CN104042528B

CN104042528B - Draft hair care anticreep anti-dandruff shampoo stock solution and manufacture method

Info

Publication number: CN104042528B
Application number: CN201410324556.6A
Authority: CN
Inventors: 蒙军; 唐萌; 刘代伟; 唐良建
Original assignee: Chongqing Menglizhuri Cosmetics Co Ltd
Current assignee: Chongqing Native Grass
Priority date: 2014-07-09
Filing date: 2014-07-09
Publication date: 2016-04-13
Anticipated expiration: 2034-07-09
Also published as: CN104042528A

Abstract

The present invention relates to a kind of hair-washing hair-care articles for use, be specifically related to a kind of draft hair care anticreep anti-dandruff shampoo stock solution and manufacture method; Under agitation add sodium laureth sulfate, betanin and soapberry extract and obtain shampoo substrate, neutral with Fructus Citri Limoniae acid for adjusting pH, add Fructus Gleditsiae Abnormalis extract successively, Cacumen Platycladi extract, Herba Ecliptae extract, Radix Rhodiolae, Radix Polygoni Multiflori, Radix Ginseng combined extracting thing, Radix Angelicae Sinensis extract, Rhizoma Zingiberis Recens extract, Folium Ginkgo, Herba Taraxaci, Flos Lonicerae, Folium Mori extract, finally add plant antiseptic agent and namely obtain this finished product; The shampoo of technical solution of the present invention, adopt natural plant formula, show after tested, can clean scalp dirt, correct dermophyte has the effect of better drawing up, nutrition scalp, can dandruff-removing itching-relieve, to reduce alopecia, hair care effect obvious, gentle non-stimulated in addition, safety and Health, uses residual being easy to of rear sewage to decompose.

Description

Herbal hair-nourishing, hair-loss-preventing and dandruff-removing shampoo stock solution and preparation method thereof

Technical Field

The invention relates to a hair washing and protecting product, in particular to a shampoo of plant extracts.

Background

The main components of the traditional daily chemical shampoo are chemical raw materials, in addition, in order to meet the requirements of consumers on functional effects, even a plurality of harmful additives such as silicon sodium, silicon ester, siloxane and other organic silicon are added into the shampoo, and although the organic silicon can immediately provide good smooth feeling for human hair and skin, the organic silicon can block hair follicles and hair phosphorus sheets of human bodies after being contacted and used for a long time, the scalp is further itchy, dandruff is increased, hair quality is withered and yellow, and the shampoo is branched, easy to break and easy to fall off; in addition, the organic silicon is not soluble in water and any surfactant, is difficult to biodegrade after being discharged into the environment after shampooing, and is easy to cause environmental pollution. In addition, in order to improve scalp itching and remove dandruff, some bactericides are usually added into the shampoo, wherein the common bactericides are zinc pyrithione, the zinc-containing compound synthesized by chemical engineering has strong bactericidal performance and takes effect in the initial period, but the zinc-containing compound can not fundamentally improve sebum secretion, can damage human body embryo and harm human health, and in addition, the bactericides are not soluble in water and surfactants, like absorbing on human scalp and hair, have lasting harm to human body and are easy to cause environmental pollution.

An effective, safe and healthy hair washing and protecting product is urgently needed.

Disclosure of Invention

The invention aims to solve the technical problem of providing the shampoo which has the advantages of dandruff removal, itching relieving, good hair washing and protecting effects, safety and health.

