CN103251541A - Liquid shampoo containing notoginsenoside and preparation method thereof - Google Patents
Liquid shampoo containing notoginsenoside and preparation method thereof Download PDFInfo
- Publication number
- CN103251541A CN103251541A CN2013102065947A CN201310206594A CN103251541A CN 103251541 A CN103251541 A CN 103251541A CN 2013102065947 A CN2013102065947 A CN 2013102065947A CN 201310206594 A CN201310206594 A CN 201310206594A CN 103251541 A CN103251541 A CN 103251541A
- Authority
- CN
- China
- Prior art keywords
- parts
- ammonium salt
- radix notoginseng
- extract
- polyquaternary ammonium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a liquid shampoo containing notoginsenoside and a preparation method of the liquid shampoo, relates to the liquid shampoo containing the notoginsenoside and simultaneously relates to the preparation method of the liquid shampoo. The liquid shampoo is prepared from the following raw materials in parts by weight: 12-22 parts of an anionic surfactant, 1-10 parts of an nonionic surfactant, 0-7 parts of a zwitterionic surfactant, 1.8-10 parts of a cationic surfactant, 3.6-12 parts of a conditioner, 0.5-10 parts of panax notoginseng extract, 0.8-2 parts of a pearlescing agent, 0.8-2 parts of a thickening agent, 0.03-0.15 parts of a preservative, 0.1-0.7 parts of an essence, 0.8-1.7 parts of sodium chloride, and 40-80 parts of deionized water; and the liquid shampoo is obtained by carrying out a series of processes on the raw materials. The liquid shampoo can be used for achieving the effects of washing hair, caring hair and obviously reducing hair loss.
Description
Technical field
The invention belongs to the cosmetics of everyday use technical field, be specifically related to contain the shampoo of arasaponin, simultaneously, the invention still further relates to the preparation method of this shampoo.
Background technology
Radix Notoginseng is China's tradition rare Chinese medicine, one of 40 kinds of large big medical material kinds, and the applicating history apart from modern existing more than 400 year at home and abroad has long enjoyed a good reputation, and Radix Notoginseng just has the laudatory title of " refreshing medicine stops blooding " from ancient times.Radix Notoginseng mainly contains saponin, flavonoid glycoside, aminoacid etc., has the effect of blood circulation promoting and blood stasis dispelling, subduing swelling and relieving pain, meridians dredging, expelling wind and removing dampness;
Flower of Radix Notoginseng is to contain the highest position of arasaponin in the Radix Notoginseng Herb, and content based on Rb family saponin, has pharmacological actions such as tranquillizing and allaying excitement, anti-inflammatory and antalgic, blood pressure lowering up to more than 13%;
The flower of Radix Notoginseng petal contains saponin, and its aglycon has panoxadiol (panaxadiol), 20(R)-and dammarane-3 β, 12 β, 20,25-tetrol [20(R)-panaxadiol), 20(R)-and dammarane-3 β, 12 β, 20, the 25-tetrol [20(R)-dammaran-3 β, 12 β, 20,25-tetrol], Da Ma-20(22)-and alkene-3 β, 12 β, 26-triol [dammar-20 (22)-en-3 β, 12 β, 26-triol] etc.And ginsenoside (ginsenoside) Rb1.Rb2.Rc, Rd, F2 etc. have been isolated;
Stem and leaf of Radix Notoginseng contains plurality of active ingredients: ginsenoside Rh2 (1), F2 (4), Rg3 (5), Rg1 (7), Rd (8), Re (11), Rb3 (13), Rb1 (14), Rc (15), Herba Gynostemmatis saponins X III (2), IX (9), XVII (10), arasaponin R1 (12), Fa (16), glycyrrhizin and celery sugar liquirtin, based on protopanoxadiol type saponin, also have quite little Protopanaxatriol's type saponin and the flavone compound of content in the stem and leaf of Radix Notoginseng;
In recent years, international, domestic the world of medicine studies show that, stem and leaf of Radix Notoginseng also has functions such as tranquillizing and allaying excitement that Radix Notoginseng lacks, facilitating digestion, appetite stimulator except the blood circulation promoting and blood stasis dispelling with Radix Notoginseng, easing pain and diminishing inflammation, detumescence and promoting granulation, blood fat reducing, resisting fatigue, strengthening by means of tonics;
Radix Notoginseng extract has facilitation to b-16 melanocyte activity, can increase melanic growing amount, can be used for the hair color based article;
But, also do not have product and the technology identical or similar with composition of the present invention and processing technology in the market.
Summary of the invention
The invention provides and a kind ofly have hair washing, hair care, obviously reduce natural drug shampoo that alopecia and damage hair repair and preparation method thereof.
In order to realize above-mentioned purpose of the present invention, the invention provides following technical scheme:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio: 12～22 parts of anion surfactants, 1～10 part of non-ionic surface active agent, 0～7 part of zwitterionic surfactant, 1.8～10 parts of cationic surfactants, 3.6 ~ 12 parts of conditioners, 0.5～10 part of Radix Notoginseng extract, 0.8～2 part of pearling agent, thickening agent 0.8～2,0.03～0.15 part of antiseptic, 0.1～0.7 part in essence, 0.8 ~ 1.7 part in sodium chloride, 40～80 parts of deionized waters.
Further:Described Radix Notoginseng extract is the water of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng or extractum or the solid content of alcohol extraction.
Further:Described Radix Notoginseng extract comprises: the mixing of one or more in four kinds of the extract A, extract B, extract C, extract D, and preparation method is:
(1) get one or more mixing of an amount of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio that adds 6～12L according to per kilogram adds water, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, filtered, concentrated extracting solution is measured relative density and is 1.0～1.5 and get final product, then in the time of 60 ℃, the adding alcoholic strength is 50%～70% ethanol, leave standstill and make its precipitation more than 12 hours, reclaim ethanol, concentrate, drying namely gets extract A;
(2) with the extract A water dissolution, last ion exchange resin column is 50%～70% ethanol elution with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrates drying; Namely get extract B;
(3) get one or more mixing of an amount of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, it is 50%～80% ethanol that the ratio that adds 6～12L according to per kilogram adds alcoholic strength, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, was collected ethanol extract, in above-mentioned medicinal residues, the ratio that adds 6～12L according to per kilogram adds water, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, reclaims ethanol, concentrates, drying namely gets extract C;
(4) with the extract C water dissolution, last ion exchange resin column is 50%～70% ethanol elution with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrates, and drying namely gets extract D.
Further:Described anion surfactant is selected from one or more the mixing in laureth sulfuric ester ammonium, lauryl alcohol sulfuric ester ammonium, sodium lauryl sulphate, coconut oleoyl amine sodium isethionate or the polyoxyethylenated alcohol sodium sulfate; Cationic surfactant is selected from polyquaternary ammonium salt-43, the mixing of one or more in polyquaternary ammonium salt-51 or the polyquaternary ammonium salt-10; Zwitterionic surfactant is selected from cocoamido propyl hydroxy sulfobetaine, the mixing of one or more in cocamido propyl betaine or the dodecanamide propyl betanin; Non-ionic surface active agent is selected from alkyl polyglucoside, fatty alcohol-polyoxyethylene ether, the mixing of one or more in lauric acid amide of ethanol or the coconut oil single ethanol amide; Conditioner is selected from cation guar gum, docosyl hydroxypropyl quaternary ammonium salt, polyquaternary ammonium salt-7, emulsified silicone oil, the mixing of one or more in polydimethylsiloxane or the dimethiconol; Thickening agent is in the carbomer and thickening or the direct thickening of sodium chloride.
A kind of preparation method that contains the shampoo of arasaponin may further comprise the steps:
The first step: get the raw materials ready
(1) Radix Notoginseng extract: be the water of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng or extractum or the solid content of alcohol extraction;
This Radix Notoginseng extract comprises: the mixing of one or more in four kinds of the extract A, extract B, extract C, extract D, and preparation method is:
(1) get one or more mixing of an amount of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio that adds 6～12L according to per kilogram adds water, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, filtered, concentrated extracting solution is measured relative density and is 1.0～1.5 and get final product, then in the time of 60 ℃, the adding alcoholic strength is 50%～70% ethanol, leave standstill and make its precipitation more than 12 hours, reclaim ethanol, concentrate, drying namely gets extract A;
(2) with the extract A water dissolution, last ion exchange resin column is 50%～70% ethanol elution with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrates drying; Namely get extract B;
(3) get one or more mixing of an amount of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, it is 50%～80% ethanol that the ratio that adds 6～12L according to per kilogram adds alcoholic strength, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, was collected ethanol extract, in above-mentioned medicinal residues, the ratio that adds 6～12L according to per kilogram adds water, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, reclaims ethanol, concentrates, drying namely gets extract C;
(4) with the extract C water dissolution, last ion exchange resin column is 50%～70% ethanol elution with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrates, and drying namely gets extract D;
(2) anion surfactant: be selected from one or more the mixing in laureth sulfuric ester ammonium, lauryl alcohol sulfuric ester ammonium, sodium lauryl sulphate, coconut oleoyl amine sodium isethionate or the polyoxyethylenated alcohol sodium sulfate;
(3) cationic surfactant: be selected from polyquaternary ammonium salt-43, the mixing of one or more in polyquaternary ammonium salt-51 or the polyquaternary ammonium salt-10;
(4) zwitterionic surfactant: be selected from cocoamido propyl hydroxy sulfobetaine, the mixing of one or more in cocamido propyl betaine or the dodecanamide propyl betanin;
(5) non-ionic surface active agent: be selected from alkyl polyglucoside, fatty alcohol-polyoxyethylene ether, coconut oleoyl amine MEA, the mixing of one or more in lauric acid amide of ethanol or the coconut oil single ethanol amide;
(6) conditioner: be selected from cation guar gum, docosyl hydroxypropyl quaternary ammonium salt, polyquaternary ammonium salt-7, emulsified silicone oil, one or more mixing in polydimethylsiloxane or the dimethiconol; Emulsified silicone oil is selected from big particle diameter emulsified silicone oil and small particle diameter emulsified silicone oil, perhaps uses one for two kinds;
(7) thickening agent: in the carbomer and thickening or the direct thickening of sodium chloride;
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12～22 parts of anion surfactants, 1.8～10 parts of cationic surfactants, 1～10 part of non-ionic surface active agent, 0～7 part of amphoteric surfactant, 3.6 ~ 12 parts of conditioners, 0.8～2 part of pearling agent, 0.8～2 part of thickening agent, supplying deionized water makes its ratio reach 40～80 parts, to being heated to 50～80 ℃, constant temperature stirs 10～50min; Then, be cooled to 30～60 ℃, 0.5～10 part of Radix Notoginseng extract, constant temperature stirs 10～50min; Treating that temperature is down to below 45 ℃ adds 0.1～0.7 part in essence, 0.8 ~ 1.7 part in 0.03～0.15 part of antiseptic and sodium chloride; At last, regulating pH value is 5.8～6.0, still aging 0～48 hour, gets product.
