CN105560108A - Washing and care salt for moisturizing hair, and preparation method thereof - Google Patents
Washing and care salt for moisturizing hair, and preparation method thereof Download PDFInfo
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61Q5/12—Preparations containing hair conditioners
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Abstract
The invention discloses a washing and care salt for moisturizing hair. The washing and care salt is prepared from a first part and a second part, wherein the first part comprises, by mass, 8-10 parts of Amur Corktree Bark, 9-11 parts of Cortex Lycii, 5-7 parts of semen cuscutae, 3-6 parts of Achyranthes bidentata, 6-8 parts of Radix Astragali, 4-7 parts of pumpkin seed, 5-8 parts of Gleditsia sinensis, and 3-6 parts of lemon; and the second part comprises, by mass, 12-20 parts of natural sea salt, 1.0-1.4 parts of seabuckthorm seed oil, 68-80 parts of deionized water, 2-8 parts of polydimethylsiloxane, 1-5 parts of hydroxyethyl cellulose, 1-2 parts of glycerin, 2-4 parts of propylene glycol, 15-30 parts of a surfactant, 0.5-1.0 part of ethyl cinnamate, 0.6-1.0 part of ethylene glycol monostearate and 0.1-0.5 parts of ethylparaben. The washing and care salt prepared in the invention can deeply care hair, moisturize scalps, control oil, lock water, remove dandruff and relieve itches to make hair be smooth and glossy and reduce coarseness and hair furcation.
Description
Technical field
The present invention relates to bath article field, particularly relate to a kind of washing of hair of moistening and protect Salt And Preparation Method.
Background technology
Since ancient times, salt is just brought as clean representative articles for use, no matter be used as being sacrificed to a god the one of offerings, or sumo start before just brought the corner being sprinkled upon place, and funeral return after spill custom piggyback with salt, therefrom can understand that " salt " is the effect with clean all things.The people of many countries already custom deep-sea bath salt wash one's face, foot bath, it can enhance metabolism, deep layer cleaning skin, antiinflammatory, sterilization, rapid healing minor cut or wound, dispel excess oil and horny layer, the rough epidermis of reparation, restrain thick pore, life-time service, the soft and smooth exquisiteness of skin.The salt being commonly used for bathing has sea salt, lake salt and well mine salt three kinds, and these salt have control oils and fats, remove pockmark, speckle dispelling, prevent the dandruff and dispel the effects such as oxter abnormal flavour.
Publication No. CN102631304A(application number 201210142889.8) Chinese patent literature disclose a kind of shampoo salt emulsion and preparation method thereof, comprise following component and weight proportion thereof: edible salt 10 ~ 30 parts, 10 ~ 40 parts, surfactant, suspension stabilizer 0.1 ~ 5 part, emulsified silicone oil 1 ~ 10 part, thickening agent 0.1 ~ 5 part, anti-dandruff agent 0.1 ~ 1.5 part, spice extracts quintessence oil 0.1 ~ 3 part, wetting agent 0.1 ~ 4 part, cation opsonizing agent 0.1 ~ 3 part, nourishing additive agent 0 ~ 5 part, deionized water 30 ~ 70 parts.
In prior art, salt is developed to bath salt, sufficient salt and salt of washing one's face more, and salt has multiple efficacies, is worth developing further, at present on the market there are no the product of shampoo salt, therefore can develop washing of a kind of hair care and protect salt.
Summary of the invention
For the deficiencies in the prior art, the object of this invention is to provide that a kind of technique is simple, the washing of hair of moistening of hair care and nourishing protects Salt And Preparation Method.
Technical scheme of the present invention is:
Moist washing of hair can protect salt, be prepared from by two parts, be mass parts: Part I forms: Cortex Phellodendri 8-10, Cortex Lycii 9-11, Semen Cuscutae 5-7, Radix Achyranthis Bidentatae 3-6, Radix Astragali 6-8, Semen Cucurbitae 4-7, Fructus Gleditsia 5-8, Fructus Citri Limoniae 3-6; Part II forms: natural sea salt 12-20, Fructrs Hippophae seed oil 1.0-1.4, deionized water 68-80, polydimethylsiloxane 2-8, hydroxyethyl-cellulose 1-5, glycerol 1-2, propylene glycol 2-4, surfactant 15-30, ethyl cinnamate 0.5-1.0, ethylene glycol monostearate 0.6-1.0, ethyl hydroxybenzoate 0.1-0.5.
In preferred scheme, be prepared from by two parts, be mass parts: Part I forms: Cortex Phellodendri 8.5-9.5, Cortex Lycii 9.5-10.5, Semen Cuscutae 5.5-6.5, Radix Achyranthis Bidentatae 4-5, Radix Astragali 6.5-7.5, Semen Cucurbitae 5-6, Fructus Gleditsia 6-7, Fructus Citri Limoniae 4-5; Part II forms: natural sea salt 14-18, Fructrs Hippophae seed oil 1.1-1.3, deionized water 70-78, polydimethylsiloxane 3-7, hydroxyethyl-cellulose 2-4, glycerol 1.2-1.8, propylene glycol 2.5-3.5, surfactant 20-25, ethyl cinnamate 0.6-0.9, ethylene glycol monostearate 0.7-0.9, ethyl hydroxybenzoate 0.2-0.4.