In order to realize the purpose, the invention provides a herbal hair-nourishing, anti-hair loss and anti-dandruff shampoo stock solution and a preparation method thereof: the composition is prepared by the following process, wherein the components are calculated by weight:

(1) preparing a matrix, namely adding 30 parts of sodium laureth sulfate, 5 parts of betaine and 20-25 parts of soapberry extract at normal temperature under low-speed stirring, and uniformly mixing and stirring to obtain a shampoo matrix;

(2) adding the components, namely adjusting the pH value of the matrix to be neutral by using citric acid, and sequentially adding 3-5 parts of saponin extract, 5-7 parts of cacumen biotae extract, 10-16 parts of rhodiola rosea, polygonum multiflorum and ginseng combined extract, 3-5 parts of angelica sinensis extract, 5-7 parts of ginger extract, 10 parts of ginkgo leaf, dandelion, honeysuckle and mulberry leaf combined extract and 3-5 parts of eclipta extract;

(3) and (3) preparing a finished product, adding 1 part of plant preservative, sterilizing and filling to obtain the finished product.

Wherein,

the soapberry extract is prepared by baking soapberry pure peel at 60-80 ℃, and the applicant finds that organic active substances can be kept to the maximum extent at the moment, the soapberry extract is crushed into 20 meshes, then 5 times of pure water by weight is added, the mixture is soaked at 60-80 ℃ for 24 hours to obtain filtrate, filter residues can be used as fertilizer, and the filtrate is kept still for 10 days to obtain clear liquid, so that the release of saponin is facilitated; the soapberry extract is rich in soapberry saponin (sapindussaponin), fatty oil and protein, wherein the saponin mainly comprises triterpenoid saponin and sesquiterpene saponin, is a natural plant nonionic surfactant, has strong dirt removing and decontaminating capabilities, is easy to degrade, has no harmful residue, is simple and convenient to wash, has no peculiar smell, has small irritation to skin, has antibacterial, environmental protection and pollution-free effects, and also contains a plurality of substances beneficial to a human body, such as: reducing sugar, fatty acid, oil, oleic acid, carotenoid, nicotinic acid, riboflavin, protein, vitamin C, vitamin A, vitamin B, lysine, tyrosine, phenylalanine, glutamic acid, glycine, histidine and other more than 10 amino acids, and has hair nourishing effect. Has antibacterial, skin caring, antibacterial, antiinflammatory, dandruff removing, antipruritic, speckle removing, acne removing, skin whitening, and dermatogic disease preventing and treating effects; recorded in the book "Bencao gang mu" of the Ming Dynasty Jieji physician Li Shizhen, soapberry has the functions of removing head wind (dandruff) and improving eyesight, and can whiten and remove spots by washing face.

The fructus Gleditsiae Abnormalis extract is prepared by soaking fructus Gleditsiae Abnormalis in 3 times of pure water at 80 deg.C for 24 hr, and filtering to obtain filtrate; the saponin comprises gleditschia horrida glycoside (Gledinin), ceryl alcohol (Cerylalcohol), nonacosan-ne (Nonacosa-ne), Stigmasterol (Stigmasterol), Sitosterol (Sitosterol) and the like, has the effects of preventing hair loss and blackening hair, can clear away heat and remove dampness, remove redundant fat, smoothen and block hair follicles, has good effects on preventing hair loss and blackening hair, and does not stimulate the scalp.

The ginger extract is obtained by squeezing ginger and soaking the ginger in 3 times of pure water with the weight of 40-60 ℃ for 24 hours, and taking filtrate; the ginger extract contains gingerol, shogaol and other components, and has effects of promoting normal blood circulation of scalp, activating hair follicle tissue, effectively preventing alopecia, promoting new hair growth, and nourishing hair root.

The cacumen biotae extract is obtained by soaking fresh cacumen biotae in 45% alcohol with the weight 5 times that of the cacumen biotae, evaporating the filtrate in water bath at 80-85 ℃ for 2-3 hours after 5 days, and taking clear liquid; the hair oil substance extracted from cacumen Platycladi has effects of regulating blood circulation, promoting hair growth and blackening hair, and inhibiting alopecia, and is especially used for treating blood heat alopecia and alopecia areata of middle-aged and young people.

