CN104434657B - A kind of pseudo-ginseng green peel of walnut hair blackening liquid and preparation method thereof - Google Patents
A kind of pseudo-ginseng green peel of walnut hair blackening liquid and preparation method thereof Download PDFInfo
- Publication number
- CN104434657B CN104434657B CN201410666574.2A CN201410666574A CN104434657B CN 104434657 B CN104434657 B CN 104434657B CN 201410666574 A CN201410666574 A CN 201410666574A CN 104434657 B CN104434657 B CN 104434657B
- Authority
- CN
- China
- Prior art keywords
- hair
- walnut
- green peel
- pseudo
- ginseng
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a kind of pseudo-ginseng green peel of walnut hair blackening liquid, pseudo-ginseng green peel of walnut hair blackening liquid is made up of the raw material of following weight percentage：Arasaponin 14~18%,The % of green peel of walnut medicinal extract 10~14,Glycerine 3~5%,Glucopyranoside 1~5%,The % of sorbierite 1~4,1,3 propane diols 1~3%,The % of decyl betaine 1~3,KF88 0.1~0.5%,Surplus is pure water,The present invention carries out effectively proportioning using pure natural medical material and realizes black hair hair care function,Safely and effectively,It is small to skin irritation,Have no toxic side effect,Black hair,Strengthen the hair effect is good,Invigorated blood circulation using pseudo-ginseng and green peel of walnut while black hair,Dissipating bind,Cutin-softening,Improve hair toughness,So as to strengthen hair quality,Various fungus-caused itch in scalp can effectively be killed,Improve the effect of scalp environment,Simultaneously,Realize twice laid,New way is developed for green peel of walnut processing,Realize that multipath comprehensively utilizes,Make economic benefit,Social benefit,Environmental benefit reaches maximization.
Description
Technical field
The invention belongs to cosmetic field, is related to a kind of pseudo-ginseng green peel of walnut hair blackening liquid and preparation method thereof.
Background technology
With the fast development of daily chemical product and the raising of people's life consumption level, largely petrochemical industry wash shield product at present
Into in resident's daily life.The detergent of these petrochemical industry synthesis and personal care product have that cheap, clean result is good
Advantage, but petrochemical materials is used after all, not only to water body environments such as river, lakes during production and use
Pollute, because it contains the poisonous and harmful substances such as carcinogenic substance " dioxanes ", benzene, phenol, very big danger is carried out to human body health care belt
Evil.
Green peel of walnut is also known as pericarpium juglandis, is the thick green pericarp of a thickness outside walnut.China's walnut cultivated area occupies generation
Boundary is the first, and green peel of walnut annual production is more than 350,000 tons.After Walnut Fruit harvesting, the rascal outside nut should be taken off as early as possible.Greatly
Measure rascal and pollute environment in field, the edge of a field or limes marginis as dumping, if it be used, can not only prevent environment
Pollution, the income of orchard worker can also be increased.However, at present, the processing to green peel of walnut both at home and abroad, the document in terms of comprehensive utilization
Report is few.
Therefore, how green peel of walnut is incorporated into blackening agent, as pure natural plant blackening agent, has become people
The product urgently thirsted for.
The content of the invention
The present invention provides a kind of pseudo-ginseng green peel of walnut hair blackening liquid, carries out black hair hair care using pure natural medical material, has
Black hair, promoting blood circulation, dissipating bind, cutin-softening, sterilization, desinsection, antipruritic etc. integrate effect, can effectively black hair, brighten the hair, strengthen the hair, it is anti-dandruff, it is right
Skin irritation is small, has no toxic side effect.
In order to solve the above problems, the technical solution adopted in the present invention is：
A kind of pseudo-ginseng green peel of walnut hair blackening liquid, is made up of the raw material of following weight percentage：Arasaponin 14~
18%, the % of green peel of walnut medicinal extract 10~14, glycerine 3~5%, glucopyranoside 1~5%, the % of sorbierite 1~4,1,3- third
Glycol 1~3%, the % of decyl betaine 1~3, KF88 0.1~0.5%, surplus are pure water.