Be more preferably, be prepared from by two parts, be mass parts: Part I forms: Cortex Phellodendri 9, Cortex Lycii 10, Semen Cuscutae 6, Radix Achyranthis Bidentatae 4.5, the Radix Astragali 7, Semen Cucurbitae 5.5, Fructus Gleditsia 6.5, Fructus Citri Limoniae 4.5; Part II forms: natural sea salt 16, Fructrs Hippophae seed oil 1.2, deionized water 74, polydimethylsiloxane 5, hydroxyethyl-cellulose 3, glycerol 1.5, propylene glycol 3, surfactant 22.5, ethyl cinnamate 0.7, ethylene glycol monostearate 0.8, ethyl hydroxybenzoate 0.3.
The preparation method of the shampoo salt of described hair of moistening, step is:
A. the preparation of Part I
(1) Cortex Phellodendri and Cortex Lycii roguing are cleaned, soak into mature vinegar, take out, be placed in frying pan, intense fire adds to be propagandized hotly to surface coke black, takes out, dries in the air cool;
(2) get Semen Cuscutae and Semen Cucurbitae roguing, mix moistening 20-30 minute (preferably, moistening 22-28 minute thoroughly with saline; Be more preferably, moistening 25 minutes), to be placed in watt and to dry, take out, dry in the air cool;
(3) by Radix Achyranthis Bidentatae, the Radix Astragali, Fructus Gleditsia, Fructus Citri Limoniae remove impurity, dry together with step (1) (2) made raw material, pulverize, be placed in percolating device, with seepage pressure effects after 80% soak with ethanol, collect percolate, concentrated, recycling design, to without alcohol taste, obtains extract;
B. the preparation of Part II
(1) ethyl cinnamate, ethylene glycol monostearate and ethyl hydroxybenzoate are joined stirring and evenly mixing in propylene glycol, obtained adjuvant mixture, for subsequent use, by deionized water and hydroxyethyl-cellulose stirring and evenly mixing, and be heated to 50-70 DEG C (preferred, be heated to 55-65 DEG C; Be more preferably, be heated to 60 DEG C), then add glycerol and adjuvant mixture stirring and evenly mixing, obtained mixed liquor;
(2) in step (1) made mixed liquor, add surfactant to mix thoroughly, then add polydimethylsiloxane and mix rear stopping heating thoroughly, be cooled to room temperature, add natural sea salt and Fructrs Hippophae seed oil stirring and evenly mixing, obtained mixture;
C. made for Part I extract is joined stirring and evenly mixing in the made mixture of Part II, citric acid solution regulates pH to faintly acid, obtains shampoo salt.
The preparation method of the shampoo salt of described hair of moistening, in the preparation of Part I, the amount of step (1) mature vinegar is the 3-5 of two kinds of raw materials quality doubly (preferred, the amount of mature vinegar is 4 times of two kinds of raw materials quality).
The preparation method of the shampoo salt of described hair of moistening, in the preparation of Part I, the mass concentration of step (2) saline is that 20-35%(is preferred, and the mass concentration of saline is 25-30%; Be more preferably, the mass concentration of saline is 27%).
The preparation method of the shampoo salt of described hair of moistening, in the preparation of Part I, step (3) was pulverized 40-80 mesh sieve and (preferably, was pulverized 50-70 mesh sieve; Be more preferably, pulverized 60 mesh sieves).
The preparation method of the shampoo salt of described hair of moistening, in the preparation of Part I step (3) with 80% soak with ethanol 4-10 hour (preferred, with 80% soak with ethanol 6-8 hour; Be more preferably, by 80% soak with ethanol 7 hours).
The preparation method of the shampoo salt of described hair of moistening, in the preparation of Part I, step (3) collects the percolate that obtains and raw material is by volume that 10-16:1(is preferred with weight ratio, and collecting the percolate that obtains and raw material is by volume 12-14:1 with weight ratio; Be more preferably, collecting the percolate that obtains and raw material is by volume 13:1 with weight ratio).
The preparation method of the shampoo salt of described hair of moistening, in the preparation of Part II, step (1) described surfactant is at least one in Oleum Cocois single ethanol amide, oleic acid diethyl amide, cocos nucifera oil acyl both sexes acetic acid disodium, cocamidopropyl propyl amide hydroxyl sulphonic acid betaine and lauroylamidopropyl betaine.
The washing of hair of moistening provided by the invention is protected salt binding Effective Component of Chinese Medicine and is prepared from, and simple for process, cost is low, and product safety is reliable.In addition, excellent results of the present invention also shows: products made thereby of the present invention can deep layer maintenance hair, moistens scalp, and control oil lock water, removing scurf and relieving itching, makes hair submissive glossy, reduce crude and bifurcated.
