CN115227622A

CN115227622A - Preparation process of hair loss preventing and nourishing essence

Info

Publication number: CN115227622A
Application number: CN202210906279.4A
Authority: CN
Inventors: 叶超华; 叶曼钰
Original assignee: Huizhou Faluyuan Gene Technology Co ltd
Current assignee: Huizhou Faluyuan Gene Technology Co ltd
Priority date: 2022-07-29
Filing date: 2022-07-29
Publication date: 2022-10-25

Abstract

The invention relates to a preparation process of hair loss preventing and nourishing essence, which comprises the following steps: the method comprises the steps of crushing medicinal materials, soaking the medicinal materials and preparing a first stock solution: placing the first group of soak solution in an open container, heating in water bath to volatilize alcohol, adding 8000-10000 parts by mass of purified water, and heating with open fire to boil for 2-3 hours; filtering the first group of soak solution after heating and boiling to remove the dregs of a decoction, adding 400 to 500 parts by mass of alcohol, mixing and stirring uniformly to obtain 5000 to 6000 parts by mass of first stock solution; a second stock solution preparation step: placing the second group of soak solution in a sealed tank for water bath heating, and continuously shaking the sealed tank in the heating process; filtering the second group of soak solution heated in water bath to remove the dregs of a decoction to obtain a second stock solution; the preparation method of the essence comprises the following steps: mixing and stirring 4-7 parts by mass of the first stock solution and 1 part by mass of the second stock solution to obtain the essence.

Description

Process for preparing anti-hair-loss and hair-nourishing essence

Technical Field

The invention relates to the field of hair nourishing essence preparation, in particular to a preparation process of an anti-hair loss hair nourishing essence.

Background

The traditional Chinese medicine has a long history of treating alopecia, and the treatment method mainly comprises external treatment and internal treatment, the internal treatment method approximately divides alopecia into heart and spleen qi deficiency type alopecia, liver and kidney deficiency type alopecia, liver depression blood stasis type alopecia, qi and blood deficiency type alopecia, damp-heat accumulation type alopecia, blood deficiency and wind dryness type alopecia, phlegm and damp stasis heat type alopecia, damp and blood stasis mutual type alopecia, wind evil upward disturbance type alopecia and the like, and patients are diagnosed by doctors to treat alopecia by using the formulas of nourishing blood and enriching blood, nourishing liver and kidney, strengthening spleen and tonifying qi, nourishing yin and cooling blood, soothing liver and regulating qi, astringing and dredging collaterals, dispelling wind and removing dampness and the like, and the different types of the medicines are different. From the viewpoint of modern medicine, alopecia is mainly caused by genetic factors, living habits, living and working stress, hygiene and the like, and is mainly classified into androgenic alopecia and seborrheic alopecia. Some external products are already popularized and marketed, but mainly utilize products for promoting blood circulation and removing blood stasis and dispelling pungent and warm, such as salvia miltiorrhiza, ligusticum wallichii, ginger, pepper and the like, although some stimulation effects are exerted on hair growth, the external products also damage hair follicles and skin, and are not beneficial to dredging qi activity and promoting long-term hair growth and development.

However, a large amount of hair nourishing essence appears in the market, but the traditional hair nourishing essence has poor effect, is not very friendly to the scalp environment, and cannot meet the healthy hair nourishing requirement of users.

Disclosure of Invention

Therefore, the anti-hair-loss hair-nourishing essence preparation process is needed to solve the technical problems that the traditional hair-nourishing essence is poor in effect, not very friendly to the scalp environment and incapable of meeting the healthy hair-nourishing requirements of users.

A preparation process of the anti-hair-loss and hair-nourishing essence comprises the following steps:

crushing medicinal materials: mixing and stirring 30 to 60 parts by mass of drynaria rhizome, 30 to 60 parts by mass of cacumen biotae, 6 to 14 parts by mass of ginger, 6 to 14 parts by mass of centella asiatica, 6 to 14 parts by mass of ligusticum wallichii, 24 to 36 parts by mass of polygonum multiflorum, 6 to 14 parts by mass of eclipta alba, 6 to 14 parts by mass of glossy privet fruit, 6 to 14 parts by mass of prepared rehmannia root, 6 to 14 parts by mass of hibiscus syriacus leaf, 6 to 14 parts by mass of cortex dictamni, 14 to 26 parts by mass of saponin, 4 to 8 parts by mass of rhizoma acori graminei, 6 to 14 parts by mass of fructus cnidii and 24 to 36 parts by mass of mulberry leaf, and crushing the mixture to obtain a first group of hair nourishing medicinal material; mixing and stirring 3 to 7 parts by mass of black sesame, 12 to 18 parts by mass of walnut shell, 6 to 10 parts by mass of perilla leaf, 6 to 12 parts by mass of pearl bone, 12 to 18 parts by mass of ginseng, 6 to 14 parts by mass of angelica, 5 to 10 parts by mass of astragalus, 5 to 10 parts by mass of salvia miltiorrhiza and 6 to 14 parts by mass of polygonatum and crushing the mixture to obtain a second group of hair nourishing medicinal materials;

soaking the medicinal materials: soaking a first group of hair nourishing medicinal materials in 1000-2000 parts by mass of alcohol to obtain a first group of soaking solution; soaking a second group of hair-nourishing medicinal materials in 800-1200 parts by mass of alcohol to obtain a second group of soaking solution;

a first stock solution preparation step: placing the first group of soak solution in an open container, heating in water bath to volatilize alcohol, adding 8000-10000 parts by mass of purified water, and heating and boiling with open fire for 2-3 hours; filtering the first group of soak solution after heating and boiling to remove the dregs of a decoction, adding 400 to 500 parts by mass of alcohol, mixing and stirring uniformly to obtain 5000 to 6000 parts by mass of first stock solution;

a second stock solution preparation step: placing the second group of soak solution in a sealed tank for water bath heating, and continuously shaking the sealed tank in the heating process; filtering the second group of soak solution heated in water bath to remove the dregs of a decoction to obtain a second stock solution;

the preparation method of the essence comprises the following steps: mixing and stirring 4-7 parts by mass of the first stock solution and 1 part by mass of the second stock solution to obtain the essence.

In one embodiment, before the step of crushing the medicinal material, the method further comprises a step of washing the medicinal material: rhizoma drynariae, cacumen biotae, ginger, centella, ligusticum chuanxiong hort, polygonum multiflorum, eclipta alba, glossy privet fruit, prepared rehmannia root, shrubalthea leaf, cortex dictamni, chinese honeylocust fruit, rhizoma acori graminei, fructus cnidii, folium mori black sesame, walnut peel, perilla leaf, pearl, caulis perllae, ginseng, angelica, astragalus, salvia miltiorrhiza and rhizoma polygonati are cleaned and dried.

In one embodiment, in the first stock solution preparation step, the first group of soak solutions is placed in a beaker and heated in a water bath at 70-90 ℃ to volatilize alcohol.

In one embodiment, in the preparation of the second stock solution, the second group of soaking solutions is placed in a sealed tank to be heated in a water bath at 60-80 ℃.

In one embodiment, in the preparation of the second stock solution, the heating time in the water bath is 18 to 24 hours, and the soaking is continued for 5 to 7 days at normal temperature after the water bath is finished.

In one embodiment, in the step of soaking the medicinal materials, the alcohol concentration is 60% to 80%.

In one embodiment, in the essence preparation step, 0.0001 to 0.0002 part by mass of preservative is added.

In one embodiment, in the step of smoothing treatment, the preservative comprises the following components in parts by mass: 30 to 40 parts of p-hydroxyacetophenone, 30 to 40 parts of potassium sorbate and 30 to 40 parts of calcium propionate.

In one embodiment, in the step of smoothing, 0.3 to 0.5 parts by mass of a wetting agent is added in the step of preparing the essence.

In one embodiment, the wetting agent comprises the following components in parts by mass: 30 to 40 parts of glycerol, 30 to 40 parts of propylene glycol and 30 to 40 parts of betaine.

The preparation process of the anti-hair-loss and hair-nourishing essence liquid has simple and delicate steps and easy control, each step is carefully and minutely carried out, and essences in various hair-nourishing medicinal materials are greatly extracted. The anti-hair-loss and hair-nourishing essence prepared by the preparation process of the anti-hair-loss and hair-nourishing essence adopts pure natural Chinese medicinal materials, is environment-friendly to scalp, and has good effects of nourishing hair and preventing hair loss.