According to the preferred scheme of pseudo-ginseng green peel of walnut hair blackening liquid of the present invention, the weight % numbers of each bulk drug are：Pseudo-ginseng
Green peel of walnut hair blackening liquid is made up of the raw material of following weight percentage：Arasaponin 16%, green peel of walnut medicinal extract 12%, the third three
Alcohol 5%, glucopyranoside 3%, sorbierite 2%, 1,3-PD 2%, decyl betaine 2%, KF88 0.2%, surplus are pure water.
The preparation method of above-mentioned pseudo-ginseng green peel of walnut hair blackening liquid, is comprised the steps of：
1）Formula ratio glucopyranoside is taken to be diluted with 80~90 DEG C of the pure water of use 20~30%, insulated and stirred 20~30
Minute；
2）Sorbierite, 1,3-PD 2%, KF88 are added, starts to be cooled to 50 DEG C after stirring；
3）It is cooled to 50 DEG C and adds sorbierite, glycerine, continues to cool after stirring；
4）It is cooled to 40 DEG C -45 DEG C and adds arasaponin and green peel of walnut medicinal extract, continues to stir；
5）After addition pure water stirs, stand to 38 DEG C of dischargings, it is filling to get product.
The beneficial effects of the invention are as follows：
1st, the present invention realizes black hair hair care function using using pure natural medical material progress effectively proportioning, safely and effectively,
It is small to skin irritation, have no toxic side effect.
2nd, black hair, strengthen the hair effect are good, invigorated blood circulation using pseudo-ginseng and green peel of walnut while black hair, dissipating bind, softening angle
Matter, hair toughness is improved, so as to strengthen hair quality.
3rd, there is the comprehensive effect such as sterilization, desinsection, antipruritic, can effectively kill various fungus-caused itch in scalp, change
The effect of kind scalp environment.
4th, twice laid is realized, new way is developed for green peel of walnut processing, makes full use of resource, realize that multipath integrates
Utilize, economic benefit, social benefit, environmental benefit is reached maximization.
Embodiment
Embodiment 1
1st, raw material：
Arasaponin 14%, green peel of walnut medicinal extract 10%, glycerine 3%, glucopyranoside 1%, sorbierite 1%, 1,3- third
Glycol 1%, the % of decyl betaine 1, KF88 0.1%, surplus are pure water.
2nd, preparation method：
The preparation method of above-mentioned pseudo-ginseng green peel of walnut hair blackening liquid, is comprised the steps of：
1）Formula ratio glucopyranoside is taken to be diluted with 80 DEG C of the pure water of use 20%, insulated and stirred 20 minutes；
2）Sorbierite, 1,3-PD 2%, KF88 are added, starts to be cooled to 50 DEG C after stirring；
3）It is cooled to 50 DEG C and adds sorbierite, glycerine, continues to cool after stirring；
4）It is cooled to 40 DEG C -45 DEG C and adds arasaponin and green peel of walnut medicinal extract, continues to stir；
5）After addition pure water stirs, stand to 38 DEG C of dischargings, it is filling to get product.
Embodiment 2
1st, raw material：
Arasaponin 18%, the % of green peel of walnut medicinal extract 14, glycerine 5%, glucopyranoside 5%, the % of sorbierite 4,1,3-
Propane diols 3%, the % of decyl betaine 3, KF88 0.5%, surplus are pure water.
2nd, preparation method：
The preparation method of above-mentioned pseudo-ginseng green peel of walnut hair blackening liquid, is comprised the steps of：
1）Formula ratio glucopyranoside is taken to be diluted with 80 DEG C of the pure water of use 20%, insulated and stirred 20 minutes；
2）Sorbierite, 1,3-PD 2%, KF88 are added, starts to be cooled to 50 DEG C after stirring；
3）It is cooled to 50 DEG C and adds sorbierite, glycerine, continues to cool after stirring；
4）It is cooled to 40 DEG C -45 DEG C and adds arasaponin and green peel of walnut medicinal extract, continues to stir；
5）After addition pure water stirs, stand to 38 DEG C of dischargings, it is filling to get product.
Embodiment 3
1st, raw material：
Arasaponin 16%, green peel of walnut medicinal extract 12%, glycerine 5%, the % of glucopyranoside 3, sorbierite 2%, 1,3- third
Glycol 2%, decyl betaine 2%, KF88 0.2%, surplus are pure water.
