CN104434657A - Pseudo-ginseng and walnut green seedcase hair-blacking solution and preparation method thereof - Google Patents
Pseudo-ginseng and walnut green seedcase hair-blacking solution and preparation method thereof Download PDFInfo
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- CN104434657A CN104434657A CN201410666574.2A CN201410666574A CN104434657A CN 104434657 A CN104434657 A CN 104434657A CN 201410666574 A CN201410666574 A CN 201410666574A CN 104434657 A CN104434657 A CN 104434657A
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- exocarpium juglandis
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Abstract
The invention discloses a pseudo-ginseng and walnut green seedcase hair-blacking solution. The pseudo-ginseng and walnut green seedcase hair-blacking solution is composed of the following raw materials in percentage by weight: 14-18% of pseudo-ginseng saponin, 10-14% of walnut green seedcase extract, 3-5% of glycerine, 1-5% of glucopyranoside, 1-4% of sorbitol, 1-3% of 1,3-propylene glycol, 1-3% of capric betaine, 0.1-0.5% of Caisson and the balance of purified water. The pseudo-ginseng and walnut green seedcase hair-blacking solution disclosed by the invention realizes hair-blacking and hair-protecting functions by effectively proportioning pure natural medicine materials, and is safe and effective, low in skin irritation, free from toxic and side effects, and good in hair-blacking and hair-holding effects; pseudo-ginseng and walnut green seedcase are used for invigorating blood circulation, removing stasis, softening cutin and improving the toughness of hair while blacking the hair, thus enhancing hair quality; pruritus caused by various fungi in scalp can be effectively killed, and a role of improving the environment of the scalp is played; and meanwhile, waste utilization is realized, a new way is developed for walnut green seedcase treatment, and multi-way comprehensive utilization is realized, thus economic benefit, social benefits and environmental benefits are maximized.
Description
Technical field
The invention belongs to cosmetic field, relate to a kind of Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid and preparation method thereof.
Background technology
Along with the fast development of cosmetics of everyday use and the raising of people's personal consumption level, a large amount of petrochemical industry is washed and is protected in product introduction resident daily life at present.Detergent and the personal care product of the synthesis of these petrochemical industry have low price, advantage that clean result is good, but use petrochemical materials after all, not only produce and in use procedure, the water body environment such as river, lake polluted, contain the poisonous and harmful substances such as carcinogen " dioxanes ", benzene, phenol because of it, bring very large harm to health.
Exocarpium Juglandis Immaturus also known as Exocarpium Juglandis Immaturum, the thick green peel of the one deck for Semen Juglandis outside.China's Semen Juglandis cultivated area occupies first place in the world, and Exocarpium Juglandis Immaturus annual production is more than 350,000 tons.After Walnut Fruit is gathered, the Pericarpium Citri Reticulatae Viride outside nut should be taken off as early as possible.A large amount of Pericarpium Citri Reticulatae Viride become dumping in field, the edge of a field or limes marginis contaminated environment, if be used to it, not only can prevent the pollution of the environment, the income of orchard worker can also be increased.But, at present, few to the bibliographical information of the processing of Exocarpium Juglandis Immaturus, comprehensive utilization aspect both at home and abroad.
Therefore, how Exocarpium Juglandis Immaturus is incorporated in hair blackening agent, as the plant hair blackening agent of pure natural, has become the product that people urgently thirst for.
Summary of the invention
The invention provides a kind of Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid, adopt pure natural medical material to carry out black hair hair care, there is black hair, invigorate blood circulation, eliminating stagnation, horny layer softening, sterilization, parasite killing, the comprehensive effect such as antipruritic, can effectively black hair, bright, hair strengthening, anti-dandruff, little to skin irritation, have no side effect.
In order to solve the problem, the technical solution adopted in the present invention is:
A kind of Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid, be made up of the raw material of following weight percentage: arasaponin 14 ~ 18%, Exocarpium Juglandis Immaturus extractum 10 ~ 14 %, glycerol 3 ~ 5%, glucopyranoside 1 ~ 5%, sorbitol 1 ~ 4 %, 1,3-PD 1 ~ 3%, decyl betaine 1 ~ 3 %, KF88 0.1 ~ 0.5%, surplus are pure water.
According to the preferred version of Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid of the present invention, % by weight number of each crude drug is: Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid is made up of the raw material of following weight percentage: arasaponin 16%, Exocarpium Juglandis Immaturus extractum 12%, glycerol 5%, glucopyranoside 3%, sorbitol 2%, 1,3-PD 2%, decyl betaine 2%, KF88 0.2%, surplus are pure water.
