CN103251541B - A kind of shampoo containing arasaponin and preparation method thereof - Google Patents
A kind of shampoo containing arasaponin and preparation method thereof Download PDFInfo
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- CN103251541B CN103251541B CN201310206594.7A CN201310206594A CN103251541B CN 103251541 B CN103251541 B CN 103251541B CN 201310206594 A CN201310206594 A CN 201310206594A CN 103251541 B CN103251541 B CN 103251541B
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- ammonium salt
- radix notoginseng
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- 239000002453 shampoo Substances 0.000 title claims abstract description 60
- 238000002360 preparation method Methods 0.000 title claims abstract description 38
- 235000003143 Panax notoginseng Nutrition 0.000 claims abstract description 155
- 241000180649 Panax notoginseng Species 0.000 claims abstract description 155
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 141
- 239000000284 extract Substances 0.000 claims abstract description 139
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 138
- 239000008367 deionised water Substances 0.000 claims abstract description 101
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 101
- 239000011780 sodium chloride Substances 0.000 claims abstract description 69
- 230000002421 anti-septic effect Effects 0.000 claims abstract description 65
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 65
- 239000002994 raw material Substances 0.000 claims abstract description 29
- 238000000034 method Methods 0.000 claims abstract description 11
- 239000004094 surface-active agent Substances 0.000 claims abstract description 11
- 239000003945 anionic surfactant Substances 0.000 claims abstract description 10
- 239000003093 cationic surfactant Substances 0.000 claims abstract description 10
- 239000002888 zwitterionic surfactant Substances 0.000 claims abstract description 10
- 239000002562 thickening agent Substances 0.000 claims abstract description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 181
- -1 propyl hydroxy sulfobetaine Chemical compound 0.000 claims description 171
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 168
- 238000003756 stirring Methods 0.000 claims description 115
- 150000001768 cations Chemical group 0.000 claims description 107
- 244000060011 Cocos nucifera Species 0.000 claims description 75
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 75
- 229920002907 Guar gum Polymers 0.000 claims description 68
- 239000000665 guar gum Substances 0.000 claims description 68
- 229960002154 guar gum Drugs 0.000 claims description 68
- 235000010417 guar gum Nutrition 0.000 claims description 68
- SFNALCNOMXIBKG-UHFFFAOYSA-N ethylene glycol monododecyl ether Chemical compound CCCCCCCCCCCCOCCO SFNALCNOMXIBKG-UHFFFAOYSA-N 0.000 claims description 58
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims description 53
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 51
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 51
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims description 48
- 238000002156 mixing Methods 0.000 claims description 43
- 239000000047 product Substances 0.000 claims description 41
- 241000219112 Cucumis Species 0.000 claims description 39
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 claims description 39
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 claims description 39
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims description 39
- 239000003292 glue Substances 0.000 claims description 39
- 229920002545 silicone oil Polymers 0.000 claims description 38
- ILRSCQWREDREME-UHFFFAOYSA-N dodecanamide Chemical compound CCCCCCCCCCCC(N)=O ILRSCQWREDREME-UHFFFAOYSA-N 0.000 claims description 37
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 32
- 239000000194 fatty acid Substances 0.000 claims description 32
- 229930195729 fatty acid Natural products 0.000 claims description 32
- 150000004665 fatty acids Chemical class 0.000 claims description 32
- 125000000217 alkyl group Chemical group 0.000 claims description 31
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 31
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 31
- 230000001476 alcoholic effect Effects 0.000 claims description 24
- 150000002148 esters Chemical class 0.000 claims description 23
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 21
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 21
- 238000004821 distillation Methods 0.000 claims description 18
- 239000007788 liquid Substances 0.000 claims description 18
- 230000032683 aging Effects 0.000 claims description 16
- 229910052708 sodium Inorganic materials 0.000 claims description 16
- 239000011734 sodium Substances 0.000 claims description 16
- 229940117986 sulfobetaine Drugs 0.000 claims description 13
- 230000008719 thickening Effects 0.000 claims description 13
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 12
- 238000004090 dissolution Methods 0.000 claims description 12
- 238000001035 drying Methods 0.000 claims description 12
- 239000003480 eluent Substances 0.000 claims description 12
- 238000010828 elution Methods 0.000 claims description 12
- 239000003456 ion exchange resin Substances 0.000 claims description 12
- 229920003303 ion-exchange polymer Polymers 0.000 claims description 12
- 239000002245 particle Substances 0.000 claims description 10
- 239000004141 Sodium laurylsulphate Substances 0.000 claims description 9
- 239000004575 stone Substances 0.000 claims description 9
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 8
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 8
- 235000011152 sodium sulphate Nutrition 0.000 claims description 8
- 239000000469 ethanolic extract Substances 0.000 claims description 6
- 238000000605 extraction Methods 0.000 claims description 6
- 239000002244 precipitate Substances 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 5
- 229920002125 Sokalan® Polymers 0.000 claims description 5
- 150000001412 amines Chemical class 0.000 claims description 5
- 229960001631 carbomer Drugs 0.000 claims description 5
- 125000002811 oleoyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])/C([H])=C([H])\C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 5
- 229940045998 sodium isethionate Drugs 0.000 claims description 5
- LADXKQRVAFSPTR-UHFFFAOYSA-M sodium;2-hydroxyethanesulfonate Chemical compound [Na+].OCCS([O-])(=O)=O LADXKQRVAFSPTR-UHFFFAOYSA-M 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 9
- 201000004384 Alopecia Diseases 0.000 abstract description 3
- 231100000360 alopecia Toxicity 0.000 abstract description 3
- 238000005406 washing Methods 0.000 abstract description 2
- 229930182490 saponin Natural products 0.000 description 12
- 150000007949 saponins Chemical class 0.000 description 12
- 235000017709 saponins Nutrition 0.000 description 12
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 10
- 239000003814 drug Substances 0.000 description 7
- 239000008280 blood Substances 0.000 description 6
- 210000004369 blood Anatomy 0.000 description 6
- 230000001737 promoting effect Effects 0.000 description 6
- PVLHOJXLNBFHDX-XHJPDDKBSA-N Panaxadiol Chemical compound C[C@]1([C@H]2CC[C@@]3([C@@H]2[C@H](O)C[C@H]2[C@]3(CC[C@H]3C(C)(C)[C@@H](O)CC[C@@]32C)C)C)CCCC(C)(C)O1 PVLHOJXLNBFHDX-XHJPDDKBSA-N 0.000 description 4
- SYFJYASKXNAXKC-UHFFFAOYSA-N Panaxadiol Natural products CC1(C)CCCC(O1)C2CCC3(C)C2C(O)CC4C5(C)CCC(O)C(C)(C)C5CCC34C SYFJYASKXNAXKC-UHFFFAOYSA-N 0.000 description 4
- 230000017531 blood circulation Effects 0.000 description 4
- 229930182494 ginsenoside Natural products 0.000 description 4
- 229940089161 ginsenoside Drugs 0.000 description 4
- 230000002936 tranquilizing effect Effects 0.000 description 4
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 125000001931 aliphatic group Chemical group 0.000 description 3
- 230000003750 conditioning effect Effects 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- 239000003643 water by type Substances 0.000 description 3
- CKUVNOCSBYYHIS-UHFFFAOYSA-N (20R)-ginsenoside Rg3 Natural products CC(C)=CCCC(C)(O)C1CCC(C2(CCC3C4(C)C)C)(C)C1C(O)CC2C3(C)CCC4OC1OC(CO)C(O)C(O)C1O CKUVNOCSBYYHIS-UHFFFAOYSA-N 0.000 description 2
- CKUVNOCSBYYHIS-IRFFNABBSA-N (20S)-ginsenoside Rh2 Chemical compound O([C@H]1CC[C@]2(C)[C@H]3C[C@@H](O)[C@H]4[C@@]([C@@]3(CC[C@H]2C1(C)C)C)(C)CC[C@@H]4[C@@](C)(O)CCC=C(C)C)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O CKUVNOCSBYYHIS-IRFFNABBSA-N 0.000 description 2
- CKUVNOCSBYYHIS-LGYUXIIVSA-N 20(R)-Ginsenoside Rh2 Natural products O([C@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1)[C@@H]1C(C)(C)[C@H]2[C@@](C)([C@H]3[C@](C)([C@@]4(C)[C@H]([C@H](O)C3)[C@@H]([C@](O)(CC/C=C(\C)/C)C)CC4)CC2)CC1 CKUVNOCSBYYHIS-LGYUXIIVSA-N 0.000 description 2
- 240000007087 Apium graveolens Species 0.000 description 2
- 235000015849 Apium graveolens Dulce Group Nutrition 0.000 description 2
- 235000010591 Appio Nutrition 0.000 description 2
- 206010016322 Feeling abnormal Diseases 0.000 description 2
- 239000004378 Glycyrrhizin Substances 0.000 description 2
- 206010061218 Inflammation Diseases 0.000 description 2
- DEMKZLAVQYISIA-UHFFFAOYSA-N Liquirtin Natural products OC1C(O)C(O)C(CO)OC1OC1=CC=C(C2OC3=CC(O)=CC=C3C(=O)C2)C=C1 DEMKZLAVQYISIA-UHFFFAOYSA-N 0.000 description 2
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 235000001014 amino acid Nutrition 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 230000000146 antalgic effect Effects 0.000 description 2
- 230000003110 anti-inflammatory effect Effects 0.000 description 2
- 230000036528 appetite Effects 0.000 description 2
- 235000019789 appetite Nutrition 0.000 description 2
- 230000036772 blood pressure Effects 0.000 description 2
- 230000029087 digestion Effects 0.000 description 2