The eclipta alba extract is obtained by soaking the whole plant of the eclipta alba in 2 times of pure water, boiling for 15 minutes and taking filtrate; ecliptae herba contains volatile oil, tannin, saponin, Ecliptae herba extract and vitamin A. "Ben Cao gang mu" records that it can blacken moustache and tonify kidney yin, among the records of Chinese herbal medicine, Ecliptae herba is the best medicine for blackening white hair.

The mixed extract of rhodiola, polygonum multiflorum and ginseng adopts three components in a slice form, and the weight ratio of the three components is 1: 2: soaking 1 weight of ginseng in 3 times of pure water for 2 hours, boiling for 1 hour, draining, supplementing 3 times of pure water, boiling for 1 hour again, draining, supplementing 3 times of pure water, boiling for 1 hour, mixing the filtrate for 3 times, centrifuging, and taking clear liquid to obtain the shampoo, wherein the defect that the shampoo is turbid due to a single ginseng extract can be overcome by adopting a mixed extraction mode, and the quality of the final shampoo is greatly improved; rhodiola rosea is known as a medicine top product in Shen nong Ben Cao Jing, and rhodiola sachalinensis has miraculous effects of resisting oxidation and aging, effectively removing free radicals and delaying scalp aging. The Polygoni Multiflori radix extract, especially Polygoni Multiflori radix root extract, is rich in anthraquinone compounds, stilbene compounds, gallic acid (gallic acid), catechin (catechin), lecithin, and Polygoni Multiflori radix extract, and can be used as tonic and antiaging agent for treating alopecia and premature gray hair, blackening hair, resisting aging, enhancing immunity, promoting adrenal cortex function, and improving sleep; ginseng contains rich ginsenoside, it has effects of regulating human central nervous system, antifatigue, regulating metabolism of material, etc., these three kinds of raw materials are matched, and adopt the high temperature to wash and boil, can make its active ingredient fully released, the hair care efficacy can be given full play best.

The combined extract of ginkgo leaves, dandelion, honeysuckle and frosted mulberry leaves is prepared according to the weight ratio of 1.5: 1: 1: 1.5, mixing and immersing in pure water, adding 3 times of boiling water, soaking for 8-10 hours, and taking the filtrate to obtain the product; the ginkgo leaf shampoo can 'remove head wind', the scalp is effectively cleaned by unique flavone compounds, rich mineral substances and vitamins, and saponin contained in the ginkgo leaf shampoo has the effect of purifying the scalp. The dandelion contains various healthy nutritional ingredients such as taraxol, taraxacin, choline, organic acid, inulin and the like, has the effects of diminishing inflammation, improving eczema and relieving dermatitis, and is described in compendium of materia Medica: blackening beard and hair, and strengthening bones and muscles; frost mulberry leaf contains inokosterone (inokosterone), ecdysteroid (ecdysterone), rutin, morcarin (morcetin), trigonelline (trigonelline), choline, adenine, aspartic acid and chlorogenic acid, and has antibacterial, antibacterial and antiinflammatory effects on human skin; the honeysuckle contains inositol, flavonoid, inositol, saponin, tannin and the like, has broad-spectrum antibacterial action, has stronger inhibiting action on staphylococcus aureus, shigella dysenteriae and other pathogenic bacteria, also has inhibiting action on leptospira, influenza virus, pathogenic fungi and other pathogenic microorganisms, and also has obvious anti-inflammatory and antipyretic actions, and the 4 plants are all flower leaves, and the research of the applicant finds that: the honeysuckle and the frosted mulberry leaf can effectively inhibit the growth of bacteria and fungi, achieve the efficacy of removing dandruff and relieving itching, and keep the scalp fresh, and the mixed extraction of the four medicines can enhance the effects of clearing heat and removing toxicity, and resisting bacteria and diminishing inflammation.

The radix Angelicae sinensis extract is prepared by decocting dried radix Angelicae sinensis in 4 times of pure water for 3 hr, cooling, and collecting filtrate; the angelica has the functions of antibiosis and antiphlogosis in vitro, and can cause local hyperemia, leukocyte and fiber infiltration of skin and regeneration of new-born epithelium.

