CN114344201A - Shampoo containing microalgae extract and preparation method thereof - Google Patents

Shampoo containing microalgae extract and preparation method thereof Download PDF

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CN114344201A
CN114344201A CN202210056340.0A CN202210056340A CN114344201A CN 114344201 A CN114344201 A CN 114344201A CN 202210056340 A CN202210056340 A CN 202210056340A CN 114344201 A CN114344201 A CN 114344201A
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extract
parts
nannochloropsis oculata
shampoo
preparation
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赵璐
李达
常彦磊
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Rizhao Polytechnic
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Rizhao Polytechnic
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Abstract

The invention belongs to the technical field of washing and caring products, and particularly relates to a shampoo containing a microalgae extract and a preparation method thereof. The preparation method specifically comprises the following steps: preparing a camellia seed extract and a nannochloropsis oculata extract; respectively adding the camellia seed extract, polyethylene glycol laurate and alkyl glycoside into deionized water, heating and stirring the mixed solution; adding nannochloropsis oculata extract, linseed oil and xanthan gum into the mixed solution and stirring to obtain an intermediate mixed solution; finally, adding polyglycerol-10, polyglycerol ester, stearyl alcohol and citric acid, stirring and keeping the temperature for a certain time; sampling and detecting, discharging shampoo qualified in detection, filling by using a filling machine, and then packaging and packaging. The invention adopts butanediol water to extract nannochloropsis oculata, and applies the nannochloropsis oculata and other components to shampoo together, so that the nannochloropsis oculata can act on scalp cells deeply, increase cell activity, provide nutrient substances, reduce scalp and hair damage, and improve the problems of hair loss, withered and yellow hair and the like.

