CN109939061B - Safe and non-irritant white hair blackening essence and preparation method thereof - Google Patents
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Abstract
The invention discloses safe and non-irritant white hair blackening essence and a preparation method thereof, and the safe and non-irritant white hair blackening essence comprises the following raw materials: water, linseed extract, angelica extract, aloe extract, tea polyphenol, ethanol, sodium benzoate, potassium sorbate, citric acid, ginseng extract, polygonum multiflorum extract, gamma-linolenic acid, glucomannan and sepia crude extract. The invention improves the effect of blackening white hair and regenerating black hair of the safe and non-irritant white hair blackening essence by adopting the gamma-linolenic acid, the glucomannan and the crude extract of the cuttlefish ink to cooperate.
Description
[ technical field ] A method for producing a semiconductor device
The invention belongs to a hair care and maintenance technology, and particularly relates to safe and non-irritant white hair blackening essence and a preparation method thereof.
[ background of the invention ]
White hair is a common disease and brings endless troubles to patients. Because of more causes of alopecia and leukotrichia, the rhythm of life is fast, and more chemicals are contained, the meat with meat is rich and sweet, the deficiency of liver and kidney is caused, the yin and blood are insufficient, the yin deficiency causes yang excess, the yang excess causes heat excess and the body fluid is not distributed, and the hair follicle is exhausted and the hair is not nourished; blood heat and blood stasis, deficiency of both qi and blood failing to nourish the hair. Wind-cold syndrome can be caused by external wind-dampness affecting the skin and striae; excessive oil and fat, more dandruff, fungal infection, hair dyeing, hair perming and hair follicle injury causing white hair. However, the use of a wide range of hair dyes can only cover up the white hair, and no effective drug for treating white hair exists at present, so that the development of a drug for blackening white hair is a hot point of research.
Chinese patent document "A liquid for blackening white hair (No. CN 106668368B)" discloses a liquid for blackening white hair, which is prepared by pulverizing 2-10 parts by weight of Ginseng radix, 3-15 parts by weight of cortex Mori, 5-15 parts by weight of fructus Piperis, 5-20 parts by weight of cortex Tetrastigmatis Hypoglauci, 2-10 parts by weight of Lavender and 2-10 parts by weight of Aloe, decocting, soaking in 60% edible alcohol, sealing and fermenting for 3 months, and filtering to remove residue. Quantitatively subpackaging the herbal liquid preparation; the Chinese herbal medicine liquid is externally applied to the root of white hair, so that the growth of leucocyte of hair mother (hair follicle) is quickly prevented, nutrient elements required by black hair are supplemented, the effective components of the Chinese herbal medicine liquid are promoted to deeply penetrate into cerebral cortex, and the formation of hair follicle melanocyte is effectively enhanced. But the preparation period is too long, and the actual test effect is not ideal; chinese patent (CN10349754A) discloses an anti-hair loss and hair-growing shampoo with herbal essence and biochemical component formula and a preparation method thereof, the natural, safe and effective anti-hair loss and hair-growing shampoo which is more in line with modern health concept is provided by extracting herbal essence and conventional biochemical components, but the adhesion time of the effective components on the epidermis at the root of the hair is short, the effect on the growth of the white hair to the black hair and the regenerated black hair is not good enough, and the adopted biological extracts are mainly polypeptides, fatty acids and the like which are known components used for promoting the white hair to the black hair and regenerating the black hair in the existing theory, and the effect is not obvious; chinese patent CN104887594A) discloses an anti-hair loss repairing essence oil, which can replace the existing basic nursing materials such as essence, nursing liquid and the like, has broad-effect hair care and cleaning effects, prevents inflammation of hair follicles and excessive oil of hair, can promote cell regeneration, balances sebum secretion, helps hair growth, is an effective essence liquid for treating hair loss and hair thinning, but the essence liquid mainly inhibits hair loss and helps hair regeneration, but has no obvious effect on the change of white hair to black hair; chinese patent (CN108743506A) discloses a white hair blackening essence which adopts natural traditional Chinese medicine extracts, has no toxic or side effect, is mild and non-irritant, can effectively supplement melanin required by hair, and has the effects of blackening and brightening the hair, but only adopts the natural traditional Chinese medicine extracts to provide the melanin required by the hair, so that the white hair is blackened, but has no obvious effect on the regeneration of the black hair, and only adopts the natural traditional Chinese medicine extracts with limited effect, and the effect on the blackening of the white hair is not obvious; chinese patent (CN108653119A) discloses a herbal pure natural shampoo, which can increase hair nutrition, make hair have good flexibility and function of uneasy to become brittle, and can delay the growth of white hair, keep hair smooth and glossy, remove dandruff, relieve itching and prevent alopecia. For the problem that the effect of the existing white hair blackening and black hair regeneration essence is not obvious, the applicant creatively provides a safe and non-irritant white hair blackening essence and a preparation method thereof through continuous exploration, research and accumulation, the preparation is simple, and the white hair blackening rate and the black hair regeneration rate can be obviously improved.
