sulfate (purity is 70%), 5 parts of cocamido propyl betaine (purity is 30%), 2 parts of sodium lauroyl sarcosines (purity is 50%), 2 parts of coconut oil single ethanol amides (purity is 92%), 1 part of lauryl glucoside (purity is 50%), 1 part of two phthalic acid amide (purity is 98%), 2 parts of ZPT suspensions (purity is 50%), 3 parts of polydimethylsiloxane, 0.3 part of Herba Lysimachiae foenum-graeci quintessence oil, 1.2 parts of glycerol, 0.4 part of guar gum hydroxypropyl-trimethyl ammonium chloride, 0.6 part of xanthan gum, 1.5 parts of Aloe extraction solution, 0.5 part of fibroin, 53.5 parts in water, above-mentioned is mass percent.
Method for preparing includes following steps:
One, places reaction pot to be heated to 60 ℃ distilled water, will join in the distilled water and stir with the scattered xanthan gum of glycerol, guar gum hydroxypropyl-trimethyl ammonium chloride again;
Two, then, adding sodium laureth sulfate, cocamido propyl betaine, sodium lauroyl sarcosine, coconut oil single ethanol amide, lauryl glucoside and two phthalic acid amide stir and are incubated;
Three, then, after the mixture that stirs is evacuated, add polydimethylsiloxane, climbazole, vitamin B5, Aloe extraction solution and fibroin, be stirred to and be uniformly dispersed;
Four, last, add sea salt and Herba Lysimachiae foenum-graeci quintessence oil, and stir, cooling back discharging is finished product.
The application implementation example:
Object of study: the anti-dandruff effect assessment of product
Research method: the antibacterial ring test in-vitro evaluation method that adopts the anti-dandruff effect of product
Implementation step:
1, the collection of chlosma, separation, cultivation
Gather: employing is scraped the bits method and is drawn materials at the normal person's head with dandruff;
Isolation identification: be inoculated in the Leeming & Notman culture medium flat plate; Cultivated about 10 days down for 32 ℃; Single bacterium colony is isolated in the line on same culture medium flat plate of the various chlosmas of gained, identified according to the authentication method in the document " classification of Malassezia and several kinds of dermopathic distribution situations ".
2, the antibacterial ring test of product
1. the preparation of test specimen: the proportion of composing of choosing the commercially available preferably anti-dandruff shampoo of anti-dandruff effect 1 and shampoo 2 sample sea salt and anti-dandruff dose:
| Numbering | Sea salt content | Anti-dandruff dose of (ZPT) content |
| 1 | 10 parts | 0.8 part |
| 2 | 12.5 part | 0.8 part |
| 3 | 15 parts | 0.8 part |
| 4 | 17.5 part | 0.8 part |
| 5 | 20 parts | 0.8 part |
2. the preparation of coupons: get qualitative filter paper of Xinhua; Break into diameter 5mm circular filter paper sheet with card punch, through pressuresteam sterilization, it is some to get the coupons of drying after the sterilization treatment; Dip in respectively with aseptic nipper and to get shampoo Xiao Xu to be checked on coupons, coupons is smeared evenly as far as possible.
3. dull and stereotyped preparation: the Malassezia furfur that activation is good is mixed with the bacteria suspension of 106cfu/ml ~ 107cfu/ml, gets on the Leeming & Notman culture medium flat plate that bacteria suspension 0.3ml is applied in 12cm.With above-mentioned contain the dull and stereotyped 10min of placement of bacterium after, in aseptic superclean bench, open dull and stereotyped lid, do flat board (about 20min) with aseptic wind.
4. the mensuration of fungistatic effect: put 1 test print in each dull and stereotyped subsides, 1 negative control (not containing test hair washing sample) print, totally 2.After subsides are put well, gently press print, make it be close to planar surface with aseptic paster.Build plate, put to be inverted in 32 ℃ of constant incubators and cultivated 7 days, with the diameter of vernier caliper measurement record inhibition zone.
Antibacterial ring test result:
As a kind of natural antiseptic agent, the protection product is avoided microbial contamination in the shelf-life with pure natural sea salt elite.Main component sodium chloride physicochemical properties are stable in the sea salt in addition; Can not cause raw material rotten and make skin occur irritated or stimulate because of illumination or with other substance reactions in the product; Simultaneously itself also can not discharge poisonous and harmful substance, this antiseptic is a kind of natural, safe cosmetics preservative.Sea salt can also be assisted cleaning skin or hair, utilizes the permeability of salt during hair washing, gos deep into skin, and blood circulation promoting enhances metabolism, and takes redundant moisture and fine material in the pore, fat etc. out of, plays the effect of weight-reducing; Utilize the frosted property of salt, remove the cutin of skin surface, the skin that thirst smoothly comes off; Delaying decrepitude of skin plays the effect of body building and beauty treatment, and life-time service can promote skin metabolism; The deep layer cleaning skin, unnecessary oils and fats and horny layer are removed in antiinflammatory, antibacterial, antipruritic.During hair washing, utilize sea salt and anti-dandruff dose of bactericidal action, can reduce the infection of sending out skin and root of hair, replenish the mineral of hair simultaneously, remove the greasy of hair, suppress the dandruff growth, many researchs show has anticreep with the salt hair washing effect is arranged in addition hair.
