CN114848569A - Formula and preparation method of hair loss prevention and hair nourishing product - Google Patents

Formula and preparation method of hair loss prevention and hair nourishing product Download PDF

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Publication number
CN114848569A
CN114848569A CN202210658336.1A CN202210658336A CN114848569A CN 114848569 A CN114848569 A CN 114848569A CN 202210658336 A CN202210658336 A CN 202210658336A CN 114848569 A CN114848569 A CN 114848569A
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hair
percent
agent
traditional chinese
chinese medicine
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杨继安
刘艳玲
王恩桃
张青青
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Shaanxi Bosen Bio Pharmaceutical Group Co ltd
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Shaanxi Bosen Bio Pharmaceutical Group Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
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Abstract

The invention belongs to the technical field of daily chemicals, and discloses a formula of an anti-hair loss hair conditioner product, which comprises the following raw materials in percentage by weight: 40.7 to 44.7 percent of water agent; 29-31% of traditional Chinese medicine extracting solution; 5.7 to 7.9 percent of humectant; 5.8 to 8.2 percent of thickening agent; 8.7 to 10.3 percent of conditioner; 1.8 to 2.2 percent of emulsifier; 0.05 to 0.15 percent of complexing agent; 0.4-0.6% of hair-strengthening agent; 0.4 to 0.6 percent of antioxidant; 0.9 to 1.1 percent of flavoring agent. The formula of the invention can deeply nourish hair roots and hair silks and promote hair regeneration; also can repair damaged scalp, make hair black and moist, and restore healthy luster; the invention also discloses a method for preparing the anti-hair loss hair conditioner, which comprises the following steps: step S1, preparing a traditional Chinese medicine extracting solution by adopting cacumen biotae, tung tree leaves, hemp seeds, lotus seeds, ginseng, rhizoma anemarrhenae, ginger, angelica and polygonum multiflorum; and step S2, mixing the traditional Chinese medicine extracting solution with other raw materials to obtain a finished product.

Description

Formula and preparation method of hair loss prevention and hair nourishing product
Technical Field
The invention belongs to the technical field of daily chemicals, and particularly relates to a formula of an anti-hair loss hair conditioner product and a preparation method thereof.
Background
In modern society, people have an increasing number of people who suffer from alopecia due to increased living pressure, addition of food additives, poor work and rest habits, and the like, and alopecia prevention becomes an important task of modern people. The symptoms of alopecia are manifested on the exterior and the origin is the interior, i.e. the exterior is diseased, and clinically, alopecia is mainly manifested as atrophy of hair follicles, hair loss, easy breakage, much oil and no elasticity, and even worse, alopecia is completely. The origin of alopecia is complex, and known causes are related to genetic factors, immunity factors, infection factors, metabolism factors, nutritional conditions, mental health factors, environmental factors and the like.
Alopecia has a serious impact on the life, work and mental health of patients, and a method for preventing alopecia is continuously sought clinically. Most of the existing methods for preventing and treating alopecia are to perform smearing, massaging and the like on the head by adopting medicines, but the method has poor treatment effect, slow effect taking and long time consumption, a professional treatment place is required during treatment, most alopecia patients do not have enough time and energy to perform treatment for a complete treatment course, so that the time and the energy are wasted, and the treatment effect is poor. In another method, drugs containing minoxidil, hormones and the like are used as hair loss products, but the drugs have side effects on human bodies after being used, and the regrown hair has poor quality, is easy to fall off, is not durable and the like.
Based on the analysis, the existing method for treating alopecia has poor treatment effect, and the satisfactory effects of preventing alopecia and promoting hair growth are difficult to obtain. Therefore, the field needs to provide an anti-hair loss hair conditioner, so as to solve the defects of poor scalp care effect, poor anti-hair loss and hair growth promotion effect, side effect and the like of the existing medicines.
Disclosure of Invention
The invention aims to provide a formula of a hair loss preventing and nourishing hair essence product, which can deeply nourish hair roots and hair silks and promote hair regeneration; also can repair damaged scalp, make hair black and moist, and restore healthy luster.