Further:Described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 6 ~ 10 parts of laureth sulfuric ester ammoniums, 6 ~ 7 parts of lauryl alcohol sulfuric ester ammoniums, 0.7 ~ 0.9 part of polyquaternary ammonium salt-10,1 ~ 3 part of polyquaternary ammonium salt-51,2 ~ 5 parts of cocoamido propyl hydroxy sulfobetaine, 1 ~ 3 part of alkyl polyglucoside, 0.8 ~ 2 parts of fatty alcohol-polyoxyethylene ether, 1 ~ 3 part of docosyl hydroxypropyl quaternary ammonium salt, 0.5 ~ 2 portions of polyquaternary ammonium salt-7,1.3 ~ 1.7 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, be heated to 70 ~ 80 ℃, constant temperature stirs 20min; Then, be cooled to 50 ℃, add 2 ~ 5 parts of small particle diameter emulsified silicone oils, 1 ~ 4 part of Radix Notoginseng extract, constant temperature stirs 20min; Treating that temperature is down to below 45 ℃ adds 0.1 ~ 0.4 part in essence, and 1 ~ 3 part in 0.05 ~ 0.07 portion of antiseptic and sodium chloride stir; Regulating pH value is 6.2, still aging 24 hours, gets product.
Further:Described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 10 ~ 15 parts of laureth sulfuric ester ammoniums, 5 ~ 7 parts of coconut oleoyl amine sodium isethionates, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-51,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of coconut oil single ethanol amide, 0.8 ~ 1.5 parts of lauric acid amide of ethanol, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,1.3 ~ 1.7 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, be heated to 70 ~ 80 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.3 ~ 1.7 parts of polydimethylsiloxane, 1.3 ~ 1.7 parts of emulsified silicone oils, 1.3 ~ 1.7 parts of Radix Notoginseng extracts, constant temperature stirs 30nin; Treating that temperature is down to adds 0.1 ~ 0.4 part of essence below 40 ℃, 0.03 ~ 0.1 portion of antiseptic and 1.3 ~ 1.7 parts of sodium chloride stir; Regulating pH value is 5.8, still aging 36 hours, gets product.
Further:Described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 ~ 16 parts of sodium lauryl sulphates, 2 ~ 5 parts of coconut oleoyl amine sodium isethionates, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of coconut oil single ethanol amide, 0.8 ~ 1.5 parts of lauric acid amide of ethanol, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,0.8 ~ 1.5 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, water is heated to 70 ~ 80 ℃, and constant temperature stirs 20min; Then, be cooled to 50 ℃, add 1.3 ~ 1.7 parts of polydimethylsiloxane, 1.3 ~ 1.7 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract constant temperature stirs 30nin; Treating that temperature is down to adds 0.3 ~ 0.5 part of essence below 45 ℃, 0.05 ~ 0.15 portion of antiseptic and 1.3 ~ 1.7 parts of sodium chloride stir; Regulating pH value is 6.0, gets product.
Further:Described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of sodium lauryl sulphate, 0.8 ~ 1.5 parts of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-10,2 ~ 5 parts of coconut oleoyl amine MEA, 1 ~ 3 part of fatty alcohol-polyoxyethylene ether, 0.8 ~ 1.5 parts of lauric acid amide of ethanol, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,0.8 ~ 1.5 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, water is heated to 70 ~ 80 ℃, and constant temperature stirs 20min; Then, be cooled to 50 ℃, add 2 ~ 5 parts of emulsified silicone oils, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 20nin; Treat that temperature is down to below 45 ℃, add 0.3 ~ 0.7 part of essence, 0.05 ~ 0.15 portion of antiseptic and 1.3 ~ 1.7 parts of sodium chloride stir; Regulating pH value is 5.8, still aging 48 hours, gets product.
Further:Described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of alkyl polyglucoside, 0.8 ~ 1.5 parts of lauric acid amide of ethanol, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,0.8 ~ 1.5 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, be heated to 75 ~ 85 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.3 ~ 1.7 parts of polydimethylsiloxane, 1.3 ~ 1.7 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 30nin; Treating that temperature is down to adds 0.2 ~ 0.4 part of essence below 45 ℃, 0.05 ~ 0.15 portion of antiseptic and 1 ~ 1.5 part of sodium chloride stir; Regulating pH value is 6.0, gets product.
Further:Described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of coconut oleoyl amine MEA, 0.8 ~ 1.5 parts of coconut oil single ethanol amides, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,0.8 ~ 1.5 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, be heated to 75 ~ 85 ℃, constant temperature stirs 20min; Then, be cooled to 65 ℃, add 1.3 ~ 1.6 parts of polydimethylsiloxane, 1 ~ 1.4 part of dimethiconol, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 30nin; Treating that temperature is down to adds 0.2 ~ 0.4 part of essence below 45 ℃, 0.05 ~ 0.15 portion of antiseptic and 1 ~ 1.5 part of sodium chloride stir; Regulating pH value is 6.0, gets product.
Further:Described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of fatty alcohol-polyoxyethylene ether, 0.8 ~ 1.5 parts of alkyl polyglucoside, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,0.8 ~ 1.5 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, be heated to 80 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.1 ~ 1.4 parts of polydimethylsiloxane, 1.2 ~ 1.5 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 30nin; Treating that temperature is down to adds 0.2 ~ 0.4 part of essence below 45 ℃, 0.05 ~ 0.15 portion of antiseptic and 0.8 ~ 1.5 part of sodium chloride stir; Regulating pH value is 6.0, gets product.
Useful technique effect:
The present invention has obvious effects to aspects such as cleaning hair, hair care, minimizing alopecia, the reparations of damage hair;
Effect analysis:
Anion surfactant, zwitterionic surfactant, non-ionic surface active agent all can provide cleaning power, keep the abundant, stable, fine and smooth of foam.Wherein zwitterionic surfactant and non-ionic surface active agent have the effect of auxiliary foaming, thickening, steady bubble;
The general tool film property of cationic surfactant gives that hair and skin are comfortable, lubricated, soft feeling improves hair texture that conditioning is arranged, and antistatic improves characteristics such as cardability, gives the fluffy sense of hair, soft feeling, good cardability;
Cation guar gum in the conditioner is adsorbed on the hair, improves the cardability of hair, is used for conditioning, the thickening and stable of hair-washing hair-care product, improves wet cardability.Remaining conditioner such as docosyl hydroxypropyl quaternary ammonium salt, dimethiconol, polydimethylsiloxane etc. can be given the fabulous moisture retention of hair, gloss, for superior smooth sense, can improve do wet cardability, anti-entanglement, good hand, rational to a high-profile be arranged;
Radix Notoginseng is China's tradition rare Chinese medicine, one of 40 kinds of large big medical material kinds, and the applicating history apart from modern existing more than 400 year at home and abroad has long enjoyed a good reputation, and Radix Notoginseng just has the laudatory title of " refreshing medicine stops blooding " from ancient times.Radix Notoginseng mainly contains saponin, flavonoid glycoside, aminoacid etc., has the effect of blood circulation promoting and blood stasis dispelling, subduing swelling and relieving pain, meridians dredging, expelling wind and removing dampness;
Flower of Radix Notoginseng is to contain the highest position of arasaponin in the Radix Notoginseng Herb, and content based on Rb family saponin, has pharmacological actions such as tranquillizing and allaying excitement, anti-inflammatory and antalgic, blood pressure lowering up to more than 13%;
The flower of Radix Notoginseng petal contains saponin, and its aglycon has panoxadiol (panaxadiol), 20(R)-and dammarane-3 β, 12 β, 20,25-tetrol [20(R)-panaxadiol), 20(R)-and dammarane-3 β, 12 β, 20, the 25-tetrol [20(R)-dammaran-3 β, 12 β, 20,25-tetrol], Da Ma-20(22)-and alkene-3 β, 12 β, the 26-triol [dammar-20(22)-en-3 β, 12 β, 26-triol] etc.And ginsenoside (ginsenoside) Rb1.Rb2.Rc, Rd, F2 etc. have been isolated;
Stem and leaf of Radix Notoginseng contains plurality of active ingredients: ginsenoside Rh2 (1), F2 (4), Rg3(5), Rg1(7), Rd(8), Re(11), Rb3(13), Rb1(14), Rc(15), Herba Gynostemmatis saponins X III(2), XVII(10 IX(9)), arasaponin R1 (12), Fa(16), glycyrrhizin and celery sugar liquirtin, based on protopanoxadiol type saponin, also have quite little Protopanaxatriol's type saponin and the flavone compound of content in the stem and leaf of Radix Notoginseng;
In recent years, international, domestic the world of medicine studies show that, stem and leaf of Radix Notoginseng also has functions such as tranquillizing and allaying excitement that Radix Notoginseng lacks, facilitating digestion, appetite stimulator except the blood circulation promoting and blood stasis dispelling with Radix Notoginseng, easing pain and diminishing inflammation, detumescence and promoting granulation, blood fat reducing, resisting fatigue, strengthening by means of tonics;
Radix Notoginseng extract has facilitation to b-16 melanocyte activity, can increase melanic growing amount, can be used for the hair color based article.
Further specify essentiality content of the present invention by specific embodiment given below, but do not limit the present invention with this.
Embodiment 1: a kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.6 part cation guar gum, 10 parts of laureth sulfuric ester ammoniums, 6 parts of coconut oleoyl amine sodium isethionates, 1 part of polyquaternary ammonium salt-43,1 part polyquaternary ammonium salt-51,2 part cocamido propyl betaine, 1 part of coconut oil single ethanol amide, 0.8 part lauric acid amide of ethanol, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,1.3 portion pearling agent, 40 parts of deionized waters, 1.3 parts of polydimethylsiloxane, 1.3 parts of emulsified silicone oils, 1.3 part Radix Notoginseng extract A, 0.1 part essence, 0.03 portion of antiseptic, 1.3 parts of sodium chloride;
Described Radix Notoginseng extract: be the water of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng or extractum or the solid content of alcohol extraction;
This Radix Notoginseng extract comprises: the mixing of one or more in four kinds of the extract A, extract B, extract C, extract D, and preparation method is:
(1) get one or more mixing of an amount of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio that adds 6～12L according to per kilogram adds water, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, filtered, concentrated extracting solution is measured relative density and is 1.0～1.5 and get final product, then in the time of 60 ℃, the adding alcoholic strength is 50%～70% ethanol, leave standstill and make its precipitation more than 12 hours, reclaim ethanol, concentrate, drying namely gets extract A;
(2) with the extract A water dissolution, last ion exchange resin column is 50%～70% ethanol elution with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrates drying; Namely get extract B;
(3) get one or more mixing of an amount of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, it is 50%～80% ethanol that the ratio that adds 6～12L according to per kilogram adds alcoholic strength, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, was collected ethanol extract, in above-mentioned medicinal residues, the ratio that adds 6～12L according to per kilogram adds water, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, reclaims ethanol, concentrates, drying namely gets extract C;
(4) with the extract C water dissolution, last ion exchange resin column is 50%～70% ethanol elution with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrates, and drying namely gets extract D.