Drawings

FIG. 1 is a schematic flow chart of a process for preparing the hair loss preventing and nourishing essence in one embodiment;

fig. 2 is a schematic flow chart of a process for preparing the hair loss preventing and nourishing essence in another embodiment.

Detailed Description

In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.

Referring to fig. 1 and 2 together, the present invention provides a process for preparing an anti-alopecia and hair-nourishing essence, comprising the following steps:

step 102: crushing medicinal materials: mixing and stirring 30 to 60 parts by mass of drynaria rhizome, 30 to 60 parts by mass of cacumen biotae, 6 to 14 parts by mass of ginger, 6 to 14 parts by mass of centella asiatica, 6 to 14 parts by mass of ligusticum wallichii, 24 to 36 parts by mass of polygonum multiflorum, 6 to 14 parts by mass of eclipta alba, 6 to 14 parts by mass of glossy privet fruit, 6 to 14 parts by mass of prepared rehmannia root, 6 to 14 parts by mass of hibiscus syriacus leaf, 6 to 14 parts by mass of cortex dictamni, 14 to 26 parts by mass of saponin, 4 to 8 parts by mass of rhizoma acori graminei, 6 to 14 parts by mass of fructus cnidii and 24 to 36 parts by mass of mulberry leaf, and crushing the mixture to obtain a first group of hair nourishing medicinal material; mixing and stirring 3 to 7 parts of black sesame, 12 to 18 parts of walnut skin, 6 to 10 parts of perilla leaf, 6 to 12 parts of pearl bone, 12 to 18 parts of ginseng, 6 to 14 parts of angelica, 5 to 10 parts of astragalus, 5 to 10 parts of salvia miltiorrhiza and 6 to 14 parts of rhizoma polygonati in parts by mass, and crushing to obtain the second group of hair nourishing medicinal materials.

Particularly, the bone-breaking tonic has the effects of improving alopecia and treating alopecia areata, and can nourish the scalp and hair follicles to enable the hair follicles to generate new hairs. The cacumen biotae is a traditional Chinese medicine commonly used for treating alopecia, and has a good treatment effect mainly aiming at alopecia areata, alopecia, premature graying of hair and the like with blood heat in the alopecia treatment. Rhizoma Zingiberis recens can improve hair quality, reduce oil and fat, and reduce alopecia. The ginger is filled with capsaicin, and can stimulate scalp, promote scalp hyperemia, promote blood circulation, increase vascular permeability, accelerate scalp metabolism, enhance nutrient absorption of hair follicle, activate hair follicle tissue, relieve itching, prevent alopecia, and promote hair growth. The centella asiatica clears heat and promotes diuresis, detoxifies and reduces swelling, can effectively accelerate the generation of collagen, and plays a non-negligible supporting role in the filling of subcutaneous cells; promoting activity of scar fibroblast, increasing synthesis and secretion of collagen fiber and matrix component, and promoting expression of collagen protein. The ligusticum chuanxiong hort is a clinical commonly used traditional Chinese medicine, has the main functions of promoting qi and blood circulation and dispelling wind and relieving pain, and is called as a qi medicine in blood because the medicine can reach the head and the face. The medicine has wide functions, can be used for treating headache and gout and regulating qi and blood at ordinary times, and is often used in traditional Chinese medicine. Chuan Xiong is a commonly used medicine for treating alopecia. The traditional Chinese medicine has the main effects of tonifying qi and activating blood circulation, and can be used in combination with traditional Chinese medicines to treat alopecia. The ligusticum wallichii has a good moisturizing effect on hair, can play a role in relieving itching, moisturizing skin and activating blood, has a function of expanding capillary vessels of the head, and accordingly promotes blood circulation, enables the hair of each person to be nourished and moistened in a sufficient amount, and meanwhile enables the hair to have a good flexibility and a function of being not easy to become brittle.