- 230000003467 diminishing effect Effects 0.000 description 2
- 229930003944 flavone Natural products 0.000 description 2
- 235000011949 flavones Nutrition 0.000 description 2
- 229930182486 flavonoid glycoside Natural products 0.000 description 2
- 150000007955 flavonoid glycosides Chemical class 0.000 description 2
- LPLVUJXQOOQHMX-UHFFFAOYSA-N glycyrrhetinic acid glycoside Natural products C1CC(C2C(C3(CCC4(C)CCC(C)(CC4C3=CC2=O)C(O)=O)C)(C)CC2)(C)C2C(C)(C)C1OC1OC(C(O)=O)C(O)C(O)C1OC1OC(C(O)=O)C(O)C(O)C1O LPLVUJXQOOQHMX-UHFFFAOYSA-N 0.000 description 2
- 229960004949 glycyrrhizic acid Drugs 0.000 description 2
- UYRUBYNTXSDKQT-UHFFFAOYSA-N glycyrrhizic acid Natural products CC1(C)C(CCC2(C)C1CCC3(C)C2C(=O)C=C4C5CC(C)(CCC5(C)CCC34C)C(=O)O)OC6OC(C(O)C(O)C6OC7OC(O)C(O)C(O)C7C(=O)O)C(=O)O UYRUBYNTXSDKQT-UHFFFAOYSA-N 0.000 description 2
- 235000019410 glycyrrhizin Nutrition 0.000 description 2
- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 description 2
- 238000005469 granulation Methods 0.000 description 2
- 230000003179 granulation Effects 0.000 description 2
- 230000037308 hair color Effects 0.000 description 2
- 230000004054 inflammatory process Effects 0.000 description 2
- 239000012567 medical material Substances 0.000 description 2
- 210000002752 melanocyte Anatomy 0.000 description 2
- 230000000144 pharmacologic effect Effects 0.000 description 2
- SHCBCKBYTHZQGZ-DLHMIPLTSA-N protopanaxatriol Chemical compound C1C[C@H](O)C(C)(C)[C@@H]2[C@@H](O)C[C@@]3(C)[C@]4(C)CC[C@H]([C@](C)(O)CCC=C(C)C)[C@H]4[C@H](O)C[C@@H]3[C@]21C SHCBCKBYTHZQGZ-DLHMIPLTSA-N 0.000 description 2
- BBEUDPAEKGPXDG-UHFFFAOYSA-N protopanaxatriol Natural products CC(CCC=C(C)C)C1CCC2(C)C1C(O)CC3C4(C)CCC(O)C(C)(C)C4C(O)CC23C BBEUDPAEKGPXDG-UHFFFAOYSA-N 0.000 description 2
- 238000005728 strengthening Methods 0.000 description 2
- 230000008961 swelling Effects 0.000 description 2
- DKVBOUDTNWVDEP-NJCHZNEYSA-N teicoplanin aglycone Chemical compound N([C@H](C(N[C@@H](C1=CC(O)=CC(O)=C1C=1C(O)=CC=C2C=1)C(O)=O)=O)[C@H](O)C1=CC=C(C(=C1)Cl)OC=1C=C3C=C(C=1O)OC1=CC=C(C=C1Cl)C[C@H](C(=O)N1)NC([C@H](N)C=4C=C(O5)C(O)=CC=4)=O)C(=O)[C@@H]2NC(=O)[C@@H]3NC(=O)[C@@H]1C1=CC5=CC(O)=C1 DKVBOUDTNWVDEP-NJCHZNEYSA-N 0.000 description 2
- 235000015961 tonic Nutrition 0.000 description 2
- 230000001256 tonic effect Effects 0.000 description 2
- 229960000716 tonics Drugs 0.000 description 2
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 2
- 239000002280 amphoteric surfactant Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 210000003491 skin Anatomy 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
A kind of shampoo containing arasaponin and preparation method thereof, relates to the shampoo containing arasaponin, meanwhile, the invention still further relates to the preparation method of this shampoo; Be made up of the raw material of following weight parts ratio: anion surfactant 12 ~ 22 parts, non-ionic surface active agent 1 ~ 10 part, zwitterionic surfactant 0 ~ 7 part, cationic surfactant 1.8 ~ 10 parts, conditioner 3.6 ~ 12 parts, Radix Notoginseng extract 0.5 ~ 10 part, pearling agent 0.8 ~ 2 part, thickening agent 0.8 ~ 2, antiseptic 0.03 ~ 0.15 part, 0.1 ~ 0.7 part, essence, 0.8 ~ 1.7 part, sodium chloride, deionized water 40 ~ 80 parts; Be made through series of process; There is the effect of hair washing, hair care, obviously minimizing alopecia.
Description
Technical field
The invention belongs to cosmetics of everyday use technical field, be specifically related to the shampoo containing arasaponin, meanwhile, the invention still further relates to the preparation method of this shampoo.
Background technology
Radix Notoginseng is China's tradition rare Chinese medicine, and one of 40 kinds of large large medical material kinds, apart from the applicating history of modern existing more than 400 year, at home and abroad have long enjoyed a good reputation, the laudatory title that Radix Notoginseng just has from ancient times " stop blooding refreshing medicine ".Radix Notoginseng mainly containing saponin, flavonoid glycoside, aminoacid etc., has effect of blood circulation promoting and blood stasis dispelling, subduing swelling and relieving pain, meridians dredging, expelling wind and removing dampness;
Flower of Radix Notoginseng is position the highest containing arasaponin in Radix Notoginseng Herb, and content, up to more than 13%, based on Rb race saponin, has the pharmacological actions such as tranquillizing and allaying excitement, anti-inflammatory and antalgic, blood pressure lowering;
Flower of Radix Notoginseng petal is containing saponin, and its aglycon has panoxadiol (panaxadiol), 20(R)-dammarane-3 beta, 12 β, 20,25-tetrol [20(R)-panaxadiol), 20(R)-dammarane-3 beta, 12 β, 20,25-tetrol [20(R)-dammaran-3 β, 12 β, 20,25-tetrol], Da Ma-20(22)-alkene-3 β, 12 β, 26-triol [dammar-20 (22)-en-3 β, 12 β, 26-triol] etc.And isolated ginsenoside (ginsenoside) Rb1.Rb2.Rc, Rd, F2 etc.;
Stem and leaf of Radix Notoginseng contains plurality of active ingredients: ginsenoside Rh2 (1), F2 (4), Rg3 (5), Rg1 (7), Rd (8), Re (11), Rb3 (13), Rb1 (14), Rc (15), Herba Gynostemmatis saponins X III (2), IX (9), XVII (10), arasaponin R1 (12), Fa (16), glycyrrhizin and celery sugar liquirtin, based on protopanaxadiol-type's saponin in stem and leaf of Radix Notoginseng, the Protopanaxatriol's type saponin also having content quite micro-and flavone compound;
In recent years, the research of international, domestic the world of medicine shows, stem and leaf of Radix Notoginseng, except having the blood circulation promoting and blood stasis dispelling of Radix Notoginseng, easing pain and diminishing inflammation, detumescence and promoting granulation, blood fat reducing, resisting fatigue, strengthening by means of tonics, also has the function such as tranquillizing and allaying excitement, facilitating digestion, appetite stimulator that Radix Notoginseng lacks;
Radix Notoginseng extract has facilitation to b-16 melanocyte activity, can increase melanic growing amount, can be used for hair color based article;
But, also there is no the product identical or similar with composition of the present invention and processing technology and technique in the market.
Summary of the invention
The invention provides and a kind of there is hair washing, hair care, obviously reduce natural drug shampoo that alopecia and damage hair repair and preparation method thereof.
In order to realize above-mentioned purpose of the present invention, the invention provides following technical scheme:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio: anion surfactant 12 ~ 22 parts, non-ionic surface active agent 1 ~ 10 part, zwitterionic surfactant 0 ~ 7 part, cationic surfactant 1.8 ~ 10 parts, conditioner 3.6 ~ 12 parts, Radix Notoginseng extract 0.5 ~ 10 part, pearling agent 0.8 ~ 2 part, thickening agent 0.8 ~ 2, antiseptic 0.03 ~ 0.15 part, 0.1 ~ 0.7 part, essence, 0.8 ~ 1.7 part, sodium chloride, deionized water 40 ~ 80 parts.
further:described Radix Notoginseng extract is Radix Notoginseng, flower of Radix Notoginseng, the water of stem and leaf of Radix Notoginseng or the extractum of alcohol extraction or solid content.
further:described Radix Notoginseng extract comprises: the mixing of one or more in extract A, extract B, extract C, extract D tetra-kinds, and preparation method is:
(1) get the mixing of one or more of appropriate Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio adding 6 ~ 12L according to per kilogram adds water, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, filtered, concentrated extracting solution, 60 DEG C time, measure relative density is 1.0 ~ 1.5, then, add the ethanol that alcoholic strength is 50% ~ 70%, leaving standstill makes it precipitate in more than 12 hours, reclaims ethanol, concentrated, drying, obtains extract A;
(2) by extract A water dissolution, upper ion exchange resin column is the ethanol elution of 50% ~ 70% with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrated, dry; Obtain extract B;
(3) get the mixing of one or more of appropriate Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio adding 6 ~ 12L according to per kilogram adds the ethanol that alcoholic strength is 50% ~ 80%, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, collected ethanol extract, in above-mentioned medicinal residues, the ratio adding 6 ~ 12L according to per kilogram adds water, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, reclaims ethanol, concentrated, drying, obtains extract C;
(4) by extract C water dissolution, upper ion exchange resin column is the ethanol elution of 50% ~ 70% with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrated, dry, obtains extract D.
further:described anion surfactant is selected from the mixing of one or more in laureth sulfuric ester ammonium, lauryl alcohol sulfuric ester ammonium, sodium lauryl sulphate, coconut oleoyl amine sodium isethionate or polyoxyethylenated alcohol sodium sulfate; Cationic surfactant is selected from polyquaternary ammonium salt-43, the mixing of one or more in polyquaternary ammonium salt-51 or Polyquaternium-10; Zwitterionic surfactant is selected from cocoamido propyl hydroxy sulfobetaine, the mixing of one or more in cocamido propyl betaine or lauroylamidopropyl betaine; Non-ionic surface active agent is selected from alkyl polyglucoside, fatty alcohol-polyoxyethylene ether, the mixing of one or more in lauric acid amide of ethanol or Coconut Fatty Acid Monoethanolamide; Conditioner is selected from cation guar gum, docosyl hydroxypropyl quaternary ammonium salt, polyquaternary ammonium salt-7, emulsified silicone oil, the mixing of one or more in polydimethylsiloxane or dimethiconol; Thickening agent is in carbomer and thickening or the direct thickening of sodium chloride.