2nd, preparation method：
The preparation method of above-mentioned pseudo-ginseng green peel of walnut hair blackening liquid, is comprised the steps of：
1）Formula ratio glucopyranoside is taken to be diluted with 80 DEG C of the pure water of use 20%, insulated and stirred 20 minutes；
2）Sorbierite, 1,3-PD 2%, KF88 are added, starts to be cooled to 50 DEG C after stirring；
3）It is cooled to 50 DEG C and adds sorbierite, glycerine, continues to cool after stirring；
4）It is cooled to 40 DEG C -45 DEG C and adds arasaponin and green peel of walnut medicinal extract, continues to stir；
5）After addition pure water stirs, stand to 38 DEG C of dischargings, it is filling to get product.
Experimental analysis:The black hair strengthen the hair experiment of hair blackening liquid of the present invention：
1. experiment material：
Hair sample, UV757CRT ultraviolet-uisible spectrophotometers
Experimental group A：Hair blackening liquid described in the present patent application is configured to the standard liquid of various concentrations；
Experimental group B：Commercially available common hair blackening liquid is configured to the standard liquid of various concentrations；
Cleaning solution：5.000 g neopelexes are weighed in 500 mL beaker, add 500 mL distillations
Water, 60 DEG C are heated in a water bath, it is all dissolved, cooling, be slowly transferred in 1000 mL volumetric flask, obtain
5.000mg/mL cleaning solution
2nd, experimental method：
Using AAS, the maximum absorption wavelength of different black hair liquors is measured, according to the line of absorbance and concentration
Standard curve and regression equation are made in sexual intercourse, the hair after washing dyeing with surfactant solution, measure at maximum wavelength
Absorbance, the concentration of contained hair dye in each secondary cleaning solution is gone out according to regression equation calculation, deduces its content, so as to predict black hair
The dyeing firmness of liquid：
Experimental group A and each 0.300g of experimental group B are taken, the two is uniformly applied on 0.500g hairs respectively, at 40 DEG C
Under, it is stirred continuously with glass bar, is allowed to fully contact with air, react 40min, observes color change.
The hair for contaminating lustful is put into 100ml beaker, adds the detergent alkylate that 50mL concentration is 5.000mg/mL
Sodium sulfonate cleaning solution, and be stirred continuously, 5min is soaked, this cleaning solution is outwelled, foam on hair is washed with 50mL distilled water,
Washing is three times.The cleaning solution that 30mL concentration is 5.000mg/mL is added into washed hair again, is stirred continuously, after 5 minutes
Filtering, filtrate is transferred in 50mL volumetric flask, constant volume, obtains first time cleaning solution.It will be steeped with distilled water 50mL on hair
Foam is rinsed well, be washed once every 0.5h time with neopelex cleaning solution, is stirred, filtering, constant volume, gradually
Obtain second, third time, the 4th time, the 5th time, the 6th time, the 7th cleaning solution.Measure the solution after seven constant volumes shake up
Absorbance, according to the size of the absorbance of measure measure the hair dye hair dyeing after firmness.
3rd, experimental result
It is above-mentioned test result indicates that, by the contrast of the absorbance and concentration of seven cleaning solutions of experimental group A and experimental group B,
It was found that the absorbance and concentration of experimental group A cleaning solution are distal to experimental group B, and therefore, hair blackening liquid of the present invention
It is right
Firmness after hair dyeing is better than common hair blackening liquid, is rationally matched somebody with somebody using notoginsenoside and green peel of walnut medicinal extract
5, will
Notoginsenoside is combined to the hair dyeing function of scalp and green peel of walnut, becomes apparent from its Color.
Test hair blackening liquid observation of curative effect experiment of the present invention
Product voluntarily receives the application to the therapeutic effect of all kinds of white hairs, alopecia and dandruff, patient to illustrate the invention
Shampoo carries out washing shield, and refuses other treatment schemes, wherein：
Patient with grey hair（Age 14-75 year）：198, wherein 14-55 year：108,56-75 year：90；
Dandruff severe patient：93；The bad person of hair quality：106.