Embodiment 2: a kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.6 part cation guar gum, 15 parts of laureth sulfuric ester ammoniums, 7 parts of coconut oleoyl amine sodium isethionates, 3 parts of polyquaternary ammonium salt-43,3 part polyquaternary ammonium salt-51,5 part cocamido propyl betaine, 3 parts of coconut oil single ethanol amides, 1.5 part lauric acid amide of ethanol, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.7 portion pearling agent, 80 parts of deionized waters, 1.7 parts of polydimethylsiloxane, 1.7 parts of emulsified silicone oils, 1.7 part Radix Notoginseng extract A, 0.4 part essence, 0.1 portion of antiseptic, 1.7 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 3: a kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.6 part cation guar gum, 12 parts of laureth sulfuric ester ammoniums, 5 parts of coconut oleoyl amine sodium isethionates, 2 parts of polyquaternary ammonium salt-43,2 part polyquaternary ammonium salt-51,3 part cocamido propyl betaine, 2 parts of coconut oil single ethanol amides, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1.5 portion pearling agent, 60 parts of deionized waters, 1.5 parts of polydimethylsiloxane, 1.5 parts of emulsified silicone oils, 1.5 part Radix Notoginseng extract A, 0.2 part essence, 0.06 portion of antiseptic, 1.5 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 4:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 6 parts of laureth sulfuric ester ammoniums, 6 parts of lauryl alcohol sulfuric ester ammoniums, 0.7 part polyquaternary ammonium salt-10,1 part polyquaternary ammonium salt-51,2 part cocoamido propyl hydroxy sulfobetaine, 1 part of alkyl polyglucoside, 0.8 part of fatty alcohol-polyoxyethylene ether, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 0.5 portion polyquaternary ammonium salt-7,1.3 portion pearling agent, 40 parts of deionized waters, 2 parts of small particle diameter emulsified silicone oils, Radix Notoginseng extract A part, 0.1 part in essence, 0.05 portion antiseptic, 1 part in sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 5:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 10 parts of laureth sulfuric ester ammoniums, 7 parts of lauryl alcohol sulfuric ester ammoniums, 0.9 part polyquaternary ammonium salt-10,3 part polyquaternary ammonium salt-51,5 part cocoamido propyl hydroxy sulfobetaine, 3 parts of alkyl polyglucoside, 2 parts of fatty alcohol-polyoxyethylene ether, 3 parts of docosyl hydroxypropyl quaternary ammonium salts, 2 portions of polyquaternary ammonium salt-7,1.7 portion pearling agents, 80 parts of deionized waters, 5 parts of small particle diameter emulsified silicone oils, 4 parts of Radix Notoginseng extract A, 0.4 part of essence, 0.07 portion antiseptic, 3 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 6:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 8 parts of laureth sulfuric ester ammoniums, 5 parts of lauryl alcohol sulfuric ester ammoniums, 0.8 part polyquaternary ammonium salt-10,2 part polyquaternary ammonium salt-51,3 part cocoamido propyl hydroxy sulfobetaine, 2 parts of alkyl polyglucoside, 1 part of fatty alcohol-polyoxyethylene ether, 2 parts of docosyl hydroxypropyl quaternary ammonium salts, 1 portion of polyquaternary ammonium salt-7,1.5 portion pearling agent, 60 parts of deionized waters, 3 parts of small particle diameter emulsified silicone oils, 2 parts of Radix Notoginseng extract A, 0.2 part of essence, 0.06 portion antiseptic, 2 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 7:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 14 parts of sodium lauryl sulphates, 3 parts of coconut oleoyl amine sodium isethionates, 2 parts of polyquaternary ammonium salt-43,2 part polyquaternary ammonium salt-10,3 part cocamido propyl betaine, 2 parts of coconut oil single ethanol amides, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, 60 parts of deionized waters, 1.5 parts of polydimethylsiloxane, 1.5 parts of dimethiconols, 1 part of Radix Notoginseng extract A, 0.4 part essence, 0.1 portion of antiseptic, 1.5 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 7:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 12 parts of sodium lauryl sulphates, 2 parts of coconut oleoyl amine sodium isethionates, 1 part of polyquaternary ammonium salt-43,1 part polyquaternary ammonium salt-10,2 part cocamido propyl betaine, 1 part of coconut oil single ethanol amide, 0.8 part lauric acid amide of ethanol, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,0.8 portion pearling agent, 40 parts of deionized waters, 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 0.8 part Radix Notoginseng extract, 0.3 part essence, 0.05 portion of antiseptic, 1.3 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 8:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 16 parts of sodium lauryl sulphates, 5 parts of coconut oleoyl amine sodium isethionates, 3 parts of polyquaternary ammonium salt-43,3 part polyquaternary ammonium salt-10,5 part cocamido propyl betaine, 3 parts of coconut oil single ethanol amides, 1.5 part lauric acid amide of ethanol, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portion pearling agent, 80 parts of deionized waters, 1.7 parts of polydimethylsiloxane, 1.7 parts of dimethiconols, 1.5 part Radix Notoginseng extract, 0.5 part essence, 0.15 portion of antiseptic, 1.7 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 9:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.3 part cation guar gum, 12 parts of laureth sulfuric ester ammoniums, 1 part of sodium lauryl sulphate, 0.8 part polyquaternary ammonium salt-43,1 part polyquaternary ammonium salt-10,2 part coconut oleoyl amine MEA, 1 part of fatty alcohol-polyoxyethylene ether, 0.8 part of lauric acid amide of ethanol, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 portion polyquaternary ammonium salt-7,0.8 portion pearling agent, 40 parts of deionized waters, 2 parts big particle diameter emulsified silicone oils, 0.8 part Radix Notoginseng extract B, 0.3 part of essence, 0.05 portion of antiseptic, 1.3 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 10:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.3 part cation guar gum, 16 parts of laureth sulfuric ester ammoniums, 3 parts of sodium lauryl sulphates, 1.5 part polyquaternary ammonium salt-43,3 parts of polyquaternary ammonium salt-10,5 parts of coconut oleoyl amine MEA, 3 parts of fatty alcohol-polyoxyethylene ether, 1.5 parts of lauric acid amide of ethanol, 1.5 part docosyl hydroxypropyl quaternary ammonium salt, 1.5 portion polyquaternary ammonium salt-7,1.5 portion pearling agent, 80 parts of deionized waters, 5 parts big particle diameter emulsified silicone oils, 1.5 part Radix Notoginseng extract B, 0.7 part of essence, 0.15 portion of antiseptic, 1.7 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 11:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.3 part cation guar gum, 14 parts of laureth sulfuric ester ammoniums, 2 parts of sodium lauryl sulphates, 1 part of polyquaternary ammonium salt-43,1 part polyquaternary ammonium salt-10,3 part coconut oleoyl amine MEA, 2 parts of fatty alcohol-polyoxyethylene ether, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 portion of polyquaternary ammonium salt-7,1 portion pearling agent, 60 parts of deionized waters, 3 parts big particle diameter emulsified silicone oils, 1 part of Radix Notoginseng extract B, 0.4 part of essence, 0.1 portion of antiseptic, 1.5 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 12:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 12 parts of laureth sulfuric ester ammoniums, 1 part of lauryl alcohol sulfuric ester ammonium, 1 part of polyquaternary ammonium salt-43,1 part polyquaternary ammonium salt-10,2 part cocamido propyl betaine, 1 part of alkyl polyglucoside, 0.8 part lauric acid amide of ethanol, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,0.8 portion pearling agent, 40 parts of deionized waters, 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 0.8 part Radix Notoginseng extract B, 0.2 part essence, 0.05 portion of antiseptic, 1 part of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 13:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 16 parts of laureth sulfuric ester ammoniums, 3 parts of lauryl alcohol sulfuric ester ammoniums, 3 parts of polyquaternary ammonium salt-43,3 part polyquaternary ammonium salt-10,5 part cocamido propyl betaine, 3 parts of alkyl polyglucoside, 1.5 part lauric acid amide of ethanol, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portion pearling agent, 80 parts of deionized waters, 1.7 parts of polydimethylsiloxane, 1.7 parts of dimethiconols, 1.5 part Radix Notoginseng extract B, 0.4 part essence, 0.15 portion of antiseptic, 1 ~ 1.5 part of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 14:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 14 parts of laureth sulfuric ester ammoniums, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 part polyquaternary ammonium salt-10,3 part cocamido propyl betaine, 2 parts of alkyl polyglucoside, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 portion of polyquaternary ammonium salt-7,1 portion pearling agent, 70 parts of deionized waters, 1.5 part polydimethylsiloxane, 1.5 parts of dimethiconols, 1 part of Radix Notoginseng extract B, 0.3 part essence, 0.1 portion of antiseptic, 1.3 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 15:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 12 parts of laureth sulfuric ester ammoniums, 1 part of lauryl alcohol sulfuric ester ammonium, 1 part of polyquaternary ammonium salt-43,1 part polyquaternary ammonium salt-10,2 part cocamido propyl betaine, 1 part of coconut oleoyl amine MEA, 0.8 part coconut oil single ethanol amide, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,0.8 portion pearling agent, 40 parts of deionized waters, 1.3 parts of polydimethylsiloxane, 1 part of dimethiconol, 0.8 part Radix Notoginseng extract C, 0.2 part essence, 0.05 portion of antiseptic, 1 ~ 1.5 part of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 16:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 16 parts of laureth sulfuric ester ammoniums, 3 parts of lauryl alcohol sulfuric ester ammoniums, 3 parts of polyquaternary ammonium salt-43,3 part polyquaternary ammonium salt-10,5 part cocamido propyl betaine, 3 parts of coconut oleoyl amine MEA, 1.5 part coconut oil single ethanol amide, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portion pearling agent, 80 parts of deionized waters, 1.6 parts of polydimethylsiloxane, 1.4 parts of dimethiconols, 1.5 part Radix Notoginseng extract C, 0.4 part essence, 0.15 portion of antiseptic, 1.5 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 17:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 14 parts of laureth sulfuric ester ammoniums, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 part polyquaternary ammonium salt-10,2 part cocamido propyl betaine, 2 parts of coconut oleoyl amine MEA, 1 part of coconut oil single ethanol amide, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, 50 parts of deionized waters, 1.5 parts of polydimethylsiloxane, 1.2 parts of dimethiconols, 1 part of Radix Notoginseng extract C, 0.3 part