Sea salt among above-mentioned each embodiment also can adopt well mine salt or lake salt to substitute, and effect is very nearly the same, embodiment be not provided here.
Claims (10)
1. a hair washing salt is newborn, it is characterized in that comprising following component and weight proportion thereof:
10 ~ 30 parts of edible salts, 10 ~ 40 parts in surfactant, 0.1 ~ 5 part of suspension stabilizer; 1 ~ 10 part of emulsified silicone oil, 0.1 ~ 5 part of thickening agent, anti-dandruff dose 0.1 ~ 1.5 part; Spice extracts 0.1 ~ 3 part of quintessence oil, 0.1 ~ 4 part of wetting agent, 0.1 ~ 3 part of cation opsonizing agent; 0 ~ 5 part of nourishing additive agent, 30 ~ 70 parts of deionized waters.
2. hair washing salt according to claim 1 breast is characterized in that described surfactant is at least a in sodium laureth sulfate, laureth ammonium sulfate, sodium lauryl sulfate, ammonium lauryl sulfate, dodecanamide propyl hydroxy sulfo lycine, cocamido propyl betaine, lauryl glucoside, lauryl alcohol phosphate ester potassium, coconut oil single ethanol amide sulfosuccinic acid monoesters disodium, coconut oil single ethanol amide, the sodium lauroyl sarcosine.
3. hair washing salt according to claim 1 breast is characterized in that described edible salt is at least a in sea salt, well mine salt or the lake salt.
4. hair washing salt breast according to claim 1 is characterized in that described suspension stabilizer is two phthalic acid amide.
5. hair washing salt breast according to claim 1 is characterized in that described anti-dandruff dose is ZPT.
6. hair washing salt according to claim 1 breast is characterized in that described wetting agent is at least a in glycerol, propylene glycol, the butanediol.
7. hair washing salt according to claim 1 breast is characterized in that described cation opsonizing agent is at least a in guar gum hydroxypropyl-trimethyl ammonium chloride, cationic cellulose, polyquaternary ammonium salt, the cation high molecular protein peptide.
8. hair washing salt according to claim 1 breast is characterized in that described emulsified silicone oil is at least a in polydimethylsiloxane, the dimethiconol; Described thickening agent is at least a in xanthan gum, hydroxyethyl-cellulose, the cithrol; Described nourishing additive agent is at least a in Jojoba oil, Aloe extract, pantothenylol, vitamins, amino acids, olive oil, hyaluronate sodium, the sodium lactate.
9. hair washing salt breast according to claim 1 is characterized in that comprising following component and weight proportion thereof:
10 ~ 30 parts of edible salts, 10 ~ 40 parts in surfactant, 0.1 ~ 5 part of suspension stabilizer; 1 ~ 10 part of emulsified silicone oil, 0.1 ~ 5 part of thickening agent, anti-dandruff dose 0.1 ~ 1.5 part; Spice extracts 0.1 ~ 3 part of quintessence oil, 0.1 ~ 4 part of wetting agent, 0.1 ~ 3 part of cation opsonizing agent; 0 ~ 5 part of nourishing additive agent, 30 ~ 70 parts of deionized waters.
