CN113197805A - Polygonum multiflorum soft moisturizing shampoo and preparation method thereof - Google Patents

Polygonum multiflorum soft moisturizing shampoo and preparation method thereof Download PDF

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Publication number
CN113197805A
CN113197805A CN202110487177.9A CN202110487177A CN113197805A CN 113197805 A CN113197805 A CN 113197805A CN 202110487177 A CN202110487177 A CN 202110487177A CN 113197805 A CN113197805 A CN 113197805A
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parts
extract
polygonum multiflorum
shampoo
soft
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刘绍贵
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Xiamen Lijiacheng Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q7/00Preparations for affecting hair growth
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

Abstract

The invention discloses a polygonum multiflorum soft moisturizing shampoo and a preparation method thereof, wherein the polygonum multiflorum soft moisturizing shampoo comprises the following components in parts by weight: 17-25 parts of polygonum multiflorum extract, 12-16 parts of ginseng extract, 12-17 parts of angelica extract, 2-5 parts of argy wormwood leaf essential oil, 1-6 parts of ginger extract, 0.5-1 part of rose essential oil, 14-20 parts of polydimethylsiloxane, 4-11 parts of lauryl alcohol sulfate ammonium salt, 6-10 parts of glycerol, 2-6 parts of EDTA disodium, 0.01-0.05 part of hydroxyethyl cellulose, 0.2-0.7 part of phenoxyethanol, 14-21 parts of glossy privet fruit extract and 16-30 parts of deionized water. The polygonum multiflorum soft moistening shampoo disclosed by the invention can prevent hair loss and promote hair growth.