Detailed description of the invention
Describe technical scheme of the present invention in detail below in conjunction with embodiment and experimental example, but protection domain is not limited thereto.
embodiment 1moist washing of hair can protect salt, be prepared from (every part of 100g) by two parts: Part I forms: Cortex Phellodendri 8 parts, Cortex Lycii 9 parts, Semen Cuscutae 5 parts, Radix Achyranthis Bidentatae 3 parts, the Radix Astragali 6 parts, Semen Cucurbitae 4 parts, 5 parts, Fructus Gleditsia, 3 parts, Fructus Citri Limoniae; Part II forms: natural sea salt 12 parts, Fructrs Hippophae seed oil 1.0 parts, deionized water 68 parts, polydimethylsiloxane 2 parts, hydroxyethyl-cellulose 1 part, glycerol 1 part, propylene glycol 2 parts, Oleum Cocois single ethanol amide 15 parts, ethyl cinnamate 0.5 part, ethylene glycol monostearate 0.6 part, ethyl hydroxybenzoate 0.1 part.
The preparation method of protecting salt of washing of above-mentioned hair of moistening is:
The preparation of Part I
A.(1) Cortex Phellodendri and Cortex Lycii roguing are cleaned, soak into the mature vinegar of two kinds of raw materials quality 3 times, take out, be placed in frying pan, intense fire adds to be propagandized hotly to surface coke black, takes out, dries in the air cool;
(2) get Semen Cuscutae and Semen Cucurbitae roguing, mix moistening thoroughly 20 minutes with the saline that mass concentration is 20%, to be placed in watt and to dry, take out, dry in the air cool;
(3) by Radix Achyranthis Bidentatae, the Radix Astragali, Fructus Gleditsia, Fructus Citri Limoniae remove impurity, dry together with step (1) (2) made raw material, pulverized 40 mesh sieves, be placed in percolating device, with 80% soak with ethanol seepage pressure effects after 4 hours, collect percolate, collecting the percolate that obtains and raw material is by volume 10:1 with weight ratio, concentrated, recycling design, to without alcohol taste, obtains extract;
B. the preparation of Part II
(1) ethyl cinnamate, ethylene glycol monostearate and ethyl hydroxybenzoate are joined stirring and evenly mixing in propylene glycol, obtained adjuvant mixture, again by deionized water and hydroxyethyl-cellulose stirring and evenly mixing, and be heated to 50 DEG C, add glycerol and adjuvant mixture stirring and evenly mixing obtains mixed liquor;
(2) in step (1) made mixed liquor, add Oleum Cocois single ethanol amide to mix thoroughly, then add polydimethylsiloxane and mix rear stopping heating thoroughly, be cooled to room temperature, add natural sea salt and Fructrs Hippophae seed oil stirring and evenly mixing, obtained mixture;
C. made for Part I extract is joined stirring and evenly mixing in the made mixture of Part II, citric acid solution regulates pH to faintly acid, obtains shampoo salt.
embodiment 2moist washing of hair can protect salt, be prepared from (every part of 100g) by two parts: Part I forms: Cortex Phellodendri 10 parts, Cortex Lycii 11 parts, Semen Cuscutae 7 parts, Radix Achyranthis Bidentatae 6 parts, the Radix Astragali 8 parts, Semen Cucurbitae 7 parts, 8 parts, Fructus Gleditsia, 6 parts, Fructus Citri Limoniae; Part II forms: natural sea salt 20 parts, Fructrs Hippophae seed oil 1.4 parts, deionized water 80 parts, polydimethylsiloxane 8 parts, hydroxyethyl-cellulose 5 parts, glycerol 2 parts, propylene glycol 4 parts, cocamidopropyl propyl amide hydroxyl sulphonic acid betaine 30 parts, ethyl cinnamate 1.0 parts, ethylene glycol monostearate 1.0 parts, ethyl hydroxybenzoate 0.5 part.
The preparation method of protecting salt of washing of the moist hair of energy is:
A. the preparation of Part I
(1) Cortex Phellodendri and Cortex Lycii roguing are cleaned, soak into the mature vinegar of two kinds of raw materials quality 5 times, take out, be placed in frying pan, intense fire adds to be propagandized hotly to surface coke black, takes out, dries in the air cool;
(2) get Semen Cuscutae and Semen Cucurbitae roguing, mix moistening thoroughly 30 minutes with the saline that mass concentration is 35%, to be placed in watt and to dry, take out, dry in the air cool;
(3) by Radix Achyranthis Bidentatae, the Radix Astragali, Fructus Gleditsia, Fructus Citri Limoniae remove impurity, dry together with step (1) (2) made raw material, pulverized 80 mesh sieves, be placed in percolating device, with 80% soak with ethanol seepage pressure effects after 10 hours, collect percolate, collecting the percolate that obtains and raw material is by volume 16:1 with weight ratio, concentrated, recycling design, to without alcohol taste, obtains extract;
B. the preparation of Part II
(1) ethyl cinnamate, ethylene glycol monostearate and ethyl hydroxybenzoate are joined stirring and evenly mixing in propylene glycol, obtained adjuvant mixture, again by deionized water and hydroxyethyl-cellulose stirring and evenly mixing, and be heated to 70 DEG C, add glycerol and adjuvant mixture stirring and evenly mixing obtains mixed liquor;
(2) in step (1) made mixed liquor, add cocamidopropyl propyl amide hydroxyl sulphonic acid betaine to mix thoroughly, then add polydimethylsiloxane and mix rear stopping heating thoroughly, be cooled to room temperature, add natural sea salt and Fructrs Hippophae seed oil stirring and evenly mixing, obtained mixture;
C. made for Part I extract is joined stirring and evenly mixing in the made mixture of Part II, citric acid solution regulates pH to faintly acid, obtains shampoo salt.