The technical scheme adopted for realizing the purpose of the invention is as follows:
the formula of the anti-hair loss hair conditioner product comprises the following raw materials in percentage by weight: 40.7 to 44.7 percent of water agent; 29-31% of traditional Chinese medicine extracting solution; 5.7 to 7.9 percent of humectant; 5.8 to 8.2 percent of thickening agent; 8.7 to 10.3 percent of conditioner; 1.8 to 2.2 percent of emulsifier; 0.05 to 0.15 percent of complexing agent; 0.4-0.6% of hair-strengthening agent; 0.4 to 0.6 percent of antioxidant; 0.9 to 1.1 percent of flavoring agent.
Further, the traditional Chinese medicine components in the traditional Chinese medicine extracting solution comprise cacumen biotae, tung tree leaves, hemp seeds, lotus seeds, ginseng, rhizoma anemarrhenae, ginger, angelica and polygonum multiflorum.
Furthermore, the traditional Chinese medicine components in the traditional Chinese medicine extracting solution comprise cacumen biotae, tung tree leaves, hemp seeds, lotus seeds, ginseng, rhizoma anemarrhenae, ginger, angelica and polygonum multiflorum, and the ratio of the traditional Chinese medicine components to the traditional Chinese medicine extracting solution is 15: 8: 3.2: 1: 2.
Further, the water agent is deionized water;
the humectant comprises glycerol, panthenol, and 1, 2-ethylene glycol;
the thickener comprises hydroxyethyl cellulose;
the conditioner comprises behenyl trimethyl ammonium chloride, dimethicone, jojoba oil, and aminopropyl polydimethylsiloxane;
the emulsifier comprises polyoxyethylene sorbitan monooleate;
the complexing agent is EDTA-disodium;
hair fixatives include diaminopyrimidine oxides;
the antioxidant comprises p-hydroxyacetophenone;
the flavoring agent comprises essence.
Further, the thickening agent also comprises cetyl alcohol or stearyl alcohol.
The invention also aims to provide a method for preparing the hair conditioner by the anti-hair-loss hair conditioner product formula, which has simple process and is easy to realize and produce in a large scale.
The technical scheme adopted for realizing the other purpose of the invention is as follows:
a method for preparing hair conditioner by using a hair-loss-preventing hair conditioner product formula specifically comprises the following steps:
step S1, preparing a traditional Chinese medicine extracting solution by adopting cacumen biotae, tung tree leaves, hemp seeds, lotus seeds, ginseng, rhizoma anemarrhenae, ginger, angelica and polygonum multiflorum;
and step S2, mixing the traditional Chinese medicine extract with a water aqua, a humectant, a thickening agent, a conditioning agent, an emulsifier, a complexing agent, a hair-strengthening agent, an antioxidant and a flavoring agent to obtain a finished product.
Further, the method for preparing the traditional Chinese medicine extracting solution in the step S1 specifically comprises the following steps:
step S101, crushing the hempseed and the lotus seeds, and uniformly mixing the crushed hempseed and the lotus seeds with the cacumen biotae, the tung tree leaves, the ginseng, the rhizoma anemarrhenae, the ginger, the angelica and the polygonum multiflorum to obtain a mixed material;
step S102, decocting the mixed material obtained in the step S101 and 4000-;
step S103, adding 3000-4000ml of water into the mixing residue obtained in the step S102, decocting for 2-3h again, and then carrying out secondary filtration;
and step S104, combining the filtrates in the steps S102 and S103, concentrating under reduced pressure to 3100ml 2900-.
Further, step S2 specifically includes the following steps:
step S201, adding hydroxyethyl cellulose into deionized water, heating to 40-51 ℃, and uniformly stirring to obtain a hydroxyethyl cellulose solution;
step S202, adding glycerol, ethanol, p-hydroxyacetophenone, EDTA-disodium and the hydroxyethyl cellulose solution obtained in the step S201 into a material tank at one time, stirring and heating to completely mix and dissolve the materials uniformly;
step S203, raising the temperature of the material tank to 70-75 ℃, sequentially adding cetyl alcohol, behenyl trimethyl ammonium chloride and polyoxyethylene sorbitan monooleate into the material tank, and stirring to uniformly mix and dissolve the materials;
step S204, raising the temperature of the material tank to 80-82 ℃ again, adding simethicone, jojoba oil and aminopropyl polydimethylsiloxane into the material tank, uniformly mixing the materials, homogenizing after uniform stirring, and keeping the temperature;
step S205, cooling the material tank to 49-51 ℃, adding the traditional Chinese medicine extracting solution prepared in the step S1 into the material tank, and uniformly stirring;
step S206, cooling the material tank to 44-46 ℃ again, adding diaminopyrimidine oxide, 1, 2-glycol and essence while stirring, then stirring and uniformly mixing the materials, and cooling to 34-36 ℃;
and S207, discharging, sampling and inspecting, filling and packaging the qualified intermediate product, and warehousing the qualified finished product.