The preparation method of above-mentioned Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid, is made up of following steps:
1) dilution of formula ratio glucopyranoside use 20 ~ 30% pure water of 80 ~ 90 DEG C is got, insulated and stirred 20 ~ 30 minutes;
2) add sorbitol, 1,3-PD 2%, KF88, start after stirring to be cooled to 50 DEG C;
3) be cooled to 50 DEG C and add sorbitol, glycerol, after stirring, continue cooling;
4) be cooled to 40 DEG C-45 DEG C and add arasaponin and Exocarpium Juglandis Immaturus extractum, continue to stir;
5) add after pure water stirs, leave standstill to 38 DEG C of dischargings, fill gets product.
The invention has the beneficial effects as follows:
1, the present invention adopts pure natural medical material to carry out effective proportioning and realizes black hair hair care function, safe and effective, little to skin irritation, has no side effect.
2, black hair, hair strengthening are effective, utilize Radix Notoginseng and Exocarpium Juglandis Immaturus to carry out invigorating blood circulation while black hair, eliminating stagnation, horny layer softening, improve hair toughness, thus strengthen hair quality.
3, there is sterilization, parasite killing, the comprehensive effect such as antipruritic, effectively can kill various fungus-caused pruritus in scalp, improve the effect of scalp environment.
4, realize twice laid, for new way is developed in Exocarpium Juglandis Immaturus process, make full use of resource, realize multipath comprehensive utilization, make economic benefit, social benefit, environmental benefit reach maximization.
Detailed description of the invention
embodiment 1
1, raw material:
Arasaponin 14%, Exocarpium Juglandis Immaturus extractum 10%, glycerol 3%, glucopyranoside 1%, sorbitol 1%, 1,3-PD 1%, decyl betaine 1 %, KF88 0.1%, surplus are pure water.
2, preparation method:
The preparation method of above-mentioned Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid, is made up of following steps:
1) dilution of formula ratio glucopyranoside use 20% pure water of 80 DEG C is got, insulated and stirred 20 minutes;
2) add sorbitol, 1,3-PD 2%, KF88, start after stirring to be cooled to 50 DEG C;
3) be cooled to 50 DEG C and add sorbitol, glycerol, after stirring, continue cooling;
4) be cooled to 40 DEG C-45 DEG C and add arasaponin and Exocarpium Juglandis Immaturus extractum, continue to stir;
5) add after pure water stirs, leave standstill to 38 DEG C of dischargings, fill gets product.
embodiment 2
1, raw material:
Arasaponin 18%, Exocarpium Juglandis Immaturus extractum 14 %, glycerol 5%, glucopyranoside 5%, sorbitol 4 %, 1,3-PD 3%, decyl betaine 3 %, KF88 0.5%, surplus are pure water.
2, preparation method:
The preparation method of above-mentioned Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid, is made up of following steps:
1) dilution of formula ratio glucopyranoside use 20% pure water of 80 DEG C is got, insulated and stirred 20 minutes;
2) add sorbitol, 1,3-PD 2%, KF88, start after stirring to be cooled to 50 DEG C;
3) be cooled to 50 DEG C and add sorbitol, glycerol, after stirring, continue cooling;
4) be cooled to 40 DEG C-45 DEG C and add arasaponin and Exocarpium Juglandis Immaturus extractum, continue to stir;
5) add after pure water stirs, leave standstill to 38 DEG C of dischargings, fill gets product.
embodiment 3
1, raw material:
Arasaponin 16%, Exocarpium Juglandis Immaturus extractum 12%, glycerol 5%, glucopyranoside 3 %, sorbitol 2%, 1,3-PD 2%, decyl betaine 2%, KF88 0.2%, surplus are pure water.
2, preparation method:
The preparation method of above-mentioned Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid, is made up of following steps:
1) dilution of formula ratio glucopyranoside use 20% pure water of 80 DEG C is got, insulated and stirred 20 minutes;
2) add sorbitol, 1,3-PD 2%, KF88, start after stirring to be cooled to 50 DEG C;
3) be cooled to 50 DEG C and add sorbitol, glycerol, after stirring, continue cooling;
4) be cooled to 40 DEG C-45 DEG C and add arasaponin and Exocarpium Juglandis Immaturus extractum, continue to stir;
5) add after pure water stirs, leave standstill to 38 DEG C of dischargings, fill gets product.