The folium Hibisci can remove greasy dirt and dandruff on head, and improve hair dryness and knotting. The hibiscus leaf contains sapogenin, saponin and inositol which can play a role similar to soap, and also contains carotene, lutein, chrysanthemum, hibiscus mucilage and the like, and the substances can provide nutrition for hair, promote hair growth and solve the problems of excessive hair oil and scurf and the like caused by vigorous sebum secretion and vigorous liver fire. The black sesame contains various nutritional ingredients such as fat, protein, saccharides, lecithin, vitamin A, vitamin E, calcium, iron and the like, and can be beneficial to the growth of hair and increase melanin. The black sesame can improve hair luster, increase melanin formation, promote hair growth and regeneration, and has effects of anti-dandruff, anti-dryness, and depth regulation. The walnut skin can effectively provide nutrition required by hair, prevent hair from whitening, and increase the smoothness of hair. The Polygoni Multiflori radix has effects of promoting hair growth, preventing alopecia, and preventing premature gray hair. The Ecliptae herba has effects of promoting hair growth, blackening hair, and blackening hair. Fructus Ligustri Lucidi has effects in invigorating kidney and blackening hair. Radix rehmanniae Preparata for external use can promote hair growth. Ginseng radix has effects of promoting hair growth, reducing alopecia, repairing damaged hair, and nourishing and caring hair.

Cortex Dictamni Radicis has effects of clearing heat, eliminating dampness, dispelling pathogenic wind, removing toxic substances, etc. The Chinese honeylocust fruit has the effects of clearing heat, activating blood, preventing alopecia, helping hair regeneration, relieving itching and the like. Especially, the skin itch caused by dandruff is remarkably improved after washing hair with Chinese honeylocust fruit. The perilla leaf boiled water hair washing liquid has the effects of gloss, elasticity and blackening hair, because the perilla leaf can promote the absorption and metabolism of the hair and the hair to melanin and the blackening of the hair, can promote the absorption of the hair to mineral substances and trace elements, promotes the metabolism of the hair and can promote the absorption of nutrient substances. Blood circulation in the head promotes regeneration. The angelica has the effects of promoting blood circulation, enriching blood, relieving pain and moistening skin, and can also expand capillary vessels of scalp and skin and promote blood circulation. Radix astragali is a traditional Chinese medicine with hair loss preventing effect, contains various amino acids, betaine, folic acid, alkaloids and trace elements essential to human body, and has effects of dilating blood vessel, improving skin nutrition, preventing hair loss and promoting hair growth. The red sage root has the main functions of promoting blood circulation to disperse blood clots, and contains rich vitamins and trace elements Zn, cu, fe, etc. to promote the generation of hair melanin and improve white hair, yellow hair, dry hair, etc. caused by trace element deficiency.

Fructus Cnidii has good effects on itch, desquamation, excessive shedding, etc. of skin caused by bacteria and mites on scalp, and can be used for rapidly recovering hair. The mulberry leaf can promote hair growth, relieve alopecia, cool blood, stop bleeding, remove oil on hair, relieve itching, and nourish scalp. Herba Speranskiae Tuberculatae has effects of treating alopecia, and can also be used for treating seborrheic dermatitis, seborrheic alopecia, etc.

Step 103: soaking the medicinal materials: soaking the first group of hair nourishing medicinal materials in 1000-2000 parts by mass of alcohol to obtain a first group of soaking solution. Soaking the second group of hair nourishing medicinal materials in 800 to 1200 parts by mass of alcohol to obtain a second group of soaking solution.

Specifically, soak the first group of hair care medicinal materials in 1000 parts to 2000 parts of alcohol by mass to obtain a first group of soak solution, and on the one hand, the alcohol can sterilize the first group of hair care medicinal materials, and on the other hand, essence in the first group of hair care medicinal materials can be dissolved in the alcohol. Soaking the second group of hair nourishing medicinal materials in 800-1200 parts by mass of alcohol to obtain a second group of soaking solution. Likewise, on the one hand, the alcohol can sterilize and disinfect the second group of hair care medicinal materials, and on the other hand, essence in the second group of hair care medicinal materials can be dissolved into the alcohol. In this embodiment, in the step of soaking the herbs, the alcohol concentration is 60% to 80%.

Step 104: a first stock solution preparation step: and (3) placing the first group of soak solution in an open container, heating in water bath to volatilize alcohol, adding 8000-10000 parts by mass of purified water, and heating and boiling for 2-3 hours by using open fire. Filtering the first group of soak solution after heating and boiling to remove dregs, adding 400-500 parts by mass of alcohol, mixing and stirring uniformly to obtain 5000-6000 parts by mass of first stock solution.