essence, 0.1 portion of antiseptic, 1.3 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 18:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 12 parts of laureth sulfuric ester ammoniums, 1 part of lauryl alcohol sulfuric ester ammonium, 1 part of polyquaternary ammonium salt-43,1 part polyquaternary ammonium salt-10,2 part cocamido propyl betaine, 1 part of fatty alcohol-polyoxyethylene ether, 0.8 part alkyl polyglucoside, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,0.8 portion pearling agent, 40 parts of deionized waters, 1.1 parts of polydimethylsiloxane, 1.2 parts of dimethiconols, 0.8 part Radix Notoginseng extract D, 0.2 part essence, 0.05 portion of antiseptic, 0.8 part of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 19:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 16 parts of laureth sulfuric ester ammoniums, 3 parts of lauryl alcohol sulfuric ester ammoniums, 3 parts of polyquaternary ammonium salt-43,3 part polyquaternary ammonium salt-10,5 part cocamido propyl betaine, 3 parts of fatty alcohol-polyoxyethylene ether, 1.5 part alkyl polyglucoside, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portion pearling agent, 80 parts of deionized waters, 1.4 parts of polydimethylsiloxane, 1.5 parts of dimethiconols, 1.5 part Radix Notoginseng extract D, 0.4 part essence, 0.15 portion of antiseptic, 1.5 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 20:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.4 part cation guar gum, 14 parts of laureth sulfuric ester ammoniums, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 part polyquaternary ammonium salt-10,3 part cocamido propyl betaine, 2 parts of fatty alcohol-polyoxyethylene ether, 1 part of alkyl polyglucoside, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 portion of polyquaternary ammonium salt-7,1 portion pearling agent, 60 parts of deionized waters, 1.3 part polydimethylsiloxane, 1.3 parts of dimethiconols, 1 part of Radix Notoginseng extract D, 0.3 part essence, 0.1 portion of antiseptic, 1 part of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 21:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.5 part cation guar gum, 14 parts of laureth sulfuric ester ammoniums, 2 parts of aliphatic acid polyethenoxy ether sodium sulfate, 2 parts of polyquaternary ammonium salt-43,2 part polyquaternary ammonium salt-10,2 part cocamido propyl betaine, 2 parts of coconut oleoyl amine MEA, 1 part of coconut oil single ethanol amide, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, 50 parts of deionized waters, 1.5 parts of polydimethylsiloxane, 1.2 parts of dimethiconols, 1 part of Radix Notoginseng extract C, 0.3 part essence, 0.1 portion of antiseptic, 1.3 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 22:
A kind ofThe shampoo that contains arasaponin comprises the raw material of following weight parts ratio:
0.5 part cation guar gum, 14 parts of laureth sulfuric ester ammoniums, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 part polyquaternary ammonium salt-10,3 part dodecanamide propyl betanins, 2 parts of fatty alcohol-polyoxyethylene ether, 1 part of alkyl polyglucoside, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 portion of polyquaternary ammonium salt-7,1 portion pearling agent, 60 parts of deionized waters, 1.3 part polydimethylsiloxane, 1.3 parts of dimethiconols, 1 part of Radix Notoginseng extract D, 0.3 part essence, 0.1 portion of antiseptic, 1 part of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 23: a kind of preparation method that contains the shampoo of arasaponin, it is characterized in that, and may further comprise the steps:
The first step: get the raw materials ready
(1) Radix Notoginseng extract: be the water of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng or extractum or the solid content of alcohol extraction;
This Radix Notoginseng extract comprises: the mixing of one or more in four kinds of the extract A, extract B, extract C, extract D, and preparation method is:
(1) get one or more mixing of an amount of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio that adds 6～12L according to per kilogram adds water, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, filtered, concentrated extracting solution is measured relative density and is 1.0～1.5 and get final product, then in the time of 60 ℃, the adding alcoholic strength is 50%～70% ethanol, leave standstill and make its precipitation more than 12 hours, reclaim ethanol, concentrate, drying namely gets extract A;
(2) with the extract A water dissolution, last ion exchange resin column is 50%～70% ethanol elution with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrates drying; Namely get extract B;
(3) get one or more mixing of an amount of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, it is 50%～80% ethanol that the ratio that adds 6～12L according to per kilogram adds alcoholic strength, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, was collected ethanol extract, in above-mentioned medicinal residues, the ratio that adds 6～12L according to per kilogram adds water, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, reclaims ethanol, concentrates, drying namely gets extract C;
(4) with the extract C water dissolution, last ion exchange resin column is 50%～70% ethanol elution with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrates, and drying namely gets extract D;
(2) anion surfactant: be selected from one or more the mixing in laureth sulfuric ester ammonium, lauryl alcohol sulfuric ester ammonium, sodium lauryl sulphate, coconut oleoyl amine sodium isethionate or the polyoxyethylenated alcohol sodium sulfate;
(3) cationic surfactant: be selected from polyquaternary ammonium salt-43, the mixing of one or more in polyquaternary ammonium salt-51 or the polyquaternary ammonium salt-10;
(4) zwitterionic surfactant: be selected from cocoamido propyl hydroxy sulfobetaine, the mixing of one or more in cocamido propyl betaine or the dodecanamide propyl betanin;
(5) non-ionic surface active agent: be selected from alkyl polyglucoside, fatty alcohol-polyoxyethylene ether, coconut oleoyl amine MEA, the mixing of one or more in lauric acid amide of ethanol or the coconut oil single ethanol amide;
(6) conditioner: be selected from cation guar gum, docosyl hydroxypropyl quaternary ammonium salt, polyquaternary ammonium salt-7, emulsified silicone oil, one or more mixing in polydimethylsiloxane or the dimethiconol; Emulsified silicone oil is selected from big particle diameter emulsified silicone oil and small particle diameter emulsified silicone oil, perhaps uses one for two kinds;
(7) thickening agent: in the carbomer and thickening or the direct thickening of sodium chloride;
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 6 parts of laureth sulfuric ester ammoniums, 6 parts of lauryl alcohol sulfuric ester ammoniums, 0.7 part of polyquaternary ammonium salt-10,1 part of polyquaternary ammonium salt-51,2 parts of cocoamido propyl hydroxy sulfobetaine, 1 part of alkyl polyglucoside, 0.8 part of fatty alcohol-polyoxyethylene ether, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 0.5 portion polyquaternary ammonium salt-7,1.3 portion pearling agent is supplied deionized water and is made its ratio reach 40 parts, be heated to 70 ℃, constant temperature stirs 20min; Then, be cooled to 50 ℃, 2 parts of small particle diameter emulsified silicone oils, 1 part of Radix Notoginseng extract A, constant temperature stirs 20min; Treating that temperature is down to below 45 ℃ adds 0.1 part in essence, and 1 part in 0.05 portion of antiseptic and sodium chloride stir; Regulating pH value is 6.2, still aging 24 hours, gets product.
Embodiment 24: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.5 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 10 parts of laureth sulfuric ester ammoniums, 7 parts of lauryl alcohol sulfuric ester ammoniums, 0.9 part of polyquaternary ammonium salt-10,3 parts of polyquaternary ammonium salt-51,5 parts of cocoamido propyl hydroxy sulfobetaine, 3 parts of alkyl polyglucoside, 2 parts of fatty alcohol-polyoxyethylene ether, 3 parts of docosyl hydroxypropyl quaternary ammonium salts, 2 portions of polyquaternary ammonium salt-7,1.7 portion pearling agents are supplied deionized water and are made its ratio reach 80 parts, be heated to 80 ℃, constant temperature stirs 20min; Then, be cooled to 50 ℃, 5 parts of small particle diameter emulsified silicone oils, 4 parts of Radix Notoginseng extract A, constant temperature stirs 20min; Treating that temperature is down to below 45 ℃ adds 0.4 part in essence, and 3 parts in 0.07 portion of antiseptic and sodium chloride stir; Regulating pH value is 6.2, still aging 24 hours, gets product; Other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 25: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 8 parts of laureth sulfuric ester ammoniums, 5 parts of lauryl alcohol sulfuric ester ammoniums, 0.8 part of polyquaternary ammonium salt-10,2 parts of polyquaternary ammonium salt-51,3 parts of cocoamido propyl hydroxy sulfobetaine, 2 parts of alkyl polyglucoside, 1 part of fatty alcohol-polyoxyethylene ether, 2 parts of docosyl hydroxypropyl quaternary ammonium salts, 1 portion of polyquaternary ammonium salt-7,1.5 portion pearling agent is supplied deionized water and is made its ratio reach 60 parts, be heated to 75 ℃, constant temperature stirs 20min; Then, be cooled to 50 ℃, 3 parts of small particle diameter emulsified silicone oils, 2 parts of Radix Notoginseng extract A, constant temperature stirs 20min; Treating that temperature is down to below 45 ℃ adds 0.2 part in essence, and 2 parts in 0.06 portion of antiseptic and sodium chloride stir; Regulating pH value is 6.2, still aging 24 hours, gets product; Other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 26: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.3 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 10 parts of laureth sulfuric ester ammoniums, 6 parts of coconut oleoyl amine sodium isethionates, 1 part of polyquaternary ammonium salt-43,1 part of polyquaternary ammonium salt-51,2 parts of cocamido propyl betaine, 1 part of coconut oil single ethanol amide, 0.8 part of lauric acid amide of ethanol, 0.8 part docosyl hydroxypropyl quaternary ammonium salt, 0.8 portion polyquaternary ammonium salt-7,1.3 portion pearling agent is supplied deionized water and is made its ratio reach 40 parts, be heated to 70 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.3 parts of polydimethylsiloxane, 1.3 parts of emulsified silicone oils, 1.3 parts of Radix Notoginseng extract A, constant temperature stirs 30nin; Treating that temperature is down to below 40 ℃ adds 0.1 part of essence, and 0.03 portion of antiseptic and 1.3 parts of sodium chloride stir; Regulating pH value is 5.8, still aging 36 hours, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 27: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 15 parts of laureth sulfuric ester ammoniums, 7 parts of coconut oleoyl amine sodium isethionates, 3 parts of polyquaternary ammonium salt-43,3 parts of polyquaternary ammonium salt-51,5 parts of cocamido propyl betaine, 3 parts of coconut oil single ethanol amides, 1.5 parts of lauric acid