CN104042528B

CN104042528B - Draft hair care anticreep anti-dandruff shampoo stock solution and manufacture method

Info

Publication number: CN104042528B
Application number: CN201410324556.6A
Authority: CN
Inventors: 蒙军; 唐萌; 刘代伟; 唐良建
Original assignee: Chongqing Menglizhuri Cosmetics Co Ltd
Current assignee: Chongqing native grass
Priority date: 2014-07-09
Filing date: 2014-07-09
Publication date: 2016-04-13
Anticipated expiration: 2034-07-09
Also published as: CN104042528A

Abstract

The present invention relates to a kind of hair-washing hair-care articles for use, be specifically related to a kind of draft hair care anticreep anti-dandruff shampoo stock solution and manufacture method; Under agitation add sodium laureth sulfate, betanin and soapberry extract and obtain shampoo substrate, neutral with Fructus Citri Limoniae acid for adjusting pH, add Fructus Gleditsiae Abnormalis extract successively, Cacumen Platycladi extract, Herba Ecliptae extract, Radix Rhodiolae, Radix Polygoni Multiflori, Radix Ginseng combined extracting thing, Radix Angelicae Sinensis extract, Rhizoma Zingiberis Recens extract, Folium Ginkgo, Herba Taraxaci, Flos Lonicerae, Folium Mori extract, finally add plant antiseptic agent and namely obtain this finished product; The shampoo of technical solution of the present invention, adopt natural plant formula, show after tested, can clean scalp dirt, correct dermophyte has the effect of better drawing up, nutrition scalp, can dandruff-removing itching-relieve, to reduce alopecia, hair care effect obvious, gentle non-stimulated in addition, safety and Health, uses residual being easy to of rear sewage to decompose.

Description

Draft hair care anticreep anti-dandruff shampoo stock solution and manufacture method

Technical field

The present invention relates to a kind of hair-washing hair-care articles for use, be specifically related to the shampoo of a Plant Extracts.

Background technology

The main component of tradition daily use chemicals shampoo is industrial chemicals, in addition in order to meet the demand on consumer's functional effect, with the addition of multiple harmful additive even wherein, as organosilicons such as silicon sodium, estersil, siloxanes, although organosilicon can immediately for the hair of people and skin provide fine smooth feeling, but Long Term Contact and use can block hair follicle and the hair hair phosphorus sheet of human body, get over and then cause scalp itch, dandruff increases, hair quality is withered and yellow, bifurcated, easily broken, easily come off; In addition these organosilicons are not only water insoluble but also be insoluble to any surfactant, enter environment and are also difficult to biodegradation, easily cause environmental pollution after hair washing.In addition in order to improve scalp Pruritus and dandruff removing; shampoo also adds some antibacterial usually; wherein common fungicide is Zinc Pyrithione; the zinc compound bactericidal property of this chemical industry synthesis is very strong; initial stage takes effect; but it fundamentally can not improve the secretion of sebum; also can destroy human body mold simultaneously; be detrimental to health; these antibacterial also water insoluble and surfactant in addition; like absorption on the scalp and hair of people, lasting to human body infringement, and equally easily cause the pollution to environment.

People are effective in the urgent need to one, and the hair-washing hair-care articles for use of safety and Health.

Summary of the invention

The technical problem that will solve of the present invention is to provide a kind of dandruff-removing itching-relieve, hair-washing hair-care is effective, and the shampoo of safety and Health.

To achieve these goals, the invention provides a kind of draft hair care anticreep anti-dandruff shampoo stock solution and manufacture method: prepare according to following technique, wherein component is with parts by weight:

(1) matrix composition, add sodium laureth sulfate 30 parts, betanin 5 parts and soapberry extract 20 ~ 25 parts under room temperature stirring at low speed, mixing and stirring obtains shampoo substrate;

(2) component is added, regulate above-mentioned substrate pH value to neutral with citric acid, add Fructus Gleditsiae Abnormalis extract 3 ~ 5 parts successively, Cacumen Platycladi extract 5 ~ 7 parts, Radix Rhodiolae, Radix Polygoni Multiflori, Radix Ginseng combined extracting thing 10 ~ 16 parts, Radix Angelicae Sinensis extract 3 ~ 5 parts, Rhizoma Zingiberis Recens extract 5 ~ 7 parts, Folium Ginkgo, Herba Taraxaci, Flos Lonicerae, Folium Mori combined extracting thing 10 parts, Herba Ecliptae extract 3 ~ 5 parts;

(3) finished product makes, and add plant antiseptic agent 1 part, sterilization filling obtains finished product.

Wherein,

Soapberry extract is dried at 60 ~ 80 DEG C by the pure peel of Fructus Sapindi Mukouossi, applicant finds now to keep its organic active thing to greatest extent, be crushed to 20 orders, then the pure water of 5 times of weight is added, soak at 60 ~ 80 DEG C and get filtrate in 24 hours, filtering residue can make fertilizer, leaves standstill and within 10th, gets clear liquid and obtain, and is beneficial to saponin release, soapberry extract is rich in sapindoside (sapindussaponin), fatty oil, protein, wherein saponin is mainly triterpene saponin and sesquiterpene saponin, for a kind of natural plants non-ionic surface active agent, take out stains strong detergency, easy degraded, and without hazard residue, rinse simple and convenient, free from extraneous odour, little to skin irritation, have antibacterial, environmental protection, nuisanceless, in addition containing many materials useful to human body, as: reducing sugar, fatty acid, oils and fats, oleic acid, carotenoid, nicotinic acid, riboflavin, protein, vitamin C, vitamin A, vitamin B and lysine, tyrosine, phenylalanine, glutamic acid, 10 several amino acids such as glycine and histidine, tool hair care effect.Human body skin is had to antibacterial beauty treatment, bactericidal antiphlogistic, dandruff-removing itching-relieve, speckle removing, acne removing, brightens, prevents and treats the effects such as dermatosis; Record in the Ming Dynasty's outstanding physician's Li Shizhen (1518-1593 A.D.) Compendium of Material Medica that " Fructus Sapindi Mukouossi hair washing can be decaptitated wind (dandruff) improving eyesight, washes one's face and can brighten speckle.

Fructus Gleditsiae Abnormalis extract is that Fructus Gleditsia soaks 24 hours in the 3 times of weight pure water being greater than 80 DEG C, gets filtrate obtaining; Fructus Gleditsiae Abnormalis extract is containing triterpenoid saponin, tannin. and Saponin has gledinin (Gledinin), the tool anticreep black hair effects such as ceryl alcohol (Cerylalcohol), nonacosane (Nonacosa-ne), stigmasterol (Stigmasterol), sitosterol (Sitosterol), can clearing away heat and eliminating dampness, dispel superabundant fats, unobstructed obstruction hair follicle, to Anti-hair loss and black hair effect rather good, can not scalp irritation.

Rhizoma Zingiberis Recens extract is Rhizoma Zingiberis Recens squeezing and soaks 24 hours in 3 times of weight pure water of 40 ~ 60 DEG C, gets filtrate obtaining; Rhizoma Zingiberis Recens extract contains gingerol, and zingiberene wet goods composition, can promote scalp normal blood circulation, activation hair follicle tissue, effectively anti-loss, helps kainogenesis long, enriched nutritive root of hair.

Cacumen Platycladi extract is that fresh Cacumen Platycladi is soaked in 45% ethanol of 5 times of weight, and after 5 days, filtrate is at 80 ~ 85 DEG C of water-bath evaporation 2-3 hour, gets clear liquid and obtains; What Cacumen Platycladi was extracted sends out oily substance, has obvious effect to adjustment blood circulation, growing and blacking hair, has original effect, especially for young and middle-aged heat in blood alopecia and alopecia areata to suppression alopecia.

Herba Ecliptae extract is that Herba Ecliptae herb boils 15 minutes after 2 times of pure water soak, and gets filtrate obtaining; Herba Ecliptae contains the chemical compositions such as volatile oil, tannin, Saponin, Herba Ecliptae element and vitamin A." Compendium of Material Medica record energy " black moustache (palpus) is sent out, and kidney tonifying is cloudy ", in Chinese herbal medicine is recorded, Herba Ecliptae is the optimal drug of poliosis blackening.

Radix Rhodiolae, Radix Polygoni Multiflori and Radix Ginseng mixed extract, adopt these three kinds of components of sliced form, soak 2 hours according to 1:2:1 weight in 3 times of pure water, brewing 1 hour, strains dry, supplements 3 times of pure water, brewing 1 hour again, strain dry, then supplement 3 times of pure water, brewing 1 hour, 3 filtrate mixing through centrifugalize, get clear liquid to obtain, adopt mixed extraction mode can overcome the shortcoming that single Radix Ginseng extract makes shampoo muddiness herein, substantially increase the quality of final shampoo; Radix Rhodiolae is described as " medicine top grade " at Shennong's Herbal, and Radix Rhodiolae possesses magical effect of antioxidation, defying age, and effective scavenging free radicals delays scalp aging.Radix Polygoni Multiflori extract is Radix Polygoni Multiflori root block extract particularly, be rich in anthraquinone analog compound, stilbene compound, gallate-based (gallicacid), cachou extract (catechin), lecithin, Radix Polygoni Multiflori extract is used as tonifying recipes and antidotal agent, is usually used in hair growth and early whitening of hair, there is black hair, defying age, enhancing human body immunity power, promotes adrenal cortex function, improving water flood; Radix Ginseng includes abundant ginsenoside, it has obvious effect to the central nervous system, resisting fatigue, Auto-regulator metabolism etc. of mediator, and these three kinds of raw materials through collocation, and adopt high temperature brewing, its active ingredient can be made to be able to abundant release, and hair care effect can preferably play.

Folium Ginkgo, Herba Taraxaci, Flos Lonicerae, Folium Mori combined extracting thing mix according to the weight ratio of 1.5:1:1:1.5 and be immersed in pure water, adds 3 times of boiling water immersions and get filtrate obtaining after 8 ~ 10 hours; Folium Ginkgo hair washing can " wind of decaptitating ", and its exclusive chromocor compound and the mineral be rich in, the effectively clean scalp of vitamin, Saponin contained by it has effect of purification to scalp.Herba Taraxaci contains the multiple health-nutrition compositions such as taraxol, taraxacin, choline, organic acid, inulin, has antiinflammation, improves eczema, the effect of dermatitis of releiving, Compendium of Material Medica: black beard and hair, strengthening bone and muscle, Folium Mori cuts (ecdysterone), rutin, Mulberry glycosides (morcetin), trigonelline (trigonelline), choline, adenine, aspartic acid, chlorogenic acid containing inokosterone (inokosterone), decortication steroid, acting on human body skin has antibacterial, sterilization and inflammation-diminishing function, Flos Lonicerae is containing cyclohexanhexanol, flavonoid, inositol, Saponin and tannin etc., there is broad-spectrum antibacterial action, to staphylococcus aureus, the various pathogens such as dysentery bacterium all have stronger inhibitory action, to leptospira, the multiple pathogenic microorganisms such as influenza virus and pathogenic moulds also has inhibitory action, in addition, Flos Lonicerae also has obvious antiinflammatory and refrigeration function, above-mentioned 4 taste plants are floral leaf, applicant studies discovery: Flos Lonicerae and Folium Mori compatibility can antibacterials effectively processed, conk, to removing dandruff itching-relieving efficacies, keep scalp salubrious, and the above-mentioned four Chinese medicine of mixed extraction can strengthen heat-clearing and toxic substances removing, anti-inflammation effect.

Radix Angelicae Sinensis extract is dry Radix Angelicae Sinensis brewing 3 hours in 4 times of weight pure water, and filtrate obtaining is got in cooling; Radix Angelicae Sinensis has antibacterial, antiinflammation in vitro, local skin hyperemia, leukocyte and fiber is infiltrated, newborn epithelium regeneration.

The shampoo of technique scheme is adopted to have as follows a little: owing to have employed natural plant component, no longer containing the industrial chemicals that could dissolve under high temperature, change traditional heat preparation to do as cold preparation, so both can reduce the loss of volatile organic matter in plant extraction liquid, again can energy savings.In addition owing to being main component with natural plant component, multiple formulations complements each other.With soapberry extract, Fructus Gleditsiae Abnormalis extract for monarch, tool strong detergency foam is fine and smooth, easily rinses, and use safety is non-stimulated to eye, skin, mucosa, effective to the control oil of oiliness hair quality; With Folium Ginkgo, Herba Taraxaci, Flos Lonicerae, Folium Mori combined extracting thing for minister, instead of chemical industry medicine anti-dandruff and itching-relieving agent Zinc Pyrithione, not only to epidermis antibacterial, fungus, there is efficient inhibitory action, removing scurf and relieving itching successful, and use safer; With Cacumen Platycladi extract, Herba Ecliptae extract, Rhizoma Zingiberis Recens extract for adjuvant drug, decrease alopecia, promote kainogenesis length and black hair; With Radix Rhodiolae, Radix Polygoni Multiflori, Radix Ginseng extract, Radix Angelicae Sinensis extract, for making medicine, with can effective blood circulation promoting, provides nutrient to scalp, repair disconnectedly to send out, fork sends out, and improves hair quality; All medicine compatibilities, arrive while cleaning scalp, hair, make scalp more healthy, hair increases, and reduce dandruff, hair quality is shiny black submissive.The composition of stock solution of finally having one's hair wash is plant extract, does not produce the residue of harmful health and hostile environment, is of value to environmental protection.

Detailed description of the invention

Provide embodiment of the present invention draft hair care anticreep anti-dandruff shampoo stock solution component, preparation technology and effect assessment situation below, wherein component is according to parts by weight:

With the component proportion product of above-described embodiment 6, describe shampoo preparation method, and contrast with commercially available conventional daily use chemicals shampoo:

(1) matrix composition, add sodium laureth sulfate 30 parts, betanin 5 parts and soapberry extract 25 parts under room temperature stirring at low speed, mixing and stirring obtains shampoo substrate;

(2) component is added, regulate above-mentioned substrate pH value to neutral with citric acid, add Fructus Gleditsiae Abnormalis extract 7 parts successively, Cacumen Platycladi extract 8 parts, Radix Rhodiolae, Radix Polygoni Multiflori, Radix Ginseng combined extracting thing 9 parts, Radix Angelicae Sinensis extract 4 parts, Rhizoma Zingiberis Recens extract 5 parts, Herba Ecliptae extract 7 parts, Folium Ginkgo, Herba Taraxaci, Flos Lonicerae, Folium Mori combined extracting thing 6 parts;

Wherein,

Soapberry extract is dried at 60 ~ 80 DEG C by the pure peel of Fructus Sapindi Mukouossi, be crushed to 20 orders, then the pure water of 5 times of weight is added, soak at 60 ~ 80 DEG C and get filtrate in 24 hours, for the benefit of saponin fully discharges, filtrate preferably leaves standstill and within 10th, gets clear liquid and obtain, and for ensureing that Fructus Sapindi Mukouossi organic active thing is not destroyed, drying herein and soak can preferably 65 DEG C;

Fructus Gleditsiae Abnormalis extract soaks 24 hours in the 3 times of weight pure water being greater than 80 DEG C after Fructus Gleditsia squeezing, gets filtrate obtaining;

Rhizoma Zingiberis Recens extract is Rhizoma Zingiberis Recens squeezing and soaks 24 hours in 3 times of weight pure water of 40 ~ 60 DEG C, gets filtrate obtaining; For extracting Rhizoma Zingiberis Recens active substance to greatest extent, can destroy lifting biological cell structure by squeezing, after squeezing, Sucus Zingberis and slag soak simultaneously, temperature preferably 45 DEG C.

Cacumen Platycladi extract is that fresh Cacumen Platycladi is soaked in 45% ethanol of 5 times of weight, and after 5 days, filtrate was 80 ~ 85 DEG C of water-bath evaporations 2 ~ 3 hours, got clear liquid and obtained;

Herba Ecliptae extract is that Herba Ecliptae herb boils 15 minutes after 2 times of weight pure water soak, and gets filtrate obtaining;

Radix Rhodiolae, Radix Polygoni Multiflori and Radix Ginseng mixed extract, for ensureing extraction effect, these three kinds of preferred sliced forms of component, soak 2 hours in 3 times of pure water according to 1:2:1 weight, brewing 3 times, each 1 hour, centrifugalize after cooling, gets clear liquid and obtains;

Folium Ginkgo, Herba Taraxaci, Flos Lonicerae, Folium Mori combined extracting thing mix according to the weight ratio of 3:2:2:3, adds in 3 times of weight boiling water to soak after 8 ~ 10 hours to get filtrate obtaining;

Radix Angelicae Sinensis extract is dry Radix Angelicae Sinensis brewing 3 hours in 4 times of weight pure water, and filtrate obtaining is got in cooling.

The hair washing stock solution that above-mentioned manufacture method obtains, resultant effect evaluation and test situation refers to table 2:

Table 2, resultant effect evaluation and test table

It is as follows that the hair washing stock solution obtained above-mentioned manufacture method carries out human body effect experimental:

Inclusion criteria: 15 ~ 55 years old age, life-time service daily use chemicals shampoo, head has that hair is in various degree dry, dandruff and pruritus phenomenon, and men and women does not limit and selects 75 examples at random.Wherein first group of random selecting wherein 25 examples, use shampoo of the present invention instead, conventional amount used, use three times weekly, continue to use January more than; Second group of random selecting remains 25 examples in 50 examples, uses shampoo of the present invention instead, conventional amount used, uses twice weekly, continue use 1 week; Remain 25 examples as a control group, still adopt original shampoo, conventional amount used, week uses three times, continues use one month.

Effect standard:

Quan Xiao: hair quality is submissive, naked eyes are without visible dandruff, and pruritus phenomenon disappears completely;

Effective: hair is not tied a knot, naked eyes have fragmentary dandruff, without the sensation of head pruritus;

Invalid: unchanged before and after using;

Worsen: dandruff and pruritus phenomenon worsen.

Table 3 experiment effect table:

Result	First group	Second group	3rd group
				Quan Xiao	23	15	0
Effectively	2	9	1
				Invalid	0	1	12 5 -->
Worsen	0	0	13

As can be seen from the above table, continue to use shampoo of the present invention more than a week, good effect can be received, and continue to use more than shampoo of the present invention January, substantially full effect can be reached, not only hair quality is submissive, and dandruff and pruritus phenomenon can disappear completely, owing to adopting plant formula, crowd's suitability is up to more than 92%, and continue to use traditional daily chemical products, due to the use of organosilicon and zinc compound, constantly there is pruritus and dandruff corruptions.

Typical case:

Miss Li, 16 years old; Long hair, Miss's Li life-time service chemoprevention commercially available one day takes off shampoo, though hair is enough submissive, long-term scalp itch, after continuing to use shampoo provided by the present invention, hair is still submissive, dandruff without, scalp itch symptom becomes disappearance gradually by alleviating.

Mrs She, 31 years old, bob, used certain daily use chemicals conditioning shampoo commercially available before Mrs She, and hair is dry, and first use during shampoo provided by the present invention feels that scalp is totally salubrious, and comb gets up very smooth; Lasting use one month, present hair is smooth, has no dandruff and pruritus phenomenon.

Mr. Zhang, 53 years old, hair quality oiliness, usually with the submissive shampoo of certain daily use chemicals commercially available, although it is salubrious to wash rear hair, after interval half a day, hair starts again greasy pruritus, after employing shampoo provided by the present invention, clean effect is fine, and after using one week, the greasy phenomenon of hair is eliminated; After adhering to three weeks, hair washing interval can keep hair non-greasy in three days.

Mr. Tu, 41 years old, because seborrheic dermatitis causes alopecia, after using shampoo provided by the present invention 1 week, alopecia reduced, and substantially no longer alopecia after the 3rd month, new sending out is increased.

Mr. Zhang, 36 years old, because hair is always rare soft, dare not hair long, after using shampoo 400ml provided by the present invention, hair increases thick, Hardening, and after half a year, hair increases, hair long.

Above-described is only certain preferred embodiments of the present invention; it should be pointed out that for a person skilled in the art, under the prerequisite not departing from instant component proportioning and technique; can also make some improvement, these also should be considered as protection scope of the present invention.

Claims

1. the manufacture method of draft hair care anticreep anti-dandruff shampoo stock solution, it is characterized in that: prepare according to following technique, wherein component is with parts by weight: (1) matrix composition, add sodium laureth sulfate 30 parts, betanin 5 parts and soapberry extract 20 ~ 25 parts under room temperature stirring at low speed, mixing and stirring must be had one's hair wash stock solution substrate; (2) component is added, regulate above-mentioned substrate pH value to neutral with citric acid, add Fructus Gleditsiae Abnormalis extract 5 ~ 8 parts successively, Cacumen Platycladi extract 5 ~ 8 parts, Radix Rhodiolae, Radix Polygoni Multiflori, Radix Ginseng combined extracting thing 8 ~ 12 parts, Radix Angelicae Sinensis extract 4 ~ 6 parts, Rhizoma Zingiberis Recens extract 5 ~ 7 parts, Herba Ecliptae extract 5 ~ 7 parts, Folium Ginkgo, Herba Taraxaci, Flos Lonicerae, Folium Mori combined extracting thing 5 ~ 7 parts; (3) finished product makes, and add plant antiseptic agent 1 part, sterilization filling obtains finished product; Wherein, soapberry extract is dried at 60 ~ 80 DEG C by the pure peel of Fructus Sapindi Mukouossi, is crushed to 20 orders, then adds the pure water of 5 times of weight, soaks and gets filtrate in 24 hours, leave standstill and within 10th, get clear liquid and obtain at 60 ~ 80 DEG C; Fructus Gleditsiae Abnormalis extract is Fructus Gleditsia squeezing and soaks 24 hours in the 3 times of weight pure water being greater than 80 DEG C, gets filtrate obtaining; Rhizoma Zingiberis Recens extract is that Rhizoma Zingiberis Recens squeezing is soaked 24 hours in 3 times of weight pure water of 40 ~ 60 DEG C, gets filtrate obtaining; Cacumen Platycladi extract is that fresh Cacumen Platycladi is soaked in 45% ethanol of 5 times of weight, and after 5 days, filtrate was 80 ~ 85 DEG C of water-bath evaporations 2 ~ 3 hours, and remainder stays liquid to obtain; Herba Ecliptae extract is that Herba Ecliptae herb soaks half an hour at 2 times of weight pure water, boils 15 minutes, gets filtrate obtaining; Radix Rhodiolae, Radix Polygoni Multiflori and Radix Ginseng combined extracting thing, adopt these three kinds of components of sliced form, soak 2 hours in 3 times of pure water according to 1:2:1 weight, brewing 1 hour, strain dry, supplement 3 times of pure water, brewing 1 hour, strains dry again, supplement 3 times of pure water again, brewing 1 hour, 3 filtrate mixing also through centrifugalize, are got clear liquid and are obtained; Folium Ginkgo, Herba Taraxaci, Flos Lonicerae, Folium Mori combined extracting thing are mixed according to the weight ratio of 3:2:2:3 Folium Ginkgo, Herba Taraxaci, Flos Lonicerae, Folium Mori, adds the rear 3 times of weight boiling water immersion of mixing and get filtrate obtaining after 8 ~ 10 hours; Radix Angelicae Sinensis extract is dry Radix Angelicae Sinensis brewing 3 hours in 4 times of weight pure water, and filtrate obtaining is got in cooling.