CN110840762A - Shampoo containing camellia seed extract and preparation method thereof - Google Patents
Shampoo containing camellia seed extract and preparation method thereof Download PDFInfo
- Publication number
- CN110840762A CN110840762A CN201911196431.9A CN201911196431A CN110840762A CN 110840762 A CN110840762 A CN 110840762A CN 201911196431 A CN201911196431 A CN 201911196431A CN 110840762 A CN110840762 A CN 110840762A
- Authority
- CN
- China
- Prior art keywords
- shampoo
- polyglycerol
- weight
- accounting
- seed extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention belongs to the technical field of tea oil shampoo, and particularly relates to shampoo containing a tea-oil camellia seed extract and a preparation method thereof. The invention comprises the following components besides the conventional receiving components of the shampoo: (A) oil tea seed extract accounting for 10-15% of the weight of the shampoo; (B) glycol laurate accounting for 2-3 percent of the weight of the shampoo; (C) cationic guar gum accounting for 0.15 percent of the weight of the shampoo; (D) polyglycerol-10 accounting for 1-12% of the weight of the shampoo and polyglycerol ester accounting for 0.05-1% of the weight of the shampoo, wherein the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows, the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows: polyglycerol-6 dioleate 2-4: 1; (E) sodium citrate accounting for 1.5-3% of the weight of the shampoo; (F) the deionized water accounts for 40-60% of the weight of the shampoo. The invention aims to provide a preparation method of shampoo containing camellia seed extract, which is suitable for mass production, simple to operate and high in economic benefit.
Description
Technical Field
The invention belongs to the technical field of tea oil shampoo, and particularly relates to shampoo containing a tea-oil camellia seed extract and a preparation method thereof.
Background
The existing shampoo is an indispensable necessity in daily life, and aims to eliminate sweat scale, dust, microorganisms, dandruff and other impurities attached to the scalp and keep the scalp and the hair clean and beautiful. With the continuous improvement of living standard, people have higher and higher requirements on the shampoo, and the shampoo is required to have multiple functions.
Hair oil, scalp itching and scurf which are caused by bacteria growing on the head are divided into seborrheic dermatitis, tinea capitis, psoriasis and atopic dermatitis according to individual differences and different types of infected bacteria: the shampoo is characterized in that the scalp is diffuse dry dandruff, people need to clean hair through the shampoo in order to prevent the situations, and the hair washing and protecting products in the market are various and contain a large amount of chemical preparations, so that the hair washing and protecting products can cause certain negative effects on the hair after long-term use, and the requirements of modern consumers on the shampoo cannot be met.
Disclosure of Invention
The invention aims to solve the problems, and provides shampoo containing camellia seed extract, which can effectively remove dandruff, relieve itching, prevent alopecia and hair loss, effectively repair split hair tails, has good hair cleaning capability and is environment-friendly.
The invention aims to provide a preparation method of shampoo containing camellia seed extract, which is suitable for mass production, simple to operate and high in economic benefit.
In order to realize the purpose, the invention adopts the technical scheme that:
a shampoo containing camellia seed extract comprises the following components in addition to the conventional receiving components of the shampoo: (A) oil tea seed extract accounting for 10-15% of the weight of the shampoo; (B) glycol laurate accounting for 2-3 percent of the weight of the shampoo; (C) cationic guar gum accounting for 0.05-0.15% of the weight of the shampoo; (D) polyglycerol-10 accounting for 1-12% of the weight of the shampoo and polyglycerol ester accounting for 0.05-1% of the weight of the shampoo, wherein the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows, the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows: polyglycerol-6 dioleate 2-4: 1; (E) sodium citrate accounting for 1.5-3% of the weight of the shampoo; (F) the balance being deionized water.
Further, the camellia seed extract is prepared by the following method: weighing camellia seeds, grinding, adding 50-65 wt% of ethanol aqueous solution, extracting for 1-6h at 50-65 ℃ for three times, filtering and combining filtrates to obtain ethanol extract, centrifuging to obtain upper-layer oily matter, and evaporating to remove ethanol.
Further, the shampoo also comprises the following components in parts by weight:
vitamin C1-3%; 0.2 to 0.5 percent of sodium chloride; 7.5-10% of carbomer; foaming agent 1.0-2.5%.