embodiment 3moist washing of hair can protect salt, be prepared from (every part of 100g) by two parts: Part I forms: Cortex Phellodendri 8.5 parts, Cortex Lycii 9.5 parts, Semen Cuscutae 5.5 parts, Radix Achyranthis Bidentatae 4 parts, the Radix Astragali 6.5 parts, Semen Cucurbitae 5 parts, 6 parts, Fructus Gleditsia, 4 parts, Fructus Citri Limoniae; Part II forms: natural sea salt 14 parts, Fructrs Hippophae seed oil 1.1 parts, deionized water 70 parts, polydimethylsiloxane 3 parts, hydroxyethyl-cellulose 2 parts, glycerol 1.2 parts, propylene glycol 2.5 parts, cocos nucifera oil acyl both sexes acetic acid disodium 20 parts, ethyl cinnamate 0.6 part, ethylene glycol monostearate 0.7 part, ethyl hydroxybenzoate 0.2 part.
The preparation method of protecting salt of washing of the moist hair of energy is:
A. the preparation of Part I
(1) Cortex Phellodendri and Cortex Lycii roguing are cleaned, soak into the mature vinegar of two kinds of raw materials quality 3 times, take out, be placed in frying pan, intense fire adds to be propagandized hotly to surface coke black, takes out, dries in the air cool;
(2) get Semen Cuscutae and Semen Cucurbitae roguing, mix moistening thoroughly 22 minutes with the saline that mass concentration is 25%, to be placed in watt and to dry, take out, dry in the air cool;
(3) by Radix Achyranthis Bidentatae, the Radix Astragali, Fructus Gleditsia, Fructus Citri Limoniae remove impurity, dry together with step (1) (2) made raw material, pulverized 50 mesh sieves, be placed in percolating device, with 80% soak with ethanol seepage pressure effects after 6 hours, collect percolate, collecting the percolate that obtains and raw material is by volume 12:1 with weight ratio, concentrated, recycling design, to without alcohol taste, obtains extract;
B. the preparation of Part II
(1) ethyl cinnamate, ethylene glycol monostearate and ethyl hydroxybenzoate are joined stirring and evenly mixing in propylene glycol, obtained adjuvant mixture, again by deionized water and hydroxyethyl-cellulose stirring and evenly mixing, and be heated to 55 DEG C, add glycerol and adjuvant mixture stirring and evenly mixing obtains mixed liquor;
(2) in step (1) made mixed liquor, add cocos nucifera oil acyl both sexes acetic acid disodium to mix thoroughly, then add polydimethylsiloxane and mix rear stopping heating thoroughly, be cooled to room temperature, add natural sea salt and Fructrs Hippophae seed oil stirring and evenly mixing, obtained mixture;
C. made for Part I extract is joined stirring and evenly mixing in the made mixture of Part II, citric acid solution regulates pH to faintly acid, obtains shampoo salt.
Typical case: xxx, female, 36 years old.Hair length and loins, once hair-waving was done before one month, in order to conventional hair-dryer of saving time dries up after hair washing, hair is caused to dry up low and deep, crude bifurcated, few gloss, each hair washing is all with hair conditioner Huo hairdressing gel otherwise hair there will be knotting, be difficult to combing, there is by people's recommendation the present embodiment gained the shampoo salt of health-care effect, hair is crumpled gently during use, massaging scalp, stop 5 minutes, then clean by clean water, after using three times, hair is obviously submissive comparatively before, after using two weeks, hair is submissive glossy, bifurcated reduces, adhere to afterwards using always.
embodiment 4moist washing of hair can protect salt, be prepared from (every part of 100g) by two parts: Part I forms: Cortex Phellodendri 9.5 parts, Cortex Lycii 10.5 parts, Semen Cuscutae 6.5 parts, Radix Achyranthis Bidentatae 5 parts, the Radix Astragali 7.5 parts, Semen Cucurbitae 6 parts, 7 parts, Fructus Gleditsia, 5 parts, Fructus Citri Limoniae; Part II forms: natural sea salt 18 parts, Fructrs Hippophae seed oil 1.3 parts, deionized water 78 parts, polydimethylsiloxane 7 parts, hydroxyethyl-cellulose 4 parts, glycerol 1.8 parts, propylene glycol 3.5 parts, oleic acid diethyl amide 25 parts, ethyl cinnamate 0.9 part, ethylene glycol monostearate 0.9 part, ethyl hydroxybenzoate 0.4 part.