Further, in the method for preparing the Chinese medicinal extractive solution, the pressure of the reduced pressure concentration in step S104 is-0.07 Mpa, and the temperature is 60 deg.C.
Further, in step S204, the homogenizing speed is 3000-4000r/min, and the homogenizing time is 2-5 min.
In steps S102-S104 of the present invention, the first filtration, the second filtration and the combined filtration are all carried out in a plate-and-frame filter, and the film thickness of the plate-and-frame filter is 0.65 μm.
In step S201 of the present invention, the stirring speed is 200-300 r/min.
In the steps S203, S204, S205 and S206 of the present invention, the stirring speed is 300-500 r/min.
In step S204, the mixture is stirred for another 20min under heat preservation.
In the filtering in steps S102, S103, and S104 of the present invention, a 100-mesh screen is used for the filtering.
The hair conditioner prepared by the invention closely combines the modern pharmacological efficacy and scientific technology, and tung leaves and hemp seeds in the formula can be used as hair growth agents to promote hair growth; in the formula, the polygonum multiflorum and the lotus seeds can be used as hair nutritional agents, and can nourish hair, improve the symptoms of dry hair and split hair, improve scalp nutrition, regulate sebum secretion, and promote scalp blood circulation, so that the hair growth speed is accelerated; in the formula, the ginger can be used as a scalp local stimulant, slightly stimulates the scalp to cause the scalp to be congested and excites the scalp nervous system, thereby restoring the nutritional function; in the formula, the rhizoma anemarrhenae can be used as a sterilizing, dandruff-removing and itching-relieving agent for diminishing inflammation, sterilizing, removing dandruff and relieving itching; in the formula, the cacumen biotae and the ginseng can be used as an astringent hair-fixing agent, are easy to absorb by the scalp, can supplement blood and permeate into the hair, enhance the nutrition and the toughness of the hair root, arouse the vitality of the scalp from inside to outside, promote the growth of hair follicles, and reduce alopecia and broken hair; in the formula, the angelica can be used as a microcirculation promoter, can expand scalp capillaries, promote blood circulation, supply the quantity of hair mother cells and activate scalp tissues. The hair care and hair loss prevention compound system which is prepared by the medicines is applied to daily chemical products by using the extract of the hair care and hair loss prevention compound system, and the prepared hair conditioner has the effects of caring scalp and hair, preventing or reducing hair loss and promoting hair metabolism.
The hair conditioner has the advantages that precious traditional Chinese medicine essences such as the tuber fleeceflower root, the Chinese angelica, the tung leaf, the hemp seed, the lotus seed and the rhizoma anemarrhenae are mild for nursing scalp, the toughness of the hair is enhanced, the hair root is firm, the hair is promoted to grow new, and the effects of growing and fixing the hair are gradually realized. The anti-hair loss essence containing Chinese herbal medicines such as the cacumen biotae, the ginseng, the ginger and the like can deeply nourish hair follicles and scalp, improve the hair growth environment, effectively reduce hair loss, accelerate blood circulation of the head, accelerate metabolism of cells of the head, stimulate the affected part of the head and recover the affected part again.
The hair conditioner prepared by the invention inherits the principle of 'treatment by nourishing' in the traditional Chinese medicine, fully nourishes hair follicles and scalp by utilizing refined components of natural traditional Chinese medicines, improves the growth environment of hair, promotes the growth of hair, maintains new fine hair and enables the hair to be healthy and dense. The product has the functions of preventing and nourishing hair, nourishing and moistening hair for various alopecia such as premature alopecia, alopecia areata, physical alopecia and the like.