Containing a preparation method for the shampoo of arasaponin, comprise the following steps:
The first step: get the raw materials ready
(1) Radix Notoginseng extract: be the water of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng or the extractum of alcohol extraction or solid content;
This Radix Notoginseng extract comprises: the mixing of one or more in extract A, extract B, extract C, extract D tetra-kinds, and preparation method is:
(1) get the mixing of one or more of appropriate Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio adding 6 ~ 12L according to per kilogram adds water, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, filtered, concentrated extracting solution, 60 DEG C time, measure relative density is 1.0 ~ 1.5, then, add the ethanol that alcoholic strength is 50% ~ 70%, leaving standstill makes it precipitate in more than 12 hours, reclaims ethanol, concentrated, drying, obtains extract A;
(2) by extract A water dissolution, upper ion exchange resin column is the ethanol elution of 50% ~ 70% with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrated, dry; Obtain extract B;
(3) get the mixing of one or more of appropriate Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio adding 6 ~ 12L according to per kilogram adds the ethanol that alcoholic strength is 50% ~ 80%, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, collected ethanol extract, in above-mentioned medicinal residues, the ratio adding 6 ~ 12L according to per kilogram adds water, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, reclaims ethanol, concentrated, drying, obtains extract C;
(4) by extract C water dissolution, upper ion exchange resin column is the ethanol elution of 50% ~ 70% with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrated, dry, obtains extract D;
(2) anion surfactant: be selected from the mixing of one or more in laureth sulfuric ester ammonium, lauryl alcohol sulfuric ester ammonium, sodium lauryl sulphate, coconut oleoyl amine sodium isethionate or polyoxyethylenated alcohol sodium sulfate;
(3) cationic surfactant: be selected from polyquaternary ammonium salt-43, the mixing of one or more in polyquaternary ammonium salt-51 or Polyquaternium-10;
(4) zwitterionic surfactant: be selected from cocoamido propyl hydroxy sulfobetaine, the mixing of one or more in cocamido propyl betaine or lauroylamidopropyl betaine;
(5) non-ionic surface active agent: be selected from alkyl polyglucoside, fatty alcohol-polyoxyethylene ether, coconut oleoyl amine MEA, the mixing of one or more in lauric acid amide of ethanol or Coconut Fatty Acid Monoethanolamide;
(6) conditioner: be selected from cation guar gum, docosyl hydroxypropyl quaternary ammonium salt, polyquaternary ammonium salt-7, emulsified silicone oil, one or more mixing in polydimethylsiloxane or dimethiconol; Emulsified silicone oil is selected from Large stone emulsified silicone oil and small particle diameter emulsified silicone oil, or two kinds with one;
(7) thickening agent: in carbomer and thickening or the direct thickening of sodium chloride;
Second step: processing technology;
Ratio by weight:
(1) with deionized water, the cation melon glue of 0.3 ~ 0.6 part is heated scattered for subsequent use;
(2) in scattered cation guar gum, add anion surfactant 12 ~ 22 parts, cationic surfactant 1.8 ~ 10 parts, non-ionic surface active agent 1 ~ 10 part, amphoteric surfactant 0 ~ 7 part, conditioner 3.6 ~ 12 parts, pearling agent 0.8 ~ 2 part, thickening agent 0.8 ~ 2 part, supplying deionized water makes its ratio reach 40 ~ 80 parts, to being heated to 50 ~ 80 DEG C, constant temperature stirs 10 ~ 50min; Then, be cooled to 30 ~ 60 DEG C, Radix Notoginseng extract 0.5 ~ 10 part, constant temperature stirs 10 ~ 50min; Treat that temperature is down to less than 45 DEG C and is added 0.1 ~ 0.7 part, essence, antiseptic 0.03 ~ 0.15 part and 0.8 ~ 1.7 part, sodium chloride; Finally, regulate pH value to be 5.8 ~ 6.0, still aging 0 ~ 48 hour, get product.
further:described
Second step: processing technology;
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 6 ~ 10 parts of laureth sulfuric ester ammoniums, 6 ~ 7 parts of lauryl alcohol sulfuric ester ammoniums, 0.7 ~ 0.9 part of Polyquaternium-10,1 ~ 3 part of polyquaternary ammonium salt-51,2 ~ 5 parts of cocoamido propyl hydroxy sulfobetaine, 1 ~ 3 part of alkyl polyglucoside, 0.8 ~ 2 part of fatty alcohol-polyoxyethylene ether, 1 ~ 3 part of docosyl hydroxypropyl quaternary ammonium salt, 0.5 ~ 2 part of polyquaternary ammonium salt-7,1.3 ~ 1.7 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, be heated to 70 ~ 80 DEG C, constant temperature stirs 20min; Then, be cooled to 50 DEG C, add small particle diameter emulsified silicone oil 2 ~ 5 parts, Radix Notoginseng extract 1 ~ 4 part, constant temperature stirs 20min; Treat that temperature is down to less than 45 DEG C and is added 0.1 ~ 0.4 part, essence, 0.05 ~ 0.07 portion of antiseptic and 1 ~ 3 part, sodium chloride, stir; Regulate pH value to be 6.2, still aging 24 hours, get product.
further:described
Second step: processing technology;
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 10 ~ 15 parts of laureth sulfuric ester ammoniums, 5 ~ 7 parts of coconut oleoyl amine sodium isethionates, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-51,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of Coconut Fatty Acid Monoethanolamide, 0.8 ~ 1.5 part of lauric acid amide of ethanol, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,1.3 ~ 1.7 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, be heated to 70 ~ 80 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.3 ~ 1.7 parts of polydimethylsiloxane, 1.3 ~ 1.7 parts of emulsified silicone oils, 1.3 ~ 1.7 parts of Radix Notoginseng extracts, constant temperature stirs 30nin; Treat that temperature is down to less than 40 DEG C and is added 0.1 ~ 0.4 part of essence, 0.03 ~ 0.1 portion of antiseptic and 1.3 ~ 1.7 parts of sodium chloride stir; Regulate pH value to be 5.8, still aging 36 hours, get product.
further:described
Second step: processing technology;
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 12 ~ 16 parts of sodium lauryl sulphates are added, 2 ~ 5 parts of coconut oleoyl amine sodium isethionates, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of Polyquaternium-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of Coconut Fatty Acid Monoethanolamide, 0.8 ~ 1.5 part of lauric acid amide of ethanol, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,0.8 ~ 1.5 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, water is heated to 70 ~ 80 DEG C, and constant temperature stirs 20min; Then, be cooled to 50 DEG C, add 1.3 ~ 1.7 parts of polydimethylsiloxane, 1.3 ~ 1.7 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.3 ~ 0.5 part of essence, 0.05 ~ 0.15 portion of antiseptic and 1.3 ~ 1.7 parts of sodium chloride stir; Regulate pH value to be 6.0, get product.
further:described
Second step: processing technology;
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of sodium lauryl sulphate, 0.8 ~ 1.5 part of polyquaternary ammonium salt-43,1 ~ 3 part of Polyquaternium-10,2 ~ 5 parts of coconut oleoyl amine MEA, 1 ~ 3 part of fatty alcohol-polyoxyethylene ether, 0.8 ~ 1.5 part of lauric acid amide of ethanol, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,0.8 ~ 1.5 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, water is heated to 70 ~ 80 DEG C, and constant temperature stirs 20min; Then, be cooled to 50 DEG C, add 2 ~ 5 parts of emulsified silicone oils, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 20nin; Treat that temperature is down to less than 45 DEG C, add 0.3 ~ 0.7 part of essence, 0.05 ~ 0.15 portion of antiseptic and 1.3 ~ 1.7 parts of sodium chloride stir; Regulate pH value to be 5.8, still aging 48 hours, get product.
further:described
Second step: processing technology;
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of Polyquaternium-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of alkyl polyglucoside, 0.8 ~ 1.5 part of lauric acid amide of ethanol, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,0.8 ~ 1.5 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, be heated to 75 ~ 85 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.3 ~ 1.7 parts of polydimethylsiloxane, 1.3 ~ 1.7 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.2 ~ 0.4 part of essence, 0.05 ~ 0.15 portion of antiseptic and 1 ~ 1.5 part of sodium chloride stir; Regulate pH value to be 6.0, get product.
further:described
Second step: processing technology;
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of Polyquaternium-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of coconut oleoyl amine MEA, 0.8 ~ 1.5 part of Coconut Fatty Acid Monoethanolamide, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,0.8 ~ 1.5 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, be heated to 75 ~ 85 DEG C, constant temperature stirs 20min; Then, be cooled to 65 DEG C, add 1.3 ~ 1.6 parts of polydimethylsiloxane, 1 ~ 1.4 part of dimethiconol, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.2 ~ 0.4 part of essence, 0.05 ~ 0.15 portion of antiseptic and 1 ~ 1.5 part of sodium chloride stir; Regulate pH value to be 6.0, get product.
further:described
Second step: processing technology;
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of Polyquaternium-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of fatty alcohol-polyoxyethylene ether, 0.8 ~ 1.5 part of alkyl polyglucoside, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,0.8 ~ 1.5 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, be heated to 80 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.1 ~ 1.4 parts of polydimethylsiloxane, 1.2 ~ 1.5 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.2 ~ 0.4 part of essence, 0.05 ~ 0.15 portion of antiseptic and 0.8 ~ 1.5 part of sodium chloride stir; Regulate pH value to be 6.0, get product.
Advantageous Effects:
The present invention has obvious effect to aspects such as clean hair, hair care, minimizing alopecia, the reparations of damage hair;
Effect analysis:
Anion surfactant, zwitterionic surfactant, non-ionic surface active agent all can provide cleaning force, keeps the abundant, stable, fine and smooth of foam.Wherein zwitterionic surfactant and non-ionic surface active agent have the effect of auxiliary foaming, thickening, steady bubble;
The general tool film property of cationic surfactant, gives hair and skin comfort, lubrication, soft feeling raising hair texture have conditioning, antistatic, improves the features such as cardability, gives the fluffy sense of hair, soft feeling, excellent cardability;
Cation guar gum in conditioner is adsorbed on hair, improves the cardability of hair, for the conditioning of hair care product, thickening and stable, improves wet cardability.Remaining conditioner such as docosyl hydroxypropyl quaternary ammonium salt, dimethiconol, polydimethylsiloxane etc. can give the fabulous moisture retention of hair, gloss, for superior smooth sense, can dry wet cardability be improved, anti-entanglement, have good hand, high hair conditioning;
Radix Notoginseng is China's tradition rare Chinese medicine, and one of 40 kinds of large large medical material kinds, apart from the applicating history of modern existing more than 400 year, at home and abroad have long enjoyed a good reputation, the laudatory title that Radix Notoginseng just has from ancient times " stop blooding refreshing medicine ".Radix Notoginseng mainly containing saponin, flavonoid glycoside, aminoacid etc., has effect of blood circulation promoting and blood stasis dispelling, subduing swelling and relieving pain, meridians dredging, expelling wind and removing dampness;
Flower of Radix Notoginseng is position the highest containing arasaponin in Radix Notoginseng Herb, and content, up to more than 13%, based on Rb race saponin, has the pharmacological actions such as tranquillizing and allaying excitement, anti-inflammatory and antalgic, blood pressure lowering;
Flower of Radix Notoginseng petal is containing saponin, and its aglycon has panoxadiol (panaxadiol), 20(R)-dammarane-3 beta, 12 β, 20,25-tetrol [20(R)-panaxadiol), 20(R)-dammarane-3 beta, 12 β, 20,25-tetrol [20(R)-dammaran-3 β, 12 β, 20,25-tetrol], Da Ma-20(22)-alkene-3 β, 12 β, 26-triol [dammar-20(22)-en-3 β, 12 β, 26-triol] etc.And isolated ginsenoside (ginsenoside) Rb1.Rb2.Rc, Rd, F2 etc.;
Stem and leaf of Radix Notoginseng contains plurality of active ingredients: ginsenoside Rh2 (1), F2(4), Rg3(5), Rg1(7), Rd(8), Re(11), Rb3(13), Rb1(14), Rc(15), Herba Gynostemmatis saponins X III(2), IX(9), XVII(10), arasaponin R1 (12), Fa(16), glycyrrhizin and celery sugar liquirtin, based on protopanaxadiol-type's saponin in stem and leaf of Radix Notoginseng, the Protopanaxatriol's type saponin also having content quite micro-and flavone compound;
In recent years, the research of international, domestic the world of medicine shows, stem and leaf of Radix Notoginseng, except having the blood circulation promoting and blood stasis dispelling of Radix Notoginseng, easing pain and diminishing inflammation, detumescence and promoting granulation, blood fat reducing, resisting fatigue, strengthening by means of tonics, also has the function such as tranquillizing and allaying excitement, facilitating digestion, appetite stimulator that Radix Notoginseng lacks;
Radix Notoginseng extract has facilitation to b-16 melanocyte activity, can increase melanic growing amount, can be used for hair color based article.