Further, the foaming agent is fatty acid monoethanolamide.
Further, the shampoo comprises the following components in percentage by weight: (A) oil tea seed extract accounting for 10-15% of the weight of the shampoo; (B) glycol laurate accounting for 2-3 percent of the weight of the shampoo; (C) cationic guar gum accounting for 0.05-0.15% of the weight of the shampoo; (D) polyglycerol-10 accounting for 1-12% of the weight of the shampoo and polyglycerol ester accounting for 0.05-1% of the weight of the shampoo, wherein the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows, the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows: polyglycerol-6 dioleate 2-4: 1; (E) sodium citrate accounting for 1.5-3% of the weight of the shampoo; the components of the shampoo also comprise 8 to 12 percent of nonionic surfactant and a proper amount of citric acid, a chelating agent, spice and sodium chloride; the balance being deionized water.
A preparation method of shampoo containing camellia seed extract comprises the following steps:
s1, primary mixing of raw materials: adding deionized water into a reaction kettle, keeping the temperature of the deionized water at 35-45 ℃, sequentially adding corresponding parts by mass of camellia seed extract, ethylene glycol laurate, cationic guar gum, polyglycerol-10, polyglycerol-6 dioleate and sodium citrate into the reaction kettle, and stirring for 10-25min for emulsification to obtain an emulsion;
s2, pH value adjustment: adding a pH value regulator into the emulsion in the S1, and stirring for 5-20min to ensure that the pH value of the emulsion is 6.5-7.0;
s3, stirring in vacuum: and (4) carrying out vacuum stirring on the emulsion of the S2 for 20-25min at the stirring speed of 60-120 r/min.
Furthermore, 1-3% of vitamin C, 0.2-0.5% of sodium chloride, 7.5-10% of carbomer and 1.0-2.5% of foaming agent are added into S3, and then vacuum stirring is carried out.
Application of shampoo containing Camellia seed extract in preparing skin caring product for preventing alopecia, hair loss, and split hair tail is provided.
The invention has the beneficial effects that:
1) the polyglycerol-10 and the polyglycerol-6 dioleate form a macromolecular network structure, have the moisturizing and conditioning effects on scalp and hair, and can play a role in removing dandruff and relieving itching in multiples together with the camellia seed extract, and reduce the irritation of glycol laurate; the hair conditioner has certain antibacterial and bacteriostatic effects, is beneficial to removing dandruff and relieving itching, can effectively nourish hair, and has the effect of repairing split hair tails.
2) The natural plant source is used as the main functional component, the active component of the camellia seed extract can fundamentally slow down the excessive alopecia problem, promote the scalp stratum corneum metabolism, strengthen the nutrient absorption of hair roots, consolidate the growth of the hair roots, reduce hair loss and broken hair, has obvious anti-alopecia effect, is safe and non-toxic, and enhances the anti-alopecia effect by the synergistic action of the mixture polyglycerol-10 and polyglycerol-6 dioleate under the acidic condition.
3) The camellia seed extract, the sodium citrate and the glycol laurate are used in combination, show good synergistic cleaning effect, have good mildness and are suitable for cleaning hair.
4) The invention has no harmful chemical substance, no side effect to human body, low cost, simple preparation and wide application.
Detailed Description
The present invention is described in detail below with reference to examples for better understanding of technical solutions of the present invention by those skilled in the art, and the description of the present invention is only exemplary and explanatory and should not be construed as limiting the scope of the present invention in any way.
A shampoo containing camellia seed extract comprises the following components in addition to the conventional receiving components of the shampoo: (A) oil tea seed extract accounting for 10-15% of the weight of the shampoo; (B) glycol laurate accounting for 2-3 percent of the weight of the shampoo; (C) cationic guar gum accounting for 0.05-0.15% of the weight of the shampoo; (D) polyglycerol-10 accounting for 1-12% of the weight of the shampoo and polyglycerol ester accounting for 0.05-1% of the weight of the shampoo, wherein the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows, the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows: polyglycerol-6 dioleate 2-4: 1; (E) sodium citrate accounting for 1.5-3% of the weight of the shampoo; (F) the balance being deionized water.
Preferably, the camellia seed extract is prepared by the following method: weighing camellia seeds, grinding, adding 50-65 wt% of ethanol aqueous solution, extracting for 1-6h at 50-65 ℃ for three times, filtering and combining filtrates to obtain ethanol extract, centrifuging to obtain upper-layer oily matter, and evaporating to remove ethanol.