The preparation method of protecting salt of washing of the moist hair of energy is:
A. the preparation of Part I
(1) Cortex Phellodendri and Cortex Lycii roguing are cleaned, soak into the mature vinegar of two kinds of raw materials quality 5 times, take out, be placed in frying pan, intense fire adds to be propagandized hotly to surface coke black, takes out, dries in the air cool;
(2) get Semen Cuscutae and Semen Cucurbitae roguing, mix moistening thoroughly 28 minutes with the saline that mass concentration is 30%, to be placed in watt and to dry, take out, dry in the air cool;
(3) by Radix Achyranthis Bidentatae, the Radix Astragali, Fructus Gleditsia, Fructus Citri Limoniae remove impurity, dry together with step (1) (2) made raw material, pulverized 70 mesh sieves, be placed in percolating device, with 80% soak with ethanol seepage pressure effects after 8 hours, collect percolate, collecting the percolate that obtains and raw material is by volume 14:1 with weight ratio, concentrated, recycling design, to without alcohol taste, obtains extract;
B. the preparation of Part II
(1) ethyl cinnamate, ethylene glycol monostearate and ethyl hydroxybenzoate are joined stirring and evenly mixing in propylene glycol, obtained adjuvant mixture, again by deionized water and hydroxyethyl-cellulose stirring and evenly mixing, and be heated to 65 DEG C, add glycerol and adjuvant mixture stirring and evenly mixing obtains mixed liquor;
(2) in step (1) made mixed liquor, add oleic acid diethyl amide to mix thoroughly, then add polydimethylsiloxane and mix rear stopping heating thoroughly, be cooled to room temperature, add natural sea salt and Fructrs Hippophae seed oil stirring and evenly mixing, obtained mixture;
C. made for Part I extract is joined stirring and evenly mixing in the made mixture of Part II, citric acid solution regulates pH to faintly acid, obtains shampoo salt.
Typical case: xxx, female, 28 years old.Be negligent of at ordinary times arranging, occur that dandruff is more afterwards, hair is dry, and bifurcated is serious, when combing one's hair, hair end has knotting, and hair elasticity is poor, withered easily broken, use the present embodiment gained washing of hair of moistening to protect salt after being introduced, crumple hair gently during use, massaging scalp, stop 5 minutes, then clean by clean water, after using one week, dandruff disappears completely, and hair obviously becomes easy combing, does not occur knotting again, adhere to use one month, send out tip bifurcated and obviously improve, hair becomes smooth glossy.
embodiment 5moist washing of hair can protect salt, be prepared from (every part of 100g) by two parts: Part I forms: Cortex Phellodendri 9 parts, Cortex Lycii 10 parts, Semen Cuscutae 6 parts, Radix Achyranthis Bidentatae 4.5 parts, the Radix Astragali 7 parts, Semen Cucurbitae 5.5 parts, 6.5 parts, Fructus Gleditsia, 4.5 parts, Fructus Citri Limoniae; Part II forms: natural sea salt 16 parts, Fructrs Hippophae seed oil 1.2 parts, deionized water 74 parts, polydimethylsiloxane 5 parts, hydroxyethyl-cellulose 3 parts, glycerol 1.5 parts, propylene glycol 3 parts, lauroylamidopropyl betaine 22.5 parts, ethyl cinnamate 0.7 part, ethylene glycol monostearate 0.8 part, ethyl hydroxybenzoate 0.3 part.
The preparation method of protecting salt of washing of the moist hair of energy is:
A. the preparation of Part I
(1) Cortex Phellodendri and Cortex Lycii roguing are cleaned, soak into the mature vinegar of two kinds of raw materials quality 4 times, take out, be placed in frying pan, intense fire adds to be propagandized hotly to surface coke black, takes out, dries in the air cool;
(2) get Semen Cuscutae and Semen Cucurbitae roguing, mix moistening thoroughly 25 minutes with the saline that mass concentration is 27%, to be placed in watt and to dry, take out, dry in the air cool;
(3) by Radix Achyranthis Bidentatae, the Radix Astragali, Fructus Gleditsia, Fructus Citri Limoniae remove impurity, dry together with step (1) (2) made raw material, pulverized 60 mesh sieves, be placed in percolating device, with 80% soak with ethanol seepage pressure effects after 7 hours, collect percolate, collecting the percolate that obtains and raw material is by volume 13:1 with weight ratio, concentrated, recycling design, to without alcohol taste, obtains extract;
B. the preparation of Part II
(1) ethyl cinnamate, ethylene glycol monostearate and ethyl hydroxybenzoate are joined stirring and evenly mixing in propylene glycol, obtained adjuvant mixture, again by deionized water and hydroxyethyl-cellulose stirring and evenly mixing, and be heated to 60 DEG C, add glycerol and adjuvant mixture stirring and evenly mixing obtains mixed liquor;
(2) in step (1) made mixed liquor, add lauroylamidopropyl betaine to mix thoroughly, then add polydimethylsiloxane and mix rear stopping heating thoroughly, be cooled to room temperature, add natural sea salt and Fructrs Hippophae seed oil stirring and evenly mixing, obtained mixture;
C. made for Part I extract is joined stirring and evenly mixing in the made mixture of Part II, citric acid solution regulates pH to faintly acid, obtains shampoo salt.