10. the method for preparing of any hair washing salt breast described in claim 1 ~ 9 is characterized in that comprising the steps;
1. place reaction pot to be heated to 50 ~ 60 ℃ in water, will be added to the water together with thickening agent with the scattered cation opsonizing agent of wetting agent stirs again;
2. adding surfactant and suspension stabilizer then stirs and is incubated;
3. the mixture after the above-mentioned insulation is evacuated, adds emulsified silicone oil and anti-dandruff dose, stir; Or add emulsified silicone oil, anti-dandruff dose and nourishing additive agent, stir;
4. add edible salt and spice at last and extract quintessence oil, stir, cooling back discharging is finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012101428898A CN102631304B (en) | 2012-05-10 | 2012-05-10 | Preparation method of shampoo salt emulsion |
Applications Claiming Priority (1)
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| CN102824281A (en) * | 2012-09-17 | 2012-12-19 | 江苏隆力奇生物科技股份有限公司 | Skin cleaning foam and preparation method thereof |
| CN102961272A (en) * | 2012-12-14 | 2013-03-13 | 四川久大品种盐有限责任公司 | Salt mixed hair shampoo and preparation method thereof |
| CN104323929A (en) * | 2014-10-31 | 2015-02-04 | 重庆环驰科技有限公司 | Shampoo with controllable viscosity and preparation method thereof |
| CN104473788A (en) * | 2014-11-15 | 2015-04-01 | 陈育烨 | Preparation method of pure natural tea seed skin-moisturizing facial cleansing cream |
| CN105012164A (en) * | 2015-07-03 | 2015-11-04 | 黄庆生 | Shampoo and preparation method thereof |
| CN105434275A (en) * | 2015-12-31 | 2016-03-30 | 胡鹏 | Shampoo salt rich in mineral trace elements and preparation method |
| CN105434276A (en) * | 2015-12-31 | 2016-03-30 | 胡鹏 | Shampoo salt and preparation method thereof |
| CN105456134A (en) * | 2015-12-31 | 2016-04-06 | 胡鹏 | Shampoo salt with healthcare efficacy and preparation method thereof |
| CN105496890A (en) * | 2015-12-31 | 2016-04-20 | 胡鹏 | Shampooing hair care salt and preparation method |
| CN105496932A (en) * | 2015-12-31 | 2016-04-20 | 胡鹏 | Hair washing salt capable of nourishing scalp and preparation method thereof |
| CN105534794A (en) * | 2015-12-31 | 2016-05-04 | 胡鹏 | Cleaning salt |
| CN105534795A (en) * | 2015-12-31 | 2016-05-04 | 胡鹏 | Mild anti-dandruff hair washing salt and preparation method thereof |
| CN105560108A (en) * | 2015-12-31 | 2016-05-11 | 胡鹏 | Washing and care salt for moisturizing hair, and preparation method thereof |
| CN105997535A (en) * | 2016-05-24 | 2016-10-12 | 长沙华晨生物科技有限公司 | Personal care formula without preservative |
| CN105997596A (en) * | 2016-07-08 | 2016-10-12 | 拉芳家化股份有限公司 | Dandruff removing composition containing plant essential oil having synergistic effect and application thereof |
| CN106389154A (en) * | 2016-10-25 | 2017-02-15 | 澳宝化妆品（惠州）有限公司 | Multi-effect balanced shampoo and preparation method thereof |
| CN106511124A (en) * | 2015-09-09 | 2017-03-22 | 林宥辉 | Detergent composition, and preparation method thereof |
| CN106727240A (en) * | 2016-12-28 | 2017-05-31 | 天津市澧沛佳海水娱乐工程有限公司 | A kind of washing one's face without preservative, dual-purpose formula of taking a shower |
| CN106727241A (en) * | 2016-12-28 | 2017-05-31 | 天津市澧沛佳海水娱乐工程有限公司 | A kind of shampoo prescription containing ooze dissolved matter |
| CN107126389A (en) * | 2017-05-09 | 2017-09-05 | 南通千竹电子科技有限公司 | A kind of amino acid hair washing product and preparation method thereof |
| CN108186439A (en) * | 2018-02-09 | 2018-06-22 | 广州御延堂生物科技有限公司 | A kind of sea salt nourishes hair cream and preparation method thereof |
| CN109646352A (en) * | 2019-01-10 | 2019-04-19 | 澳宝化妆品（惠州）有限公司 | A kind of hair-washing composition with anti-dandruff performance containing pomegranate rind extract |
| CN113842331A (en) * | 2021-11-17 | 2021-12-28 | 广州宝丝捷生物科技有限公司 | Novel soothing, nursing, refreshing and anti-dandruff shampoo and preparation method thereof |
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| CN101084870A (en) * | 2007-06-22 | 2007-12-12 | 昆明理工大学 | Emulsifying salt type traditional Chinese herbs emulsion used for washing and caring hair and preparation method thereof |
| CN101249058A (en) * | 2008-02-26 | 2008-08-27 | 昆明理工大学 | Anti-dandruff relieve itching hair washing cream liquid containing inorganic salt and Chinese medicine and preparation thereof |