The shampoo adopting the technical scheme has the following advantages: because the natural plant components are adopted, chemical raw materials which can be dissolved at high temperature are not contained any more, the traditional hot preparation method is changed into cold preparation, thus the loss of volatile organic compounds in the plant extracting solution can be reduced, and the energy can be saved. In addition, because the natural plant components are used as main components, a plurality of formulas supplement each other. The soapberry extract and the Chinese honeylocust fruit extract are used as monarch drugs, so that the soap has strong detergency, fine foam, easy washing, safe use, no stimulation to eyes, skin and mucous membrane and good oil control effect on oily hair; the ginkgo leaf, dandelion, honeysuckle and frosted mulberry leaf combined extract is used as a minister to replace a chemical medicine antidandruff antipruritic zinc pyrithione, so that the composition has a high-efficiency inhibition effect on epidermal bacteria and fungi, has an obvious antidandruff and antipruritic effect, and is safer to use; the arborvitae tops extract, the eclipta alba extract and the ginger extract are used as adjuvant drugs, so that hair loss is reduced, new hair growth is promoted, and hair is blacked; rhodiola rosea, polygonum multiflorum, ginseng extract and angelica extract are used as conductant drug, so that the hair conditioner can effectively promote blood circulation, provide nutrients for scalp, repair broken hair and forked hair and improve hair quality; the medicines are compatible, so that the scalp is healthier, the hair is increased, the dandruff is reduced, and the hair is black, bright and smooth while the scalp and the hair are cleaned. And finally, the shampoo stock solution contains plant extracts, does not generate residues harmful to human health and environment, and is beneficial to environmental protection.

Detailed Description

The components, the preparation process and the effect evaluation condition of the herbal hair-nourishing, hair-loss-preventing and dandruff-removing shampoo stock solution in the embodiment of the invention are given below, wherein the components are calculated according to the parts by weight:

the shampoo preparation was described as the component proportioning product of example 6 above, and compared to commercially available daily chemical shampoos:

(1) preparing a matrix, namely adding 30 parts of sodium laureth sulfate, 5 parts of betaine and 25 parts of Chinese soapberry fruit extract at normal temperature under low-speed stirring, and uniformly mixing and stirring to obtain a shampoo matrix;

(2) adding components, namely adjusting the pH value of the matrix to be neutral by using citric acid, and sequentially adding 7 parts of Chinese honeylocust fruit extract, 8 parts of cacumen biotae extract, 9 parts of rhodiola rosea, polygonum multiflorum and ginseng combined extract, 4 parts of angelica sinensis extract, 5 parts of ginger extract, 7 parts of eclipta extract and 6 parts of ginkgo leaf, dandelion, honeysuckle and frosted mulberry leaf combined extract;

Wherein,

the soapberry extract is prepared by baking pure soapberry pericarp at 60-80 ℃, crushing to 20 meshes, adding 5 times of pure water by weight, soaking at 60-80 ℃ for 24 hours to obtain filtrate, wherein the filtrate is favorable for fully releasing saponin, preferably standing for 10 days to obtain clear liquid, and preferably baking and soaking at 65 ℃ to ensure that organic active substances of the soapberry are not damaged;

the fructus Gleditsiae Abnormalis extract is prepared by squeezing fructus Gleditsiae Abnormalis, soaking in 3 times of pure water at 80 deg.C for 24 hr, and filtering to obtain filtrate;

the ginger extract is obtained by squeezing ginger and soaking the ginger in 3 times of pure water with the weight of 40-60 ℃ for 24 hours, and taking filtrate; in order to extract ginger active substances to the maximum extent, the structure of the biological cells can be destroyed by squeezing, and the ginger juice and the residues are simultaneously soaked at the preferential temperature of 45 ℃.

The cacumen biotae extract is obtained by soaking fresh cacumen biotae in 45% alcohol with the weight 5 times that of the cacumen biotae, evaporating a filtrate in a water bath at 80-85 ℃ for 2-3 hours after 5 days, and taking a clear liquid;

the eclipta alba extract is obtained by soaking the whole plant of the eclipta alba in pure water with the weight of 2 times of that of the eclipta alba, boiling for 15 minutes and taking filtrate;

the mixed extract of rhodiola, polygonum multiflorum and ginseng is preferably sliced to ensure the extraction effect, and the three components are mixed according to the weight ratio of 1: 2: soaking 1 weight of the powder in 3 times of pure water for 2 hours, boiling for 3 times, 1 hour each time, cooling, centrifuging, and collecting clear liquid;

the combined extract of ginkgo leaves, dandelion, honeysuckle and frosted mulberry leaves is prepared from the following components in percentage by weight of 3: 2: 2: 3, adding the mixture into boiling water with the weight being 3 times that of the mixture, soaking the mixture for 8 to 10 hours, and taking filtrate to obtain the product;

the radix Angelicae sinensis extract is prepared by decocting dried radix Angelicae sinensis in 4 times of pure water for 3 hr, cooling, and collecting filtrate.

The evaluation condition of the comprehensive effect of the shampoo stock solution obtained by the preparation method is detailed in a table 2:

TABLE 2 comprehensive results evaluation Table

The human body effect experiment of the shampoo stock solution obtained by the preparation method is as follows:

and (3) inclusion standard: the age is 15-55 years old, after the daily chemical shampoo is used for a long time, the head has the phenomena of dry hair, scurf and pruritus in different degrees, and 75 cases are randomly selected for men and women. Wherein 25 cases are randomly selected from the first group, and the shampoo is used for three times per week in conventional dosage for more than one month; the second group randomly selected 25 of the rest 50 cases, changed with the shampoo of the invention, used twice a week with conventional dosage, and continuously used for 1 week; the rest 25 cases are used as control groups, and the original shampoo is still adopted, the dosage is conventional, the use is carried out three times in a week, and the use is continued for one month.

The effect standard is as follows:

full effect: the hair is soft and smooth, no scurf can be seen by naked eyes, and the phenomenon of pruritus completely disappears;

the method has the following advantages: the hair is not knotted, and sporadic scurf appears with naked eyes without the feeling of itching;

and (4) invalidation: no change is caused before and after use;

deterioration: the dandruff and itching phenomenon worsens.

Table 3 experimental results table:

results	First group	Second group	Third group
				All effects	23	15	0
Is effective	2	9	1
				Invalidation	0	1	125 -->
Deterioration of	0	0	13

It can be seen from the above table that the shampoo of the invention can achieve better effect after being continuously used for more than one week, and basically achieve full effect after being continuously used for more than one month, the hair quality is soft and smooth, and the phenomena of scurf and pruritus can completely disappear, the crowd applicability is up to more than 92 percent due to the adoption of the plant formula, while the phenomena of pruritus and scurf deterioration continuously occur due to the use of organosilicon and zinc-containing compounds after being continuously used for the traditional daily chemical products.

Typical cases are as follows:

miss plum, 16 years old; after long-term use of Miss plum, a certain daily chemical anti-hair loss shampoo sold in the market is used for a long time, although the hair is soft enough, the scalp is itchy for a long time, after the shampoo provided by the invention is continuously used, the hair is still soft, the dandruff is not generated, and the scalp itching symptom gradually disappears from relieving.

The hair of the women with the hair loss is 31 years old, the hair is short, the women with the hair loss uses a certain daily chemical hair care shampoo sold in the market before, the hair is dry, and the scalp feels clean and fresh when the shampoo provided by the invention is used for the first time, and the hair is combed smoothly; after being continuously used for one month, the hair is smooth and has no scurf and pruritus.

The shampoo provided by the invention has a good decontamination effect, and after the shampoo is used for one week, the greasy phenomenon of hair can be eliminated; after three weeks of insistence, the hair was kept non-greasy for three days between shampooings.

When the shampoo is applied for birth, the hair loss is reduced after 41 years old due to seborrheic dermatitis, the hair loss is reduced after 1 week, the hair loss is basically avoided after 3 months, and new hair is increased.

Mr. 36 years old, because the hair is always thin and soft and does not dare to accumulate, 400ml of the shampoo provided by the invention can thicken and harden the hair, and the hair is increased after half a year and already accumulates.

While only some of the preferred embodiments of the present invention have been described above, it should be understood that various modifications can be made by those skilled in the art without departing from the scope and spirit of the invention.

Claims

1. The preparation method of the herbal hair-nourishing, hair-loss-preventing and dandruff-removing shampoo stock solution is characterized by comprising the following steps: the composition is prepared by the following process, wherein the components are calculated by weight: (1) preparing a matrix, namely adding 30 parts of sodium laureth sulfate, 5 parts of betaine and 20-25 parts of soapberry extract at normal temperature under low-speed stirring, and uniformly mixing and stirring to obtain a shampoo stock solution matrix; (2) adding components, namely adjusting the pH value of the matrix to be neutral by using citric acid, and sequentially adding 5-8 parts of Chinese honeylocust fruit extract, 5-8 parts of cacumen biotae extract, 8-12 parts of rhodiola rosea, polygonum multiflorum and ginseng combined extract, 4-6 parts of angelica sinensis extract, 5-7 parts of ginger extract, 5-7 parts of eclipta extract and 5-7 parts of ginkgo leaf, dandelion, honeysuckle and folium mori combined extract; (3) preparing a finished product, adding 1 part of plant preservative, sterilizing and filling to obtain the finished product; wherein, the soapberry extract is obtained by baking pure soapberry peel at 60-80 ℃, crushing to 20 meshes, adding 5 times of pure water by weight, soaking at 60-80 ℃ for 24 hours to obtain filtrate, and standing for 10 days to obtain clear liquid; the fructus Gleditsiae Abnormalis extract is prepared by squeezing fructus Gleditsiae Abnormalis, soaking in 3 times of pure water at 80 deg.C for 24 hr, and filtering to obtain filtrate; the ginger extract is obtained by squeezing ginger and soaking the ginger in 3 times of pure water with the weight of 40-60 ℃ for 24 hours, and taking filtrate; the cacumen biotae extract is obtained by soaking fresh cacumen biotae in 45% alcohol with the weight 5 times that of the cacumen biotae, evaporating a filtrate in a water bath at 80-85 ℃ for 2-3 hours after 5 days, and taking a residual solution; the eclipta alba extract is obtained by soaking the whole plant of the eclipta alba in pure water with the weight of 2 times of the whole plant of the eclipta alba for half an hour, boiling for 15 minutes and taking filtrate; the combined extract of rhodiola, polygonum multiflorum and ginseng adopts three components in a slice form, and the weight ratio of the three components is 1: 2: soaking 1 weight of the filtrate in 3 times of pure water for 2 hours, boiling for 1 hour, draining, supplementing 3 times of pure water, boiling again for 1 hour, draining, supplementing 3 times of pure water, boiling for 1 hour, mixing the filtrates, centrifuging, and collecting the clear solution; the folium ginkgo, dandelion, honeysuckle and frosted mulberry leaf combined extract is prepared by mixing folium ginkgo, dandelion, honeysuckle and frosted mulberry leaf according to the weight ratio of 3: 2: 2: 3, adding the mixture into boiling water with the weight being 3 times of the mixed weight, soaking for 8-10 hours, and taking the filtrate to obtain the product; the radix Angelicae sinensis extract is prepared by decocting dried radix Angelicae sinensis in 4 times of pure water for 3 hr, cooling, and collecting filtrate.