Description

Polygonum multiflorum soft moisturizing shampoo and preparation method thereof
Technical Field
The invention relates to the technical field of daily necessities, in particular to polygonum multiflorum soft moistening shampoo and a preparation method thereof.
Background
The hair not only plays an important role in human instrument appearance, but also is an important index of human health condition from the perspective of traditional Chinese medicine. The factors of the fast pace of modern life, the stress and tension of work, diet and interaction and the like increase the generation of alopecia symptoms from a new field, and even partially expand to a young group in modern cities. Alopecia is mainly caused by hair pore blockage, hair follicle cell cachexia caused by excessive grease secretion and the like. Under normal conditions, the hair papilla in the hair follicle has abundant capillary vessels, and can absorb nutrients necessary for hair growth from blood to ensure the normal growth of the hair. The hair can be about 50-100 hairs lost per day due to metabolism, but the whole quantity of the hairs is not affected. However, due to the excessive secretion of sebaceous glands, the blockage of pores, etc., the environment for normal hair growth is damaged, so that the hair cannot grow normally, and phenomena such as alopecia, hair breakage, etc. occur.
With the acceleration of the pace of life of people, the alopecia caused by factors such as increased working pressure, excessive mental development, irregular diet and environmental changes accounts for the majority, and people suffering from alopecia are also younger and younger. According to the statistics of an authoritative institution, the proportion of male pattern alopecia of 25-35 years old men in China is up to 40 percent, and the total number of men is over 1.5 hundred million; it has been shown by investigation that hair loss is showing a tendency to youthful.
Chinese patent document CN106074351A discloses an anti-hair loss shampoo, which comprises the following components, by weight, 20 parts of root bark of white mulberry, 12 parts of rose twig, 2 parts of walnut, 5 parts of Chinese date, 4 parts of silicone oil, 80 parts of lemon juice, 10 parts of raspberry, 10 parts of willow branch, 10 parts of eclipta alba, 12 parts of angelica, 6 parts of polygonum multiflorum, 4 parts of cinnamon, 50 parts of honey, 20 parts of glycerol, 10 parts of paraffin, 10 parts of sodium phenylpropionate, 6 parts of glycerol, 8 parts of hemp leaf, 8 parts of mulberry leaf and 1 part of essence.
Chinese patent document CN104940116A discloses an anti-hair loss shampoo, which is prepared from the following raw materials in parts by weight: 20 to 25 portions of tuber fleeceflower root, 10 to 12 portions of astragalus root, 15 to 20 portions of acanthopanax root, 15 to 20 portions of tall gastrodia tuber, 15 to 20 portions of yeast, 10 to 12 portions of black bean, 15 to 20 portions of costus root, 10 to 15 portions of ginger, 12 to 16 portions of white mulberry root-bark, 12 to 15 portions of medlar, 0.8 to 1.0 portion of camellia seed oil, 1 to 1.2 portions of sodium dodecyl benzene sulfonate, 0.5 to 0.8 portion of coconut oleic acid monoethanolamide and 0.1 to 0.5 portion of essence.
Chinese patent document CN107510647A discloses an anti-hair loss shampoo and a preparation method thereof, wherein the anti-hair loss shampoo comprises the following components in percentage by weight: 0.2-0.6% of argyi leaf essential oil, 2.8-4.6% of stephania delavayi, 0.2-0.4% of cacumen biotae extract, 0.3-0.6% of ferment, 0.2-0.5% of probiotic freeze-dried powder, 16-20% of alpha-alkenyl sodium sulfonate, 14-16% of sodium lauroyl glutamate, 1-3% of cocamidopropyl betaine, 0.5-2% of sodium chloride, 1-3% of glycerol, 0.2-0.5% of methylparaben, 0.1-0.3% of disodium edetate, 0.1-0.2% of citric acid and 48.3-63.4% of deionized water.
At present, products for preventing hair loss on the market are various in types, but have the problems of unobvious effect and the like. Therefore, the inventor has paid creative work to develop a new shampoo.
Disclosure of Invention
In view of the above, the present invention aims to provide a polygonum multiflorum softening and moistening shampoo and a preparation method thereof, wherein the polygonum multiflorum softening and moistening shampoo can prevent hair loss and promote hair growth.
The adopted technical scheme is as follows:
the invention relates to polygonum multiflorum soft moisturizing shampoo which comprises the following components in parts by weight:
Figure BDA0003050922920000021
Figure BDA0003050922920000031
further, the polygonum multiflorum extract is obtained by the following preparation method: pulverizing Polygoni Multiflori radix, and subjecting to supercritical CO2Extracting to obtain Polygoni Multiflori radix extractive solution, and sequentially coarse filtering and fine filtering to obtain Polygoni Multiflori radix extract.
The Ginseng radix extract, radix Angelicae sinensis extract, rhizoma Zingiberis recens extract and fructus Ligustri Lucidi extract can be prepared by referring to the preparation method of Polygoni Multiflori radix.
The preparation method of the polygonum multiflorum soft and moist shampoo comprises the following steps:
s1, putting deionized water, polydimethylsiloxane, lauryl alcohol sulfate ammonium salt, glycerol and EDTA disodium into a reaction kettle according to a ratio, heating to 70-80 ℃, and fully stirring and uniformly mixing the components;
s2, putting the argy wormwood leaf essential oil and the rose essential oil into the reaction kettle according to the proportion, maintaining the temperature at 70-80 ℃, and fully stirring and uniformly mixing the components;
s3, maintaining the temperature at 70-80 ℃, adding the polygonum multiflorum extract, the ginseng extract, the angelica extract, the ginger extract and the glossy privet fruit extract according to the mixture ratio, fully stirring and uniformly mixing;
s4, cooling to 30-35 ℃, adding hydroxyethyl cellulose and phenoxyethanol according to the proportion, fully stirring and uniformly mixing.
Further, the preparation method of the polygonum multiflorum soft and moist shampoo also comprises the following steps:
and S5, discharging, filling and warehousing after the materials are qualified through inspection.
In the above-mentioned technical solution,
the Polygonum multiflorum extract can improve the activity of the melanin, and more active melanocytes and more active tyrosinase can generate more melanin, and more melanin can make hair darker. The Polygoni Multiflori radix is preferably supercritical CO2The plant activity is very high by extraction, so that the hair follicle health can be better protected, the growth of the hair follicle is promoted, and the effects of hair growth and hair blacking are achieved.
The ginseng extract can make hair softer and reduce dandruff, and can be combined with the polygonum multiflorum extract to promote hair growth and prevent alopecia.
The angelica sinensis extract has the effects of promoting hair growth and nourishing hair, has high nutrient content, can promote blood circulation and enrich blood, and can improve hair loss caused by deficiency of qi and blood, thereby preventing alopecia.
On one hand, the ginger extract can promote blood circulation and prevent alopecia; in the second aspect, the ginger extract contains gingerol, which can stimulate scalp, provide more nutrition to hair, and promote hair growth.
The fructus Ligustri Lucidi extract is mainly oleanolic acid, which can improve microcirculation around hair follicle, especially regulate blood supply of hair papilla at key part of hair follicle cycle growth, promote hair growth, and prevent alopecia.
The folium Artemisiae Argyi essential oil has effects of relieving itching, removing dandruff and caring hair.
The rose essential oil and the argy wormwood leaf essential oil have the hair care effect, and the rose essential oil enables the hair to be smoother and glossy.
The polydimethylsiloxane can effectively improve the wet combing performance and the dry combing performance of the hair, has good antistatic effect and can improve the hair flying phenomenon. Giving the hair a smooth and soft hand. Has good compatibility with hair, and can effectively repair damaged hair.
The ammonium lauryl sulfate salt is a foaming agent and has a cleaning effect.
The glycerin can keep the hair moisture and luster, and avoid hair bifurcation.
Disodium EDTA is a chelating agent used to stabilize the formulation system of the polygonum multiflorum soft moisturizing shampoo.
Hydroxyethyl cellulose is used as a thickener. The phenoxyethanol has the function of antisepsis.
The invention has the beneficial effects that:
in the polygonum multiflorum softening and moistening shampoo, the polygonum multiflorum extract has a good hair growing and blackening effect, and the ginseng extract, the angelica extract, the ginger extract and the glossy privet fruit extract can prevent hair loss and promote hair growth. The polygonum multiflorum soft and moist shampoo has the advantages that the polygonum multiflorum extract is used as a main drug, the ginseng extract, the angelica extract, the ginger extract and the glossy privet fruit extract are used as auxiliary drugs, the main drug and the auxiliary drugs mutually promote and complement each other in respective effects, and the auxiliary drugs are synergistic, so that the polygonum multiflorum soft and moist shampoo can prevent hair loss, promote hair growth and have a hair blackening effect.
Detailed Description
The present invention is described in detail below with reference to specific examples, but the use and purpose of these exemplary embodiments are merely to exemplify the present invention, and do not set forth any limitation on the actual scope of the present invention in any form, and the scope of the present invention is not limited thereto.
Example 1
The polygonum multiflorum soft moistening shampoo disclosed by the embodiment comprises the following components in parts by weight:
Figure BDA0003050922920000051
wherein the polygonum multiflorum extract is prepared by the following preparation method: pulverizing Polygoni Multiflori radix, and subjecting to supercritical CO2Extracting to obtain Polygoni Multiflori radix extractive solution, and sequentially coarse filtering and fine filtering to obtain Polygoni Multiflori radix extract.
Ginseng radix extract, radix Angelicae sinensis extract, rhizoma Zingiberis recens extract and fructus Ligustri Lucidi extract are prepared by the method of Polygoni Multiflori radix.
The preparation method of the polygonum multiflorum soft moisturizing shampoo comprises the following steps:
s1, putting deionized water, polydimethylsiloxane, lauryl alcohol sulfate ammonium salt, glycerol and EDTA disodium into a reaction kettle according to a ratio, heating to 70-80 ℃, and fully stirring and uniformly mixing the components;
s2, putting the argy wormwood leaf essential oil and the rose essential oil into the reaction kettle according to the proportion, maintaining the temperature at 70-80 ℃, and fully stirring and uniformly mixing the components;
s3, maintaining the temperature at 70-80 ℃, adding the polygonum multiflorum extract, the ginseng extract, the angelica extract, the ginger extract and the glossy privet fruit extract according to the mixture ratio, fully stirring and uniformly mixing;
s4, cooling to 30-35 ℃, adding hydroxyethyl cellulose and phenoxyethanol according to the proportion, fully stirring and uniformly mixing;
and S5, discharging, filling and warehousing after the materials are qualified through inspection.
Example 2
Referring to example 1, unlike example 1, the polygonum multiflorum soft moisturizing shampoo of the present example comprises the following components in parts by weight:
Figure BDA0003050922920000061
the preparation method is as in example 1.
Example 3
Referring to example 1, unlike example 1, the polygonum multiflorum soft moisturizing shampoo of the present example comprises the following components in parts by weight:
the polygonum multiflorum soft moistening shampoo disclosed by the embodiment comprises the following components in parts by weight:
Figure BDA0003050922920000071
comparative example 1
Referring to example 2, unlike example 2, the polygonum multiflorum soft moisturizing shampoo of this comparative example does not contain the ginseng extract and the angelica sinensis extract is 29 parts.
Comparative example 2
Referring to example 2, unlike example 2, the polygonum multiflorum soft lotion of this comparative example does not include the angelica extract and the ginseng extract is 29 parts.
Test and test:
test 1
1. Test materials: polygonum multiflorum smoothing shampoo prepared in example 1, example 2, example 3, comparative example 1 and comparative example 2.
2. Test subjects: 50 rats were selected, half male and half female, weighing about 200 g.
3. The test method comprises the following steps:
dividing the rats into five groups at random, wherein each group comprises 10 rats, each half of the rats are male and female, the back of each rat takes the spine as a midline, and the rats are uniformly divided into 4 blocks of area ABCD (2cm multiplied by 2cm) from the head to the tail, and the left half and the right half; after hair removal, the right side of each group of rats was applied with the polygonum multiflorum smoothing shampoo prepared in example 1, example 2, example 3, comparative example 1 and comparative example 2, and the left side was applied with distilled water as a blank. After 28 days, a bunch of new hairs are pulled out from the smearing region, 10 longer hairs are selected by visual inspection and measured by a vernier caliper, and the average value is taken as the growth length value of the rat hairs in the region. And carefully collecting and weighing the hair on the smearing area as a rat hair growth weight value.
4. And (3) test results:
the test results are shown in table 1.
Table 1: growth length of rat hair and growth weight of rat hair
Figure BDA0003050922920000081
Test 2
1. Test materials: polygonum multiflorum smoothing shampoo prepared in example 1, example 2, example 3, comparative example 1 and comparative example 2.
2. Test subjects: 60 persons, 50 men and 10 women with age of 28-47 years and head skin health without allergy or scar and alopecia without other local systemic diseases are selected.
3. The test method comprises the following steps:
60 hair loss patients were randomly divided into five groups, namely, example 1 group, example 2 group, example 3 group, comparative example 1 group and comparative example 2 group, each group consisting of 12 persons, male 10 persons and female 2 persons, and the polygonum multiflorum soft moistening shampoo prepared in example 1, example 2, example 3, comparative example 1 and comparative example 2 was used. Before trial, the condition of the health condition of the hair is tracked, so that a bald person combs the hair through 10 times by using a provided standard oak comb before trying to wash the hair every time, the number of the hair falling in each time is recorded, the tracking is continued for one month, and the records are summarized into a table.
During the product trial process, the testee is required to wash the hair once every two days, the polygonum multiflorum soft moistening shampoo is kept on the hair for 3 minutes and is properly massaged, and then the polygonum multiflorum soft moistening shampoo is washed clean by water.
4. And (3) test results:
the test results are shown in table 2.
Table 2: number of alopecia of trial before and after use
Figure BDA0003050922920000091
The above-listed detailed description is only a specific description of a possible embodiment of the present invention, and they are not intended to limit the scope of the present invention, and equivalent embodiments or modifications made without departing from the technical spirit of the present invention should be included in the scope of the present invention.