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| JPS5682897A (en) * | 1979-12-11 | 1981-07-06 | Sanyo Chemical Ind Ltd | Shampoo composition |
| WO1992014440A1 (en) * | 1990-02-02 | 1992-09-03 | The Procter & Gamble Company | Antidandruff shampoo compositions |
| CN101084870A (en) * | 2007-06-22 | 2007-12-12 | 昆明理工大学 | Emulsifying salt type traditional Chinese herbs emulsion used for washing and caring hair and preparation method thereof |
| CN101249058A (en) * | 2008-02-26 | 2008-08-27 | 昆明理工大学 | Anti-dandruff relieve itching hair washing cream liquid containing inorganic salt and Chinese medicine and preparation thereof |
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|---|---|---|---|---|
| CN102824281A (en) * | 2012-09-17 | 2012-12-19 | 江苏隆力奇生物科技股份有限公司 | Skin cleaning foam and preparation method thereof |
| CN102824281B (en) * | 2012-09-17 | 2014-09-10 | 江苏隆力奇生物科技股份有限公司 | Skin cleaning foam and preparation method thereof |
| CN102961272A (en) * | 2012-12-14 | 2013-03-13 | 四川久大品种盐有限责任公司 | Salt mixed hair shampoo and preparation method thereof |
| CN104323929A (en) * | 2014-10-31 | 2015-02-04 | 重庆环驰科技有限公司 | Shampoo with controllable viscosity and preparation method thereof |
| CN104323929B (en) * | 2014-10-31 | 2017-08-29 | 重庆环驰科技有限公司 | Controllable shampoo of a kind of viscosity and preparation method thereof |
| CN104473788A (en) * | 2014-11-15 | 2015-04-01 | 陈育烨 | Preparation method of pure natural tea seed skin-moisturizing facial cleansing cream |
| CN105012164A (en) * | 2015-07-03 | 2015-11-04 | 黄庆生 | Shampoo and preparation method thereof |
| CN106511124B (en) * | 2015-09-09 | 2019-12-06 | 林宥辉 | detergent composition and process for producing the same |
| CN106511124A (en) * | 2015-09-09 | 2017-03-22 | 林宥辉 | Detergent composition, and preparation method thereof |
| CN105534795A (en) * | 2015-12-31 | 2016-05-04 | 胡鹏 | Mild anti-dandruff hair washing salt and preparation method thereof |
| CN105534794A (en) * | 2015-12-31 | 2016-05-04 | 胡鹏 | Cleaning salt |
| CN105496890A (en) * | 2015-12-31 | 2016-04-20 | 胡鹏 | Shampooing hair care salt and preparation method |
| CN105560108A (en) * | 2015-12-31 | 2016-05-11 | 胡鹏 | Washing and care salt for moisturizing hair, and preparation method thereof |
| CN105456134A (en) * | 2015-12-31 | 2016-04-06 | 胡鹏 | Shampoo salt with healthcare efficacy and preparation method thereof |
| CN105496932A (en) * | 2015-12-31 | 2016-04-20 | 胡鹏 | Hair washing salt capable of nourishing scalp and preparation method thereof |
| CN105434275A (en) * | 2015-12-31 | 2016-03-30 | 胡鹏 | Shampoo salt rich in mineral trace elements and preparation method |
| CN105434276A (en) * | 2015-12-31 | 2016-03-30 | 胡鹏 | Shampoo salt and preparation method thereof |
| CN105997535A (en) * | 2016-05-24 | 2016-10-12 | 长沙华晨生物科技有限公司 | Personal care formula without preservative |
| CN105997596B (en) * | 2016-07-08 | 2018-06-26 | 拉芳家化股份有限公司 | A kind of desquamation compositions of plants essential oil synergy |
| CN105997596A (en) * | 2016-07-08 | 2016-10-12 | 拉芳家化股份有限公司 | Dandruff removing composition containing plant essential oil having synergistic effect and application thereof |
| CN106389154A (en) * | 2016-10-25 | 2017-02-15 | 澳宝化妆品（惠州）有限公司 | Multi-effect balanced shampoo and preparation method thereof |
| CN106727240A (en) * | 2016-12-28 | 2017-05-31 | 天津市澧沛佳海水娱乐工程有限公司 | A kind of washing one's face without preservative, dual-purpose formula of taking a shower |
| CN106727241A (en) * | 2016-12-28 | 2017-05-31 | 天津市澧沛佳海水娱乐工程有限公司 | A kind of shampoo prescription containing ooze dissolved matter |
| CN107126389A (en) * | 2017-05-09 | 2017-09-05 | 南通千竹电子科技有限公司 | A kind of amino acid hair washing product and preparation method thereof |
| CN108186439A (en) * | 2018-02-09 | 2018-06-22 | 广州御延堂生物科技有限公司 | A kind of sea salt nourishes hair cream and preparation method thereof |
| CN109646352A (en) * | 2019-01-10 | 2019-04-19 | 澳宝化妆品（惠州）有限公司 | A kind of hair-washing composition with anti-dandruff performance containing pomegranate rind extract |
| CN113842331A (en) * | 2021-11-17 | 2021-12-28 | 广州宝丝捷生物科技有限公司 | Novel soothing, nursing, refreshing and anti-dandruff shampoo and preparation method thereof |
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