Preferably, the shampoo further comprises the following components in parts by weight:
1-3% of vitamin C; 0.2 to 0.5 percent of sodium chloride; 7.5-10% of carbomer; foaming agent 1.0-2.5%.
Preferably, the foaming agent is fatty acid monoethanolamide.
Preferably, the shampoo comprises the following components in percentage by weight: (A) oil tea seed extract accounting for 10-15% of the weight of the shampoo; (B) glycol laurate accounting for 2-3 percent of the weight of the shampoo; (C) cationic guar gum accounting for 0.05-0.15% of the weight of the shampoo; (D) polyglycerol-10 accounting for 1-12% of the weight of the shampoo and polyglycerol ester accounting for 0.05-1% of the weight of the shampoo, wherein the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows, the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows: polyglycerol-6 dioleate 2-4: 1; (E) sodium citrate accounting for 1.5-3% of the weight of the shampoo; the components of the shampoo also comprise 8 to 12 percent of nonionic surfactant and a proper amount of citric acid, a chelating agent, spice and sodium chloride; the balance being deionized water.
A preparation method of shampoo containing camellia seed extract comprises the following steps:
s1, primary mixing of raw materials: adding deionized water into a reaction kettle, keeping the temperature of the deionized water at 35-45 ℃, sequentially adding corresponding parts by mass of camellia seed extract, ethylene glycol laurate, cationic guar gum, polyglycerol-10, polyglycerol-6 dioleate and sodium citrate into the reaction kettle, and stirring for 10-25min for emulsification to obtain an emulsion;
s2, pH value adjustment: adding a pH value regulator into the emulsion in the S1, and stirring for 5-20min to ensure that the pH value of the emulsion is 6.5-7.0;
s3, stirring in vacuum: and (4) carrying out vacuum stirring on the emulsion of the S2 for 20-25min at the stirring speed of 60-120 r/min.
Preferably, 1-3% of vitamin C, 0.2-0.5% of sodium chloride, 7.5-10% of carbomer and 1.0-2.5% of foaming agent are added into S3, and then vacuum stirring is carried out.
Application of shampoo containing Camellia seed extract in preparing skin caring product for preventing alopecia, hair loss, and split hair tail is provided.
Example 1
A shampoo containing Camellia seed extract comprises: (A) oil tea seed extract accounting for 10% of the weight of the shampoo; (B) glycol laurate accounting for 2 percent of the weight of the shampoo; (C) cationic guar gum accounting for 0.15 percent of the weight of the shampoo; (D) polyglycerol-10 accounting for 1% of the weight of the shampoo and polyglycerol ester accounting for 0.05% of the weight of the shampoo, wherein the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows, the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows: polyglycerol-6 dioleate 2: 1; (E) sodium citrate accounting for 1.5 percent of the weight of the shampoo; (F) vitamin C1%; 0.2 percent of sodium chloride; 7.5% of carbomer; 1.0% of foaming agent; the components of the shampoo also comprise 8% of nonionic surfactant; appropriate amounts of citric acid, chelating agent, perfume and sodium chloride (26% of the total weight of the shampoo); the balance being deionized water.
The foaming agent is fatty acid monoethanolamide. The nonionic surfactant is lauryl alcohol sulfate or polyoxyethylene lauryl alcohol sulfate.
The camellia seed extract is prepared by the following method: weighing camellia seeds, grinding, adding 50 wt% ethanol aqueous solution, extracting for three times at 50 ℃ for 1h, extracting for three times, filtering, mixing filtrates to obtain ethanol extract, centrifuging to obtain upper layer oily substance, and evaporating to remove ethanol.
Example 2
A shampoo containing Camellia seed extract comprises: (A) camellia seed extract accounting for 12.5 percent of the weight of the shampoo; (B) glycol laurate accounting for 2.5 percent of the weight of the shampoo; (C) cationic guar gum accounting for 0.05 percent of the weight of the shampoo; (D) polyglycerol-10 accounting for 6% of the weight of the shampoo and polyglycerol ester accounting for 0.08% of the weight of the shampoo, wherein the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows, the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows: polyglyceryl-6 dioleate ═ 3: 1; (E) sodium citrate accounting for 2 percent of the weight of the shampoo; (F) 2% of vitamin C; 0.3 percent of sodium chloride; 8% of carbomer; 2% of foaming agent; the components of the shampoo also comprise 10% of nonionic surfactant; appropriate amounts of citric acid, chelating agent, perfume and sodium chloride (22% of the total weight of the shampoo); the balance being deionized water. The foaming agent is fatty acid monoethanolamide.