Description

Shampoo containing microalgae extract and preparation method thereof
Technical Field
The invention belongs to the technical field of washing and caring products, and particularly relates to a shampoo containing a microalgae extract and a preparation method thereof.
Background
The shampoo is a hair care product with the functions of removing dandruff, treating hair oil, dyeing hair and the like, can effectively clean dirt, grease and the like attached to scalp and hair, and can meet the cleaning function of the shampoo and have higher requirements on the use safety and the hair nourishing and protecting functions of the shampoo along with the improvement of living standard, wherein the green and healthy shampoo becomes a development trend.
Nannochloropsis is a natural organism, which is rich in vitamins, proteins, minerals and trace elements, and also contains polyphenol compounds, polyhalogenated terpenoid compounds, sterol compounds, unsaturated fatty acids, polysaccharides and the like, and has been widely used in the fields of medicines, cosmetics, cosmeceuticals and the like. The protein in nannochloropsis is decomposed into amino acid after enzymolysis, and the amino acid can provide nutrients for hair growth and promote hair growth when added into shampoo, but the blocking effect of microalgae cell walls and the macromolecular structures of protein and polysaccharide in the microalgae are not beneficial to absorption of human epidermis. Therefore, finding a method for allowing microalgae to better exert hair care effect becomes a problem to be urgently broken through at the present stage.
Disclosure of Invention
In order to solve the problem that the hair care value of microalgae cannot be fully exerted, the invention provides a shampoo containing a microalgae extract and a preparation method thereof, so as to solve the problem.
On one hand, the invention provides a preparation method of shampoo containing microalgae extract, which comprises the following steps:
(1) preparing a camellia seed extract and a nannochloropsis oculata extract;
the preparation method of the nannochloropsis oculata extract comprises the following steps: grinding nannochloropsis oculata, adding a butanediol aqueous solution, mixing and soaking to obtain a treatment solution, performing microwave extraction on the treatment solution, filtering the microwave extraction solution, and drying in vacuum to obtain a nannochloropsis oculata extract;
(2) respectively adding the camellia seed extract, polyethylene glycol laurate and alkyl glycoside into deionized water, heating the mixed solution, and uniformly stirring;
(3) adding nannochloropsis oculata extract, linseed oil and xanthan gum into the mixed solution and stirring to obtain an intermediate mixed solution;
(4) finally, adding polyglycerol-10, polyglycerol ester, stearyl alcohol and citric acid, stirring and keeping the temperature for a certain time;
(5) sampling and detecting, discharging shampoo qualified in detection, filling by using a filling machine, and then packaging and packaging.
Further, in the step (1), the preparation of the camellia seed extract comprises the following steps: weighing camellia seeds, grinding the camellia seeds, adding 50-65 wt% of ethanol aqueous solution into the ground camellia seeds, extracting the ground camellia seeds and the ethanol aqueous solution for 1-6h at 50-65 ℃ for three times, filtering and combining the filtrates to obtain ethanol extract, centrifuging the ethanol extract to obtain upper-layer oily matter, and evaporating to remove ethanol.
Further, in the step (1), the feed-liquid ratio of nannochloropsis oculata to butanediol aqueous solution is 1:10-35, and the mass ratio of water to butanediol in the butanediol aqueous solution is 1: 1-3; the microwave extraction time is 5-25min, the extraction temperature is 35-60 ℃, and the microwave power is 250-550W.
Further, in the step (2), the heating temperature of the mixed solution is 35-50 ℃.
Further, in the step (4), the heat preservation temperature is 45-60 ℃, and the heat preservation time is 1.5-2.5 h.
Further, the shampoo comprises the following raw materials in parts by weight: 18-25 parts of camellia seed extract, 6-10 parts of polyethylene glycol laurate, 3-6 parts of alkyl glycoside, 3-7 parts of nannochloropsis oculata extract, 1-2 parts of linseed oil, 2-4 parts of xanthan gum, 1-2 parts of polyglycerol-10, 0.5-1 part of polyglycerol ester, 0.5-1 part of stearyl alcohol and 0.1-0.5 part of citric acid.
The camellia seed extract, the polyethylene glycol laurate and the alkyl glycoside are used as surfactants, the linseed oil is used as a thickening agent and a humectant, and the xanthan gum is used as a natural thickening agent; the nannochloropsis oculata extract can provide nutrients such as protein, etc., and protect hair and scalp; the polyglycerol-10 and the polyglycerol ester can form a macromolecular network structure, have good synergistic effects of foam characteristics and cleaning performance, are good in mildness, reduce the irritation of the polyethylene glycol laurate and are suitable for cleaning scalp and hair.
Further, the shampoo comprises the following components in parts by weight: 20 parts of camellia seed extract, 8 parts of polyethylene glycol laurate, 5 parts of nannochloropsis oculata extract, 4 parts of alkyl glycoside, 1.5 parts of linseed oil, 3 parts of xanthan gum, 1 part of polyglycerol-10, 0.7 part of polyglycerol ester, 0.6 part of stearyl alcohol and 0.2 part of citric acid.
In another aspect, the invention also provides a shampoo containing the microalgae extract prepared by the preparation method.
The invention has the beneficial effects that:
the shampoo containing the microalgae extract provided by the invention adopts butanediol to extract nannochloropsis oculata, avoids potential risk of skin injury caused by organic solvent extraction, ensures the safety and effectiveness of the extract, is applied to the shampoo together with other components, can realize synergistic effect and multiple protection, acts on scalp cells deeply, increases cell activity, provides nutrient substances, reduces scalp and hair quality injury, and improves the problems of hair loss, withered and yellow hair and the like.
The preparation method of the shampoo containing the microalgae extract provided by the invention has the advantages of simple process and low cost, selects proper steps and parameters, enables the raw materials to be combined with each other to exert the best effect, and has good application value.