amide of ethanol, 1.5 part docosyl hydroxypropyl quaternary ammonium salt, 1.5 portion polyquaternary ammonium salt-7,1.7 portion pearling agent is supplied deionized water and is made its ratio reach 80 parts, be heated to 80 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.7 parts of polydimethylsiloxane, 1.7 parts of emulsified silicone oils, 1.7 parts of Radix Notoginseng extract A, constant temperature stirs 30nin; Treating that temperature is down to below 40 ℃ adds 0.4 part of essence, and 0.1 portion of antiseptic and 1.7 parts of sodium chloride stir; Regulating pH value is 5.8, still aging 36 hours, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 28: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.4 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 parts of laureth sulfuric ester ammoniums, 5 parts of coconut oleoyl amine sodium isethionates, 2 parts of polyquaternary ammonium salt-43,2 parts of polyquaternary ammonium salt-51,3 parts of cocamido propyl betaine, 2 parts of coconut oil single ethanol amides, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 portion of polyquaternary ammonium salt-7,1.5 portion pearling agent is supplied deionized water and is made its ratio reach 60 parts, be heated to 75 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.5 parts of polydimethylsiloxane, 1.5 parts of emulsified silicone oils, 1.5 parts of Radix Notoginseng extract A, constant temperature stirs 30nin; Treating that temperature is down to below 40 ℃ adds 0.2 part of essence, and 0.06 portion of antiseptic and 1.5 parts of sodium chloride stir; Regulating pH value is 5.8, still aging 36 hours, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 29: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 16 parts of sodium lauryl sulphates, 5 parts of coconut oleoyl amine sodium isethionates, 3 parts of polyquaternary ammonium salt-43,3 parts of polyquaternary ammonium salt-10,5 parts of cocamido propyl betaine, 3 parts of coconut oil single ethanol amides, 0.8 ~ 1.5 part of lauric acid amide of ethanol, 1.5 part docosyl hydroxypropyl quaternary ammonium salt, 1.5 portion polyquaternary ammonium salt-7,1.5 portion pearling agent is supplied deionized water and is made its ratio reach 80 parts, water is heated to 80 ℃, and constant temperature stirs 20min; Then, be cooled to 50 ℃, add 1.7 parts of polydimethylsiloxane, 1.7 parts of dimethiconols, 1.5 parts of Radix Notoginseng extract A, constant temperature stirs 30nin; Treating that temperature is down to below 45 ℃ adds 0.5 part of essence, and 0.15 portion of antiseptic and 1.7 parts of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 29: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.3 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 parts of sodium lauryl sulphates, 2 parts of coconut oleoyl amine sodium isethionates, 1 part of polyquaternary ammonium salt-43,1 part of polyquaternary ammonium salt-10,2 parts of cocamido propyl betaine, 1 part of coconut oil single ethanol amide, 0.8 part of lauric acid amide of ethanol, 0.8 part docosyl hydroxypropyl quaternary ammonium salt, 0.8 portion polyquaternary ammonium salt-7,0.8 portion pearling agent is supplied deionized water and is made its ratio reach 40 parts, water is heated to 70 ℃, and constant temperature stirs 20min; Then, be cooled to 50 ℃, add 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 0.8 part of Radix Notoginseng extract A, constant temperature stirs 30nin; Treating that temperature is down to below 45 ℃ adds 0.3 part of essence, and 0.05 portion of antiseptic and 1.3 parts of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 29: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.4 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 14 parts of sodium lauryl sulphates, 3 parts of coconut oleoyl amine sodium isethionates, 2 parts of polyquaternary ammonium salt-43,2 parts of polyquaternary ammonium salt-10,3 parts of cocamido propyl betaine, 2 parts of coconut oil single ethanol amides, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 portion of polyquaternary ammonium salt-7,1 portion pearling agent is supplied deionized water and is made its ratio reach 60 parts, water is heated to 75 ℃, and constant temperature stirs 20min; Then, be cooled to 50 ℃, add 1.5 parts of polydimethylsiloxane, 1.5 parts of dimethiconols, 1 part of Radix Notoginseng extract A, constant temperature stirs 30nin; Treating that temperature is down to below 45 ℃ adds 0.4 part of essence, and 0.1 portion of antiseptic and 1.5 parts of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 30: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.4 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 parts of laureth sulfuric ester ammoniums, 1 part of sodium lauryl sulphate, 0.8 part of polyquaternary ammonium salt-43,1 part of polyquaternary ammonium salt-10,2 parts of coconut oleoyl amine MEA, 1 part of fatty alcohol-polyoxyethylene ether, 0.8 part of lauric acid amide of ethanol, 0.8 part docosyl hydroxypropyl quaternary ammonium salt, 0.8 portion polyquaternary ammonium salt-7,0.8 portion pearling agent is supplied deionized water and is made its ratio reach 40 parts, water is heated to 70 ℃, and constant temperature stirs 20min; Then, be cooled to 50 ℃, add 2 parts big particle diameter emulsified silicone oils, 0.8 part of Radix Notoginseng extract B, constant temperature stirs 20nin; Treat that temperature is down to below 45 ℃, add 0.3 part of essence, 0.05 portion of antiseptic and 1.3 parts of sodium chloride stir; Regulating pH value is 5.8, still aging 48 hours, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 31: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 16 parts of laureth sulfuric ester ammoniums, 3 parts of sodium lauryl sulphates, 1.5 parts of polyquaternary ammonium salt-43,3 parts of polyquaternary ammonium salt-10,5 parts of coconut oleoyl amine MEA, 3 parts of fatty alcohol-polyoxyethylene ether, 1.5 parts of lauric acid amide of ethanol, 1.5 part docosyl hydroxypropyl quaternary ammonium salt, 1.5 portion polyquaternary ammonium salt-7,1.5 portion pearling agent is supplied deionized water and is made its ratio reach 70 parts, water is heated to 80 ℃, and constant temperature stirs 20min; Then, be cooled to 50 ℃, add 5 parts big particle diameter emulsified silicone oils, 1.5 parts of Radix Notoginseng extract B, constant temperature stirs 20nin; Treat that temperature is down to below 45 ℃, add 0.7 part of essence, 0.15 portion of antiseptic and 1.7 parts of sodium chloride stir; Regulating pH value is 5.8, still aging 48 hours, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 32: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.3 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 14 parts of laureth sulfuric ester ammoniums, 2 parts of sodium lauryl sulphates, 1 part of polyquaternary ammonium salt-43,2 parts of polyquaternary ammonium salt-10,3 parts of coconut oleoyl amine MEA, 2 parts of fatty alcohol-polyoxyethylene ether, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 portion of polyquaternary ammonium salt-7,1 portion pearling agent is supplied deionized water and is made its ratio reach 60 parts, water is heated to 75 ℃, and constant temperature stirs 20min; Then, be cooled to 50 ℃, add 3 parts big particle diameter emulsified silicone oils, 1 part of Radix Notoginseng extract B, constant temperature stirs 20nin; Treat that temperature is down to below 45 ℃, add 0.4 part of essence, 0.1 portion of antiseptic and 1.5 parts of sodium chloride stir; Regulating pH value is 5.8, still aging 48 hours, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 33: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.3 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 parts of laureth sulfuric ester ammoniums, 1 part of lauryl alcohol sulfuric ester ammonium, 1 part of polyquaternary ammonium salt-43,1 part of polyquaternary ammonium salt-10,2 parts of cocamido propyl betaine, 1 part of alkyl polyglucoside, 0.8 part of lauric acid amide of ethanol, 0.8 part docosyl hydroxypropyl quaternary ammonium salt, 0.8 portion polyquaternary ammonium salt-7,0.8 portion pearling agent is supplied deionized water and is made its ratio reach 40 parts, be heated to 75 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 0.8 part of Radix Notoginseng extract B, constant temperature stirs 30nin; Treating that temperature is down to below 45 ℃ adds 0.2 part of essence, and 0.05 portion of antiseptic and 1 part of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 34: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 16 parts of laureth sulfuric ester ammoniums, 3 parts of lauryl alcohol sulfuric ester ammoniums, 3 parts of polyquaternary ammonium salt-43,3 parts of polyquaternary ammonium salt-10,5 parts of cocamido propyl betaine, 3 parts of alkyl polyglucoside, 1.5 parts of lauric acid amide of ethanol, 1.5 part docosyl hydroxypropyl quaternary ammonium salt, 1.5 portion polyquaternary ammonium salt-7,1.5 portion pearling agent is supplied deionized water and is made its ratio reach 80 parts, be heated to 85 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.7 parts of polydimethylsiloxane, 1.7 parts of dimethiconols, 1.5 parts of Radix Notoginseng extract B, constant temperature stirs 30nin; Treating that temperature is down to below 45 ℃ adds 0.4 part of essence, and 0.15 portion of antiseptic and 1.5 parts of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 35: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.4 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 14 parts of laureth sulfuric ester ammoniums, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 parts of polyquaternary ammonium salt-10,3 parts of cocamido propyl betaine, 2 parts of alkyl polyglucoside, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 portion of polyquaternary ammonium salt-7,1 portion pearling agent is supplied deionized water and is made its ratio reach 60 parts, be heated to 80 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.5 parts of polydimethylsiloxane, 1.5 parts of dimethiconols, 1 part of Radix Notoginseng extract B, constant temperature stirs 30nin; Treating that temperature is down to below 45 ℃ adds 0.3 part of essence, and 0.1 portion of antiseptic and 1.3 parts of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 36: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.3 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 parts of laureth sulfuric ester ammoniums, 1 part of lauryl alcohol sulfuric ester ammonium, 1 part of polyquaternary ammonium salt-43,1 part of polyquaternary ammonium salt-10,2 parts of cocamido propyl betaine, 1 part of coconut oleoyl amine MEA, 0.8 part of coconut oil single ethanol amide, 0.8 part docosyl hydroxypropyl quaternary ammonium salt, 0.8 portion polyquaternary ammonium salt-7,0.8 portion pearling agent is supplied deionized water and is made its ratio reach 40 parts, be heated to 75 ℃, constant temperature stirs 20min; Then, be cooled to 65 ℃, add 1.3 parts of polydimethylsiloxane, 1 part of dimethiconol, 0.8 part of Radix Notoginseng extract C, constant temperature stirs 30nin; Treating that temperature is down to below 45 ℃ adds 0.2 part of essence, and 0.05 