The invention has the beneficial effects that:
the hair-preventing and-treating traditional Chinese medicine composition is based on the recognition of the hair by the traditional Chinese medicine theory, tightly buckles the pathogenesis of the traditional Chinese medicine, and is used for preventing and treating the composition according to the traditional Chinese medicine syndrome differentiation and treatment principle, so that the defects that the composition in the prior art is relatively simple and the composition basis is not sufficient are overcome.
The raw materials of the formula provided by the invention are natural materials, are in the category of traditional Chinese medicines or botanical medicines meeting the requirements of the regulations of daily chemical articles, and overcome the defects that the raw materials of the formula of certain hair-care and anti-hair loss products are not in the category of daily chemical articles and can not circulate in daily chemical channels.
According to the invention, the hair loss preventing and treating shampoo is characterized in that a hair growth agent, a hair nutrient, a scalp local stimulant, a sterilization, dandruff removing and itching relieving agent, a convergence hair-fixing agent and other system schemes are introduced into the formula in a scientific and reasonable manner, besides the hair loss preventing and treating formula is removed from a plurality of reasons of hair loss according to the traditional Chinese medicine theory, the prepared hair loss preventing and treating shampoo can deeply permeate into the scalp, promote the transdermal absorption of active ingredients, improve and condition the related activity of the hair, promote the hair growth, expand the capillary vessels of the scalp, promote the blood circulation, activate the tissues of the scalp, supply hair regeneration nutrition, excite the nervous system of the scalp, diminish inflammation, sterilize, remove dandruff, relieve itching, converge and stabilize the hair roots, and achieve the purposes of promoting the hair metabolism and preventing and treating hair loss.
The preparation method of the hair conditioner provided by the invention can fully release the active ingredients in the raw materials and ensure that the active ingredients are absorbed and utilized to the maximum extent, so that the prepared shampoo has a good hair loss prevention and treatment effect and has no toxic or side effect; the preparation method is simple and convenient to operate, low in cost and beneficial to industrialization.
The hair conditioner prepared by the invention can deeply nourish hair roots and hair silks and promote hair regeneration; meanwhile, a protective film is formed on the surface of the scalp, so that the hair is kept in natural balance, the damaged hair is repaired, the hair quality is improved, the hair is black, moist, light and smooth, and the healthy luster is recovered.
Additional advantages, objects, and features of the invention will be set forth in the description which follows and in part will become apparent to those having ordinary skill in the art upon examination of the following or may be learned from practice of the invention. The objectives and other advantages of the invention may be realized and attained by the means of the instrumentalities and combinations particularly pointed out hereinafter.
Detailed Description
Example 1
The formula of the anti-hair loss hair conditioner product comprises the following raw materials in percentage by weight: 43.6 percent of water agent; 30% of traditional Chinese medicine extracting solution; 5.7 percent of humectant; 7.8% of a thickening agent; 9.35% of a conditioning agent; 1.8 percent of emulsifier; 0.05% of complexing agent; 0.4% of hair-strengthening agent; 0.4% of antioxidant; 0.9 percent of flavoring agent. Wherein the Chinese medicinal components in the Chinese medicinal extractive solution comprise folium Platycladi, folium Verniciae Fordii, semen Sesami, semen Nelumbinis, Ginseng radix, rhizoma anemarrhenae, rhizoma Zingiberis recens, radix Angelicae sinensis and Polygoni Multiflori radix. And the traditional Chinese medicine components in the traditional Chinese medicine extracting solution comprise cacumen biotae, tung tree leaves, hemp seed, lotus seed, ginseng, rhizoma anemarrhenae, ginger, angelica and polygonum multiflorum in a ratio of 15: 8: 3.2: 1: 2.
In this embodiment, the aqueous solution is deionized water;
the humectant is glycerol, panthenol, and 1, 2-ethylene glycol;
the thickening agent is hydroxyethyl cellulose and cetyl alcohol;
the conditioner is behenyl trimethyl ammonium chloride, dimethyl silicone oil, jojoba oil, aminopropyl polydimethylsiloxane;
the emulsifier is polyoxyethylene sorbitan monooleate;
the complexing agent is EDTA-disodium;
the hair-setting agent is diaminopyrimidine oxide;
the antioxidant is p-hydroxyacetophenone;
the flavoring agent is essence.