Specifically, the first group of soak solution is placed in an open container to be heated in water bath to volatilize alcohol, then purified water with the mass part of 8000-10000 parts is added, and the mixture is heated and boiled for 2-3 hours by open fire. In this embodiment, the first group of soaking solutions is placed in a beaker and heated in a water bath at 70-90 ℃ to volatilize alcohol. Filtering the first group of soak solution after heating and boiling to remove the dregs of a decoction, adding 400 to 500 parts by mass of alcohol, mixing and stirring uniformly to obtain 5000 to 6000 parts by mass of first stock solution.

Step 105: a second stock solution preparation step: and (3) placing the second group of soaking solution in a sealed tank for water bath heating, and continuously shaking the sealed tank in the heating process. And filtering the second group of soak solution heated in water bath to remove the dregs to obtain a second stock solution.

Specifically, the second group of soak solution is placed in a sealed tank for water bath heating, and the sealed tank is continuously shaken in the heating process. And filtering the second group of soak solution heated in water bath to remove the dregs to obtain a second stock solution. In the embodiment, the second group of soaking solution is placed in a sealed tank to be heated in a water bath at 60-80 ℃. Further, in this embodiment, the heating time in the water bath is 18 hours to 24 hours, and the water bath is left at room temperature for further soaking for 5 days to 7 days.

Step 106: the preparation method of the essence comprises the following steps: mixing and stirring 4-7 parts by mass of the first stock solution and 1 part by mass of the second stock solution to obtain the essence.

Specifically, 4-7 parts by mass of a first stock solution and 1 part by mass of a second stock solution are mixed and stirred to obtain the essence.

In order to remove dust impurities from hair nourishing herbs, in one embodiment, before the step of crushing the herbs, the method further comprises the step 101: the method comprises the following steps: rhizoma drynariae, cacumen biotae, ginger, centella, ligusticum chuanxiong hort, polygonum multiflorum, eclipta alba, glossy privet fruit, prepared rehmannia root, shrubalthea leaf, cortex dictamni, chinese honeylocust fruit, rhizoma acori graminei, fructus cnidii, folium mori black sesame, walnut peel, perilla leaf, pearl, caulis perllae, ginseng, angelica, astragalus, salvia miltiorrhiza and rhizoma polygonati are cleaned and dried. So, carry out effectively with the dust impurity on the hair care medicinal material, moisture content on the other hand stoving hair care medicinal material is favorable to the later stage to draw the essence in the hair care medicinal material.

In order to increase the shelf life of the essence, in one embodiment, 0.0001 to 0.0002 part by mass of a preservative is added in the essence preparation step. Further, in this embodiment, in the step of smoothing treatment, the preservative comprises the following components in parts by mass: 30 to 40 parts of p-hydroxyacetophenone, 30 to 40 parts of potassium sorbate and 30 to 40 parts of calcium propionate. 0.0001 to 0.0002 part by mass of preservative does not cause harm to human bodies on one hand, and can prolong the shelf life of the essence on the other hand.

In order to increase the moisturizing effect of the essence, in one embodiment, in the step of smoothing, in the step of preparing the essence, 0.3 to 0.5 parts by mass of a humectant is added. Further, in this embodiment, the wetting agent includes the following components in parts by mass: 30 to 40 parts of glycerol, 30 to 40 parts of propylene glycol and 30 to 40 parts of betaine. Therefore, the moisture of the essence is increased, and the skin can absorb the essence more conveniently.

In order to increase the fragrance of the essence, in one embodiment, in the step of smoothing treatment, in the step of preparing the essence, 0.0003 to 0.0005 part by mass of plant essence is added. The plant essence with the mass portion of 0.0003 to 0.0005 does not cause harm to human bodies on one hand, and can cover or adjust the original smell of the essence liquid on the other hand, so that people feel comfortable.

The preparation process of the anti-hair-loss and hair-nourishing essence is concise and delicate in steps and easy to control, each step is careful and fine, and essence in various hair-nourishing medicinal materials is greatly extracted. The anti-hair-loss and hair-nourishing essence prepared by the preparation process of the anti-hair-loss and hair-nourishing essence adopts pure natural traditional Chinese medicinal materials, is environment-friendly to scalp, and has good effects of nourishing hair and preventing hair loss.