To use this product 30 days as a course for the treatment of, therapeutic effect is as follows：
As shown in table 2, patient the young and the middle aged patient with grey hair（14-55 year）There are 108, person in middle and old age patient（56-
75 years old）There are 90；Wherein changing white hair into black hair 175, white hair gradually turn ash, turn black 20, and invalid, white hair does not improve
3, total effective rate 88.38%；Dandruff severe patient amounts to 93, wherein anti-dandruff person 85, the person of making moderate progress 7 are complete completely
Full nonresponder 1；The bad person of hair quality 106, total effective rate 91.39%；Hair quality changer 98, the person of making moderate progress 4 are invalid
Person 4, total effective rate 92.45%, meanwhile, in all 397 patients, adverse reaction only has 1 people.
The present invention carries out reasonable compatibility using notoginsenoside and green peel of walnut cream, has using hair to notoginsenoside good
Absorption, notoginsenoside can be directly entered the inside of hair fiber, and the hydroxyl of saponin(e can generate with the hydrophilic radical in hair
Hydrogen bond, the tensile strength and extension property of hair are effectively increased, have obvious effect to improving hair quality, meanwhile, using green peel of walnut
Cream, the coloration of green peel of walnut on the one hand can be utilized, is engaged with pseudo-ginseng blood-circulation-invigovating function, carries out black hair, strengthen the hair, the opposing party
Face, the juglone material in green peel of walnut can be effectively utilized, can effectively sterilize, be anti-dandruff, be antipruritic, improving scalp environment.
The present invention carries out black hair hair care using pure natural medical material, has black hair, promoting blood circulation, dissipating bind, cutin-softening, kills
Bacterium, desinsection, antipruritic etc. integrate effect, can effectively black hair, brighten the hair, strengthen the hair, it is anti-dandruff, it is small to skin irritation, have no toxic side effect.
Finally illustrate, preferred embodiment above is merely illustrative of the technical solution of the present invention and unrestricted, although logical
Cross above preferred embodiment the present invention is described in detail, it is to be understood by those skilled in the art that can be
Various changes are made to it in form and in details, without departing from claims of the present invention limited range.
Claims (2)
1. a kind of pseudo-ginseng green peel of walnut hair blackening liquid, it is characterised in that pseudo-ginseng green peel of walnut hair blackening liquid is by following weight percentage
Raw material composition：Arasaponin 14~18%, the % of green peel of walnut medicinal extract 10~14, glycerine 3~5%, glucopyranoside 1~
5%th, the % of sorbierite 1~4,1,3-PD 1~3%, the % of decyl betaine 1~3, KF88 0.1~0.5%, surplus are pure
Water, it is made up of following steps：
1）Formula ratio glucopyranoside is taken to be diluted with 80~90 DEG C of pure water, insulated and stirred 20~30 minutes；
2）Sorbierite, 1,3- propane diols, KF88 are added by formula ratio, starts to be cooled to 50 DEG C after stirring；
3）It is cooled to 50 DEG C and adds sorbierite, glycerine, continues to cool after stirring；
4）It is cooled to 40 DEG C -45 DEG C and adds arasaponin and three green peel of walnut medicinal extract, continues to stir；
5）After addition pure water stirs, stand to 38 DEG C of dischargings, it is filling to get product.