The nonionic surfactant is lauryl alcohol sulfate or polyoxyethylene lauryl alcohol sulfate.
The camellia seed extract is prepared by the following method: weighing camellia seeds, grinding, adding 60 wt% ethanol aqueous solution, extracting for three times at 60 ℃ for 3h at a mass ratio of the ground camellia seeds to the ethanol aqueous solution of 1:4, filtering, mixing filtrates to obtain ethanol extract, centrifuging to obtain upper-layer oily matter, and evaporating to remove ethanol.
Example 3
A shampoo containing Camellia seed extract comprises: (A) camellia seed extract accounting for 15% of the weight of the shampoo; (B) glycol laurate accounting for 3 percent of the weight of the shampoo; (C) cationic guar gum accounting for 0.15 percent of the weight of the shampoo; (D) polyglycerol-10 accounting for 12% of the weight of the shampoo and polyglycerol ester accounting for 1% of the weight of the shampoo, wherein the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows, the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows: polyglycerol-6 dioleate 4: 1; (E) sodium citrate accounting for 3 percent of the weight of the shampoo; (F) 3% of vitamin C; 0.5 percent of sodium chloride; 10% of carbomer; 2.5 percent of foaming agent; the components of the shampoo also comprise 12% of nonionic surfactant; appropriate amounts of citric acid, chelating agent, perfume and sodium chloride (18% of the total weight of the shampoo); the balance being deionized water.
The foaming agent is fatty acid monoethanolamide. The nonionic surfactant is lauryl alcohol sulfate or polyoxyethylene lauryl alcohol sulfate.
The camellia seed extract is prepared by the following method: weighing camellia seeds, grinding, adding 65 wt% ethanol aqueous solution, extracting for three times at 65 ℃ for 6h, extracting for three times, filtering, mixing filtrates to obtain ethanol extract, centrifuging to obtain upper-layer oily matter, and evaporating to remove ethanol.
Comparative example 1
The comparative example does not add polyglycerol-10 accounting for 1 percent of the weight of the shampoo and polyglycerol ester accounting for 0.05 percent of the weight of the shampoo on the basis of the example 1. The rest is the same as example 1.
Comparative example 2
The comparative example does not add polyglycerol-10 accounting for 6 percent of the weight of the shampoo and polyglycerol ester accounting for 0.08 percent of the weight of the shampoo on the basis of the example 2. The rest is the same as example 2.
Comparative example 3
The comparative example does not add camellia seed extract accounting for 15 percent of the weight of the shampoo on the basis of example 3. The rest is the same as example 3.
Comparative example 4
In the comparative example, sodium citrate accounting for 1.5 percent of the weight of the shampoo is not added on the basis of the example 1. The rest is the same as example 1.
Comparative example 5
In the comparative example, sodium citrate accounting for 2 percent of the weight of the shampoo is not added on the basis of the example 2. The rest is the same as example 2.
Test for preventing Hair loss
The hair loss prevention shampoos of examples 1 to 3 and comparative examples 1 to 4 were tested for hair loss prevention effects. 300 volunteers with average hair loss number more than 100/day are selected as subjects, the subjects are randomly divided into 10 groups, 30 persons in each group respectively try out shampoos of examples 1-3 and comparative examples 1-3, and comparative example 4 is a shampoo sold in a certain brand for preventing hair loss. The test method comprises the following steps: the hair was washed every two days, combed 2 times in the morning and evening, the shed hair was collected and counted for a test period of 4 weeks (28 days), and the average value was finally taken. The statistical results are shown in table 1.