Detailed Description
In order to make those skilled in the art better understand the technical solutions in the present invention, the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
A shampoo containing microalgae extract comprises the following raw materials in parts by weight: 22 parts of camellia seed extract, 9 parts of polyethylene glycol laurate, 5 parts of alkyl glycoside, 6 parts of nannochloropsis oculata extract, 1.5 parts of linseed oil, 3 parts of xanthan gum, 1.5 parts of polyglycerol-10, 0.8 part of polyglycerol ester, 0.8 part of stearyl alcohol and 0.4 part of citric acid.
A preparation method of shampoo containing microalgae extract specifically comprises the following steps:
(1) preparing oil tea seed extract and nannochloropsis oculata extract.
The preparation method of the camellia seed extract comprises the following steps: weighing camellia seeds, grinding the camellia seeds, adding 55 wt% of ethanol water solution, extracting the ground camellia seeds and the ethanol water solution for three times at the extraction temperature of 60 ℃ for 4h at the mass ratio of 1:5, filtering and combining the filtrates to obtain ethanol extract, centrifuging to obtain upper-layer oily matter, and evaporating to remove ethanol.
The preparation method of the nannochloropsis oculata extract comprises the following steps: grinding nannochloropsis oculata, adding a butanediol aqueous solution, mixing and soaking to obtain a treatment solution, wherein the material-to-liquid ratio of nannochloropsis oculata to the butanediol aqueous solution is 1:20, and the mass ratio of water to butanediol in the butanediol aqueous solution is 1: 2; then carrying out microwave extraction on the treatment solution for 20min at 45 ℃ and 350W of microwave power, filtering the microwave extraction solution, and drying in vacuum to obtain the nannochloropsis oculata extract.
(2) Respectively adding the camellia seed extract, the polyethylene glycol laurate and the alkyl glycoside into deionized water, heating the mixed solution to 45 ℃, and uniformly stirring.
(3) Adding Nannochloropsis oculata extract, oleum Lini, and xanthan gum into the mixed solution, and stirring to obtain intermediate mixed solution.
(4) And finally adding polyglycerol-10, polyglycerol ester, stearyl alcohol and citric acid, stirring, and keeping the temperature at 55 ℃ for 2 h.
(5) Sampling and detecting, discharging shampoo qualified in detection, filling by using a filling machine, and then packaging and packaging.
Comparative example 1
The shampoo of this comparative example was the same as example 1 except that no nannochloropsis oculata extract was added.
Example 2
A shampoo containing microalgae extract comprises the following components in parts by weight: 20 parts of camellia seed extract, 8 parts of polyethylene glycol laurate, 5 parts of nannochloropsis oculata extract, 4 parts of alkyl glycoside, 1.5 parts of linseed oil, 3 parts of xanthan gum, 1 part of polyglycerol-10, 0.7 part of polyglycerol ester, 0.6 part of stearyl alcohol and 0.2 part of citric acid.
A preparation method of shampoo containing microalgae extract specifically comprises the following steps:
(1) preparing oil tea seed extract and nannochloropsis oculata extract.
The preparation method of the camellia seed extract comprises the following steps: weighing camellia seeds, grinding, adding 50 wt% ethanol aqueous solution, extracting for three times at 50 ℃ for 3h at the mass ratio of the ground camellia seeds to the ethanol aqueous solution of 1:3, filtering, mixing filtrates to obtain ethanol extract, centrifuging to obtain upper-layer oily matter, and evaporating to remove ethanol.
The preparation method of the nannochloropsis oculata extract comprises the following steps: grinding nannochloropsis oculata, adding a butanediol aqueous solution, mixing and soaking to obtain a treatment solution, wherein the material-to-liquid ratio of nannochloropsis oculata to butanediol aqueous solution is 1:25, and the mass ratio of water to butanediol in the butanediol aqueous solution is 1: 2; then carrying out microwave extraction on the treatment solution for 20min at 40 ℃ and with the microwave power of 350W, filtering the microwave extraction solution, and drying in vacuum to obtain the nannochloropsis oculata extract.
(2) Respectively adding the camellia seed extract, the polyethylene glycol laurate and the alkyl glycoside into deionized water, heating the mixed solution to 40 ℃, and uniformly stirring.
(3) Adding Nannochloropsis oculata extract, oleum Lini, and xanthan gum into the mixed solution, and stirring to obtain intermediate mixed solution.
(4) And finally adding polyglycerol-10, polyglycerol ester, stearyl alcohol and citric acid, stirring, and keeping the temperature at 50 ℃ for 1.5 h.
(5) Sampling and detecting, discharging shampoo qualified in detection, filling by using a filling machine, and then packaging and packaging.
Comparative example 2
The shampoo of this comparative example was the same as example 2 except that no nannochloropsis oculata extract was added.
To better illustrate the effectiveness of the shampoos provided in the examples of the present invention, the shampoos of examples 1-2 and comparative examples 1-2 were tested, test methods: 50 patients with withered and yellow hair and easy hair loss are respectively selected to use the shampoos of the embodiments and the comparative examples of the invention, and the using effect is observed after one week, and the result is shown in table 1.
TABLE 1-50 patients Effect of using shampoos of examples and comparative examples
Figure BDA0003476390020000051
As can be seen from table 1, the shampoos of examples 1-2 have better hair-protecting effects than those of comparative examples 1-2, and the addition of the nannochloropsis oculata extract can effectively improve hair loss and withered and yellow hair, improve hair quality, and promote hair growth.
Although the present invention has been described in detail by way of preferred embodiments, the present invention is not limited thereto. Various equivalent modifications or substitutions can be made on the embodiments of the present invention by those skilled in the art without departing from the spirit and scope of the present invention, and these modifications or substitutions are within the scope of the present invention/any person skilled in the art can easily conceive of the changes or substitutions within the technical scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the claims.