The pharmacology of the present invention's raw material of Chinese medicine used is as follows:
Cortex Phellodendri: base is former: be the bark of rutaceae Cortex Phellodendri or wampee.Nature and flavor: bitter, cold.Gui Jing: return kidney, urinary bladder channel.Function cures mainly: heat clearing and damp drying, and pathogenic fire purging removes steams, detoxification sore treatment.For damp-heat dysentery, jaundice, leukorrhagia, pyretic stranguria, beriberi, flaccidity { is warded off }, hectic fever due to YIN-deficiency consumptive fever, night sweat, seminal emission, sore swollen toxin, eczema pruritus.Stir-baked CORTEX PHELLODENDRI with salt solution nourishing YIN to lower pathogenic fire.For hyperactivity of fire caused by deficiency of YIN, night sweat hectic fever due to YIN-deficiency.
Cortex Lycii: base is former: be the root bark of eggplant kind of plant Fructus Lycii etc.Nature and flavor: sweet, cold.Gui Jing: enter lung, liver, kidney channel.Function cures mainly: heat clearing away, removing heat from blood.Control asthenia hectic fever night sweat, lung-heat cough with asthma, spit blood, epistaxis, stranguria with blood, quenches one's thirst, hypertension, carbuncle, malignant boil.
Semen Cuscutae: base is former: be the seed of convolvulus cuscuta plant or cuscuta japonica Choisy.Nature and flavor: sweet, temperature.Gui Jing: return liver,kidney,spleen warp.Function cures mainly: nourishing the liver and kidney, controlling nocturnal emission with astringent drugs reducing urination, antiabortive, improving eyesight, antidiarrheal.For impotence and seminal emission, dripping urination, enuresis frequent micturition, soreness of the waist and knees, blurred vision tinnitus, vaginal bleeding due to deficiency of the kidney during pregnancy, frequent fetal movement, spleen is suffered from a deficiency of the kidney and is rushed down, externally treating leucoderma.
Radix Achyranthis Bidentatae: base is former: be the root of amaranthaceous plant Radix Achyranthis Bidentatae.Nature and flavor: bitter, sour are flat.Gui Jing: return liver, kidney channel.Function cures mainly: invigorating the liver and kidney, bone and muscle strengthening, eliminating blood stasis and inducing menstruation, conducting blood to flow downwards.For soreness of waist and knee joint, muscles and bones is unable, amenorrhea lump in the abdomen, dizziness due to hyperactivity of liver-YANG.
The Radix Astragali: base is former: be the root of leguminous plant Radix Astagali.Nature and flavor: sweet, temperature.Gui Jing: return lung, spleen channel.Function cures mainly: invigorating QI to consolidate the body surface resistance, diuresis poison holding, evacuation of pus, expelling pus and promoting granulation.Weak for the deficiency of vital energy, anorexia and loose stool, sinking of QI of middle-JIAO, chronic diarrhea proctoptosis, metrorrhagia of having blood in stool, exterior deficiency spontaneous perspiration, deficiency of vital energy edema, carbuncle difficulty is burst, and burst for a long time and do not hold back, blood deficiency dull yellowish colored skin, interior-heat is quenched one's thirst, chronic nephritis proteinuria, diabetes.
Semen Cucurbitae: base is former: be the seed of cucurbitaceous plant Fructus Cucurbitae moschatae.Nature and flavor: sweet, temperature.Function cures mainly: anthelmintic.For taeniasis, schistosomicide.
Fructus Gleditsia: base is former: be the fruit of leguminous plant Fructus Gleditsia.Nature and flavor: pungent, temperature, micro-poison.Function cures mainly: dispel the wind expectorant, except noxious dampness, and parasite killing.Control apoplexy facial hemiparalysis, wind syndrome of head is had a headache, cough phlegm dyspnea, and discharging fresh blood stool, dysentery is kept silent mouth, carbuncle inguinal bubo, skin ulcer tinea mange.
Fructus Citri Limoniae: base is former: be the fruit of rutaceae Canton lemon or lemon.Nature and flavor: taste is extremely sour.Function cures mainly: promote the production of body fluid, and quenches the thirst, and drives away summer heat, antiabortive.Pharyngalgia xerostomia, gastral cavilty flatulence, hypertension, myocardial infarction, anorexia.