Further illustrate essentiality content of the present invention by specific embodiment given below, but do not limit the present invention with this.
embodiment 1: a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.6 part of cation guar gum, 10 parts of laureth sulfuric ester ammoniums, 6 parts of coconut oleoyl amine sodium isethionates, 1 part of polyquaternary ammonium salt-43,1 part of polyquaternary ammonium salt-51,2 parts of cocamido propyl betaine, 1 part of Coconut Fatty Acid Monoethanolamide, 0.8 part of lauric acid amide of ethanol, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,1.3 portions of pearling agents, 40 parts of deionized waters, 1.3 parts of polydimethylsiloxane, 1.3 parts of emulsified silicone oils, 1.3 parts of Radix Notoginseng extract A, 0.1 part of essence, 0.03 portion of antiseptic, 1.3 parts of sodium chloride;
Described Radix Notoginseng extract: be the water of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng or the extractum of alcohol extraction or solid content;
This Radix Notoginseng extract comprises: the mixing of one or more in extract A, extract B, extract C, extract D tetra-kinds, and preparation method is:
(1) get the mixing of one or more of appropriate Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio adding 6 ~ 12L according to per kilogram adds water, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, filtered, concentrated extracting solution, 60 DEG C time, measure relative density is 1.0 ~ 1.5, then, add the ethanol that alcoholic strength is 50% ~ 70%, leaving standstill makes it precipitate in more than 12 hours, reclaims ethanol, concentrated, drying, obtains extract A;
(2) by extract A water dissolution, upper ion exchange resin column is the ethanol elution of 50% ~ 70% with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrated, dry; Obtain extract B;
(3) get the mixing of one or more of appropriate Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio adding 6 ~ 12L according to per kilogram adds the ethanol that alcoholic strength is 50% ~ 80%, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, collected ethanol extract, in above-mentioned medicinal residues, the ratio adding 6 ~ 12L according to per kilogram adds water, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, reclaims ethanol, concentrated, drying, obtains extract C;
(4) by extract C water dissolution, upper ion exchange resin column is the ethanol elution of 50% ~ 70% with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrated, dry, obtains extract D.
embodiment 2: a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.6 part of cation guar gum, 15 parts of laureth sulfuric ester ammoniums, 7 parts of coconut oleoyl amine sodium isethionates, 3 parts of polyquaternary ammonium salt-43,3 parts of polyquaternary ammonium salt-51,5 parts of cocamido propyl betaine, 3 parts of Coconut Fatty Acid Monoethanolamides, 1.5 parts of lauric acid amide of ethanol, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.7 portions of pearling agents, 80 parts of deionized waters, 1.7 parts of polydimethylsiloxane, 1.7 parts of emulsified silicone oils, 1.7 parts of Radix Notoginseng extract A, 0.4 part of essence, 0.1 portion of antiseptic, 1.7 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
embodiment 3: a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.6 part of cation guar gum, 12 parts of laureth sulfuric ester ammoniums, 5 parts of coconut oleoyl amine sodium isethionates, 2 parts of polyquaternary ammonium salt-43,2 parts of polyquaternary ammonium salt-51,3 parts of cocamido propyl betaine, 2 parts of Coconut Fatty Acid Monoethanolamides, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1.5 portions of pearling agents, 60 parts of deionized waters, 1.5 parts of polydimethylsiloxane, 1.5 parts of emulsified silicone oils, 1.5 parts of Radix Notoginseng extract A, 0.2 part of essence, 0.06 portion of antiseptic, 1.5 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 4:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 6 parts of laureth sulfuric ester ammoniums, 6 parts of lauryl alcohol sulfuric ester ammoniums, 0.7 part of Polyquaternium-10,1 part of polyquaternary ammonium salt-51,2 parts of cocoamido propyl hydroxy sulfobetaine, 1 part of alkyl polyglucoside, 0.8 part of fatty alcohol-polyoxyethylene ether, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 0.5 part of polyquaternary ammonium salt-7,1.3 portions of pearling agents, deionized water 40 parts, small particle diameter emulsified silicone oil 2 parts, Radix Notoginseng extract A part, 0.1 part, essence, 0.05 portion of antiseptic, 1 part, sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 5:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 10 parts of laureth sulfuric ester ammoniums, 7 parts of lauryl alcohol sulfuric ester ammoniums, 0.9 part of Polyquaternium-10,3 parts of polyquaternary ammonium salt-51,5 parts of cocoamido propyl hydroxy sulfobetaine, 3 parts of alkyl polyglucoside, 2 parts of fatty alcohol-polyoxyethylene ether, 3 parts of docosyl hydroxypropyl quaternary ammonium salts, 2 parts of polyquaternary ammonium salt-7,1.7 portions of pearling agents, deionized water 80 parts, small particle diameter emulsified silicone oil 5 parts, 4 parts of Radix Notoginseng extract A, 0.4 part of essence, 0.07 portion of antiseptic, 3 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 6:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 8 parts of laureth sulfuric ester ammoniums, 5 parts of lauryl alcohol sulfuric ester ammoniums, 0.8 part of Polyquaternium-10,2 parts of polyquaternary ammonium salt-51,3 parts of cocoamido propyl hydroxy sulfobetaine, 2 parts of alkyl polyglucoside, 1 part of fatty alcohol-polyoxyethylene ether, 2 parts of docosyl hydroxypropyl quaternary ammonium salts, 1 part of polyquaternary ammonium salt-7,1.5 portions of pearling agents, deionized water 60 parts, small particle diameter emulsified silicone oil 3 parts, 2 parts of Radix Notoginseng extract A, 0.2 part of essence, 0.06 portion of antiseptic, 2 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 7:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 14 parts of sodium lauryl sulphates, 3 parts of coconut oleoyl amine sodium isethionates, 2 parts of polyquaternary ammonium salt-43,2 parts of Polyquaternium-10s, 3 parts of cocamido propyl betaine, 2 parts of Coconut Fatty Acid Monoethanolamides, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, deionized water 60 parts, 1.5 parts of polydimethylsiloxane, 1.5 parts of dimethiconols, 1 part of Radix Notoginseng extract A, 0.4 part of essence, 0.1 portion of antiseptic, 1.5 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 7:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 12 parts of sodium lauryl sulphates, 2 parts of coconut oleoyl amine sodium isethionates, 1 part of polyquaternary ammonium salt-43,1 part of Polyquaternium-10,2 parts of cocamido propyl betaine, 1 part of Coconut Fatty Acid Monoethanolamide, 0.8 part of lauric acid amide of ethanol, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,0.8 portion of pearling agent, deionized water 40 parts, 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 0.8 part of Radix Notoginseng extract, 0.3 part of essence, 0.05 portion of antiseptic, 1.3 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 8:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 16 parts of sodium lauryl sulphates, 5 parts of coconut oleoyl amine sodium isethionates, 3 parts of polyquaternary ammonium salt-43,3 parts of Polyquaternium-10s, 5 parts of cocamido propyl betaine, 3 parts of Coconut Fatty Acid Monoethanolamides, 1.5 parts of lauric acid amide of ethanol, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portions of pearling agents, deionized water 80 parts, 1.7 parts of polydimethylsiloxane, 1.7 parts of dimethiconols, 1.5 parts of Radix Notoginseng extracts, 0.5 part of essence, 0.15 portion of antiseptic, 1.7 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 9:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.3 part of cation guar gum, 12 parts of laureth sulfuric ester ammoniums, 1 part of sodium lauryl sulphate, 0.8 part of polyquaternary ammonium salt-43,1 part of Polyquaternium-10,2 parts of coconut oleoyl amine MEA, 1 part of fatty alcohol-polyoxyethylene ether, 0.8 part of lauric acid amide of ethanol, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,0.8 portion of pearling agent, deionized water 40 parts, 2 parts of Large stone emulsified silicone oils, 0.8 part of Radix Notoginseng extract B, 0.3 part of essence, 0.05 part of antiseptic, 1.3 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 10:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.3 part of cation guar gum, 16 parts of laureth sulfuric ester ammoniums, 3 parts of sodium lauryl sulphates, 1.5 parts of polyquaternary ammonium salt-43,3 parts of Polyquaternium-10s, 5 parts of coconut oleoyl amine MEA, 3 parts of fatty alcohol-polyoxyethylene ether, 1.5 parts of lauric acid amide of ethanol, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portions of pearling agents, deionized water 80 parts, 5 parts of Large stone emulsified silicone oils, 1.5 parts of Radix Notoginseng extract B, 0.7 part of essence, 0.15 part of antiseptic, 1.7 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 11:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.3 part of cation guar gum, 14 parts of laureth sulfuric ester ammoniums, 2 parts of sodium lauryl sulphates, 1 part of polyquaternary ammonium salt-43,1 part of Polyquaternium-10,3 parts of coconut oleoyl amine MEA, 2 parts of fatty alcohol-polyoxyethylene ether, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, deionized water 60 parts, 3 parts of Large stone emulsified silicone oils, 1 part of Radix Notoginseng extract B, 0.4 part of essence, 0.1 part of antiseptic, 1.5 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 12:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 12 parts of laureth sulfuric ester ammoniums, 1 part of lauryl alcohol sulfuric ester ammonium, 1 part of polyquaternary ammonium salt-43,1 part of Polyquaternium-10,2 parts of cocamido propyl betaine, 1 part of alkyl polyglucoside, 0.8 part of lauric acid amide of ethanol, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,0.8 portion of pearling agent, deionized water 40 parts, 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 0.8 part of Radix Notoginseng extract B, 0.2 part of essence, 0.05 portion of antiseptic, 1 part of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 13:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 16 parts of laureth sulfuric ester ammoniums, 3 parts of lauryl alcohol sulfuric ester ammoniums, 3 parts of polyquaternary ammonium salt-43,3 parts of Polyquaternium-10s, 5 parts of cocamido propyl betaine, 3 parts of alkyl polyglucoside, 1.5 parts of lauric acid amide of ethanol, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portions of pearling agents, deionized water 80 parts, 1.7 parts of polydimethylsiloxane, 1.7 parts of dimethiconols, 1.5 parts of Radix Notoginseng extract B, 0.4 part of essence, 0.15 portion of antiseptic, 1 ~ 1.5 part of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 14:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 14 parts of laureth sulfuric ester ammoniums, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 parts of Polyquaternium-10s, 3 parts of cocamido propyl betaine, 2 parts of alkyl polyglucoside, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, deionized water 70 parts, 1.5 parts of polydimethylsiloxane, 1.5 parts of dimethiconols, 1 part of Radix Notoginseng extract B, 0.3 part of essence, 0.1 portion of antiseptic, 1.3 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 15:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 12 parts of laureth sulfuric ester ammoniums, 1 part of lauryl alcohol sulfuric ester ammonium, 1 part of polyquaternary ammonium salt-43,1 part of Polyquaternium-10,2 parts of cocamido propyl betaine, 1 part of coconut oleoyl amine MEA, 0.8 part of Coconut Fatty Acid Monoethanolamide, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,0.8 portion of pearling agent, deionized water 40 parts, 1.3 parts of polydimethylsiloxane, 1 part of dimethiconol, 0.8 part of Radix Notoginseng extract C, 0.2 part of essence, 0.05 portion of antiseptic, 1 ~ 1.5 part of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 16:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 16 parts of laureth sulfuric ester ammoniums, 3 parts of lauryl alcohol sulfuric ester ammoniums, 3 parts of polyquaternary ammonium salt-43,3 parts of Polyquaternium-10s, 5 parts of cocamido propyl betaine, 3 parts of coconut oleoyl amine MEA, 1.5 parts of Coconut Fatty Acid Monoethanolamides, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portions of pearling agents, deionized water 80 parts, 1.6 parts of polydimethylsiloxane, 1.4 parts of dimethiconols, 1.5 parts of Radix Notoginseng extract C, 0.4 part of essence, 0.15 portion of antiseptic, 1.5 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 17:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 14 parts of laureth sulfuric ester ammoniums, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 parts of Polyquaternium-10s, 2 parts of cocamido propyl betaine, 2 parts of coconut oleoyl amine MEA, 1 part of Coconut Fatty Acid Monoethanolamide, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, deionized water 50 parts, 1.5 parts of polydimethylsiloxane, 1.2 parts of dimethiconols, 1 part of Radix Notoginseng extract C, 0.3 part of essence, 0.1 portion of antiseptic, 1.3 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 18:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 12 parts of laureth sulfuric ester ammoniums, 1 part of lauryl alcohol sulfuric ester ammonium, 1 part of polyquaternary ammonium salt-43,1 part of Polyquaternium-10,2 parts of cocamido propyl betaine, 1 part of fatty alcohol-polyoxyethylene ether, 0.8 part of alkyl polyglucoside, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,0.8 portion of pearling agent, deionized water 40 parts, 1.1 parts of polydimethylsiloxane, 1.2 parts of dimethiconols, 0.8 part of Radix Notoginseng extract D, 0.2 part of essence, 0.05 portion of antiseptic, 0.8 part of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 19:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 16 parts of laureth sulfuric ester ammoniums, 3 parts of lauryl alcohol sulfuric ester ammoniums, 3 parts of polyquaternary ammonium salt-43,3 parts of Polyquaternium-10s, 5 parts of cocamido propyl betaine, 3 parts of fatty alcohol-polyoxyethylene ether, 1.5 parts of alkyl polyglucoside, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portions of pearling agents, deionized water 80 parts, 1.4 parts of polydimethylsiloxane, 1.5 parts of dimethiconols, 1.5 parts of Radix Notoginseng extract D, 0.4 part of essence, 0.15 portion of antiseptic, 1.5 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 20:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.4 part of cation guar gum, 14 parts of laureth sulfuric ester ammoniums, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 parts of Polyquaternium-10s, 3 parts of cocamido propyl betaine, 2 parts of fatty alcohol-polyoxyethylene ether, 1 part of alkyl polyglucoside, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, deionized water 60 parts, 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 1 part of Radix Notoginseng extract D, 0.3 part of essence, 0.1 portion of antiseptic, 1 part of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 21:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.5 part of cation guar gum, 14 parts of laureth sulfuric ester ammoniums, 2 parts of aliphatic acid polyethenoxy ether sodium sulfate, 2 parts of polyquaternary ammonium salt-43,2 parts of Polyquaternium-10s, 2 parts of cocamido propyl betaine, 2 parts of coconut oleoyl amine MEA, 1 part of Coconut Fatty Acid Monoethanolamide, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, deionized water 50 parts, 1.5 parts of polydimethylsiloxane, 1.2 parts of dimethiconols, 1 part of Radix Notoginseng extract C, 0.3 part of essence, 0.1 portion of antiseptic, 1.3 parts of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 22:
a kind ofcontaining the shampoo of arasaponin, comprise the raw material of following weight parts ratio:
0.5 part of cation guar gum, 14 parts of laureth sulfuric ester ammoniums, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 parts of Polyquaternium-10s, 3 parts of lauroylamidopropyl betaines, 2 parts of fatty alcohol-polyoxyethylene ether, 1 part of alkyl polyglucoside, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, deionized water 60 parts, 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 1 part of Radix Notoginseng extract D, 0.3 part of essence, 0.1 portion of antiseptic, 1 part of sodium chloride; Remainder is identical with embodiment 1, no longer repeated description.
Embodiment 23: a kind of preparation method of the shampoo containing arasaponin, is characterized in that, comprise the following steps:
The first step: get the raw materials ready
(1) Radix Notoginseng extract: be the water of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng or the extractum of alcohol extraction or solid content;
This Radix Notoginseng extract comprises: the mixing of one or more in extract A, extract B, extract C, extract D tetra-kinds, and preparation method is:
(1) get the mixing of one or more of appropriate Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio adding 6 ~ 12L according to per kilogram adds water, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, filtered, concentrated extracting solution, 60 DEG C time, measure relative density is 1.0 ~ 1.5, then, add the ethanol that alcoholic strength is 50% ~ 70%, leaving standstill makes it precipitate in more than 12 hours, reclaims ethanol, concentrated, drying, obtains extract A;
(2) by extract A water dissolution, upper ion exchange resin column is the ethanol elution of 50% ~ 70% with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrated, dry; Obtain extract B;
(3) get the mixing of one or more of appropriate Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng, the ratio adding 6 ~ 12L according to per kilogram adds the ethanol that alcoholic strength is 50% ~ 80%, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, collected ethanol extract, in above-mentioned medicinal residues, the ratio adding 6 ~ 12L according to per kilogram adds water, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, reclaims ethanol, concentrated, drying, obtains extract C;
(4) by extract C water dissolution, upper ion exchange resin column is the ethanol elution of 50% ~ 70% with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrated, dry, obtains extract D;
(2) anion surfactant: be selected from the mixing of one or more in laureth sulfuric ester ammonium, lauryl alcohol sulfuric ester ammonium, sodium lauryl sulphate, coconut oleoyl amine sodium isethionate or polyoxyethylenated alcohol sodium sulfate;
(3) cationic surfactant: be selected from polyquaternary ammonium salt-43, the mixing of one or more in polyquaternary ammonium salt-51 or Polyquaternium-10;
(4) zwitterionic surfactant: be selected from cocoamido propyl hydroxy sulfobetaine, the mixing of one or more in cocamido propyl betaine or lauroylamidopropyl betaine;
(5) non-ionic surface active agent: be selected from alkyl polyglucoside, fatty alcohol-polyoxyethylene ether, coconut oleoyl amine MEA, the mixing of one or more in lauric acid amide of ethanol or Coconut Fatty Acid Monoethanolamide;
(6) conditioner: be selected from cation guar gum, docosyl hydroxypropyl quaternary ammonium salt, polyquaternary ammonium salt-7, emulsified silicone oil, one or more mixing in polydimethylsiloxane or dimethiconol; Emulsified silicone oil is selected from Large stone emulsified silicone oil and small particle diameter emulsified silicone oil, or two kinds with one;
(7) thickening agent: in carbomer and thickening or the direct thickening of sodium chloride;
Second step: processing technology;
Ratio by weight:
(1) with deionized water, 0.3 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 6 parts of laureth sulfuric ester ammoniums are added, 6 parts of lauryl alcohol sulfuric ester ammoniums, 0.7 part of Polyquaternium-10,1 part of polyquaternary ammonium salt-51,2 parts of cocoamido propyl hydroxy sulfobetaine, 1 part of alkyl polyglucoside, 0.8 part of fatty alcohol-polyoxyethylene ether, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 0.5 part of polyquaternary ammonium salt-7,1.3 portions of pearling agents, supply deionized water and make its ratio reach 40 parts, be heated to 70 DEG C, constant temperature stirs 20min; Then, be cooled to 50 DEG C, small particle diameter emulsified silicone oil 2 parts, Radix Notoginseng extract A1 part, constant temperature stirs 20min; Treat that temperature is down to less than 45 DEG C and is added 0.1 part, essence, 0.05 portion of antiseptic and 1 part, sodium chloride, stir; Regulate pH value to be 6.2, still aging 24 hours, get product.