portion of antiseptic and 1 part of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 37: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 16 parts of laureth sulfuric ester ammoniums, 3 parts of lauryl alcohol sulfuric ester ammoniums, 3 parts of polyquaternary ammonium salt-43,3 parts of polyquaternary ammonium salt-10,5 parts of cocamido propyl betaine, 3 parts of coconut oleoyl amine MEA, 1.5 parts of coconut oil single ethanol amides, 1.5 part docosyl hydroxypropyl quaternary ammonium salt, 1.5 portion polyquaternary ammonium salt-7,1.5 portion pearling agent is supplied deionized water and is made its ratio reach 80 parts, be heated to 85 ℃, constant temperature stirs 20min; Then, be cooled to 65 ℃, add 1.6 parts of polydimethylsiloxane, 1.4 parts of dimethiconols, 1.5 parts of Radix Notoginseng extract C, constant temperature stirs 30nin; Treating that temperature is down to below 45 ℃ adds 0.4 part of essence, and 0.15 portion of antiseptic and 1.5 parts of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 38: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.4 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 14 parts of laureth sulfuric ester ammoniums, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 parts of polyquaternary ammonium salt-10,3 parts of cocamido propyl betaine, 2 parts of coconut oleoyl amine MEA, 1 part of coconut oil single ethanol amide, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 portion of polyquaternary ammonium salt-7,1 portion pearling agent is supplied deionized water and is made its ratio reach 70 parts, be heated to 80 ℃, constant temperature stirs 20min; Then, be cooled to 65 ℃, add 1.4 parts of polydimethylsiloxane, 1.2 parts of dimethiconols, 1 part of Radix Notoginseng extract C, constant temperature stirs 30nin; Treating that temperature is down to below 45 ℃ adds 0.3 part of essence, and 0.1 portion of antiseptic and 1.3 parts of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 39: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of fatty alcohol-polyoxyethylene ether, 0.8 ~ 1.5 parts of alkyl polyglucoside, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,0.8 ~ 1.5 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, be heated to 80 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.1 ~ 1.4 parts of polydimethylsiloxane, 1.2 ~ 1.5 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract D, constant temperature stirs 30nin; Treating that temperature is down to adds 0.2 ~ 0.4 part of essence below 45 ℃, 0.05 ~ 0.15 portion of antiseptic and 0.8 ~ 1.5 part of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 40: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of fatty alcohol-polyoxyethylene ether, 0.8 ~ 1.5 parts of alkyl polyglucoside, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,0.8 ~ 1.5 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, be heated to 80 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.1 ~ 1.4 parts of polydimethylsiloxane, 1.2 ~ 1.5 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract D, constant temperature stirs 30nin; Treating that temperature is down to adds 0.2 ~ 0.4 part of essence below 45 ℃, 0.05 ~ 0.15 portion of antiseptic and 0.8 ~ 1.5 part of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 41: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.4 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 14 parts of laureth sulfuric ester ammoniums, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 parts of polyquaternary ammonium salt-10,3 parts of cocamido propyl betaine, 2 parts of fatty alcohol-polyoxyethylene ether, 1 part of alkyl polyglucoside, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 portion of polyquaternary ammonium salt-7,1 portion pearling agent is supplied deionized water and is made its ratio reach 60 parts, be heated to 80 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 1 part of Radix Notoginseng extract D, constant temperature stirs 30nin; Treating that temperature is down to below 45 ℃ adds 0.3 part of essence, and 0.1 portion of antiseptic and 1 part of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 42: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.4 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 14 parts of laureth sulfuric ester ammoniums, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 parts of polyquaternary ammonium salt-10,3 parts of dodecanamide propyl betanins, 2 parts of fatty alcohol-polyoxyethylene ether, 1 part of alkyl polyglucoside, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 portion of polyquaternary ammonium salt-7,1 portion pearling agent is supplied deionized water and is made its ratio reach 60 parts, be heated to 80 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 1 part of Radix Notoginseng extract D, constant temperature stirs 30nin; Treating that temperature is down to below 45 ℃ adds 0.3 part of essence, and 0.1 portion of antiseptic and 1 part of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 43: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 16 parts of laureth sulfuric ester ammoniums, 3 parts of aliphatic acid polyethenoxy ether sodium sulfate, 3 parts of polyquaternary ammonium salt-43,3 parts of polyquaternary ammonium salt-10,5 parts of cocamido propyl betaine, 3 parts of coconut oleoyl amine MEA, 1.5 parts of coconut oil single ethanol amides, 1.5 part docosyl hydroxypropyl quaternary ammonium salt, 1.5 portion polyquaternary ammonium salt-7,1.5 portion pearling agent is supplied deionized water and is made its ratio reach 80 parts, be heated to 85 ℃, constant temperature stirs 20min; Then, be cooled to 65 ℃, add 1.6 parts of polydimethylsiloxane, 1.4 parts of dimethiconols, 1.5 parts of Radix Notoginseng extract C, constant temperature stirs 30nin; Treating that temperature is down to below 45 ℃ adds 0.4 part of essence, and 0.15 portion of antiseptic and 1.5 parts of sodium chloride stir; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Embodiment 44: a kind of preparation method that contains the shampoo of arasaponin, as different from Example 23: the described second step processing technology:
Ratio by weight:
(1) heat 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 16 parts of laureth sulfuric ester ammoniums, 3 parts of aliphatic acid polyethenoxy ether sodium sulfate, 3 parts of polyquaternary ammonium salt-43,3 parts of polyquaternary ammonium salt-10,5 parts of cocamido propyl betaine, 3 parts of coconut oleoyl amine MEA, 1.5 parts of coconut oil single ethanol amides, 1.5 part docosyl hydroxypropyl quaternary ammonium salt, 1.5 portion polyquaternary ammonium salt-7,1.5 portion pearling agent is supplied deionized water and is made its ratio reach 80 parts, be heated to 85 ℃, constant temperature stirs 20min; Then, be cooled to 65 ℃, add 1.6 parts of polydimethylsiloxane, 1.4 parts of dimethiconols, 1.5 parts of Radix Notoginseng extract C, constant temperature stirs 30nin; Treating that temperature is down to below 45 ℃ adds 0.4 part of essence, and 0.15 portion of antiseptic adopts in the ripple nurse and thickening; Regulating pH value is 6.0, gets product other parts and embodiment 23 identical no longer repeated descriptions.
Without departing from the present invention, can also carry out various conversion and be equal to replacement patent of the present invention, therefore, patent of the present invention is not limited to disclosed specific implementation process, and should comprise the whole embodiments that fall in the Patent right requirement scope of the present invention.
Claims (12)
1.
A kind ofContain the shampoo of arasaponin, it is characterized in that, comprise the raw material of following weight parts ratio: 12～22 parts of anion surfactants, 1～10 part of non-ionic surface active agent, 0～7 part of zwitterionic surfactant, 1.8～10 parts of cationic surfactants, 3.6 ~ 12 parts of conditioners, 0.5～10 part of Radix Notoginseng extract, 0.8～2 part of pearling agent, thickening agent 0.8～2,0.03～0.15 part of antiseptic, 0.1～0.7 part in essence, 0.8 ~ 1.7 part in sodium chloride, 40～80 parts of deionized waters.
2. a kind of shampoo that contains arasaponin according to claim 1 and 2 is characterized in that, described Radix Notoginseng extract is the water of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng or extractum or the solid content of alcohol extraction.
3. a kind of shampoo that contains arasaponin according to claim 1 is characterized in that described Radix Notoginseng extract comprises: the mixing of one or more in four kinds of the extract A, extract B, extract C, extract D, and preparation method is:
(1) get one or more mixing of an amount of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio that adds 6～12L according to per kilogram adds water, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, filtered, concentrated extracting solution is measured relative density and is 1.0～1.5 and get final product, then in the time of 60 ℃, the adding alcoholic strength is 50%～70% ethanol, leave standstill and make its precipitation more than 12 hours, reclaim ethanol, concentrate, drying namely gets extract A;
(2) with the extract A water dissolution, last ion exchange resin column is 50%～70% ethanol elution with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrates drying; Namely get extract B;
(3) get one or more mixing of an amount of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, it is 50%～80% ethanol that the ratio that adds 6～12L according to per kilogram adds alcoholic strength, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, was collected ethanol extract, in above-mentioned medicinal residues, the ratio that adds 6～12L according to per kilogram adds water, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, reclaims ethanol, concentrates, drying namely gets extract C;
(4) with the extract C water dissolution, last ion exchange resin column is 50%～70% ethanol elution with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrates, and drying namely gets extract D.
4. a kind of shampoo that contains arasaponin according to claim 1, it is characterized in that described anion surfactant is selected from one or more the mixing in laureth sulfuric ester ammonium, lauryl alcohol sulfuric ester ammonium, sodium lauryl sulphate, coconut oleoyl amine sodium isethionate or the polyoxyethylenated alcohol sodium sulfate; Cationic surfactant is selected from polyquaternary ammonium salt-43, the mixing of one or more in polyquaternary ammonium salt-51 or the polyquaternary ammonium salt-10; Zwitterionic surfactant is selected from cocoamido propyl hydroxy sulfobetaine, the mixing of one or more in cocamido propyl betaine or the dodecanamide propyl betanin; Non-ionic surface active agent is selected from alkyl polyglucoside, fatty alcohol-polyoxyethylene ether, the mixing of one or more in lauric acid amide of ethanol or the coconut oil single ethanol amide; Conditioner is selected from cation guar gum, docosyl hydroxypropyl quaternary ammonium salt, polyquaternary ammonium salt-7, emulsified silicone oil, the mixing of one or more in polydimethylsiloxane or the dimethiconol; Thickening agent is in the carbomer and thickening or the direct thickening of sodium chloride.