Fructrs Hippophae seed oil: base is former: brown color, to brownish red transparent oily liquid, integrates the high enrichment thing of Effective Compositions of Seabuckthorn.Include more than the 140 kind of bioactive ingredients such as flavone, organic acid, alkaloid, sterols, triterpene class and various vitamin.Fructrs Hippophae seed oil, as healthy food material, finds broad application in antioxidation, resisting fatigue, hepatoprotective, blood fat reducing etc.; Fructrs Hippophae seed oil, as medicinal raw material, has obvious biological agent, and its infection is strong, Promotive union fast, be widely used in the treatment aspect such as burn, scald, cold injury, knife injury; Fructrs Hippophae seed oil is the complex of multivitamin and bioactive substance, its can nourishes rough skin, enhance metabolism, antiallergic, bactericidal antiphlogistic, promote re-epithelilization, repair is had to skin, can keep the sour environment of skin, have stronger permeability, be the important source material of beauty and skin care.
test example 1gained of the present invention can moisten hair wash protect salt (embodiment 5) carding property characterize and hair surface microcosmic improvement situation:
1, carrying out under being determined at that hair is dry and sending out state and wet method state two states of Hair setting, by measuring the situation of change of resistance that mechanical comb runs in combing hair process and resistance, judging the carding property of hair.Resistance is less, illustrates that the cardability of hair is better.By bleaching and dyeing impaired after the common shampoo of topknot commercial type clean up, use the carding property under the combing dry state of instrument measuring head and hygrometric state, re-use made the washing of the present invention and protect salt cleaning topknot, under test hair two states, wash and dress performance.Result calculates and uses the present invention to wash the percentage ratio protecting drag reduction after salt.
2, hair surface microcosmic improves situation and adopts HitachiS-4800 type scanning electron microscope, observes and uses the made hair scale sheet regularity washing the damaged hair surface protected before and after salt of the present invention, and fitting, better to show that hair surface is repaired better, and moist effect is larger.
Result of the test: test result obtains as calculated, after use the present invention washes and protects salt, topknot is combing drag reduction 22% under hygrometric state, combing drag reduction 13% under dry state, illustrates that the present invention has compared with other common shampoos the effect improving Hair setting preferably.In addition, observe find to use the present invention made wash protect salt before, there is the hair scale sheet of more projection on topknot surface, and after using, the hair scale sheet of topknot projection substantially all disappears, and hair surface is comparatively smooth.And the gloss of hair, compliance, regularity are all better, are easy to combing and arrange.
It should be pointed out that detailed description of the invention is the more representational example of the present invention, obvious technical scheme of the present invention is not limited to above-described embodiment, can also have a lot of distortion.Those of ordinary skill in the art, with the present invention clear and definite disclosed or according to undoubted the obtaining of the written description of file, the claimed scope of this patent all should be thought.
Claims (10)
1. washing of hair of moistening protects salt, it is characterized in that, is prepared from by two parts, be mass parts: Part I forms: Cortex Phellodendri 8-10, Cortex Lycii 9-11, Semen Cuscutae 5-7, Radix Achyranthis Bidentatae 3-6, Radix Astragali 6-8, Semen Cucurbitae 4-7, Fructus Gleditsia 5-8, Fructus Citri Limoniae 3-6; Part II forms: natural sea salt 12-20, Fructrs Hippophae seed oil 1.0-1.4, deionized water 68-80, polydimethylsiloxane 2-8, hydroxyethyl-cellulose 1-5, glycerol 1-2, propylene glycol 2-4, surfactant 15-30, ethyl cinnamate 0.5-1.0, ethylene glycol monostearate 0.6-1.0, ethyl hydroxybenzoate 0.1-0.5.
2. washing of hair of moistening as claimed in claim 1 protects salt, it is characterized in that, be prepared from by two parts, be mass parts: Part I forms: Cortex Phellodendri 8.5-9.5, Cortex Lycii 9.5-10.5, Semen Cuscutae 5.5-6.5, Radix Achyranthis Bidentatae 4-5, Radix Astragali 6.5-7.5, Semen Cucurbitae 5-6, Fructus Gleditsia 6-7, Fructus Citri Limoniae 4-5; Part II forms: natural sea salt 14-18, Fructrs Hippophae seed oil 1.1-1.3, deionized water 70-78, polydimethylsiloxane 3-7, hydroxyethyl-cellulose 2-4, glycerol 1.2-1.8, propylene glycol 2.5-3.5, surfactant 20-25, ethyl cinnamate 0.6-0.9, ethylene glycol monostearate 0.7-0.9, ethyl hydroxybenzoate 0.2-0.4.
3. washing of hair of moistening as claimed in claim 1 protects salt, it is characterized in that, is prepared from by two parts, be mass parts: Part I forms: Cortex Phellodendri 9, Cortex Lycii 10, Semen Cuscutae 6, Radix Achyranthis Bidentatae 4.5, the Radix Astragali 7, Semen Cucurbitae 5.5, Fructus Gleditsia 6.5, Fructus Citri Limoniae 4.5; Part II forms: natural sea salt 16, Fructrs Hippophae seed oil 1.2, deionized water 74, polydimethylsiloxane 5, hydroxyethyl-cellulose 3, glycerol 1.5, propylene glycol 3, surfactant 22.5, ethyl cinnamate 0.7, ethylene glycol monostearate 0.8, ethyl hydroxybenzoate 0.3.