experimental analysis:the black hair hair strengthening experiment of black hair liquid of the present invention:
1. experiment material:
Hair sample, UV757CRT ultraviolet-uisible spectrophotometer
Experimental group A: the standard solution black hair liquid described in the present patent application being configured to variable concentrations;
Experimental group B: the standard solution commercially available common black hair liquid being configured to variable concentrations;
Cleaning mixture: take 5.000 g dodecylbenzene sodium sulfonate in the beaker of 500 mL, add 500 mL distilled water, be heated to 60 DEG C in a water bath, make it all dissolve, cooling, slowly transfers in the volumetric flask of 1000 mL, obtains the cleaning mixture of 5.000mg/mL
2, experimental technique:
Adopt spectrophotography, measure the maximum absorption wavelength of different black hair liquor, linear relationship according to absorbance and concentration makes standard curve and regression equation, with the hair after surfactant solution washing dyeing, measure the absorbance at maximum wavelength place, go out the concentration of contained hair dye in each cleaning mixture according to regression equation calculation, know its content by inference, thus predict the dyeing firmness of black hair liquid:
Get experimental group A and each 0.300g of experimental group B, the two is spread upon on 0.500g hair respectively uniformly, at 40 DEG C, constantly stirs with Glass rod, make it fully to contact with air, reaction 40min, observe color change.
The hair that dye is lustful is put in the beaker of 100ml, adds the dodecylbenzene sodium sulfonate cleaning mixture that 50mL concentration is 5.000mg/mL, and constantly stirs, and soaks 5min, outwells this cleaning mixture, with foam on the distilled water wash hair of 50mL, wash three times.In washed hair, add the cleaning mixture that 30mL concentration is 5.000mg/mL more again, constantly stir, filter after 5 minutes, filtrate is transferred in the volumetric flask of 50mL, standardize solution, obtain first time cleaning mixture.With distilled water 50mL, flush with foam on hair is clean, every 0.5h time with the washing of dodecylbenzene sodium sulfonate cleaning mixture once, stir, filter, standardize solution, successively obtain second time, for the third time, the 4th time, the 5th time, the 6th time, the 7th time cleaning mixture.Measure seven standardize solution shake up after the absorbance of solution, record the firmness after the hair dyeing of this hair dye according to the size of the absorbance measured.
3, experimental result
Above-mentioned experimental result shows, organizes A and the absorbance of experimental group B seven cleaning mixture and the contrast of concentration by experiment,
Find that absorbance and the concentration of the cleaning mixture of experimental group A are distal to experimental group B, therefore, black hair liquid pair of the present invention
Firmness after hair dyeing is better than common black hair liquid, utilizes arasaponin and Exocarpium Juglandis Immaturus extractum to carry out reasonable compatibility, will
The hair dyeing function of arasaponin to scalp and Exocarpium Juglandis Immaturus combines, and makes its Color more obvious.
experimentblack hair liquid observation of curative effect test of the present invention
For the therapeutic effect of product of the present invention to all kinds of poliosis, alopecia and dandruff is described, patient accepts the application's shampoo all voluntarily and carries out washing protecting, and refuses other treatment scheme, wherein:
Patient with grey hair (age 14-75 year): 198 examples, wherein 14-55 year: 108 examples, 56-75 year: 90 examples;
Dandruff severe patient: 93 examples; The bad person of hair quality: 106 examples.
To use this product within 30 days, to be a course for the treatment of, therapeutic effect is as follows:
As shown in table 2, patient (14-55 year) suffers from patient with grey hair the young and the middle aged to be had 108 examples, person in middle and old age to suffer from patient (56-75 year) to have 90 examples; Wherein changing white hair into black hair 175 example, poliosis turns ash gradually, turns black 20 examples, and invalid, poliosis does not improve 3 examples, total effective rate 88.38%; Dandruff severe patient amounts to 93 examples, wherein complete anti-dandruff person 85 example, the person of making moderate progress 7 example, complete nonresponder 1 example; Bad person 106 example of hair quality, total effective rate 91.39%; Hair quality changer 98 example, the person of making moderate progress 4 example, nonresponder 4 example, total effective rate 92.45%, meanwhile, in all 397 routine patients, untoward reaction only has 1 people.
The present invention adopts arasaponin and Exocarpium Juglandis Immaturus cream to carry out reasonable compatibility, hair is utilized to have good Absorption to arasaponin, arasaponin directly can enter the inside of hair fiber, the hydroxyl of saponin can generate hydrogen bond with the hydrophilic group in hair, the tensile strength of effective increase hair and extension property, obvious effect is had to improving hair quality, simultaneously, adopt Exocarpium Juglandis Immaturus cream, the coloration of Exocarpium Juglandis Immaturus can be utilized on the one hand, match with pseudo-ginseng blood-circulation-invigovating function, carry out black hair, hair strengthening, on the other hand, effectively can utilize the juglone material in Exocarpium Juglandis Immaturus, can effectively sterilize, anti-dandruff, antipruritic, improve scalp environment.