Claims (8)

1. The preparation method of the shampoo containing the microalgae extract is characterized by comprising the following steps:
(1) preparing a camellia seed extract and a nannochloropsis oculata extract;
the preparation method of the nannochloropsis oculata extract comprises the following steps: grinding nannochloropsis oculata, adding a butanediol aqueous solution, mixing and soaking to obtain a treatment solution, performing microwave extraction on the treatment solution, filtering the microwave extraction solution, and drying in vacuum to obtain a nannochloropsis oculata extract;
(2) respectively adding the camellia seed extract, polyethylene glycol laurate and alkyl glycoside into deionized water, heating the mixed solution, and uniformly stirring;
(3) adding nannochloropsis oculata extract, linseed oil and xanthan gum into the mixed solution and stirring to obtain an intermediate mixed solution;
(4) finally, adding polyglycerol-10, polyglycerol ester, stearyl alcohol and citric acid, stirring and keeping the temperature for a certain time;
(5) sampling and detecting, discharging shampoo qualified in detection, filling by using a filling machine, and then packaging and packaging.
2. The method for preparing shampoo containing microalgae extract according to claim 1, wherein in the step (1), the preparation of the camellia seed extract comprises the following steps: weighing camellia seeds, grinding the camellia seeds, adding 50-65 wt% of ethanol aqueous solution into the ground camellia seeds, extracting the ground camellia seeds and the ethanol aqueous solution for 1-6h at 50-65 ℃ for three times, filtering and combining the filtrates to obtain ethanol extract, centrifuging the ethanol extract to obtain upper-layer oily matter, and evaporating to remove ethanol.
3. The method for preparing shampoo containing microalgae extract according to claim 1, wherein in the step (1), the feed-liquid ratio of nannochloropsis oculata to butanediol aqueous solution is 1:10-35, and the mass ratio of water to butanediol in butanediol aqueous solution is 1: 1-3; the microwave extraction time is 5-25min, the extraction temperature is 35-60 ℃, and the microwave power is 250-550W.
4. The method for preparing shampoo containing microalgae extract as claimed in claim 1, wherein the heating temperature of the mixed solution in the step (2) is 35-50 ℃.
5. The method for preparing shampoo containing microalgae extract according to claim 1, wherein in the step (4), the temperature is kept at 45-60 ℃ for 1.5-2.5 h.
6. The preparation method of the shampoo containing the microalgae extract as claimed in claim 1, wherein the shampoo comprises the following raw materials in parts by weight: 18-25 parts of camellia seed extract, 6-10 parts of polyethylene glycol laurate, 3-6 parts of alkyl glycoside, 3-7 parts of nannochloropsis oculata extract, 1-2 parts of linseed oil, 2-4 parts of xanthan gum, 1-2 parts of polyglycerol-10, 0.5-1 part of polyglycerol ester, 0.5-1 part of stearyl alcohol and 0.1-0.5 part of citric acid.
7. The preparation method of the shampoo containing the microalgae extract as claimed in claim 6, wherein the shampoo comprises the following components in parts by weight: 20 parts of camellia seed extract, 8 parts of polyethylene glycol laurate, 5 parts of nannochloropsis oculata extract, 4 parts of alkyl glycoside, 1.5 parts of linseed oil, 3 parts of xanthan gum, 1 part of polyglycerol-10, 0.7 part of polyglycerol ester, 0.6 part of stearyl alcohol and 0.2 part of citric acid.
8. A shampoo containing microalgae extract prepared by the preparation method of claim 1.
CN202210056340.0A 2022-01-18 2022-01-18 Shampoo containing microalgae extract and preparation method thereof Pending CN114344201A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117298198A (en) * 2023-10-16 2023-12-29 山东悦翔生物有限公司 Method for applying microalgae extract to medical treatment

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110840762A (en) * 2019-11-29 2020-02-28 刘召栋 Shampoo containing camellia seed extract and preparation method thereof
CN113444578A (en) * 2021-06-24 2021-09-28 日照职业技术学院 Extraction process of nannochloropsis oculata essential oil
CN113584102A (en) * 2021-07-06 2021-11-02 济宁学院 Preparation method of nannochloropsis oculata polysaccharide with antioxidant activity
CN113616680A (en) * 2014-08-19 2021-11-09 西姆莱斯股份公司 Nannochloropsis sp extract and application thereof
CN113876612A (en) * 2021-11-12 2022-01-04 湖北省麦诗特生物科技有限公司 A facial cream composition containing liposome for increasing skin collagen density and its preparation method

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113616680A (en) * 2014-08-19 2021-11-09 西姆莱斯股份公司 Nannochloropsis sp extract and application thereof
CN110840762A (en) * 2019-11-29 2020-02-28 刘召栋 Shampoo containing camellia seed extract and preparation method thereof
CN113444578A (en) * 2021-06-24 2021-09-28 日照职业技术学院 Extraction process of nannochloropsis oculata essential oil
CN113584102A (en) * 2021-07-06 2021-11-02 济宁学院 Preparation method of nannochloropsis oculata polysaccharide with antioxidant activity
CN113876612A (en) * 2021-11-12 2022-01-04 湖北省麦诗特生物科技有限公司 A facial cream composition containing liposome for increasing skin collagen density and its preparation method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117298198A (en) * 2023-10-16 2023-12-29 山东悦翔生物有限公司 Method for applying microalgae extract to medical treatment
CN117298198B (en) * 2023-10-16 2024-03-01 山东悦翔生物有限公司 Microalgae extract and application thereof

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Application publication date: 20220415