A kind of 2. pseudo-ginseng green peel of walnut hair blackening liquid according to claim 1, it is characterised in that pseudo-ginseng green peel of walnut black hair
Liquid is made up of the raw material of following weight percentage：Arasaponin 16%, green peel of walnut medicinal extract 12%, glycerine 5%, pyrans
Heteroside 3%, sorbierite 2%, 1,3- propane diols 2%, decyl betaine 2%, KF88 0.2%, surplus are pure water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410666574.2A CN104434657B (en) | 2014-11-20 | 2014-11-20 | A kind of pseudo-ginseng green peel of walnut hair blackening liquid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410666574.2A CN104434657B (en) | 2014-11-20 | 2014-11-20 | A kind of pseudo-ginseng green peel of walnut hair blackening liquid and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104434657A CN104434657A (en) | 2015-03-25 |
| CN104434657B true CN104434657B (en) | 2018-04-06 |
Family
ID=52881928
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410666574.2A Active CN104434657B (en) | 2014-11-20 | 2014-11-20 | A kind of pseudo-ginseng green peel of walnut hair blackening liquid and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104434657B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106511176A (en) * | 2016-12-12 | 2017-03-22 | 江城中澳农业科技发展有限公司 | Natural plant care hair blacking cream and preparation method thereof |
| CN107334666B (en) * | 2017-06-05 | 2021-04-06 | 云南摩尔农庄生物科技开发有限公司 | Hair dye containing walnut green husk pigment and preparation method thereof |
| CN109498469B (en) * | 2018-11-28 | 2022-02-08 | 山东师范大学 | Walnut green seedcase hair blackening sunscreen spray and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101797217A (en) * | 2010-04-01 | 2010-08-11 | 刘全 | Method for preparing hair regrowing and blackening agent by utilizing green peel of walnut seeds |
| CN103251541A (en) * | 2013-05-30 | 2013-08-21 | 云南七丹药业股份有限公司 | Liquid shampoo containing notoginsenoside and preparation method thereof |
-
2014
- 2014-11-20 CN CN201410666574.2A patent/CN104434657B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101797217A (en) * | 2010-04-01 | 2010-08-11 | 刘全 | Method for preparing hair regrowing and blackening agent by utilizing green peel of walnut seeds |
| CN103251541A (en) * | 2013-05-30 | 2013-08-21 | 云南七丹药业股份有限公司 | Liquid shampoo containing notoginsenoside and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104434657A (en) | 2015-03-25 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN100581536C (en) | Camellia skin-care essence oil | |
| CN107496325A (en) | Facial mask containing peony essential oil, green cucumber extract solution and snail stoste and preparation method thereof | |
| CN105662916B (en) | Composition for repairing sebum membrane | |
| CN106473996B (en) | A kind of oil-control skin anti-acne that shines repairs facial cleanser and preparation method thereof | |
| CN109350591B (en) | Dry facial mask for beautifying face and preparation method thereof | |
| CN107998028A (en) | A kind of shower cream and preparation method thereof | |
| CN104434657B (en) | A kind of pseudo-ginseng green peel of walnut hair blackening liquid and preparation method thereof | |
| CN102309750A (en) | A kind of conditioning health preserving film that is exclusively used in women's privates | |
| CN109908035A (en) | A kind of freckle-removing mask based on peony seed oil | |
| CN107982135A (en) | A kind of shampoo and preparation method thereof | |
| CN105726366B (en) | Skin lipid membrane repairing composition | |
| CN106389170A (en) | Antiallergic paeonia albiflora cosmetic composition | |
| JP2024036484A (en) | Cosmetic composition containing graphene quantum dot as active ingredient | |
| CN112107533A (en) | Composition with effects of controlling oil, tendering skin and collecting fine pores and preparation method and application thereof | |
| CN108078901A (en) | A kind of Essence for adjusting skin water and oil balance, improving microgroove and preparation method thereof | |
| CN109381394B (en) | Skin anti-allergy repair composition and application | |
| CN110251611A (en) | A kind of Chinese medicine composition and its preparation method and application with skin repair effect | |
| CN106176455B (en) | A kind of whitening anti-aging skin care item and preparation method thereof | |
| CN107648137A (en) | A kind of mildy wash | |
| CN106566683A (en) | Cleaning liquid as well as preparation method and application thereof | |
| CN108354891B (en) | Soothing cream and preparation method thereof | |
| CN102949311B (en) | Additive-free children bath liquid and preparation method thereof | |
| KR20010008007A (en) | A manufacture methode of cleaning water for skin | |
| CN106265243A (en) | A kind of crissum wet tissue annex solution and its preparation method and application | |
| CN110025515B (en) | Anti-allergy polysaccharide compound composition and application thereof in cosmetics |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20220916 Address after: No. 401, Building K28, Phase II Industrial Project, Luoshiwan International Trade City Small Commodity Processing Base, Luoyang Street Office, Economic Development Zone, Kunming Free Trade Pilot Zone, Kunming City (Yunnan), Yunnan Province, 650506 Patentee after: Yunnan Qianrong Biotechnology Co.,Ltd. Address before: Yunnan Wenshan Sanqi Industrial Park, Wenshan Zhuang and Miao Autonomous Prefecture, Yunnan 663000 Patentee before: YUNNAN REN XIU HUA COSMETICS Co.,Ltd. |