Embodiment 24: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.5 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 10 parts of laureth sulfuric ester ammoniums are added, 7 parts of lauryl alcohol sulfuric ester ammoniums, 0.9 part of Polyquaternium-10,3 parts of polyquaternary ammonium salt-51,5 parts of cocoamido propyl hydroxy sulfobetaine, 3 parts of alkyl polyglucoside, 2 parts of fatty alcohol-polyoxyethylene ether, 3 parts of docosyl hydroxypropyl quaternary ammonium salts, 2 parts of polyquaternary ammonium salt-7,1.7 portions of pearling agents, supply deionized water and make its ratio reach 80 parts, be heated to 80 DEG C, constant temperature stirs 20min; Then, be cooled to 50 DEG C, small particle diameter emulsified silicone oil 5 parts, Radix Notoginseng extract A4 part, constant temperature stirs 20min; Treat that temperature is down to less than 45 DEG C and is added 0.4 part, essence, 0.07 portion of antiseptic and 3 parts, sodium chloride, stir; Regulate pH value to be 6.2, still aging 24 hours, get product; Other parts no longer repeated description identical with embodiment 23.
Embodiment 25: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 8 parts of laureth sulfuric ester ammoniums are added, 5 parts of lauryl alcohol sulfuric ester ammoniums, 0.8 part of Polyquaternium-10,2 parts of polyquaternary ammonium salt-51,3 parts of cocoamido propyl hydroxy sulfobetaine, 2 parts of alkyl polyglucoside, 1 part of fatty alcohol-polyoxyethylene ether, 2 parts of docosyl hydroxypropyl quaternary ammonium salts, 1 part of polyquaternary ammonium salt-7,1.5 portions of pearling agents, supply deionized water and make its ratio reach 60 parts, be heated to 75 DEG C, constant temperature stirs 20min; Then, be cooled to 50 DEG C, small particle diameter emulsified silicone oil 3 parts, Radix Notoginseng extract A2 part, constant temperature stirs 20min; Treat that temperature is down to less than 45 DEG C and is added 0.2 part, essence, 0.06 portion of antiseptic and 2 parts, sodium chloride, stir; Regulate pH value to be 6.2, still aging 24 hours, get product; Other parts no longer repeated description identical with embodiment 23.
Embodiment 26: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.3 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 10 parts of laureth sulfuric ester ammoniums are added, 6 parts of coconut oleoyl amine sodium isethionates, 1 part of polyquaternary ammonium salt-43,1 part of polyquaternary ammonium salt-51,2 parts of cocamido propyl betaine, 1 part of Coconut Fatty Acid Monoethanolamide, 0.8 part of lauric acid amide of ethanol, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,1.3 portions of pearling agents, supply deionized water and make its ratio reach 40 parts, be heated to 70 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.3 parts of polydimethylsiloxane, 1.3 parts of emulsified silicone oils, 1.3 parts of Radix Notoginseng extract A, constant temperature stirs 30nin; Treat that temperature is down to less than 40 DEG C and is added 0.1 part of essence, 0.03 portion of antiseptic and 1.3 parts of sodium chloride stir; Regulate pH value to be 5.8, still aging 36 hours, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 27: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 15 parts of laureth sulfuric ester ammoniums are added, 7 parts of coconut oleoyl amine sodium isethionates, 3 parts of polyquaternary ammonium salt-43,3 parts of polyquaternary ammonium salt-51,5 parts of cocamido propyl betaine, 3 parts of Coconut Fatty Acid Monoethanolamides, 1.5 parts of lauric acid amide of ethanol, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.7 portions of pearling agents, supply deionized water and make its ratio reach 80 parts, be heated to 80 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.7 parts of polydimethylsiloxane, 1.7 parts of emulsified silicone oils, 1.7 parts of Radix Notoginseng extract A, constant temperature stirs 30nin; Treat that temperature is down to less than 40 DEG C and is added 0.4 part of essence, 0.1 portion of antiseptic and 1.7 parts of sodium chloride stir; Regulate pH value to be 5.8, still aging 36 hours, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 28: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.4 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 12 parts of laureth sulfuric ester ammoniums are added, 5 parts of coconut oleoyl amine sodium isethionates, 2 parts of polyquaternary ammonium salt-43,2 parts of polyquaternary ammonium salt-51,3 parts of cocamido propyl betaine, 2 parts of Coconut Fatty Acid Monoethanolamides, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1.5 portions of pearling agents, supply deionized water and make its ratio reach 60 parts, be heated to 75 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.5 parts of polydimethylsiloxane, 1.5 parts of emulsified silicone oils, 1.5 parts of Radix Notoginseng extract A, constant temperature stirs 30nin; Treat that temperature is down to less than 40 DEG C and is added 0.2 part of essence, 0.06 portion of antiseptic and 1.5 parts of sodium chloride stir; Regulate pH value to be 5.8, still aging 36 hours, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 29: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 16 parts of sodium lauryl sulphates are added, 5 parts of coconut oleoyl amine sodium isethionates, 3 parts of polyquaternary ammonium salt-43,3 parts of Polyquaternium-10s, 5 parts of cocamido propyl betaine, 3 parts of Coconut Fatty Acid Monoethanolamides, 0.8 ~ 1.5 part of lauric acid amide of ethanol, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portions of pearling agents, supply deionized water and make its ratio reach 80 parts, water is heated to 80 DEG C, and constant temperature stirs 20min; Then, be cooled to 50 DEG C, add 1.7 parts of polydimethylsiloxane, 1.7 parts of dimethiconols, 1.5 parts of Radix Notoginseng extract A, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.5 part of essence, 0.15 portion of antiseptic and 1.7 parts of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 29: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.3 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 12 parts of sodium lauryl sulphates are added, 2 parts of coconut oleoyl amine sodium isethionates, 1 part of polyquaternary ammonium salt-43,1 part of Polyquaternium-10,2 parts of cocamido propyl betaine, 1 part of Coconut Fatty Acid Monoethanolamide, 0.8 part of lauric acid amide of ethanol, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,0.8 portion of pearling agent, supplies deionized water and makes its ratio reach 40 parts, water is heated to 70 DEG C, and constant temperature stirs 20min; Then, be cooled to 50 DEG C, add 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 0.8 part of Radix Notoginseng extract A, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.3 part of essence, 0.05 portion of antiseptic and 1.3 parts of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 29: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.4 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 14 parts of sodium lauryl sulphates are added, 3 parts of coconut oleoyl amine sodium isethionates, 2 parts of polyquaternary ammonium salt-43,2 parts of Polyquaternium-10s, 3 parts of cocamido propyl betaine, 2 parts of Coconut Fatty Acid Monoethanolamides, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, supplies deionized water and makes its ratio reach 60 parts, water is heated to 75 DEG C, and constant temperature stirs 20min; Then, be cooled to 50 DEG C, add 1.5 parts of polydimethylsiloxane, 1.5 parts of dimethiconols, 1 part of Radix Notoginseng extract A, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.4 part of essence, 0.1 portion of antiseptic and 1.5 parts of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 30: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.4 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 12 parts of laureth sulfuric ester ammoniums are added, 1 part of sodium lauryl sulphate, 0.8 part of polyquaternary ammonium salt-43,1 part of Polyquaternium-10,2 parts of coconut oleoyl amine MEA, 1 part of fatty alcohol-polyoxyethylene ether, 0.8 part of lauric acid amide of ethanol, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,0.8 portion of pearling agent, supplies deionized water and makes its ratio reach 40 parts, water is heated to 70 DEG C, and constant temperature stirs 20min; Then, be cooled to 50 DEG C, add 2 parts of Large stone emulsified silicone oils, 0.8 part of Radix Notoginseng extract B, constant temperature stirs 20nin; Treat that temperature is down to less than 45 DEG C, add 0.3 part of essence, 0.05 portion of antiseptic and 1.3 parts of sodium chloride stir; Regulate pH value to be 5.8, still aging 48 hours, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 31: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 16 parts of laureth sulfuric ester ammoniums are added, 3 parts of sodium lauryl sulphates, 1.5 parts of polyquaternary ammonium salt-43,3 parts of Polyquaternium-10s, 5 parts of coconut oleoyl amine MEA, 3 parts of fatty alcohol-polyoxyethylene ether, 1.5 parts of lauric acid amide of ethanol, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portions of pearling agents, supply deionized water and make its ratio reach 70 parts, water is heated to 80 DEG C, and constant temperature stirs 20min; Then, be cooled to 50 DEG C, add 5 parts of Large stone emulsified silicone oils, 1.5 parts of Radix Notoginseng extract B, constant temperature stirs 20nin; Treat that temperature is down to less than 45 DEG C, add 0.7 part of essence, 0.15 portion of antiseptic and 1.7 parts of sodium chloride stir; Regulate pH value to be 5.8, still aging 48 hours, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 32: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.3 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 14 parts of laureth sulfuric ester ammoniums are added, 2 parts of sodium lauryl sulphates, 1 part of polyquaternary ammonium salt-43,2 parts of Polyquaternium-10s, 3 parts of coconut oleoyl amine MEA, 2 parts of fatty alcohol-polyoxyethylene ether, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, supplies deionized water and makes its ratio reach 60 parts, water is heated to 75 DEG C, and constant temperature stirs 20min; Then, be cooled to 50 DEG C, add 3 parts of Large stone emulsified silicone oils, 1 part of Radix Notoginseng extract B, constant temperature stirs 20nin; Treat that temperature is down to less than 45 DEG C, add 0.4 part of essence, 0.1 portion of antiseptic and 1.5 parts of sodium chloride stir; Regulate pH value to be 5.8, still aging 48 hours, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 33: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.3 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 12 parts of laureth sulfuric ester ammoniums are added, 1 part of lauryl alcohol sulfuric ester ammonium, 1 part of polyquaternary ammonium salt-43,1 part of Polyquaternium-10,2 parts of cocamido propyl betaine, 1 part of alkyl polyglucoside, 0.8 part of lauric acid amide of ethanol, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,0.8 portion of pearling agent, supplies deionized water and makes its ratio reach 40 parts, be heated to 75 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 0.8 part of Radix Notoginseng extract B, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.2 part of essence, 0.05 portion of antiseptic and 1 part of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 34: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 16 parts of laureth sulfuric ester ammoniums are added, 3 parts of lauryl alcohol sulfuric ester ammoniums, 3 parts of polyquaternary ammonium salt-43,3 parts of Polyquaternium-10s, 5 parts of cocamido propyl betaine, 3 parts of alkyl polyglucoside, 1.5 parts of lauric acid amide of ethanol, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portions of pearling agents, supply deionized water and make its ratio reach 80 parts, be heated to 85 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.7 parts of polydimethylsiloxane, 1.7 parts of dimethiconols, 1.5 parts of Radix Notoginseng extract B, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.4 part of essence, 0.15 portion of antiseptic and 1.5 parts of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 