The results in table 1 show that the shampoos of examples 1 to 3 all have good anti-hair-loss effects, and the average hair loss number per day after 4 weeks of use is reduced to below 70, which indicates that the shampoo of the present invention can effectively alleviate excessive hair loss, consolidate hair root growth, and have significant anti-hair-loss effects. In addition, it can be seen that the hair loss preventing effect of the shampoos in the examples is different, which indicates that different proportions of the components in the formula of the invention also have a certain influence on the efficacy of the shampoo, wherein the effects of the shampoos in the examples 1 and 2 are better. From the results of comparative examples 1 to 4, it can be seen that when one or more of polyglycerol-10 and polyglycerol-6 dioleate is absent in the formula, the anti-hair loss effect of the shampoo is reduced, so that the compounding of the polyglycerol-10 and polyglycerol-6 dioleate and the extract of the camellia seed can generate a synergistic effect, and the anti-hair loss effect is better.
TABLE 10-28 days alopecia Effect table
Hair washing Effect test
1. Grouping
60 persons with dandruff were randomly selected and divided into 6 groups, and the dandruff removing shampoo of the present invention of examples 1 to 3, comparative examples 1 to 3 and a brand commercially available therefrom was used in a regular amount of 3 times per week for 2 months.
2. Standard of effect
The hair washing effect adopts a grading system, and the grading standard is as follows:
and 5, dividing: the hair is soft and smooth, is easy to comb, has no visible scurf with naked eyes, and completely disappears the phenomenon of pruritus;
and 4, dividing: the hair dye has no obvious tangling phenomenon, is easy to comb, can be used for seeing sporadic scurf by naked eyes, and has no pruritus phenomenon;
and 3, dividing: the phenomenon of tangling exists at the beginning of carding, the carding is easy after the carding, and scurf can be seen by naked eyes and slight itching can occur;
and 2, dividing: during carding, the phenomenon of strong entanglement and strong carding resistance exist, and scurf and pruritus can be obviously seen by naked eyes;
1 minute: difficult combing, no improvement in dandruff and itching.
The average score results for each group are shown in table 2.
TABLE 2 anti-dandruff and antipruritic effects of shampoo containing Camellia seed extract
Cleaning test
Preparing the shampoo of the above examples 1-3 into 5% aqueous solution, 5% shampoo (example 1) + 95% deionized water by volume ratio; 5% shampoo (example 2) + 95% deionized water; 5% shampoo (example 3) + 95% deionized water and stirred well for use.
Preparing synthetic grease:
synthetic oils are designed to mimic the composition of oil in hair:
1, placing 30% of olive oil, 10% of palmitic acid, 10% of stearic acid, 10% of oleic acid, 10% of paraffin, 15% of squalene and 15% of beeswax together according to the weight ratio, and heating until the olive oil, the palmitic acid, the stearic acid, the oleic acid, the paraffin, the squalene and the beeswax are dissolved and dispersed uniformly for later use.
And 2, adding 5 wt% of the prepared synthetic grease into 95 wt% of ethanol to prepare a 5% synthetic grease solution.
Three groups of 15 tresses were taken, the size of the tress being 10 cm long, 3 cm wide, and each tress sample weighed and recorded. And putting the sample hair bundle into 5% synthetic oil solution, soaking for 1-3 minutes, taking out, air-drying, and weighing to determine the weight (mg) of the residual synthetic oil in the hair bundle sample. Then, preparing an aqueous solution of 5% by volume and respectively containing (a) the shampoo containing the camellia seed extract of the present invention; (b) 500 ml of each of a control shampoo (containing no camellia seed extract) and (c) a commercial shampoo (a certain brand of oil-removing shampoo) was used. Three groups of tresses treated with 5% synthetic oil solution were immersed in the above three 500 ml shampoos for 2 minutes, rinsed with water for 1 minute, then placed in a drying oven for drying for 12 hours, taken out and weighed again, and the amount of residual substances (synthetic oil) on the hair was calculated, and finally the average amount of removal of the tresses was calculated as shown in table 3.
TABLE 3
| Shampoo liquid | Synthetic oil (mg) | Removal amount (mg) | Cleaning power% |
| Example 1 | 258 | 183 | 70.9％ |
| Comparative example 4 | 258 | 144 | 55.8％ |
| Example 2 | 264 | 195 | 73.9％ |
| Comparative example 5 | 264 | 150 | 56.8％ |
| Example 3 | 252 | 192 | 76.2％ |
| Comparative example 3 | 252 | 42 | 16.7％ |
| Shampoo sold in market | 270 | 165 | 61.1％ |
It should be noted that, in this document, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
The principles and embodiments of the present invention are explained herein using specific examples, which are presented only to assist in understanding the method and its core concepts of the present invention. The foregoing is only a preferred embodiment of the present invention, and it should be noted that there are objectively infinite specific structures due to the limited character expressions, and it will be apparent to those skilled in the art that a plurality of modifications, decorations or changes may be made without departing from the principle of the present invention, and the technical features described above may be combined in a suitable manner; such modifications, variations, combinations, or adaptations of the invention using its spirit and scope, as defined by the claims, may be directed to other uses and embodiments.