[ summary of the invention ]
The invention provides safe and non-irritant white hair blackening essence and a preparation method thereof, the essence is simple to prepare, and the conversion rate of white hair and the regeneration and blackening rate can be obviously improved.
In order to solve the technical problems, the invention adopts the following technical scheme:
the safe and non-irritant white hair blackening essence is characterized by comprising the following raw materials: water, linseed extract, angelica extract, aloe extract, tea polyphenol, ethanol, sodium benzoate, potassium sorbate, citric acid, ginseng extract, polygonum multiflorum extract, gamma-linolenic acid, glucomannan and sepia crude extract; the mass ratio of the gamma-linolenic acid, the glucomannan and the crude extract of the cuttlefish ink is 1-3:2-4: 10-14; the crude extract of cuttlefish ink is prepared by taking out whole ink sac of cuttlefish, pulverizing, adding 10 times of ethanol, stirring, soaking for 5-7 days, filtering, and high vacuum rotary evaporating to remove 8 times of ethanol.
Further, the mass ratio of the gamma-linolenic acid, the glucomannan and the crude extract of the cuttlefish ink is 2:3: 12.
Further, the safe and non-irritant white hair blackening essence is characterized by comprising the following raw materials in parts by mass: 70-80 parts of water, 1-3 parts of linseed extract, 1-3 parts of angelica sinensis extract, 1-3 parts of aloe extract, 1-3 parts of tea polyphenol, 5-10 parts of ethanol, 1-3 parts of sodium benzoate, 1-3 parts of potassium sorbate, 1-3 parts of citric acid, 1-3 parts of ginseng extract, 4-6 parts of polygonum multiflorum extract, 1-3 parts of gamma-linolenic acid, 2-4 parts of glucomannan and 10-14 parts of cuttlefish ink crude extract.
Further, the safe and non-irritant white hair blackening essence comprises the following raw materials in parts by mass: 75 parts of water, 2 parts of linseed extract, 2 parts of Chinese angelica extract, 2 parts of aloe extract, 2 parts of tea polyphenol, 7.5 parts of ethanol, 2 parts of sodium benzoate, 2 parts of potassium sorbate, 2 parts of citric acid, 2 parts of ginseng extract, 5 parts of polygonum multiflorum extract, 2 parts of gamma-linolenic acid, 3 parts of glucomannan and 12 parts of sepia crude extract.
Further, the ginseng extract, the linseed extract, the angelica extract, the aloe extract and the polygonum multiflorum extract are prepared by crushing raw materials, cooking the raw materials in water for multiple times, combining filtrates obtained by the multiple cooking, and concentrating the combined filtrates.
The preparation method of the safe and non-irritant white hair blackening essence comprises the following steps:
(1) adding water into gamma-linolenic acid, glucomannan and crude extract of cuttlefish ink, and stirring for 1-2 hr; (2) adding tea polyphenol, sodium benzoate, potassium sorbate and citric acid into the mixed solution in the step (1) and fully stirring for 1-2 hours; (3) adding Ginseng radix extract, semen Lini extract, radix Angelicae sinensis extract, Aloe extract, and Polygoni Multiflori radix extract into ethanol, dispersing, and slowly adding dropwise into the water solution of step 2 while stirring to obtain the final product.