Example 2
44.25 percent of water agent; 29% of traditional Chinese medicine extracting solution; 6.7 percent of humectant; 7.8% of a thickening agent; 8.7% of a conditioning agent; 1.8 percent of emulsifier; 0.05 percent of complexing agent; 0.4% of hair-strengthening agent; 0.4% of antioxidant; 0.9 percent of flavoring agent. Wherein the Chinese medicinal components in the Chinese medicinal extractive solution comprise folium Platycladi, folium Verniciae Fordii, semen Sesami, semen Nelumbinis, Ginseng radix, rhizoma anemarrhenae, rhizoma Zingiberis recens, radix Angelicae sinensis and Polygoni Multiflori radix. And the traditional Chinese medicine components in the traditional Chinese medicine extracting solution comprise cacumen biotae, tung tree leaves, hemp seed, lotus seed, ginseng, rhizoma anemarrhenae, ginger, angelica and polygonum multiflorum in a ratio of 15: 8: 3.2: 1: 2.
In this embodiment, the aqueous solution is deionized water;
the humectant is glycerol, panthenol, and 1, 2-ethylene glycol;
the thickening agent is hydroxyethyl cellulose and hexadecanol;
the conditioner is behenyl trimethyl ammonium chloride, dimethyl silicone oil, jojoba oil, aminopropyl polydimethylsiloxane;
the emulsifier is polyoxyethylene sorbitan monooleate;
the complexing agent is EDTA-disodium;
the hair-setting agent is diaminopyrimidine oxide;
the antioxidant is p-hydroxyacetophenone;
the flavoring agent is essence.
Example 3
The formula of the anti-hair loss hair conditioner product comprises the following raw materials in percentage by weight: 40.7 percent of water agent; 31% of traditional Chinese medicine extracting solution; 7.9 percent of humectant; 8.15% of a thickening agent; 8.7% of a conditioning agent; 1.8 percent of emulsifier; 0.05% of complexing agent; 0.4% of hair-strengthening agent; 0.4% of antioxidant; 0.9 percent of flavoring agent. Wherein the Chinese medicinal components in the Chinese medicinal extractive solution comprise folium Platycladi, folium Verniciae Fordii, semen Sesami, semen Nelumbinis, Ginseng radix, rhizoma anemarrhenae, rhizoma Zingiberis recens, radix Angelicae sinensis and Polygoni Multiflori radix. And the traditional Chinese medicine components in the traditional Chinese medicine extracting solution comprise cacumen biotae, tung tree leaves, hemp seeds, lotus seeds, ginseng, rhizoma anemarrhenae, ginger, angelica and polygonum multiflorum in a ratio of 15: 8: 3.2: 1: 2.
In this embodiment, the aqueous solution is deionized water;
the humectant is glycerol, panthenol, and 1, 2-ethylene glycol;
the thickening agent is hydroxyethyl cellulose and cetyl alcohol;
the conditioner is behenyl trimethyl ammonium chloride, dimethyl silicone oil, jojoba oil, aminopropyl polydimethylsiloxane;
the emulsifier is polyoxyethylene sorbitan monooleate;
the complexing agent is EDTA-disodium;
the hair-setting agent is diaminopyrimidine oxide;
the antioxidant is p-hydroxyacetophenone;
the flavoring agent is essence.
Example 4
The formula of the anti-hair loss hair conditioner product comprises the following raw materials in percentage by weight: 42.15 percent of water agent; 29% of traditional Chinese medicine extracting solution; 5.7 percent of humectant; 8.2% of a thickening agent; 10.3% of a conditioner; 2.2 percent of emulsifier; 0.15 percent of complexing agent; 0.6% of hair-strengthening agent; 0.6 percent of antioxidant; 1.1% of flavoring agent.
Wherein the Chinese medicinal components in the Chinese medicinal extractive solution comprise folium Platycladi, folium Verniciae Fordii, semen Sesami, semen Nelumbinis, Ginseng radix, rhizoma anemarrhenae, rhizoma Zingiberis recens, radix Angelicae sinensis and Polygoni Multiflori radix. And the traditional Chinese medicine components in the traditional Chinese medicine extracting solution comprise cacumen biotae, tung tree leaves, hemp seed, lotus seed, ginseng, rhizoma anemarrhenae, ginger, angelica and polygonum multiflorum in a ratio of 15: 8: 3.2: 1: 2.