Claims (8)
1. A shampoo containing camellia seed extract is characterized by comprising the following components in addition to the conventional receiving components of the shampoo: (A) oil tea seed extract accounting for 10-15% of the weight of the shampoo; (B) glycol laurate accounting for 2-3 percent of the weight of the shampoo; (C) cationic guar gum accounting for 0.05-0.15% of the weight of the shampoo; (D) polyglycerol-10 accounting for 1-12% of the weight of the shampoo and polyglycerol ester accounting for 0.05-1% of the weight of the shampoo, wherein the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows, the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows: polyglycerol-6 dioleate 2-4: 1; (E) sodium citrate accounting for 1.5-3% of the weight of the shampoo; (F) the balance being deionized water.
2. The shampoo containing the camellia seed extract as claimed in claim 1, wherein the camellia seed extract is prepared by the following method: weighing camellia seeds, grinding, adding 50-65 wt% of ethanol aqueous solution, extracting for 1-6h at 50-65 ℃ for three times, filtering and combining filtrates to obtain ethanol extract, centrifuging to obtain upper-layer oily matter, and evaporating to remove ethanol.
3. The shampoo containing the camellia seed extract as claimed in claim 1, wherein the shampoo further comprises the following components in parts by weight:
vitamin C1-3%; 0.2 to 0.5 percent of sodium chloride; 7.5-10% of carbomer; foaming agent 1.0-2.5%.
4. The shampoo containing camellia seed extract as claimed in claim 3, wherein the foaming agent is fatty acid monoethanolamide.
5. The shampoo containing the camellia seed extract as claimed in claim 1, wherein the shampoo comprises the following components in percentage by weight: (A) oil tea seed extract accounting for 10-15% of the weight of the shampoo; (B) glycol laurate accounting for 2-3 percent of the weight of the shampoo; (C) cationic guar gum accounting for 0.05-0.15% of the weight of the shampoo; (D) polyglycerol-10 accounting for 1-12% of the weight of the shampoo and polyglycerol ester accounting for 0.05-1% of the weight of the shampoo, wherein the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows, the weight ratio of the polyglycerol-10 to the polyglycerol-6 dioleate is as follows: polyglycerol-6 dioleate 2-4: 1; (E) sodium citrate accounting for 1.5-3% of the weight of the shampoo; the components of the shampoo also comprise 8 to 12 percent of nonionic surfactant and a proper amount of citric acid, a chelating agent, spice and sodium chloride; the balance being deionized water.
6. The method for preparing shampoo containing camellia seed extract as claimed in any one of claims 1 to 5, comprising the steps of:
s1, primary mixing of raw materials: adding deionized water into a reaction kettle, keeping the temperature of the deionized water at 35-45 ℃, sequentially adding corresponding parts by mass of camellia seed extract, ethylene glycol laurate, cationic guar gum, polyglycerol-10, polyglycerol-6 dioleate and sodium citrate into the reaction kettle, and stirring for 10-25min for emulsification to obtain an emulsion;
s2, pH value adjustment: adding a pH value regulator into the emulsion in the S1, and stirring for 5-20min to ensure that the pH value of the emulsion is 6.5-7.0;
s3, stirring in vacuum: and (4) carrying out vacuum stirring on the emulsion of the S2 for 20-25min at the stirring speed of 60-120 r/min.
7. The method for preparing a shampoo containing camellia seed extract as claimed in claim 6, wherein vitamin C1-3%, sodium chloride 0.2-0.5%, carbomer 7.5-10%, foaming agent 1.0-2.5% are added to S3, and then vacuum stirring is performed.