35: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.4 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 14 parts of laureth sulfuric ester ammoniums are added, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 parts of Polyquaternium-10s, 3 parts of cocamido propyl betaine, 2 parts of alkyl polyglucoside, 1 part of lauric acid amide of ethanol, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, supplies deionized water and makes its ratio reach 60 parts, be heated to 80 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.5 parts of polydimethylsiloxane, 1.5 parts of dimethiconols, 1 part of Radix Notoginseng extract B, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.3 part of essence, 0.1 portion of antiseptic and 1.3 parts of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 36: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.3 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 12 parts of laureth sulfuric ester ammoniums are added, 1 part of lauryl alcohol sulfuric ester ammonium, 1 part of polyquaternary ammonium salt-43,1 part of Polyquaternium-10,2 parts of cocamido propyl betaine, 1 part of coconut oleoyl amine MEA, 0.8 part of Coconut Fatty Acid Monoethanolamide, 0.8 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 part of polyquaternary ammonium salt-7,0.8 portion of pearling agent, supplies deionized water and makes its ratio reach 40 parts, be heated to 75 DEG C, constant temperature stirs 20min; Then, be cooled to 65 DEG C, add 1.3 parts of polydimethylsiloxane, 1 part of dimethiconol, 0.8 part of Radix Notoginseng extract C, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.2 part of essence, 0.05 portion of antiseptic and 1 part of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 37: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 16 parts of laureth sulfuric ester ammoniums are added, 3 parts of lauryl alcohol sulfuric ester ammoniums, 3 parts of polyquaternary ammonium salt-43,3 parts of Polyquaternium-10s, 5 parts of cocamido propyl betaine, 3 parts of coconut oleoyl amine MEA, 1.5 parts of Coconut Fatty Acid Monoethanolamides, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portions of pearling agents, supply deionized water and make its ratio reach 80 parts, be heated to 85 DEG C, constant temperature stirs 20min; Then, be cooled to 65 DEG C, add 1.6 parts of polydimethylsiloxane, 1.4 parts of dimethiconols, 1.5 parts of Radix Notoginseng extract C, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.4 part of essence, 0.15 portion of antiseptic and 1.5 parts of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 38: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.4 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 14 parts of laureth sulfuric ester ammoniums are added, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 parts of Polyquaternium-10s, 3 parts of cocamido propyl betaine, 2 parts of coconut oleoyl amine MEA, 1 part of Coconut Fatty Acid Monoethanolamide, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, supplies deionized water and makes its ratio reach 70 parts, be heated to 80 DEG C, constant temperature stirs 20min; Then, be cooled to 65 DEG C, add 1.4 parts of polydimethylsiloxane, 1.2 parts of dimethiconols, 1 part of Radix Notoginseng extract C, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.3 part of essence, 0.1 portion of antiseptic and 1.3 parts of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 39: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of Polyquaternium-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of fatty alcohol-polyoxyethylene ether, 0.8 ~ 1.5 part of alkyl polyglucoside, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,0.8 ~ 1.5 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, be heated to 80 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.1 ~ 1.4 parts of polydimethylsiloxane, 1.2 ~ 1.5 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract D, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.2 ~ 0.4 part of essence, 0.05 ~ 0.15 portion of antiseptic and 0.8 ~ 1.5 part of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 40: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of Polyquaternium-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of fatty alcohol-polyoxyethylene ether, 0.8 ~ 1.5 part of alkyl polyglucoside, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,0.8 ~ 1.5 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, be heated to 80 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.1 ~ 1.4 parts of polydimethylsiloxane, 1.2 ~ 1.5 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract D, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.2 ~ 0.4 part of essence, 0.05 ~ 0.15 portion of antiseptic and 0.8 ~ 1.5 part of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 41: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.4 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 14 parts of laureth sulfuric ester ammoniums are added, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 parts of Polyquaternium-10s, 3 parts of cocamido propyl betaine, 2 parts of fatty alcohol-polyoxyethylene ether, 1 part of alkyl polyglucoside, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, supplies deionized water and makes its ratio reach 60 parts, be heated to 80 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 1 part of Radix Notoginseng extract D, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.3 part of essence, 0.1 portion of antiseptic and 1 part of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 42: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.4 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 14 parts of laureth sulfuric ester ammoniums are added, 2 parts of lauryl alcohol sulfuric ester ammoniums, 2 parts of polyquaternary ammonium salt-43,2 parts of Polyquaternium-10s, 3 parts of lauroylamidopropyl betaines, 2 parts of fatty alcohol-polyoxyethylene ether, 1 part of alkyl polyglucoside, 1 part of docosyl hydroxypropyl quaternary ammonium salt, 1 part of polyquaternary ammonium salt-7,1 portion of pearling agent, supplies deionized water and makes its ratio reach 60 parts, be heated to 80 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.3 parts of polydimethylsiloxane, 1.3 parts of dimethiconols, 1 part of Radix Notoginseng extract D, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.3 part of essence, 0.1 portion of antiseptic and 1 part of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 43: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 16 parts of laureth sulfuric ester ammoniums are added, 3 parts of aliphatic acid polyethenoxy ether sodium sulfate, 3 parts of polyquaternary ammonium salt-43,3 parts of Polyquaternium-10s, 5 parts of cocamido propyl betaine, 3 parts of coconut oleoyl amine MEA, 1.5 parts of Coconut Fatty Acid Monoethanolamides, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portions of pearling agents, supply deionized water and make its ratio reach 80 parts, be heated to 85 DEG C, constant temperature stirs 20min; Then, be cooled to 65 DEG C, add 1.6 parts of polydimethylsiloxane, 1.4 parts of dimethiconols, 1.5 parts of Radix Notoginseng extract C, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.4 part of essence, 0.15 portion of antiseptic and 1.5 parts of sodium chloride stir; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Embodiment 44: a kind of preparation method of the shampoo containing arasaponin, as different from Example 23: described second step processing technology:
Ratio by weight:
(1) with deionized water, 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 16 parts of laureth sulfuric ester ammoniums are added, 3 parts of aliphatic acid polyethenoxy ether sodium sulfate, 3 parts of polyquaternary ammonium salt-43,3 parts of Polyquaternium-10s, 5 parts of cocamido propyl betaine, 3 parts of coconut oleoyl amine MEA, 1.5 parts of Coconut Fatty Acid Monoethanolamides, 1.5 parts of docosyl hydroxypropyl quaternary ammonium salts, 1.5 parts of polyquaternary ammonium salt-7,1.5 portions of pearling agents, supply deionized water and make its ratio reach 80 parts, be heated to 85 DEG C, constant temperature stirs 20min; Then, be cooled to 65 DEG C, add 1.6 parts of polydimethylsiloxane, 1.4 parts of dimethiconols, 1.5 parts of Radix Notoginseng extract C, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.4 part of essence, 0.15 portion of antiseptic, adopt in ripple nurse and thickening; Regulate pH value to be 6.0, get product, other parts no longer repeated description identical with embodiment 23.
Without departing from the present invention, various conversion and equivalent replacement can also be carried out to patent of the present invention, therefore, patent of the present invention is not limited to disclosed specific implementation process, and should comprise the whole embodiments fallen within the scope of Patent right requirement of the present invention.
Claims (3)
1., containing a shampoo for arasaponin, it is characterized in that, comprise the raw material of following weight parts ratio: anion surfactant 12 ~ 22 parts, non-ionic surface active agent 1 ~ 10 part, zwitterionic surfactant 0 ~ 7 part, cationic surfactant 1.8 ~ 10 parts, conditioner 3.6 ~ 12 parts, Radix Notoginseng extract 0.5 ~ 10 part, pearling agent 0.8 ~ 2 part, thickening agent 0.8 ~ 2 part, antiseptic 0.03 ~ 0.15 part, 0.1 ~ 0.7 part, essence, 0.8 ~ 1.7 part, sodium chloride, deionized water 40 ~ 80 parts; Described Radix Notoginseng extract is Radix Notoginseng, flower of Radix Notoginseng, the water of stem and leaf of Radix Notoginseng or the extractum of alcohol extraction or solid content; Described Radix Notoginseng extract comprises: the mixing of one or more in extract A, extract B, extract C, extract D tetra-kinds, and preparation method is:
(1) get appropriate Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng mixing, the ratio adding 6 ~ 12L according to per kilogram adds water, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, filtered, concentrated extracting solution, 60 DEG C time, measure relative density is 1.0 ~ 1.5, then, add the ethanol that alcoholic strength is 50% ~ 70%, leaving standstill makes it precipitate in more than 12 hours, reclaims ethanol, concentrated, drying, obtains extract A;
(2) by extract A water dissolution, upper ion exchange resin column is the ethanol elution of 50% ~ 70% with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrated, dry; Obtain extract B;
(3) get appropriate Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng mixing, the ratio adding 6 ~ 12L according to per kilogram adds the ethanol that alcoholic strength is 50% ~ 80%, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, collected ethanol extract, in above-mentioned medicinal residues, the ratio adding 6 ~ 12L according to per kilogram adds water, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, reclaims ethanol, concentrated, drying, obtains extract C;
(4) by extract C water dissolution, upper ion exchange resin column is the ethanol elution of 50% ~ 70% with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrated, dry, obtains extract D.
2. a kind of shampoo containing arasaponin according to claim 1, it is characterized in that, described anion surfactant is selected from the mixing of one or more in laureth sulfuric ester ammonium, lauryl alcohol sulfuric ester ammonium, sodium lauryl sulphate, coconut oleoyl amine sodium isethionate or polyoxyethylenated alcohol sodium sulfate; Cationic surfactant is selected from polyquaternary ammonium salt-43, the mixing of one or more in polyquaternary ammonium salt-51 or Polyquaternium-10; Zwitterionic surfactant is selected from cocoamido propyl hydroxy sulfobetaine, the mixing of one or more in cocamido propyl betaine or lauroylamidopropyl betaine; Non-ionic surface active agent is selected from alkyl polyglucoside, fatty alcohol-polyoxyethylene ether, the mixing of one or more in lauric acid amide of ethanol or Coconut Fatty Acid Monoethanolamide; Conditioner is selected from cation guar gum, docosyl hydroxypropyl quaternary ammonium salt, polyquaternary ammonium salt-7, emulsified silicone oil, the mixing of one or more in polydimethylsiloxane or dimethiconol; Thickening agent is in carbomer and thickening or the direct thickening of sodium chloride.