The present invention adopts pure natural medical material to carry out black hair hair care, there is black hair, invigorate blood circulation, eliminating stagnation, horny layer softening, sterilization, parasite killing, the comprehensive effect such as antipruritic, can effectively black hair, bright, hair strengthening, anti-dandruff, little to skin irritation, have no side effect.
What finally illustrate is, above preferred embodiment is only in order to illustrate technical scheme of the present invention and unrestricted, although by above preferred embodiment to invention has been detailed description, but those skilled in the art are to be understood that, various change can be made to it in the form and details, and not depart from claims of the present invention limited range.
Claims (3)
1. a Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid, it is characterized in that, Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid is made up of the raw material of following weight percentage: arasaponin 14 ~ 18%, Exocarpium Juglandis Immaturus extractum 10 ~ 14 %, glycerol 3 ~ 5%, glucopyranoside 1 ~ 5%, sorbitol 1 ~ 4 %, 1,3-PD 1 ~ 3%, decyl betaine 1 ~ 3 %, KF88 0.1 ~ 0.5%, surplus are pure water.
2. a kind of Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid according to claim 1, it is characterized in that, Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid is made up of the raw material of following weight percentage: arasaponin 16%, Exocarpium Juglandis Immaturus extractum 12%, glycerol 5%, glucopyranoside 3%, sorbitol 2%, 1,3-PD 2%, decyl betaine 2%, KF88 0.2%, surplus are pure water.
3. the preparation method of Radix Notoginseng Exocarpium Juglandis Immaturus black hair liquid according to claim 1 or 2, is characterized in that, be made up of following steps:
1) dilution of the formula ratio glucopyranoside pure water of 80 ~ 90 DEG C is got, insulated and stirred 20 ~ 30 minutes;
2) add sorbitol, 1,3-PD, KF88 by formula ratio, start after stirring to be cooled to 50 DEG C;
3) be cooled to 50 DEG C and add sorbitol, glycerol, after stirring, continue cooling;
4) be cooled to 40 DEG C-45 DEG C and add arasaponin and three Exocarpium Juglandis Immaturus extractum, continue to stir;
5) add after pure water stirs, leave standstill to 38 DEG C of dischargings, fill gets product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410666574.2A CN104434657B (en) | 2014-11-20 | 2014-11-20 | A kind of pseudo-ginseng green peel of walnut hair blackening liquid and preparation method thereof |
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| CN201410666574.2A CN104434657B (en) | 2014-11-20 | 2014-11-20 | A kind of pseudo-ginseng green peel of walnut hair blackening liquid and preparation method thereof |
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| CN104434657A true CN104434657A (en) | 2015-03-25 |
| CN104434657B CN104434657B (en) | 2018-04-06 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106511176A (en) * | 2016-12-12 | 2017-03-22 | 江城中澳农业科技发展有限公司 | Natural plant care hair blacking cream and preparation method thereof |
| CN107334666A (en) * | 2017-06-05 | 2017-11-10 | 云南摩尔农庄生物科技开发有限公司 | A kind of hair dye containing walnut green husk pigment and preparation method thereof |
| CN109498469A (en) * | 2018-11-28 | 2019-03-22 | 山东师范大学 | Black sunscreen spray of a kind of green peel of walnut hair dye and its preparation method and application |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101797217A (en) * | 2010-04-01 | 2010-08-11 | 刘全 | Method for preparing hair regrowing and blackening agent by utilizing green peel of walnut seeds |
| CN103251541A (en) * | 2013-05-30 | 2013-08-21 | 云南七丹药业股份有限公司 | Liquid shampoo containing notoginsenoside and preparation method thereof |
-
2014
- 2014-11-20 CN CN201410666574.2A patent/CN104434657B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101797217A (en) * | 2010-04-01 | 2010-08-11 | 刘全 | Method for preparing hair regrowing and blackening agent by utilizing green peel of walnut seeds |
| CN103251541A (en) * | 2013-05-30 | 2013-08-21 | 云南七丹药业股份有限公司 | Liquid shampoo containing notoginsenoside and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106511176A (en) * | 2016-12-12 | 2017-03-22 | 江城中澳农业科技发展有限公司 | Natural plant care hair blacking cream and preparation method thereof |
| CN107334666A (en) * | 2017-06-05 | 2017-11-10 | 云南摩尔农庄生物科技开发有限公司 | A kind of hair dye containing walnut green husk pigment and preparation method thereof |
| CN109498469A (en) * | 2018-11-28 | 2019-03-22 | 山东师范大学 | Black sunscreen spray of a kind of green peel of walnut hair dye and its preparation method and application |
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| CN104434657B (en) | 2018-04-06 |
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