8. Use of the shampoo containing camellia seed extract according to any one of claims 1 to 5 for preparing a beauty skin care product for preventing hair loss, hair loss and split hair.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911196431.9A CN110840762A (en) | 2019-11-29 | 2019-11-29 | Shampoo containing camellia seed extract and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911196431.9A CN110840762A (en) | 2019-11-29 | 2019-11-29 | Shampoo containing camellia seed extract and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110840762A true CN110840762A (en) | 2020-02-28 |
Family
ID=69606052
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911196431.9A Withdrawn CN110840762A (en) | 2019-11-29 | 2019-11-29 | Shampoo containing camellia seed extract and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110840762A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112812906A (en) * | 2021-01-22 | 2021-05-18 | 王建功 | Shampoo soap containing selenium sulfide plant extract and preparation method and application thereof |
| CN114344201A (en) * | 2022-01-18 | 2022-04-15 | 日照职业技术学院 | Shampoo containing microalgae extract and preparation method thereof |
| CN115054557A (en) * | 2022-08-05 | 2022-09-16 | 广州德谷个人护理用品有限公司 | Anti-hair loss composition and application thereof |
-
2019
- 2019-11-29 CN CN201911196431.9A patent/CN110840762A/en not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112812906A (en) * | 2021-01-22 | 2021-05-18 | 王建功 | Shampoo soap containing selenium sulfide plant extract and preparation method and application thereof |
| CN114344201A (en) * | 2022-01-18 | 2022-04-15 | 日照职业技术学院 | Shampoo containing microalgae extract and preparation method thereof |
| CN115054557A (en) * | 2022-08-05 | 2022-09-16 | 广州德谷个人护理用品有限公司 | Anti-hair loss composition and application thereof |
| CN115054557B (en) * | 2022-08-05 | 2024-03-19 | 广州德谷个人护理用品有限公司 | Alopecia preventing composition and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN112656732B (en) | Dandruff-removing and itching-relieving shampoo and preparation method thereof | |
| CN107349122A (en) | A kind of desquamation compositions and its application | |
| CN110840762A (en) | Shampoo containing camellia seed extract and preparation method thereof | |
| CN108078796B (en) | Silicone-oil-free moistening and smoothing hair mask and preparation method thereof | |
| CN107496317B (en) | Repairing and nursing shampoo containing periplaneta americana active ingredient | |
| EP0440363B1 (en) | Hair grower | |
| CN107375059B (en) | Folium artemisiae argyi anti-hair loss shampoo and preparation method thereof | |
| CN107550795A (en) | Nourish reparation, black hair anticreep camellia oleifera fruit shampoo and preparation method thereof | |
| CN111544332A (en) | Anti-dandruff shampoo and preparation method thereof | |
| CN115120547B (en) | Non-irritating hair repair composition and anti-hair-loss shampoo | |
| CN112156039A (en) | Depilatory preparation and preparation method thereof | |
| CN114533647B (en) | Silicone oil-free anti-dandruff shampoo composition and preparation method thereof | |
| CN112107533A (en) | Composition with effects of controlling oil, tendering skin and collecting fine pores and preparation method and application thereof | |
| CN110960463A (en) | Shampoo composition containing hemp leaf extract composite preparation | |
| KR100579710B1 (en) | Shampoo composition for treating dandruff and alopecia containing compounds obtained from ginkgo biloba l. leaves | |
| CN104188859B (en) | A kind of crease-resistant skin care emulsion containing natural component extract and preparation method thereof | |
| CN112807251A (en) | Silicone-oil-free shampoo with scalp care effect and preparation process thereof | |
| CN113876672A (en) | Amino acid mild tear-free natural plant shampoo and preparation method thereof | |
| CN110882172A (en) | Paeonol-containing multi-effect hair care shampoo and preparation method thereof | |
| CN115282098B (en) | Composition with antibacterial and anti-dandruff effects and preparation method and application thereof | |
| CN113768846B (en) | Nourishing anti-dandruff shampoo and preparation method thereof | |
| CN111096917B (en) | Long-acting anti-dandruff itching-relieving composition and application thereof | |
| CN110946787A (en) | Non-irritating aloe hair conditioner | |
| CN116585245B (en) | Shampoo containing ginger root extract and preparation method thereof | |
| US11135152B2 (en) | Natural shampoo composition comprising white dandelion extract solution for hair loss prevention and hair growth |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20200228 |
|
| WW01 | Invention patent application withdrawn after publication |