3., containing a preparation method for the shampoo of arasaponin, it is characterized in that, comprise the following steps:
The first step: get the raw materials ready
(1) Radix Notoginseng extract: be the water of Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng or the extractum of alcohol extraction or solid content;
This Radix Notoginseng extract comprises: the mixing of one or more in extract A, extract B, extract C, extract D tetra-kinds, and preparation method is:
(1) get appropriate Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng mixing, the ratio adding 6 ~ 12L according to per kilogram adds water, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, filtered, concentrated extracting solution, 60 DEG C time, measure relative density is 1.0 ~ 1.5, then, add the ethanol that alcoholic strength is 50% ~ 70%, leaving standstill makes it precipitate in more than 12 hours, reclaims ethanol, concentrated, drying, obtains extract A;
(2) by extract A water dissolution, upper ion exchange resin column is the ethanol elution of 50% ~ 70% with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrated, dry; Obtain extract B;
(3) get appropriate Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng mixing, the ratio adding 6 ~ 12L according to per kilogram adds the ethanol that alcoholic strength is 50% ~ 80%, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, collected ethanol extract, in above-mentioned medicinal residues, the ratio adding 6 ~ 12L according to per kilogram adds water, circumfluence distillation 2 ~ 3 times, each 1 ~ 3 hour, merge extractive liquid, reclaims ethanol, concentrated, drying, obtains extract C;
(4) by extract C water dissolution, upper ion exchange resin column is the ethanol elution of 50% ~ 70% with alcoholic strength, decolouring, and eluent reclaims ethanol, concentrated, dry, obtains extract D;
(2) anion surfactant: be selected from the mixing of one or more in laureth sulfuric ester ammonium, lauryl alcohol sulfuric ester ammonium, sodium lauryl sulphate, coconut oleoyl amine sodium isethionate or polyoxyethylenated alcohol sodium sulfate;
(3) cationic surfactant: be selected from polyquaternary ammonium salt-43, the mixing of one or more in polyquaternary ammonium salt-51 or Polyquaternium-10;
(4) zwitterionic surfactant: be selected from cocoamido propyl hydroxy sulfobetaine, the mixing of one or more in cocamido propyl betaine or lauroylamidopropyl betaine;
(5) non-ionic surface active agent: be selected from alkyl polyglucoside, fatty alcohol-polyoxyethylene ether, coconut oleoyl amine MEA, the mixing of one or more in lauric acid amide of ethanol or Coconut Fatty Acid Monoethanolamide;
(6) conditioner: be selected from cation guar gum, docosyl hydroxypropyl quaternary ammonium salt, polyquaternary ammonium salt-7, emulsified silicone oil, one or more mixing in polydimethylsiloxane or dimethiconol; Emulsified silicone oil is selected from Large stone emulsified silicone oil and small particle diameter emulsified silicone oil, or two kinds with one;
(7) thickening agent: in carbomer and thickening or the direct thickening of sodium chloride;
Second step: manufacture method is selected from one of following:
Method one:
(1) with deionized water, the cation melon glue of 0.3 ~ 0.6 part is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 6 ~ 10 parts of laureth sulfuric ester ammoniums, 6 ~ 7 parts of lauryl alcohol sulfuric ester ammoniums, 0.7 ~ 0.9 part of Polyquaternium-10,1 ~ 3 part of polyquaternary ammonium salt-51,2 ~ 5 parts of cocoamido propyl hydroxy sulfobetaine, 1 ~ 3 part of alkyl polyglucoside, 0.8 ~ 2 part of fatty alcohol-polyoxyethylene ether, 1 ~ 3 part of docosyl hydroxypropyl quaternary ammonium salt, 0.5 ~ 2 part of polyquaternary ammonium salt-7,1.3 ~ 1.7 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, be heated to 70 ~ 80 DEG C, constant temperature stirs 20min; Then, be cooled to 50 DEG C, add emulsified silicone oil 2 ~ 5 parts, Radix Notoginseng extract 1 ~ 4 part, constant temperature stirs 20min; Treat that temperature is down to less than 45 DEG C and is added 0.1 ~ 0.4 part, essence, 0.05 ~ 0.07 portion of antiseptic and 1 ~ 3 part, sodium chloride, stir; Regulate pH value to be 6.2, still aging 24 hours, get product;
Method two:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 10 ~ 15 parts of laureth sulfuric ester ammoniums, 5 ~ 7 parts of coconut oleoyl amine sodium isethionates, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of polyquaternary ammonium salt-51,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of Coconut Fatty Acid Monoethanolamide, 0.8 ~ 1.5 part of lauric acid amide of ethanol, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,1.3 ~ 1.7 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, be heated to 70 ~ 80 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.3 ~ 1.7 parts of polydimethylsiloxane, 1.3 ~ 1.7 parts of emulsified silicone oils, 1.3 ~ 1.7 parts of Radix Notoginseng extracts, constant temperature stirs 30nin; Treat that temperature is down to less than 40 DEG C and is added 0.1 ~ 0.4 part of essence, 0.03 ~ 0.1 portion of antiseptic and 1.3 ~ 1.7 parts of sodium chloride stir; Regulate pH value to be 5.8, still aging 36 hours, get product;
Method three:
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, 12 ~ 16 parts of sodium lauryl sulphates are added, 2 ~ 5 parts of coconut oleoyl amine sodium isethionates, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of Polyquaternium-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of Coconut Fatty Acid Monoethanolamide, 0.8 ~ 1.5 part of lauric acid amide of ethanol, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,0.8 ~ 1.5 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, water is heated to 70 ~ 80 DEG C, and constant temperature stirs 20min; Then, be cooled to 50 DEG C, add 1.3 ~ 1.7 parts of polydimethylsiloxane, 1.3 ~ 1.7 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.3 ~ 0.5 part of essence, 0.05 ~ 0.15 portion of antiseptic and 1.3 ~ 1.7 parts of sodium chloride stir; Regulate pH value to be 6.0, get product;
Method four:
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of sodium lauryl sulphate, 0.8 ~ 1.5 part of polyquaternary ammonium salt-43,1 ~ 3 part of Polyquaternium-10,2 ~ 5 parts of coconut oleoyl amine MEA, 1 ~ 3 part of fatty alcohol-polyoxyethylene ether, 0.8 ~ 1.5 part of lauric acid amide of ethanol, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,0.8 ~ 1.5 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, water is heated to 70 ~ 80 DEG C, and constant temperature stirs 20min; Then, be cooled to 50 DEG C, add 2 ~ 5 parts of emulsified silicone oils, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 20nin; Treat that temperature is down to less than 45 DEG C, add 0.3 ~ 0.7 part of essence, 0.05 ~ 0.15 portion of antiseptic and 1.3 ~ 1.7 parts of sodium chloride stir; Regulate pH value to be 5.8, still aging 48 hours, get product;
Method five:
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of Polyquaternium-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of alkyl polyglucoside, 0.8 ~ 1.5 part of lauric acid amide of ethanol, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,0.8 ~ 1.5 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, be heated to 75 ~ 85 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.3 ~ 1.7 parts of polydimethylsiloxane, 1.3 ~ 1.7 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.2 ~ 0.4 part of essence, 0.05 ~ 0.15 portion of antiseptic and 1 ~ 1.5 part of sodium chloride stir; Regulate pH value to be 6.0, get product;
Method six:
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of Polyquaternium-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of coconut oleoyl amine MEA, 0.8 ~ 1.5 part of Coconut Fatty Acid Monoethanolamide, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,0.8 ~ 1.5 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, be heated to 75 ~ 85 DEG C, constant temperature stirs 20min; Then, be cooled to 65 DEG C, add 1.3 ~ 1.6 parts of polydimethylsiloxane, 1 ~ 1.4 part of dimethiconol, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.2 ~ 0.4 part of essence, 0.05 ~ 0.15 portion of antiseptic and 1 ~ 1.5 part of sodium chloride stir; Regulate pH value to be 6.0, get product;
Method seven:
Ratio by weight:
(1) with deionized water, 0.3 ~ 0.6 part of cation melon glue is heated scattered for subsequent use;
(2) in scattered cation guar gum, add 12 ~ 16 parts of laureth sulfuric ester ammoniums, 1 ~ 3 part of lauryl alcohol sulfuric ester ammonium, 1 ~ 3 part of polyquaternary ammonium salt-43,1 ~ 3 part of Polyquaternium-10,2 ~ 5 parts of cocamido propyl betaine, 1 ~ 3 part of fatty alcohol-polyoxyethylene ether, 0.8 ~ 1.5 part of alkyl polyglucoside, 0.8 ~ 1.5 part of docosyl hydroxypropyl quaternary ammonium salt, 0.8 ~ 1.5 part of polyquaternary ammonium salt-7,0.8 ~ 1.5 portions of pearling agents, supply deionized water and make its ratio reach 40 ~ 80 parts, be heated to 80 DEG C, constant temperature stirs 20min; Then, be cooled to 60 DEG C, add 1.1 ~ 1.4 parts of polydimethylsiloxane, 1.2 ~ 1.5 parts of dimethiconols, 0.8 ~ 1.5 part of Radix Notoginseng extract, constant temperature stirs 30nin; Treat that temperature is down to less than 45 DEG C and is added 0.2 ~ 0.4 part of essence, 0.05 ~ 0.15 portion of antiseptic and 0.8 ~ 1.5 part of sodium chloride stir; Regulate pH value to be 6.0, get product.
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| WO2017175005A1 (en) * | 2016-04-08 | 2017-10-12 | Innospec Limited | Compositions with acylisethionate surfactant and methods of use |
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| CN103506051A (en) * | 2013-07-22 | 2014-01-15 | 广州环亚化妆品科技有限公司 | Preparation method of plant surface active agent composition and application of the composition to washing supplies |
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| US11116220B2 (en) | 2017-12-22 | 2021-09-14 | Ecolab Usa Inc. | Antimicrobial compositions with enhanced efficacy |
| CN108815088A (en) * | 2018-09-18 | 2018-11-16 | 云南邦乐生物科技有限公司 | A kind of phalacrosis prevention and hair generation shampoo and preparation method thereof |
| CN111374912A (en) * | 2018-12-28 | 2020-07-07 | 上海瑞帝安生物科技有限公司 | A composition for promoting hair growth |
| CN111494286A (en) * | 2020-06-15 | 2020-08-07 | 广州头道医药生物科技有限公司 | Alopecia-stopping and hair-growing shampoo |
| CN115590804A (en) * | 2022-11-02 | 2023-01-13 | 温州大学（Cn） | Shampoo containing traditional Chinese medicine extract |
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Inventor after: Gao Mingju Inventor after: Wang Yin Inventor after: Huang Zhaozhong Inventor before: Zhang Peng Inventor before: Wang Yin Inventor before: Gao Mingju |
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Denomination of invention: A shampoo containing Sanqi saponins and its preparation method Granted publication date: 20160113 Pledgee: Wenshan Minfeng Rural Bank Co.,Ltd. Pledgor: YUNNAN QIDAN PHARMACEUTICAL Co.,Ltd. Registration number: Y2024980040240 |