Claims (4)

1. The fleece-flower root soft moistening shampoo is characterized by comprising the following components in parts by weight:
Figure FDA0003050922910000011
2. the polygonum multiflorum smoothing shampoo of claim 1, wherein polygonum multiflorum is crushed and then subjected to supercritical CO2Extracting to obtain Polygoni Multiflori radix extractive solution, and sequentially coarse filtering and fine filtering to obtain Polygoni Multiflori radix extract.
3. A method of preparing the polygonum multiflorum soft moisturizing shampoo of claim 1 or 2, comprising the steps of:
s1, putting deionized water, polydimethylsiloxane, lauryl alcohol sulfate ammonium salt, glycerol and EDTA disodium into a reaction kettle according to a ratio, heating to 70-80 ℃, and fully stirring and uniformly mixing the components;
s2, putting the argy wormwood leaf essential oil and the rose essential oil into the reaction kettle according to the proportion, maintaining the temperature at 70-80 ℃, and fully stirring and uniformly mixing the components;
s3, maintaining the temperature at 70-80 ℃, adding the polygonum multiflorum extract, the ginseng extract, the angelica extract, the ginger extract and the glossy privet fruit extract according to the mixture ratio, fully stirring and uniformly mixing;
s4, cooling to 30-35 ℃, adding hydroxyethyl cellulose and phenoxyethanol according to the proportion, fully stirring and uniformly mixing.
4. The method for preparing polygonum multiflorum soft and moist shampoo according to claim 3, further comprising:
and S5, discharging, filling and warehousing after the materials are qualified through inspection.
CN202110487177.9A 2021-05-05 2021-05-05 Polygonum multiflorum soft moisturizing shampoo and preparation method thereof Pending CN113197805A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114159367A (en) * 2022-01-19 2022-03-11 广州莎莎化妆品制造有限公司 Long-acting hair blackening liquid and preparation method thereof

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CN104606118A (en) * 2015-02-14 2015-05-13 龚俊豪 Plant liquid shampoo for nourishing scalp hairs and preventing hair loss and white hairs and preparation method for plant liquid shampoo
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CN108578328A (en) * 2018-07-18 2018-09-28 广州市辰诺生物科技有限公司 A kind of composition and its shampoo and preparation method for improving alopecia and nursing scalp
CN109316430A (en) * 2017-07-31 2019-02-12 何学军 A kind of nourishing type shampoo
CN109453357A (en) * 2018-12-25 2019-03-12 山东盛宏医药科技有限公司 A kind of external application Chinese medicine paste and preparation method thereof with hair growing black hair
CN112043647A (en) * 2020-10-16 2020-12-08 湖南金昌生物技术有限公司 Formula and preparation process of smoothing and anti-dandruff tea bran shampoo

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WO1997042964A1 (en) * 1996-05-14 1997-11-20 Universal Biolog Enterprises I Method and product for promoting hair growth and treating skin conditions
CN101904908A (en) * 2010-07-08 2010-12-08 北京章光101科技股份有限公司 Anti-hair loss traditional Chinese medicine composition, preparation method and application thereof to preparing anti-hair loss products
CN104606118A (en) * 2015-02-14 2015-05-13 龚俊豪 Plant liquid shampoo for nourishing scalp hairs and preventing hair loss and white hairs and preparation method for plant liquid shampoo
CN109316430A (en) * 2017-07-31 2019-02-12 何学军 A kind of nourishing type shampoo
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CN112043647A (en) * 2020-10-16 2020-12-08 湖南金昌生物技术有限公司 Formula and preparation process of smoothing and anti-dandruff tea bran shampoo

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114159367A (en) * 2022-01-19 2022-03-11 广州莎莎化妆品制造有限公司 Long-acting hair blackening liquid and preparation method thereof

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