In this embodiment, the aqueous solution is deionized water;
the humectant is glycerol, panthenol, and 1, 2-ethylene glycol;
the thickening agent is hydroxyethyl cellulose and hexadecanol;
the conditioner is behenyl trimethyl ammonium chloride, dimethyl silicone oil, jojoba oil, aminopropyl polydimethylsiloxane;
the emulsifier is polyoxyethylene sorbitan monooleate;
the complexing agent is EDTA-disodium;
the hair-setting agent is diaminopyrimidine oxide;
the antioxidant is p-hydroxyacetophenone;
the flavoring agent is essence.
Example 5
A method for preparing hair conditioner by using a hair-loss-preventing hair conditioner product formula specifically comprises the following steps:
step S1, preparing a traditional Chinese medicine extracting solution by adopting cacumen biotae, tung tree leaves, hemp seeds, lotus seeds, ginseng, rhizoma anemarrhenae, ginger, angelica and polygonum multiflorum; the specific step of step S1 is as follows.
Step S101, crushing the hempseed and the lotus seeds, and uniformly mixing the crushed hempseed and the lotus seeds with the cacumen biotae, the tung tree leaves, the ginseng, the rhizoma anemarrhenae, the ginger, the angelica and the polygonum multiflorum to obtain a mixed material;
step S102, decocting the mixed material obtained in the step S101 and 4500ml of water for 2.5 hours, and filtering for the first time by using a 100-mesh screen;
step S103, adding 3500ml of water into the mixing residue in the step S102, decocting for 2.5h again, and filtering for the second time by using a 100-mesh screen;
step S104, combining the filtrates in the steps S102 and S103, and concentrating under reduced pressure to 3000ml, wherein the pressure of the reduced pressure concentration is-0.07 Mpa, and the temperature is 60 ℃; standing for 22h, filtering the combined filtrate with 100 mesh sieve, and refrigerating.
Step S2, mixing the traditional Chinese medicine extract with aqua, humectant, thickener, conditioner, emulsifier, complexing agent, hair-setting agent, antioxidant and flavoring agent to obtain the final product. The specific steps of step S2 are as follows:
step S201, adding hydroxyethyl cellulose into deionized water, heating to 45 ℃, and uniformly stirring to obtain a hydroxyethyl cellulose solution;
step S202, adding glycerol, ethanol, p-hydroxyacetophenone, EDTA-disodium and the hydroxyethyl cellulose solution obtained in the step S201 into a material tank at one time, stirring and heating to completely mix and dissolve the materials uniformly;
step S203, raising the temperature of the material tank to 73 ℃, sequentially adding cetyl alcohol, behenyl trimethyl ammonium chloride and polyoxyethylene sorbitan monooleate into the material tank, and stirring to uniformly mix and dissolve the materials;
step S204, raising the temperature of the material tank to 81 ℃ again, adding simethicone, jojoba oil and aminopropyl polydimethylsiloxane into the material tank, uniformly mixing the materials, homogenizing and keeping the temperature after uniform stirring, wherein the homogenizing speed is 3500r/min, and the homogenizing time is 2.5 min;
step S205, cooling the material tank to 50 ℃, adding the traditional Chinese medicine extracting solution prepared in the step S1 into the material tank, and uniformly stirring;
step S206, cooling the material tank to 45 ℃ again, adding diaminopyrimidine oxide, 1, 2-ethylene glycol and essence while stirring, then stirring and uniformly mixing the materials, and cooling to 35 ℃;
and S207, discharging, sampling and inspecting, filling and packaging the qualified intermediate product, and warehousing the qualified finished product.
Example 1 to example 4 were processed by the method of example 5, thereby obtaining a hair tonic product.
Experiment of
Randomly screening 50 women with hair health of 25-45 years old and length of more than 20cm for test, averagely dividing into 5 groups, wherein each group contains 10 people, respectively named as experiment group 1, experiment group 2, experiment group 3, experiment group 4 and control group 1, and respectively carrying out glossiness, toughness and softness test. The experimental results of this experiment are specifically shown in table 1 below.