The technical features of the above embodiments can be arbitrarily combined, and for the sake of brevity, all possible combinations of the technical features in the above embodiments are not described, but should be considered as the scope of the present specification as long as there is no contradiction between the combinations of the technical features.

The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is specific and detailed, but not to be understood as limiting the scope of the invention. It should be noted that various changes and modifications can be made by those skilled in the art without departing from the spirit of the invention, and these changes and modifications are all within the scope of the invention. Therefore, the protection scope of the present patent should be subject to the appended claims.

Claims

1. The preparation process of the anti-hair-loss and hair-nourishing essence is characterized by comprising the following steps of:

crushing medicinal materials: mixing and stirring 30 to 60 parts of rhizoma drynariae, 30 to 60 parts of cacumen biotae, 6 to 14 parts of ginger, 6 to 14 parts of centella, 6 to 14 parts of ligusticum wallichii, 24 to 36 parts of polygonum multiflorum, 6 to 14 parts of eclipta alba, 6 to 14 parts of glossy privet fruit, 6 to 14 parts of prepared rehmannia root, 6 to 14 parts of hibiscus syriacus leaf, 6 to 14 parts of cortex dictamni, 14 to 26 parts of Chinese honeylocust fruit, 4 to 8 parts of rhizoma acori graminei, 6 to 14 parts of fructus cnidii and 24 to 36 parts of mulberry leaf by mass, and crushing to obtain a first group of hair nourishing medicinal material; mixing and stirring 3 to 7 parts by mass of black sesame, 12 to 18 parts by mass of walnut skin, 6 to 10 parts by mass of perilla leaf, 6 to 12 parts by mass of pearl bone, 12 to 18 parts by mass of ginseng, 6 to 14 parts by mass of angelica, 5 to 10 parts by mass of astragalus, 5 to 10 parts by mass of salvia miltiorrhiza and 6 to 14 parts by mass of polygonatum and crushing to obtain a second group of hair nourishing medicinal materials;

a second stock solution preparation step: placing the second group of soak solution in a sealed tank for water bath heating, and continuously shaking the sealed tank in the heating process; filtering the second group of soak solution heated in water bath to remove the dregs to obtain a second stock solution;

2. The process according to claim 1, further comprising a step of washing the crude drug before the step of pulverizing the crude drug: rhizoma drynariae, cacumen biotae, ginger, centella, ligusticum chuanxiong hort, polygonum multiflorum, eclipta alba, glossy privet fruit, prepared rehmannia root, shrubalthea leaf, cortex dictamni, chinese honeylocust fruit, rhizoma acori graminei, fructus cnidii, folium mori black sesame, walnut peel, perilla leaf, pearl, caulis perllae, ginseng, angelica, astragalus, salvia miltiorrhiza and rhizoma polygonati are cleaned and dried.

3. The process of claim 1, wherein in the first stock solution preparation step, the first group of soaking solutions are placed in a beaker and heated in a water bath at 70-90 ℃ to volatilize alcohol.

4. The process of claim 1, wherein in the preparation of the second stock solution, the second group of soaking solutions is placed in a sealed tank and subjected to water bath heating at 60-80 ℃.

5. The process as claimed in claim 1, wherein the second stock solution is prepared by heating in water bath for 18-24 hr, and soaking at room temperature for 5-7 days.

6. The process according to claim 5, wherein in the step of soaking the medicinal material, the alcohol concentration is 60 to 80%.

7. The process according to claim 6, wherein in the essence preparation step, 0.0001 to 0.0002 parts by mass of preservative is added.

8. The process according to claim 7, wherein in the slip-polishing step, the preservative comprises the following components in parts by mass: 30 to 40 parts of p-hydroxyacetophenone, 30 to 40 parts of potassium sorbate and 30 to 40 parts of calcium propionate.

9. The process according to claim 1, wherein in the step of smoothing treatment, in the step of preparing the essence, 0.3 to 0.5 parts by mass of a wetting agent is added.

10. The process according to claim 9, wherein the wetting agent comprises the following components in parts by mass: 30 to 40 parts of glycerol, 30 to 40 parts of propylene glycol and 30 to 40 parts of betaine.