4. the hair of moistening as described in as arbitrary in claim 1-3 wash the preparation method of protecting salt, it is characterized in that, step is:
A. the preparation of Part I
(1) Cortex Phellodendri and Cortex Lycii roguing are cleaned, soak into mature vinegar, take out, be placed in frying pan, intense fire adds to be propagandized hotly to surface coke black, takes out, dries in the air cool;
(2) get Semen Cuscutae and Semen Cucurbitae roguing, mix moistening 20-30 minute (preferably, moistening 22-28 minute thoroughly with saline; Be more preferably, moistening 25 minutes), to be placed in watt and to dry, take out, dry in the air cool;
(3) by Radix Achyranthis Bidentatae, the Radix Astragali, Fructus Gleditsia, Fructus Citri Limoniae remove impurity, dry together with step (1) (2) made raw material, pulverize, be placed in percolating device, with seepage pressure effects after 80% soak with ethanol, collect percolate, concentrated, recycling design, to without alcohol taste, obtains extract;
B. the preparation of Part II
(1) ethyl cinnamate, ethylene glycol monostearate and ethyl hydroxybenzoate are joined stirring and evenly mixing in propylene glycol, obtained adjuvant mixture, for subsequent use, by deionized water and hydroxyethyl-cellulose stirring and evenly mixing, and be heated to 50-70 DEG C (preferred, be heated to 55-65 DEG C; Be more preferably, be heated to 60 DEG C), then add glycerol and adjuvant mixture stirring and evenly mixing, obtained mixed liquor;
(2) in step (1) made mixed liquor, add surfactant to mix thoroughly, then add polydimethylsiloxane and mix rear stopping heating thoroughly, be cooled to room temperature, add natural sea salt and Fructrs Hippophae seed oil stirring and evenly mixing, obtained mixture;
C. made for Part I extract is joined stirring and evenly mixing in the made mixture of Part II, citric acid solution regulates pH to faintly acid, must wash and protect salt.
5. that can moisten as claimed in claim 4 hair washes the preparation method of protecting salt, and it is characterized in that, in the preparation of Part I, the amount of step (1) mature vinegar is 3-5 times (preferably, the amount of mature vinegar is 4 times of two kinds of raw materials quality) of two kinds of raw materials quality.
6. that can moisten as claimed in claim 4 hair washes the preparation method of protecting salt, it is characterized in that, in the preparation of Part I the mass concentration of step (2) saline be 20-35%(preferably, the mass concentration of saline is 25-30%; Be more preferably, the mass concentration of saline is 27%).
7. that can moisten as claimed in claim 4 hair washes the preparation method of protecting salt, and it is characterized in that, in the preparation of Part I, step (3) was pulverized 40-80 mesh sieve and (preferably, pulverized 50-70 mesh sieve; Be more preferably, pulverized 60 mesh sieves).
8. that can moisten as claimed in claim 4 hair washes the preparation method of protecting salt, it is characterized in that, in the preparation of Part I step (3) with 80% soak with ethanol 4-10 hour (preferably, with 80% soak with ethanol 6-8 hour; Be more preferably, by 80% soak with ethanol 7 hours).
9. that can moisten as claimed in claim 4 hair washes the preparation method of protecting salt, it is characterized in that, in the preparation of Part I, step (3) collects the percolate that obtains and raw material is by volume that 10-16:1(is preferred with weight ratio, and collecting the percolate that obtains and raw material is by volume 12-14:1 with weight ratio; Be more preferably, collecting the percolate that obtains and raw material is by volume 13:1 with weight ratio).
10. that can moisten as claimed in claim 4 hair washes the preparation method of protecting salt, it is characterized in that, in the preparation of Part II, step (1) described surfactant is at least one in Oleum Cocois single ethanol amide, oleic acid diethyl amide, cocos nucifera oil acyl both sexes acetic acid disodium, cocamidopropyl propyl amide hydroxyl sulphonic acid betaine and lauroylamidopropyl betaine.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102631304A (en) * | 2012-05-10 | 2012-08-15 | 浙江绿海制盐有限责任公司 | Shampoo salt emulsion and preparation method thereof |
| CN102885742A (en) * | 2012-11-06 | 2013-01-23 | 蒋亚飞 | Fleece flower root wet wipe for wiping hair and scalp and preparation method of fleece flower root wet wipe |
| CN105125472A (en) * | 2015-10-21 | 2015-12-09 | 皖南医学院 | Nourishing and hair-blacking cream shampoo with natural extracts and preparation method of nourishing and hair-blacking cream shampoo |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102631304A (en) * | 2012-05-10 | 2012-08-15 | 浙江绿海制盐有限责任公司 | Shampoo salt emulsion and preparation method thereof |
| CN102885742A (en) * | 2012-11-06 | 2013-01-23 | 蒋亚飞 | Fleece flower root wet wipe for wiping hair and scalp and preparation method of fleece flower root wet wipe |
| CN105125472A (en) * | 2015-10-21 | 2015-12-09 | 皖南医学院 | Nourishing and hair-blacking cream shampoo with natural extracts and preparation method of nourishing and hair-blacking cream shampoo |
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Address after: 755000 Ningxia central defender Shapotou district the Great Wall street, No. 99 Beiyuan District, building 1-202, 3 Applicant after: Hu Peng Address before: 250000 Ji'nan, central city, Shandong Lang Lang Road, No. 10 Applicant before: Hu Peng |
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Application publication date: 20160511 |