5. a preparation method that contains the shampoo of arasaponin is characterized in that, may further comprise the steps:
The first step: get the raw materials ready
(1) Radix Notoginseng extract: be the water of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng or extractum or the solid content of alcohol extraction;
This Radix Notoginseng extract comprises: the mixing of one or more in four kinds of the extract A, extract B, extract C, extract D, and preparation method is:
(1) get one or more mixing of an amount of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio that adds 6～12L according to per kilogram adds water, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, filtered, concentrated extracting solution is measured relative density and is 1.0～1.5 and get final product, then in the time of 60 ℃, the adding alcoholic strength is 50%～70% ethanol, leave standstill and make its precipitation more than 12 hours, reclaim ethanol, concentrate, drying namely gets extract A;
(2) with the extract A water dissolution, last ion exchange resin column is 50%～70% ethanol elution with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrates drying; Namely get extract B;
(3) get one or more mixing of an amount of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, it is 50%～80% ethanol that the ratio that adds 6～12L according to per kilogram adds alcoholic strength, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, was collected ethanol extract, in above-mentioned medicinal residues, the ratio that adds 6～12L according to per kilogram adds water, and hot reflux is extracted 2～3 times, each 1～3 hour, merge extractive liquid, reclaims ethanol, concentrates, drying namely gets extract C;
(4) with the extract C water dissolution, last ion exchange resin column is 50%～70% ethanol elution with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrates, and drying namely gets extract D;
(2) anion surfactant: be selected from one or more the mixing in laureth sulfuric ester ammonium, lauryl alcohol sulfuric ester ammonium, sodium lauryl sulphate, coconut oleoyl amine sodium isethionate or the polyoxyethylenated alcohol sodium sulfate;
(3) cationic surfactant: be selected from polyquaternary ammonium salt-43, the mixing of one or more in polyquaternary ammonium salt-51 or the polyquaternary ammonium salt-10;
(4) zwitterionic surfactant: be selected from cocoamido propyl hydroxy sulfobetaine, the mixing of one or more in cocamido propyl betaine or the dodecanamide propyl betanin;
(5) non-ionic surface active agent: be selected from alkyl polyglucoside, fatty alcohol-polyoxyethylene ether, coconut oleoyl amine MEA, the mixing of one or more in lauric acid amide of ethanol or the coconut oil single ethanol amide;
(6) conditioner: be selected from cation guar gum, docosyl hydroxypropyl quaternary ammonium salt, polyquaternary ammonium salt-7, emulsified silicone oil, one or more mixing in polydimethylsiloxane or the dimethiconol; Emulsified silicone oil is selected from big particle diameter emulsified silicone oil and small particle diameter emulsified silicone oil, perhaps uses one for two kinds;
(7) thickening agent: in the carbomer and thickening or the direct thickening of sodium chloride;
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12～22 parts of anion surfactants, 1.8～10 parts of cationic surfactants, 1～10 part of non-ionic surface active agent, 0～7 part of amphoteric surfactant, 3.6 ~ 12 parts of conditioners, 0.8～2 part of pearling agent, 0.8～2 part of thickening agent, supplying deionized water makes its ratio reach 40～80 parts, to being heated to 50～80 ℃, constant temperature stirs 10～50min; Then, be cooled to 30～60 ℃, 0.5～10 part of Radix Notoginseng extract, constant temperature stirs 10～50min; Treating that temperature is down to below 45 ℃ adds 0.1～0.7 part in essence, 0.8 ~ 1.7 part in 0.03～0.15 part of antiseptic and sodium chloride; At last, regulating pH value is 5.8～6.0, still aging 0～48 hour, gets product.
6. a kind of preparation method that contains the shampoo of arasaponin according to claim 5 is characterized in that, and is described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 6 ~ 10 parts of laureth sulfuric ester ammoniums, 6 ~ 7 parts of lauryl alcohol sulfuric ester ammoniums, 0.7 ~ 0.9 part of polyquaternary ammonium salt-10,1 ~ 3 part of polyquaternary ammonium salt-51,2 ~ 5 parts of cocoamido propyl hydroxy sulfobetaine, 1 ~ 3 part of alkyl polyglucoside, 0.8 ~ 2 parts of fatty alcohol-polyoxyethylene ether, 1 ~ 3 part of docosyl hydroxypropyl quaternary ammonium salt, 0.5 ~ 2 portions of polyquaternary ammonium salt-7,1.3 ~ 1.7 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, be heated to 70 ~ 80 ℃, constant temperature stirs 20min; Then, be cooled to 50 ℃, 2 ~ 5 parts of emulsified silicone oils, 1 ~ 4 part of Radix Notoginseng extract, constant temperature stirs 20min; Treating that temperature is down to below 45 ℃ adds 0.1 ~ 0.4 part in essence, and 1 ~ 3 part in 0.05 ~ 0.07 portion of antiseptic and sodium chloride stir; Regulating pH value is 6.2, still aging 24 hours, gets product.
7. a kind of preparation method that contains the shampoo of arasaponin according to claim 5 is characterized in that, and is described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 10 ~ 15 parts of laureth sulfuric ester ammoniums, 5 ~ 7 parts of coconut oleoyl amine sodium isethionates, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-51,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of coconut oil single ethanol amide, 0.8 ~ 1.5 parts of lauric acid amide of ethanol, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,1.3 ~ 1.7 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, be heated to 70 ~ 80 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.3 ~ 1.7 parts of polydimethylsiloxane, 1.3 ~ 1.7 parts of emulsified silicone oils, 1.3 ~ 1.7 parts of Radix Notoginseng extracts, constant temperature stirs 30nin; Treating that temperature is down to adds 0.1 ~ 0.4 part of essence below 40 ℃, 0.03 ~ 0.1 portion of antiseptic and 1.3 ~ 1.7 parts of sodium chloride stir; Regulating pH value is 5.8, still aging 36 hours, gets product.
8. a kind of preparation method that contains the shampoo of arasaponin according to claim 5 is characterized in that, and is described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 ~ 16 parts of sodium lauryl sulphates, 2 ~ 5 parts of coconut oleoyl amine sodium isethionates, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of coconut oil single ethanol amide, 0.8 ~ 1.5 parts of lauric acid amide of ethanol, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,0.8 ~ 1.5 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, water is heated to 70 ~ 80 ℃, and constant temperature stirs 20min; Then, be cooled to 50 ℃, add 1.3 ~ 1.7 parts of polydimethylsiloxane, 1.3 ~ 1.7 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract constant temperature stirs 30nin; Treating that temperature is down to adds 0.3 ~ 0.5 part of essence below 45 ℃, 0.05 ~ 0.15 portion of antiseptic and 1.3 ~ 1.7 parts of sodium chloride stir; Regulating pH value is 6.0, gets product.
9. a kind of preparation method that contains the shampoo of arasaponin according to claim 5 is characterized in that, and is described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of sodium lauryl sulphate, 0.8 ~ 1.5 parts of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-10,2 ~ 5 parts of coconut oleoyl amine MEA, 1 ~ 3 part of fatty alcohol-polyoxyethylene ether, 0.8 ~ 1.5 parts of lauric acid amide of ethanol, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,0.8 ~ 1.5 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, water is heated to 70 ~ 80 ℃, and constant temperature stirs 20min; Then, be cooled to 50 ℃, add 2 ~ 5 parts of emulsified silicone oils, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 20nin; Treat that temperature is down to below 45 ℃, add 0.3 ~ 0.7 part of essence, 0.05 ~ 0.15 portion of antiseptic and 1.3 ~ 1.7 parts of sodium chloride stir; Regulating pH value is 5.8, still aging 48 hours, gets product.
10. a kind of preparation method that contains the shampoo of arasaponin according to claim 5 is characterized in that, and is described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of alkyl polyglucoside, 0.8 ~ 1.5 parts of lauric acid amide of ethanol, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,0.8 ~ 1.5 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, be heated to 75 ~ 85 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.3 ~ 1.7 parts of polydimethylsiloxane, 1.3 ~ 1.7 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 30nin; Treating that temperature is down to adds 0.2 ~ 0.4 part of essence below 45 ℃, 0.05 ~ 0.15 portion of antiseptic and 1 ~ 1.5 part of sodium chloride stir; Regulating pH value is 6.0, gets product.
11. a kind of preparation method that contains the shampoo of arasaponin according to claim 5 is characterized in that, and is described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of coconut oleoyl amine MEA, 0.8 ~ 1.5 parts of coconut oil single ethanol amides, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,0.8 ~ 1.5 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, be heated to 75 ~ 85 ℃, constant temperature stirs 20min; Then, be cooled to 65 ℃, add 1.3 ~ 1.6 parts of polydimethylsiloxane, 1 ~ 1.4 part of dimethiconol, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 30nin; Treating that temperature is down to adds 0.2 ~ 0.4 part of essence below 45 ℃, 0.05 ~ 0.15 portion of antiseptic and 1 ~ 1.5 part of sodium chloride stir; Regulating pH value is 6.0, gets product.