And (3) testing the glossiness:
experiment groups 1 to 4 were performed by using the products prepared in examples 1 to 4, respectively, and volunteers in experiment groups 1 to 4 applied with the products of examples 1 to 4 for 5min after preliminary hair washing. The hair conditioner of the application is not smeared after the hair is preliminarily washed in the control group, and the hair conditioner is naturally dried. Combing the cleaned hair, flatly arranging a mirror at a position which is right aligned to the hair direction and is accurate to the position where the user can clear and see the top of the head, irradiating the light from the top of the head, wherein the brighter the round halo on the hair, the better the glossiness of the hair; the persons in experimental groups 1-4 had lighter crown blush indicating good gloss, while the persons in the control group had smaller and less blush.
And (3) testing the toughness:
before the volunteers in the experimental group 1-the experimental group 4 and the control group wash the hair, a bundle of hair with the length of about one inch is cut off and put into water, so that the hair with poor hair quality is easy to absorb water, and then sinks quickly; experimental group 1-experimental group 4 volunteers of each group applied the product of the present invention in examples 1-4 for 5min after washing their hair, and it was found that the hair of the test group personnel applied the product was significantly slow to sink after washing their hair and applying the hair conditioner of the product. The sinking speed of the hair of the control group personnel before and after hair washing is not different, so that the toughness test of the test group is better than that of the control group.
TABLE 1 comparison of experimental group 1-4 and control experiment results
Figure BDA0003689340580000081
Finally, it is noted that the above-mentioned preferred embodiments illustrate rather than limit the invention, and that, while the invention has been described in detail with reference to the above-mentioned preferred embodiments, it will be understood by those skilled in the art that various changes in form and detail may be made therein without departing from the scope of the invention as defined by the appended claims.

Claims (10)

1. The formula of the anti-hair loss hair conditioner product is characterized by comprising the following raw materials in percentage by weight: 40.7 to 44.7 percent of water agent; 29-31% of traditional Chinese medicine extracting solution; 5.7 to 7.9 percent of humectant; 5.8 to 8.2 percent of thickening agent; 8.7 to 10.3 percent of conditioner; 1.8 to 2.2 percent of emulsifier; 0.05 to 0.15 percent of complexing agent; 0.4-0.6% of hair-strengthening agent; 0.4 to 0.6 percent of antioxidant; 0.9 to 1.1 percent of flavoring agent.
2. The anti-alopecia hair conditioner product formula according to claim 1, wherein: the Chinese medicinal components in the Chinese medicinal extractive solution comprise folium Platycladi, folium Turpiniae, fructus Cannabis, semen Nelumbinis, Ginseng radix, rhizoma anemarrhenae, rhizoma Zingiberis recens, radix Angelicae sinensis and Polygoni Multiflori radix.
3. The anti-alopecia hair conditioner product formula according to claim 2, wherein: the Chinese medicinal components in the Chinese medicinal extractive solution comprise folium Platycladi, folium Tung, fructus Cannabis, semen Nelumbinis, Ginseng radix, rhizoma anemarrhenae, rhizoma Zingiberis recens, radix Angelicae sinensis and Polygoni Multiflori radix at a ratio of 15: 8: 3.2: 1: 2.
4. The anti-alopecia hair conditioner product formulation according to claim 1, 2 or 3, wherein:
the water agent is deionized water;
the humectant comprises glycerol, panthenol, and 1, 2-ethylene glycol;
the thickener comprises hydroxyethyl cellulose;
the conditioner comprises behenyl trimethyl ammonium chloride, dimethicone, jojoba oil, and aminopropyl polydimethylsiloxane;
the emulsifier comprises polyoxyethylene sorbitan monooleate;
the complexing agent is EDTA-disodium;
the hair setting agent comprises diaminopyrimidine oxide;
the antioxidant comprises p-hydroxyacetophenone;
the flavoring agent comprises essence.
5. The hair loss prevention and hair nourishing product formula according to claim 4, wherein the formula comprises the following components: the thickening agent also comprises cetyl alcohol or stearyl alcohol.
6. The hair loss preventing hair conditioner product formula according to any one of claims 1 to 5, further comprising a method for preparing a hair conditioner by using the hair loss preventing hair conditioner product formula, wherein the method specifically comprises the following steps:
step S1, preparing a traditional Chinese medicine extracting solution by adopting cacumen biotae, tung tree leaves, hemp seeds, lotus seeds, ginseng, rhizoma anemarrhenae, ginger, angelica and polygonum multiflorum;
and step S2, mixing the traditional Chinese medicine extract with a water aqua, a humectant, a thickening agent, a conditioning agent, an emulsifier, a complexing agent, a hair-strengthening agent, an antioxidant and a flavoring agent to obtain a finished product.
7. The method for preparing the formula of the hair loss prevention and hair nourishing product according to claim 6, wherein the method for preparing the traditional Chinese medicine extracting solution in the step S1 specifically comprises the following steps:
step S101, crushing the hempseed and the lotus seeds, and uniformly mixing the crushed hempseed and the lotus seeds with the cacumen biotae, the tung tree leaves, the ginseng, the rhizoma anemarrhenae, the ginger, the angelica and the polygonum multiflorum to obtain a mixed material;
step S102, decocting the mixed material obtained in the step S101 and 4000-;
step S103, adding 3000-4000ml of water into the mixing residue obtained in the step S102, decocting for 2-3h again, and then carrying out secondary filtration;
and step S104, combining the filtrates in the steps S102 and S103, concentrating under reduced pressure to 3100ml 2900-.
8. The method for preparing the formula of the hair tonic product of claim 6, wherein the step S2 comprises the following steps:
step S201, adding hydroxyethyl cellulose into deionized water, heating to 40-51 ℃, and uniformly stirring to obtain a hydroxyethyl cellulose solution;
step S202, adding glycerol, ethanol, p-hydroxyacetophenone, EDTA-disodium and the hydroxyethyl cellulose solution obtained in the step S201 into a material tank at one time, stirring and heating to completely mix and dissolve the materials uniformly;
step S203, raising the temperature of the material tank to 70-75 ℃, sequentially adding cetyl alcohol, behenyl trimethyl ammonium chloride and polyoxyethylene sorbitan monooleate into the material tank, and stirring to uniformly mix and dissolve the materials;
step S204, raising the temperature of the material tank to 80-82 ℃ again, adding simethicone, jojoba oil and aminopropyl polydimethylsiloxane into the material tank, uniformly mixing the materials, homogenizing after uniform stirring, and keeping the temperature;
step S205, cooling the material tank to 49-51 ℃, adding the traditional Chinese medicine extracting solution prepared in the step S1 into the material tank, and uniformly stirring;
step S206, cooling the material tank to 44-46 ℃ again, adding diaminopyrimidine oxide, 1, 2-glycol and essence while stirring, then stirring and uniformly mixing the materials, and cooling to 34-36 ℃;
and S207, discharging, sampling and inspecting, filling and packaging the qualified intermediate product, and warehousing the qualified finished product.
9. The method for preparing hair conditioner according to claim 7, wherein the pressure of the reduced pressure concentration in step S104 is-0.07 MPa and the temperature is 60 ℃ in the method for preparing the chinese herbal medicine extract.
10. The method as claimed in claim 8, wherein the step S204 comprises a homogenizing speed of 3000-4000r/min and a homogenizing time of 2-5 min.
CN202210658336.1A 2022-06-10 2022-06-10 Formula and preparation method of hair loss prevention and hair nourishing product Pending CN114848569A (en)

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CN115155356A (en) * 2022-09-06 2022-10-11 广州市发雅丝精细化工有限公司 Preparation method of hair loss preventing, hair strengthening and hair care cream

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CN104095792A (en) * 2014-07-22 2014-10-15 广州好迪集团有限公司 Hair conditioner capable of nourishing hair and repairing damage
CN111803426A (en) * 2020-07-17 2020-10-23 广州市逸轩精细化工有限公司 Anti-hair loss and hair-fixing nutrient solution and preparation method thereof
CN113476354A (en) * 2021-07-08 2021-10-08 科盈生物科技(惠州)有限公司 Hair loss preventing and hair nourishing hair conditioner

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CN104095792A (en) * 2014-07-22 2014-10-15 广州好迪集团有限公司 Hair conditioner capable of nourishing hair and repairing damage
CN111803426A (en) * 2020-07-17 2020-10-23 广州市逸轩精细化工有限公司 Anti-hair loss and hair-fixing nutrient solution and preparation method thereof
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