The invention has the following beneficial effects:
the invention adopts various traditional Chinese medicine extracts including ginseng extract, linseed extract, angelica extract and aloe extract as effective components, and can promote scalp blood circulation, enhance scalp vitality and promote white hair to turn black. However, the addition of the above components does not improve the therapeutic effect, and through a large number of tests and combinations, the applicant finds that gamma-linolenic acid, glucomannan and crude extract of sepia have a synergistic effect.
The possible mechanism is presumed to be as follows: the gamma-linolenic acid enhances the fluidity of phospholipid on cell membranes, promotes the absorption effect of scalp on various traditional Chinese medicines and active ingredients of the sepia extract, has the effects of protecting skin, moistening skin, delaying skin aging, treating chronic eczema, promoting blood circulation and the like, has weak acidity and reducibility, and has the effect of stabilizing the sepia crude extract; the concrete components of the crude extract of the cuttlefish ink are unknown, but the extract is a black sticky substance, experiments show that the extract has extremely high activity, can greatly improve the conversion from white hair to black hair and the growth efficiency of the black hair, can play a stable effect by adding the gamma-linolenic acid and the glucomannan, and also shows that the extract obtained by extracting the whole ink sac has higher activity than the extract obtained by extracting the pure ink, and the presumption is that certain active components can also exist in the skin of the ink sac; the glucomannan can adsorb crude extract of sepia and improve dispersibility, and can cover cuticle of hair root to increase adhesion time and action time.
All the components of the hair blackening agent are natural and environment-friendly, are mild and have no side effect on human bodies, and can effectively improve the growth of the black hair from white hair to black hair and the growth of regenerated black hair.
[ detailed description ] embodiments
In order to facilitate a better understanding of the invention, the following examples are given to illustrate, but not to limit the scope of the invention.
The following is a more specific example.
Example 1
The safe and non-irritant white hair blackening essence comprises the following raw materials in parts by mass: 75 parts of water, 2 parts of linseed extract, 2 parts of Chinese angelica extract, 2 parts of aloe extract, 2 parts of tea polyphenol, 7.5 parts of ethanol, 2 parts of sodium benzoate, 2 parts of potassium sorbate, 2 parts of citric acid, 2 parts of ginseng extract, 5 parts of polygonum multiflorum extract, 2 parts of gamma-linolenic acid, 3 parts of glucomannan and 12 parts of sepia crude extract. The Ginseng radix extract, semen Lini extract, radix Angelicae sinensis extract, Aloe extract, and Polygoni Multiflori radix extract are prepared by pulverizing raw materials, decocting in water for several times, mixing filtrates, and concentrating. The crude extract of cuttlefish ink is prepared by taking out whole ink sac of cuttlefish, pulverizing, adding 10 times of ethanol, stirring, soaking for 5-7 days, filtering, and high vacuum rotary evaporating to remove 8 times of ethanol.
The preparation method of the safe and non-irritant white hair blackening essence comprises the following steps:
adding water into gamma-linolenic acid, glucomannan and crude extract of cuttlefish ink, and stirring for 1-2 hr; (2) adding tea polyphenol, sodium benzoate, potassium sorbate and citric acid into the mixed solution in the step (1) and fully stirring for 1-2 hours; (3) adding Ginseng radix extract, semen Lini extract, radix Angelicae sinensis extract, Aloe extract, and Polygoni Multiflori radix extract into ethanol, dispersing, and slowly adding dropwise into the water solution of step 2 while stirring to obtain the final product.
Example 2
The safe and non-irritant white hair blackening essence comprises the following raw materials in parts by mass: 70 parts of water, 3 parts of linseed extract, 1 part of Chinese angelica extract, 3 parts of aloe extract, 1 part of tea polyphenol, 10 parts of ethanol, 1 part of sodium benzoate, 3 parts of potassium sorbate, 1 part of citric acid, 3 parts of ginseng extract, 4 parts of polygonum multiflorum extract, 3 parts of gamma-linolenic acid, 2 parts of glucomannan and 14 parts of inkfish ink crude extract.
Example 3
The safe and non-irritant white hair blackening essence comprises the following raw materials in parts by mass: 80 parts of water, 1 part of linseed extract, 3 parts of Chinese angelica extract, 1 part of aloe extract, 3 parts of tea polyphenol, 5 parts of ethanol, 3 parts of sodium benzoate, 1 part of potassium sorbate, 3 parts of citric acid, 1 part of ginseng extract, 6 parts of polygonum multiflorum extract, 1 part of gamma-linolenic acid, 4 parts of glucomannan and 10 parts of crude extract of inkfish ink.
Comparative example 1
The preparation process is basically the same as that of example 1, except that the raw materials for preparing the safe and non-irritant white hair blackening essence lack the gamma-linolenic acid, the glucomannan and the crude extract of sepia.
Comparative example 2
The preparation process is substantially the same as that of example 1, except that gamma-linolenic acid is absent from the raw materials for preparing the safe and non-irritating white hair blackening essence.
Comparative example 3
The preparation process was substantially the same as that of example 1, except that glucomannan was used as a raw material for preparing the safe and non-irritating white hair blackening essence.
Comparative example 4
The procedure of example 1 was followed except that the raw materials for preparing the safe and non-irritating essence for blackening white hair lacked the crude extract of sepia.
Comparative example 5
The process of example 1 of the chinese patent document "a liquid for blackening human white hair (grant publication No. CN 106668368B)" was used to prepare a white hair blackening liquid.
Comparative example 6
The preparation process is basically the same as that of example 1, except that the raw materials for preparing the safe and non-irritant white hair blackening essence comprise 0.5 part of gamma-linolenic acid and 1 part of glucomannan.
Comparative example 7
The preparation process is basically the same as that of example 1, except that the raw materials for preparing the safe and non-irritant white hair blackening essence comprise 4 parts of gamma-linolenic acid and 1 part of glucomannan.
Comparative example 8
The preparation process is basically the same as that of example 1, except that the raw materials for preparing the safe and non-irritant white hair blackening essence comprise 0.5 part of gamma-linolenic acid and 5 parts of glucomannan.
Comparative example 9
The preparation process was substantially the same as that of example 1, except that the crude extract of sepia used pure sepia as a raw material.
A total of 22 male patients with age of 20-30 years and course of disease longer than 1 year were selected. The hair is not dyed or taken in the first 2 months, and the hair is shaved to be about 3-5cm in length, so that statistics can be conveniently carried out. The using method comprises the following steps: after the scalp is cleaned by clear water, the composition of the invention is directly sprayed on the root of the scalp, the spraying amount is fixed once every two days, two months are 1 course of treatment, and the use is 1 course of treatment. The 22 patients were divided into 11 groups, and the products of examples and comparative examples were subjected to test evaluation with a scale of 1 to 5. The effect of turning white hair to black 5 indicates that the root of the original white hair is mostly turned to black, and 1 indicates no effect. The regeneration black hair rate 5 indicates that new hair has no white hair basically, and 1 indicates no effect. Counting the white hair blackening effect and the regenerated black hair blackening effect into the same area region, and counting, wherein the regenerated hair is newly generated hair, the length of the regenerated hair is less than 1cm, and the length is listed in the following table.
From the above table, it can be seen that: as can be seen from the data of example 1 and comparative examples 1-4, the gamma-linolenic acid, glucomannan and crude extract of sepia act synergistically in the use process of the safe and non-irritant white hair blackening essence, and synergistically improve the effects of turning white hair into black hair and regenerating black hair. As can be seen from the data of comparative examples 6 to 8, the addition amounts of the gamma-linolenic acid and the glucomannan have great influence on the effectiveness of the crude extract of the sepia, and the addition of the gamma-linolenic acid and the glucomannan in a certain proportion range can effectively improve the effect of the crude extract of the sepia. As is apparent from the comparison between comparative example 9 and example 1, the extract obtained when the whole ink sac is extracted together has a higher therapeutic effect.
The above description should not be taken as limiting the invention to the embodiments, but rather, as will be apparent to those skilled in the art to which the invention pertains, numerous simplifications or substitutions may be made without departing from the spirit of the invention, which shall be deemed to fall within the scope of the invention as defined by the claims appended hereto.
Claims (4)
1. The safe and non-irritant white hair blackening essence is characterized by comprising the following raw materials in parts by mass: 70-80 parts of water, 1-3 parts of linseed extract, 1-3 parts of angelica sinensis extract, 1-3 parts of aloe extract, 1-3 parts of tea polyphenol, 5-10 parts of ethanol, 1-3 parts of sodium benzoate, 1-3 parts of potassium sorbate, 1-3 parts of citric acid, 1-3 parts of ginseng extract, 4-6 parts of polygonum multiflorum extract, 1-3 parts of gamma-linolenic acid, 2-4 parts of glucomannan and 10-14 parts of cuttlefish ink crude extract; the mass ratio of the gamma-linolenic acid, the glucomannan and the crude extract of the cuttlefish ink is 1-3:2-4: 10-14; the crude extract of cuttlefish ink is prepared by taking out whole ink sac of cuttlefish, pulverizing, adding 10 times of ethanol, stirring, soaking for 5-7 days, filtering, and high vacuum rotary evaporating to remove 8 times of ethanol; the Ginseng radix extract, semen Lini extract, radix Angelicae sinensis extract, Aloe extract, and Polygoni Multiflori radix extract are prepared by pulverizing raw materials, decocting in water for several times, mixing filtrates, and concentrating.
2. The safe and non-irritant white hair blackening essence liquid according to claim 1, wherein the mass ratio of the gamma-linolenic acid, the glucomannan and the crude sepia extract is 2:3: 12.
3. The safe and non-irritant white hair blackening essence liquid according to claim 1, which is characterized by comprising the following raw materials in parts by mass: 75 parts of water, 2 parts of linseed extract, 2 parts of Chinese angelica extract, 2 parts of aloe extract, 2 parts of tea polyphenol, 7.5 parts of ethanol, 2 parts of sodium benzoate, 2 parts of potassium sorbate, 2 parts of citric acid, 2 parts of ginseng extract, 5 parts of polygonum multiflorum extract, 2 parts of gamma-linolenic acid, 3 parts of glucomannan and 12 parts of sepia crude extract.
4. A method for preparing the safe and non-irritating whitening and blackening essence according to claims 1-3, comprising the steps of:
(1) adding water into gamma-linolenic acid, glucomannan and crude extract of cuttlefish ink, and stirring for 1-2 hr;
(2) adding tea polyphenol, sodium benzoate, potassium sorbate and citric acid into the mixed solution in the step (1) and fully stirring for 1-2 hours; (3) adding Ginseng radix extract, semen Lini extract, radix Angelicae sinensis extract, Aloe extract, and Polygoni Multiflori radix extract into ethanol, dispersing, and slowly adding dropwise into the water solution of step 2 while stirring to obtain the final product.
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| CN1059591C (en) * | 1997-12-30 | 2000-12-20 | 于景宏 | Hair-care medicine able to make hair blacker |
| KR100755525B1 (en) * | 2006-08-17 | 2007-09-05 | 이원기 | Hair coloring composition comprising cephalopoda ink extracts |
| CN1943549B (en) * | 2006-09-13 | 2010-05-12 | 乔爱娴 | Application of litchi seed extract in hair shampoo article |
| KR20100084041A (en) * | 2009-01-15 | 2010-07-23 | 이원기 | Hair treatment composition |
| CN102772336B (en) * | 2012-08-13 | 2015-03-18 | 宋子奎 | Washing agent composition for colored hairs and preparation method for washing agent composition |
| KR101547920B1 (en) * | 2012-12-05 | 2015-08-27 | 강원도립대학산학협력단 | Natural shampoo bar for preventing and treating of scalp and hair, and manufacturing method thereof |
| CN105534873A (en) * | 2016-02-29 | 2016-05-04 | 广西南岜仔科技有限公司 | Bletilla striata hair colorant and preparation method thereof |
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