12. a kind of preparation method that contains the shampoo of arasaponin according to claim 5 is characterized in that, and is described
Second step: processing technology;
Ratio by weight:
(1) heat 0.3 ~ 0.6 part of cation melon glue scattered standby with deionized water;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of fatty alcohol-polyoxyethylene ether, 0.8 ~ 1.5 parts of alkyl polyglucoside, 0.8 ~ 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 0.8 ~ 1.5 portions of polyquaternary ammonium salt-7,0.8 ~ 1.5 portion pearling agents are supplied deionized water and are made its ratio reach 40～80 parts, be heated to 80 ℃, constant temperature stirs 20min; Then, be cooled to 60 ℃, add 1.1 ~ 1.4 parts of polydimethylsiloxane, 1.2 ~ 1.5 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 30nin; Treating that temperature is down to adds 0.2 ~ 0.4 part of essence below 45 ℃, 0.05 ~ 0.15 portion of antiseptic and 0.8 ~ 1.5 part of sodium chloride stir; Regulating pH value is 6.0, gets product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310206594.7A CN103251541B (en) | 2013-05-30 | 2013-05-30 | A kind of shampoo containing arasaponin and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310206594.7A CN103251541B (en) | 2013-05-30 | 2013-05-30 | A kind of shampoo containing arasaponin and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103251541A true CN103251541A (en) | 2013-08-21 |
| CN103251541B CN103251541B (en) | 2016-01-13 |
Family
ID=48955986
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310206594.7A Active CN103251541B (en) | 2013-05-30 | 2013-05-30 | A kind of shampoo containing arasaponin and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103251541B (en) |
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103506051A (en) * | 2013-07-22 | 2014-01-15 | 广州环亚化妆品科技有限公司 | Preparation method of plant surface active agent composition and application of the composition to washing supplies |
| CN104434656A (en) * | 2014-11-20 | 2015-03-25 | 云南人羞花化妆品有限公司 | Pseudo-ginseng shampoo and preparation method thereof |
| CN104434657A (en) * | 2014-11-20 | 2015-03-25 | 云南人羞花化妆品有限公司 | Pseudo-ginseng and walnut green seedcase hair-blacking solution and preparation method thereof |
| CN106265261A (en) * | 2016-08-16 | 2017-01-04 | 南通蛇类治疗研究所 | Plant nutrient extract for washing hair |
| CN106389154A (en) * | 2016-10-25 | 2017-02-15 | 澳宝化妆品（惠州）有限公司 | Multi-effect balanced shampoo and preparation method thereof |
| CN106619271A (en) * | 2016-10-19 | 2017-05-10 | 重庆市五洁新材料有限公司 | Liquid shampoo for children and preparation method of liquid shampoo |
| CN106726704A (en) * | 2016-12-25 | 2017-05-31 | 江西宜信堂医疗科技有限公司 | A kind of sterilization shampoo and preparation method thereof |
| CN107485590A (en) * | 2017-07-29 | 2017-12-19 | 兴仁县引力农产品加工商贸有限责任公司 | A kind of shampoo containing adlay rice extracts |
| CN108815088A (en) * | 2018-09-18 | 2018-11-16 | 云南邦乐生物科技有限公司 | A kind of phalacrosis prevention and hair generation shampoo and preparation method thereof |
| CN111374912A (en) * | 2018-12-28 | 2020-07-07 | 上海瑞帝安生物科技有限公司 | A composition for promoting hair growth |
| CN111494286A (en) * | 2020-06-15 | 2020-08-07 | 广州头道医药生物科技有限公司 | Alopecia-stopping and hair-growing shampoo |
| US11116220B2 (en) | 2017-12-22 | 2021-09-14 | Ecolab Usa Inc. | Antimicrobial compositions with enhanced efficacy |
| US11202747B2 (en) | 2016-04-08 | 2021-12-21 | Innospec Limited | Compositions with acylisethionate surfactant and methods of use |
| CN115590804A (en) * | 2022-11-02 | 2023-01-13 | 温州大学（Cn） | Shampoo containing traditional Chinese medicine extract |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1114556A (en) * | 1994-07-02 | 1996-01-10 | 重庆奥妮化妆品有限公司(中外合资) | Shampoo containing nutritive dandruff-removing antipruritic traditional Chinese medicine additive |
| US5663160A (en) * | 1992-09-17 | 1997-09-02 | Lvmh Recherche | Cosmetic or dermatological composition containing at least one saponin of the ginsenoside type, and its applications, especially for treating the hair |
| CN1334267A (en) * | 2001-06-28 | 2002-02-06 | 中国科学院昆明植物研究所 | Process for preparing total sanchinoside |
| CN101352516A (en) * | 2008-09-10 | 2009-01-28 | 周小萍 | Safety high-efficient pilatory and preparation method |
| JP2009114082A (en) * | 2007-11-02 | 2009-05-28 | Maruzen Pharmaceut Co Ltd | Hair papilla cell proliferation promoter, fibroblast growth factor-7 (fgf-7) production promoter, vascular endothelial growth factor (vegf) production promoter, antiandrogenic agent, hair grower and hair cosmetic |
| CN102210644A (en) * | 2011-06-11 | 2011-10-12 | 董家华 | APG (alkyl polyglucoside) plant environmentally-friendly shampoo |
| CN102274260A (en) * | 2011-08-09 | 2011-12-14 | 北京中海康医药科技发展有限公司 | Medicinal composition of notoginseng root extract and preparation method thereof |
| KR20120034300A (en) * | 2010-10-01 | 2012-04-12 | 주식회사 래디안 | Composition for promoting growth of hair |
| CN102885740A (en) * | 2012-10-22 | 2013-01-23 | 广州立白企业集团有限公司 | Hair cleanser containing no dioxane residue and preparation method of hair cleanser |
-
2013
- 2013-05-30 CN CN201310206594.7A patent/CN103251541B/en active Active
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5663160A (en) * | 1992-09-17 | 1997-09-02 | Lvmh Recherche | Cosmetic or dermatological composition containing at least one saponin of the ginsenoside type, and its applications, especially for treating the hair |
| CN1114556A (en) * | 1994-07-02 | 1996-01-10 | 重庆奥妮化妆品有限公司(中外合资) | Shampoo containing nutritive dandruff-removing antipruritic traditional Chinese medicine additive |
| CN1334267A (en) * | 2001-06-28 | 2002-02-06 | 中国科学院昆明植物研究所 | Process for preparing total sanchinoside |
| JP2009114082A (en) * | 2007-11-02 | 2009-05-28 | Maruzen Pharmaceut Co Ltd | Hair papilla cell proliferation promoter, fibroblast growth factor-7 (fgf-7) production promoter, vascular endothelial growth factor (vegf) production promoter, antiandrogenic agent, hair grower and hair cosmetic |
| CN101352516A (en) * | 2008-09-10 | 2009-01-28 | 周小萍 | Safety high-efficient pilatory and preparation method |
| KR20120034300A (en) * | 2010-10-01 | 2012-04-12 | 주식회사 래디안 | Composition for promoting growth of hair |
| CN102210644A (en) * | 2011-06-11 | 2011-10-12 | 董家华 | APG (alkyl polyglucoside) plant environmentally-friendly shampoo |
| CN102274260A (en) * | 2011-08-09 | 2011-12-14 | 北京中海康医药科技发展有限公司 | Medicinal composition of notoginseng root extract and preparation method thereof |
| CN102885740A (en) * | 2012-10-22 | 2013-01-23 | 广州立白企业集团有限公司 | Hair cleanser containing no dioxane residue and preparation method of hair cleanser |
Non-Patent Citations (1)
| Title |
|---|
| 钟振声 等: "《表面活性剂在化妆品中的应用》", 31 August 2003, article "《洗发香波的配方设计与生产工艺》", pages: 350-366 * |
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103506051A (en) * | 2013-07-22 | 2014-01-15 | 广州环亚化妆品科技有限公司 | Preparation method of plant surface active agent composition and application of the composition to washing supplies |
| CN104434657B (en) * | 2014-11-20 | 2018-04-06 | 云南人羞花化妆品有限公司 | A kind of pseudo-ginseng green peel of walnut hair blackening liquid and preparation method thereof |
| CN104434656A (en) * | 2014-11-20 | 2015-03-25 | 云南人羞花化妆品有限公司 | Pseudo-ginseng shampoo and preparation method thereof |
| CN104434657A (en) * | 2014-11-20 | 2015-03-25 | 云南人羞花化妆品有限公司 | Pseudo-ginseng and walnut green seedcase hair-blacking solution and preparation method thereof |
| CN104434656B (en) * | 2014-11-20 | 2018-07-13 | 云南人羞花化妆品有限公司 | A kind of Radix Notoginseng shampoo and preparation method thereof |
| US11202747B2 (en) | 2016-04-08 | 2021-12-21 | Innospec Limited | Compositions with acylisethionate surfactant and methods of use |
| CN106265261A (en) * | 2016-08-16 | 2017-01-04 | 南通蛇类治疗研究所 | Plant nutrient extract for washing hair |
| CN106619271A (en) * | 2016-10-19 | 2017-05-10 | 重庆市五洁新材料有限公司 | Liquid shampoo for children and preparation method of liquid shampoo |
| CN106389154A (en) * | 2016-10-25 | 2017-02-15 | 澳宝化妆品（惠州）有限公司 | Multi-effect balanced shampoo and preparation method thereof |
| CN106726704A (en) * | 2016-12-25 | 2017-05-31 | 江西宜信堂医疗科技有限公司 | A kind of sterilization shampoo and preparation method thereof |
| CN107485590A (en) * | 2017-07-29 | 2017-12-19 | 兴仁县引力农产品加工商贸有限责任公司 | A kind of shampoo containing adlay rice extracts |
| US11116220B2 (en) | 2017-12-22 | 2021-09-14 | Ecolab Usa Inc. | Antimicrobial compositions with enhanced efficacy |
| US11930819B2 (en) | 2017-12-22 | 2024-03-19 | Ecolab Usa Inc. | Antimicrobial compositions with enhanced efficacy |
| CN108815088A (en) * | 2018-09-18 | 2018-11-16 | 云南邦乐生物科技有限公司 | A kind of phalacrosis prevention and hair generation shampoo and preparation method thereof |
| CN111374912A (en) * | 2018-12-28 | 2020-07-07 | 上海瑞帝安生物科技有限公司 | A composition for promoting hair growth |
| CN111494286A (en) * | 2020-06-15 | 2020-08-07 | 广州头道医药生物科技有限公司 | Alopecia-stopping and hair-growing shampoo |
| CN115590804A (en) * | 2022-11-02 | 2023-01-13 | 温州大学（Cn） | Shampoo containing traditional Chinese medicine extract |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103251541B (en) | 2016-01-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103251541B (en) | A kind of shampoo containing arasaponin and preparation method thereof | |
| CN102133162B (en) | Anti-dropping and hair reviving shampoo and preparation method thereof | |
| CN100448426C (en) | All-effect liquid shampoo | |
| CN102614102B (en) | Dandruff-removing medicinal composition and preparation method thereof | |
| CN105078850A (en) | Liquid shampoo and preparation method thereof | |
| CN102038626B (en) | Traditional Chinese medicinal hair-restoring and anti-alopecia shampoo and preparation method thereof | |
| CN103784358A (en) | Shampoo | |
| CN107496317B (en) | Repairing and nursing shampoo containing periplaneta americana active ingredient | |
| CN103877550A (en) | Herbal hair growth solution and shampoo prepared by same | |
| CN103877549A (en) | Hair growth liquid taking fresh gingers as main component | |
| CN102688165A (en) | Anti-hair loss shampoo containing Chinese herbal medicines | |
| CN103933508A (en) | Hair regenerator of sharing chills and fever medicines and preparation method thereof | |
| CN102232917A (en) | Use of traditional Chinese drug compound extract in preparing whitening and moisturizing products | |
| CN108434051B (en) | Traditional Chinese medicine for percutaneous absorption of hair follicle, preparation method and application in shampoo | |
| CN102755280B (en) | Chinese herbal medicine shampoo and preparation method thereof | |
| CN114224807A (en) | Shampoo containing Chinese honeylocust fruits and bitter apricot seeds and preparation method thereof | |
| CN108815088A (en) | A kind of phalacrosis prevention and hair generation shampoo and preparation method thereof | |
| CN112494407A (en) | Composition for preventing hair loss and nourishing hair and preparation method thereof | |
| CN105168074A (en) | Antidandruff and antipruritic traditional Chinese medicine composition and application and preparation method thereof | |
| CN109939061B (en) | Safe and non-irritant white hair blackening essence and preparation method thereof | |
| CN110693786A (en) | Traditional Chinese medicine hair care agent and preparation method thereof | |
| CN103284901B (en) | Safflower emollient care solution preparation method | |
| CN103371956A (en) | Novel honey moistening liquid shampoo | |
| CN105168041A (en) | Anti-dandruff antipruritic shampoo and preparation method thereof | |
| CN101214206A (en) | Ginsenoside whitening face cream and its manufacturing method |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB03 | Change of inventor or designer information |
Inventor after: Gao Mingju Inventor after: Wang Yin Inventor after: Huang Zhaozhong Inventor before: Zhang Peng Inventor before: Wang Yin Inventor before: Gao Mingju |
|
| COR | Change of bibliographic data | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant |