CN108498410A - A kind of anti-dandruff nourishing shampoo of plant essence and preparation method thereof - Google Patents
A kind of anti-dandruff nourishing shampoo of plant essence and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
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- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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Abstract
The present invention provides a kind of anti-dandruff nourishings shampoo of plant essence and preparation method thereof, in the shampoo Chinese honey locust (fruit) extract liquor can anti-dandruff nourishing scalp, for monarch drug in a prescription；Thuja branch extract liquor can assist Chinese honey locust (fruit) extract liquor to treat alopecia seborrheica, be ministerial drug；Mulberry leaf extract fluid has effects that white hair blackening, is adjutant；Irascibility is moved back in chamomile extract liquor improving eyesight, and pacifying improves anaphylaxis skin quality, is nourished scalp, is kept the skin wet, to make medicine；Using above-mentioned Four Plants essence as primary efficacy part in shampoo provided by the invention, their mutual compatibilities, collaboration reaches removal dandruff, the effect of nourishing root of hair, supplement scalp nutrition；The shampoo is using sodium sulfate of polyethenoxy ether of fatty alcohol, lauric alcohol sodium sulphate, coconut oleoyl amine, Cocoamidopropyl betaine as surfactant, using lauric alcohol sodium sulphate as foaming agent, using poly hexamethylene biguanide as bacteriostatic preservative, major ingredient cooperation auxiliary material plays the dual anti-dandruff nourishes effect of Chinese and Western medicine.
Description
Technical field
The invention belongs to daily chemicals fields, and in particular to a kind of anti-dandruff nourishing shampoo of plant essence and preparation method thereof.
Background technology
Shampoo is a kind of hair care articles for cleaning scalp and hair, is widely used in the basic nursing of scalp.It is logical
Ingredient in normal shampoo is numerous, these ingredients synthesis plays the function of cleaning scalp and hair, and is played in shampoo clear
The main matter object surfactant of clean effect.And surfactant has taken away the dirt of scalp during cleaning scalp, but
It is the enough nutriments of the growth needs of hair, therefore the withered short-tempered of hair is be easy to cause using conventional shampoo.And
And the cleaning of hair is not only to remove the dirt of scalp and hair, scalp is usually also accompanied by obstinate dandruff, general
Shampoo is difficult effective removing dandruff.
Invention content
In order to solve the above technical problems, the present invention provide it is a kind of with anti-dandruff, nourish hair plant essence it is anti-dandruff
Shampoo and preparation method thereof is nourished, the anti-dandruff nourishing shampoo of plant essence is with removal of surfactant scalp and hair
In dirt, be with extract Chinese honey locust (fruit) extract liquor, thuja branch extract liquor, mulberry leaf extract fluid and the chamomile extract liquor of pure plant
Main nutritional supplement ingredient, various components coordinate jointly, while reaching decontamination, remove dandruff, nourish root of hair, optimization hair
The effect of matter.
The object of the present invention is to provide a kind of anti-dandruff nourishing shampoos of plant essence.
It is a further object of the present invention to provide a kind of anti-dandruff preparation methods for nourishing shampoo of above-mentioned plant essence.
According to the anti-dandruff nourishing shampoo of the plant essence of the specific embodiment of the invention, include the component of following parts by weight：
13~15 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, 3.5~4.5 parts of lauric alcohol sodium sulphate, coconut oleoyl amine 0.5~1
Part, 0.5~1 part of phthalic acid amide, 1.5~2 parts of Cocoamidopropyl betaine, 0.15~0.2 part of titanium dioxide, emulsification silicon
4~5 parts of oil, 0.08~0.12 part of citric acid, 0.8~1.2 part of sodium chloride, 10~12 parts of Chinese honey locust (fruit) extract liquor, thuja branch extraction
4.5~5.5 parts of liquid, 2.8~3.2 parts of mulberry leaf extract fluid, 1.8~2.2 parts of chamomile extract liquor, polyhexamethylene guanide 0.15~
0.3 part and 45~55 parts of water.
Preferably, further include 1~1.5 part of glycol distearate；It is further preferred that further including essence 0.5~0.6
Part.Glycol distearate is dissolved after being heated in surfactant complex or emulsification, and eyeglass can be precipitated in temperature-fall period
Shape crystallizes, thus generates nacreous lustre, and provided by the invention wash in aircraft contains a variety of surfactants, ethylene glycol distearyl
The addition of acid esters increases the effect of emulsification, and can increase the viscosity of shampoo, also have moisturize the skin, hair care hair care and
Anlistatig effect.The addition of essence increases the fragrance of shampoo, improves performance.
According to the anti-dandruff nourishing shampoo of the plant essence of the specific embodiment of the invention, it is preferable that including following parts by weight
Component：14.45 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, 4.05 parts of lauric alcohol sodium sulphate, 0.72 part of coconut oleoyl amine, ethylene glycol
1.28 parts of distearate, 0.76 part of phthalic acid amide, 1.64 parts of Cocoamidopropyl betaine, 0.17 part of titanium dioxide,
4.45 parts of silicone emulsion, 0.1 part of citric acid, 1 part of sodium chloride, 10.48 parts of Chinese honey locust (fruit) extract liquor, 5 parts of thuja branch extract liquor, mulberry leaf
50 parts of 3 parts of extract liquor, 2 parts of chamomile extract liquor, 0.3 part of polyhexamethylene guanide, 0.6 part of essence and water.
Invention provides a kind of anti-dandruff nourishing shampoo of plant essence, the present invention with plant extracts be main effect at
Point, it is lived as surface using sodium sulfate of polyethenoxy ether of fatty alcohol, lauric alcohol sodium sulphate, coconut oleoyl amine, Cocoamidopropyl betaine
Property agent, using lauric alcohol sodium sulphate as foaming agent, using poly hexamethylene biguanide as bacteriostatic preservative, in coordinating other auxiliary materials to play
The dual anti-dandruff nourishes effect of Western medicine.By reasonably matching carry out compatibility, collective effect, warp between component provided by the invention
Inventor is crossed the study found that when said components carry out compatibility with above-mentioned proportioning, there is more preferably anti-dandruff nourishes effect, plant to carry
The synergistic effect of object is taken to reach best.
According to the anti-dandruff preparation method for nourishing shampoo of the plant essence of the specific embodiment of the invention, including following step
Suddenly：
(1) Chinese honey locust (fruit) extract liquor is prepared：200~210 parts by weight of Chinese honey locust (fruit) are taken, 500~600 parts by weight water, heating is added
To 75~80 DEG C, it is ultrasonically treated, filtering takes filtrate, obtains 550~580 parts by weight extracting solutions, is then 75-80 DEG C in temperature,
Pressure is that distillation obtains Chinese honey locust (fruit) extract liquor to 150-160 parts by weight under -1~-0.5MPa；
(2) thuja branch extract liquor is prepared：Arbor-vitae 50-60 parts by weight are taken, the water of 280-320 parts by weight is added, is heated to 72-
It 76 DEG C, is ultrasonically treated, filtering takes filtrate, obtains the extracting solution of 300-320 parts by weight, is then 72-76 DEG C in temperature, pressure
Power is that distillation obtains thuja branch extract liquor to 105-110 parts by weight under -1~-0.5MPa；
(3) mulberry leaf extract fluid is prepared：25~35 parts by weight of mulberry leaf are taken, are crushed, the water of 220~300 parts by weight, heating is added
To 65~75 DEG C, be ultrasonically treated 60~75min, filtering, take filtrate, then temperature be 65~75 DEG C, pressure be -1~-
It is distilled under 0.5MPa, obtains mulberry leaf extract fluid；
(4) chamomile extract liquor is prepared：18~22 parts by weight of chamomile are taken, the water of 180~220 parts by weight, heating is added
To 85~95 DEG C, be ultrasonically treated 50~80min, filtering, take filtrate, then temperature be 85~95 DEG C, pressure be -1~-
It is distilled under 0.5MPa, obtains chamomile extract liquor；
(5) raw material is added to the water according to weight ratio, is heated to 40-55 DEG C, stirred evenly, it is cooling, obtain the plant
The anti-dandruff nourishing shampoo of object essence.Contain various plants extract in shampoo provided by the invention, it is first during preparation
It first passes through and prepares each extract, by heat treatment, accelerate plant cell water swelling, be ultrasonically treated so that in plant cell
Active ingredient dissolution, improve extraction efficiency, due to being rich in volatile effective component in plant extracts, the present invention is directed to
The characteristics of different plant extracts, extracts, and the extraction efficiency of obtained extract is high, and active constituent content is high, molecular weight
It is small, easily absorbed by scalp.
Preferably, in step (1), the time of supersound process is 60~75min.The time effects Chinese honey locust (fruit) of supersound process carries
The efficiency taken, during ultrasonic vibration, the microbubble dissolved in Chinese honey locust (fruit) aqueous solution generates cavitation effect, causes plant cell
The rupture of wall promotes the dissolution of active ingredient, and the quality of Chinese honey locust (fruit) is hard, during supersound process the time too short cause
Dissolution is incomplete, overlong time meeting waste of resource, and can not improve extraction efficiency, is the above-mentioned time when the time of ultrasound
When, extraction efficiency is high.
Preferably, in step (2), the time of supersound process is 45-60min.
Preferably, in step (3), the mulberry leaf crushed 20-200 mesh sieve.Mulberry leaf are obtained by being crushed to 20-200 mesh
For Mulberry Leaf in ultrasonic procedure, dissolution efficiency is high, and comprehensive benefit is best.
Preferably, in step (4), the edible salt of 2-3 parts by weight is added when supersound process into chamomile.In the mistake of ultrasound
Edible salt is added in journey, edible salt can change the permeability of cell, improve extraction efficiency.
Preferably, in step (5), the rate of stirring is 500-1500r/min, and the time of stirring is 15-30min.
Beneficial effects of the present invention are：
A kind of anti-dandruff nourishing shampoo of plant essence of present invention offer and preparation method thereof, Chinese honey locust (fruit) extracts in the shampoo
Take fluidity pungent-warm, external application hair washing, can anti-dandruff nourishing scalp, be monarch drug in a prescription；Thuja branch extract liquor cold nature, can assist Chinese honey locust (fruit)
Extract liquor treats alopecia seborrheica, is ministerial drug；Mulberry leaf extract fluid dispelling wind and heat from the body, clearing away the lungheat and moisturizing, clear liver and improve vision, and have white hair blackening
The effect of, it is adjutant；Irascibility is moved back in chamomile extract liquor improving eyesight, and pacifying improves anaphylaxis skin quality, is nourished scalp, is kept the skin wet, be
Make medicine；Using above-mentioned Four Plants essence as primary efficacy part in shampoo provided by the invention, mutual compatibility between them, altogether
The effect of same-action, collaboration reaches removal dandruff, nourishes root of hair, supplement scalp nutrition；The shampoo is with fatty alcohol polyoxy
Ethylene ether sodium sulfate, lauric alcohol sodium sulphate, coconut oleoyl amine, Cocoamidopropyl betaine are surfactant, with lauric alcohol sulphur
Sour sodium is foaming agent, using poly hexamethylene biguanide as bacteriostatic preservative, other auxiliary materials is coordinated to play dual anti-dandruff of Chinese and Western medicine
Nourishes effect.
Preparation method provided by the invention is fully extracted in plant by the method for low temperature ultrasonic extraction, vacuum distillation
Active ingredient utmostly retains the nutritional ingredient in plant, and extraction efficiency is high, and it is high to obtain activity substance content in shampoo；
It is easy to operate, it being capable of industrialized production.
Specific implementation mode
To make the object, technical solutions and advantages of the present invention clearer, technical scheme of the present invention will be carried out below
Detailed description.Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are obtained all without making creative work
Other embodiment belongs to the range that the present invention is protected.
Embodiment 1
The anti-dandruff nourishing shampoo of plant essence, includes the component of following weight：
Sodium sulfate of polyethenoxy ether of fatty alcohol 13kg, lauric alcohol sodium sulphate 3.5kg, coconut oleoyl amine 0.5kg, phthalic acid
Amide 0.5kg, Cocoamidopropyl betaine 1.5kg, titanium dioxide 0.15kg, silicone emulsion 4kg, citric acid 0.08kg, chlorination
Sodium 0.8kg, Chinese honey locust (fruit) extract liquor 10kg, thuja branch extract liquor 4.5kg, mulberry leaf extract fluid 2.8kg, chamomile extract liquor 1.8kg,
Polyhexamethylene guanide 0.15kg and water 55kg.
The anti-dandruff preparation method for nourishing shampoo of above-mentioned plant essence, includes the following steps：
(1) Chinese honey locust (fruit) extract liquor is prepared：200 parts by weight of Chinese honey locust (fruit) are taken, 500 parts by weight water are added, are heated to 75 DEG C, ultrasound
75min is handled, filtering takes filtrate, obtains 550 parts by weight extracting solutions, is then 75 DEG C in temperature, pressure is to be distilled under -1MPa
To 150 parts by weight, Chinese honey locust (fruit) extract liquor is obtained；
(2) thuja branch extract liquor is prepared：50 parts by weight of arbor-vitae are taken, the water of 280 parts by weight is added, are heated to 72 DEG C, ultrasound
60min is handled, filtering takes filtrate, obtains the extracting solution of 300 parts by weight, is then 72 DEG C in temperature, pressure is under -1MPa
Distillation obtains thuja branch extract liquor to 105 parts by weight；
(3) mulberry leaf extract fluid is prepared：25 parts by weight of mulberry leaf are taken, are crushed, the water of 220 parts by weight is added, is heated to 65 DEG C, are surpassed
Sonication 75min, filtering, takes filtrate, is then 65 DEG C in temperature, pressure is to be distilled under -1MPa, obtains mulberry leaf extract fluid；
(4) chamomile extract liquor is prepared：18 parts by weight of chamomile are taken, the water of 180 parts by weight is added, is heated to 85 DEG C, are surpassed
Sonication 80min, filtering, takes filtrate, is then 85 DEG C in temperature, pressure is to be distilled under -1MPa, obtains chamomile extract liquor；
(5) raw material is added to the water according to weight ratio, is heated to 40 DEG C, stirs evenly, it is cooling, obtain the plant essence
The anti-dandruff nourishing shampoo of China.
Embodiment 2
The anti-dandruff nourishing shampoo of plant essence, includes the component of following weight：
Sodium sulfate of polyethenoxy ether of fatty alcohol 15kg, lauric alcohol sodium sulphate 4.5kg, coconut oleoyl amine 1kg, phthalic acid acyl
Amine 1kg, Cocoamidopropyl betaine 2kg, titanium dioxide 0.2kg, silicone emulsion 5kg, citric acid 0.12kg, sodium chloride 1.2kg,
Chinese honey locust (fruit) extract liquor 12kg, thuja branch extract liquor 5.5kg, mulberry leaf extract fluid 3.2kg, chamomile extract liquor 2.2kg, poly- six methylene
Base guanidine 0.3kg and water 50kg.
The anti-dandruff preparation method for nourishing shampoo of above-mentioned plant essence, includes the following steps：
(1) Chinese honey locust (fruit) extract liquor is prepared：210 parts by weight of Chinese honey locust (fruit) are taken, 600 parts by weight water are added, are heated to 80 DEG C, ultrasound
60min is handled, filtering takes filtrate, obtains 580 parts by weight extracting solutions, is then 80 DEG C in temperature, pressure is to be steamed under -0.5MPa
It evaporates to 160 parts by weight, obtains Chinese honey locust (fruit) extract liquor；
(2) thuja branch extract liquor is prepared：60 parts by weight of arbor-vitae are taken, the water of 320 parts by weight is added, are heated to 76 DEG C, ultrasound
45min is handled, filtering takes filtrate, obtains the extracting solution of 320 parts by weight, is then 76 DEG C in temperature, pressure is -0.5MPa
Lower distillation obtains thuja branch extract liquor to 110 parts by weight；
(3) mulberry leaf extract fluid is prepared：35 parts by weight of mulberry leaf are taken, are crushed, the water of 300 parts by weight is added, is heated to 75 DEG C, are surpassed
Sonication 60min, filtering, takes filtrate, is then 75 DEG C in temperature, pressure is to be distilled under -0.5MPa, obtains mulberry leaf extraction
Liquid；
(4) chamomile extract liquor is prepared：22 parts by weight of chamomile are taken, the water of 220 parts by weight is added, is heated to 95 DEG C, are surpassed
Sonication 50min, filtering, takes filtrate, is then 95 DEG C in temperature, pressure is to be distilled under -0.5MPa, obtains chamomile extraction
Liquid；
(5) raw material is added to the water according to weight ratio, is heated to 55 DEG C, stirs evenly, it is cooling, obtain the plant essence
The anti-dandruff nourishing shampoo of China.
Embodiment 3
The anti-dandruff nourishing shampoo of plant essence, includes the component of following weight：
Sodium sulfate of polyethenoxy ether of fatty alcohol 15kg, lauric alcohol sodium sulphate 4.5kg, coconut oleoyl amine 1kg, ethylene glycol distearyl
Acid esters 1kg, phthalic acid amide 1kg, Cocoamidopropyl betaine 2kg, titanium dioxide 0.2kg, silicone emulsion 5kg, lemon
Sour 0.12kg, sodium chloride 1.2kg, Chinese honey locust (fruit) extract liquor 12kg, thuja branch extract liquor 5.5kg, mulberry leaf extract fluid 3.2kg, ocean are sweet
Chrysanthemum extract liquor 2.2kg, polyhexamethylene guanide 0.15kg and water 45kg
The anti-dandruff preparation method for nourishing shampoo of above-mentioned plant essence, includes the following steps：
(1) Chinese honey locust (fruit) extract liquor is prepared：200 parts by weight of Chinese honey locust (fruit) are taken, 500 parts by weight water are added, are heated to 75 DEG C, ultrasound
70min is handled, filtering takes filtrate, obtains 550 parts by weight extracting solutions, is then 75 DEG C in temperature, pressure is to be steamed under -0.8MPa
It evaporates to 150 parts by weight, obtains Chinese honey locust (fruit) extract liquor；
(2) thuja branch extract liquor is prepared：50 parts by weight of arbor-vitae are taken, the water of 300 parts by weight is added, are heated to 75 DEG C, ultrasound
Handle 50min, filtering, take filtrate, obtain the extracting solution of 300-320 parts by weight, then temperature be 75 DEG C, pressure be-
Distillation obtains thuja branch extract liquor to 1058 parts by weight under 1MPa；
(3) mulberry leaf extract fluid is prepared：30 parts by weight of mulberry leaf are taken, 20 mesh sieve is crushed, the water of 250 parts by weight, heating is added
To 70 DEG C, it is ultrasonically treated 70min, filtering takes filtrate, is then 70 DEG C in temperature, pressure is to be distilled under -1MPa, obtains mulberry
Leaf extract liquor；
(4) chamomile extract liquor is prepared：20 parts by weight of chamomile are taken, the water of 200 parts by weight is added, is heated to 90 DEG C, are surpassed
Sonication 60min, filtering, takes filtrate, is then 90 DEG C in temperature, pressure is to be distilled under -1MPa, obtains chamomile extract liquor；
(5) raw material is added to the water according to weight ratio, is heated to 50 DEG C, stirs evenly, the rate of the stirring is
The time of 500r/min, stirring are 30min, cooling, obtain the anti-dandruff nourishing shampoo of the plant essence.
Embodiment 4
The anti-dandruff nourishing shampoo of plant essence, includes the component of following weight：
Sodium sulfate of polyethenoxy ether of fatty alcohol 15kg, lauric alcohol sodium sulphate 4.5kg, coconut oleoyl amine 1kg, ethylene glycol distearyl
Acid esters 1.5kg, phthalic acid amide 1kg, Cocoamidopropyl betaine 2kg, titanium dioxide 0.2kg, silicone emulsion 5kg, lemon
Lemon acid 0.12kg, sodium chloride 1.2kg, Chinese honey locust (fruit) extract liquor 12kg, thuja branch extract liquor 5.5kg, mulberry leaf extract fluid 3.2kg are foreign
Camomile extract liquor 2.2kg, polyhexamethylene guanide 0.15kg, essence 0.5kg and water 45kg
The anti-dandruff preparation method for nourishing shampoo of above-mentioned plant essence, includes the following steps：
(1) Chinese honey locust (fruit) extract liquor is prepared：200 parts by weight of Chinese honey locust (fruit) are taken, 500 parts by weight water are added, are heated to 75 DEG C, ultrasound
70min is handled, filtering takes filtrate, obtains 550 parts by weight extracting solutions, is then 75 DEG C in temperature, pressure is to be steamed under -0.8MPa
It evaporates to 150 parts by weight, obtains Chinese honey locust (fruit) extract liquor；
(2) thuja branch extract liquor is prepared：50 parts by weight of arbor-vitae are taken, the water of 300 parts by weight is added, are heated to 75 DEG C, ultrasound
Handle 50min, filtering, take filtrate, obtain the extracting solution of 300-320 parts by weight, then temperature be 75 DEG C, pressure be-
Distillation obtains thuja branch extract liquor to 1058 parts by weight under 1MPa；
(3) mulberry leaf extract fluid is prepared：30 parts by weight of mulberry leaf are taken, 200 mesh sieve is crushed, the water of 250 parts by weight, heating is added
To 70 DEG C, it is ultrasonically treated 70min, filtering takes filtrate, is then 70 DEG C in temperature, pressure is to be distilled under -1MPa, obtains mulberry
Leaf extract liquor；
(4) chamomile extract liquor is prepared：20 parts by weight of chamomile are taken, the water of 200 parts by weight is added, is heated to 90 DEG C, adds
Enter 3 parts by weight of salt, be ultrasonically treated 60min, filtering takes filtrate, is then 90 DEG C in temperature, pressure is to be distilled under -1MPa, is obtained
To chamomile extract liquor；
(5) raw material is added to the water according to weight ratio, is heated to 50 DEG C, stirs evenly, the rate of the stirring is
The time of 1500r/min, stirring are 15min, cooling, obtain the anti-dandruff nourishing shampoo of the plant essence.
Embodiment 5
The anti-dandruff nourishing shampoo of plant essence, includes the component of following weight：
Sodium sulfate of polyethenoxy ether of fatty alcohol 14.45kg, lauric alcohol sodium sulphate 4.05kg, coconut oleoyl amine 0.72kg, second two
Alcohol distearate 1.28kg, phthalic acid amide 0.76kg, Cocoamidopropyl betaine 1.64kg, titanium dioxide
0.17kg, silicone emulsion 4.45kg, citric acid 0.1kg, sodium chloride 1kg, Chinese honey locust (fruit) extract liquor 10.48kg, thuja branch extract liquor
5kg, mulberry leaf extract fluid 3kg, chamomile extract liquor 2kg, polyhexamethylene guanide 0.3kg, essence 0.6kg and water 50kg.
The anti-dandruff preparation method for nourishing shampoo of above-mentioned plant essence, includes the following steps：
(1) Chinese honey locust (fruit) extract liquor is prepared：200 parts by weight of Chinese honey locust (fruit) are taken, 500 parts by weight water are added, are heated to 75 DEG C, ultrasound
70min is handled, filtering takes filtrate, obtains 550 parts by weight extracting solutions, is then 75 DEG C in temperature, pressure is to be steamed under -0.8MPa
It evaporates to 150 parts by weight, obtains Chinese honey locust (fruit) extract liquor；
(2) thuja branch extract liquor is prepared：50 parts by weight of arbor-vitae are taken, the water of 300 parts by weight is added, are heated to 75 DEG C, ultrasound
Handle 50min, filtering, take filtrate, obtain the extracting solution of 300-320 parts by weight, then temperature be 75 DEG C, pressure be-
Distillation obtains thuja branch extract liquor to 1058 parts by weight under 1MPa；
(3) mulberry leaf extract fluid is prepared：It takes 30 parts by weight of mulberry leaf, crushing to sieve with 100 mesh sieve, the water of 250 parts by weight, heating is added
To 70 DEG C, it is ultrasonically treated 70min, filtering takes filtrate, is then 70 DEG C in temperature, pressure is to be distilled under -1MPa, obtains mulberry
Leaf extract liquor；
(4) chamomile extract liquor is prepared：20 parts by weight of chamomile are taken, the water of 200 parts by weight is added, is heated to 90 DEG C, adds
Enter 2 parts by weight of salt, be ultrasonically treated 60min, filtering takes filtrate, is then 90 DEG C in temperature, pressure is to be distilled under -1MPa, is obtained
To chamomile extract liquor；
(5) raw material is added to the water according to weight ratio, is heated to 50 DEG C, stirs evenly, the rate of the stirring is
The time of 500r/min, stirring are 30min, cooling, obtain the anti-dandruff nourishing shampoo of the plant essence.
Test example
It is checked according to the QB/T 1974-2004 shampoos obtained to embodiment 5, wherein hygienic testing result is shown in Table
1, sense organ, physical and chemical index testing result are shown in Table 2.
The sanitary index testing result of 1 shampoo provided by the invention of table
The sense organ of 2 shampoo provided by the invention of table, physical and chemical index testing result
Shampoo provided by the invention is can be seen that from the result of Tables 1 and 2 and complies with standard regulation, contains high level
Active principle.
The present invention is on probation by 150 volunteers, the results showed that non-stimulated, no allergic reaction can be effectively relieved and go
Except dandruff, after 30 days, the hair quality of the hair of volunteer is clearly better, and hair water moistens, is pitch-black, having gloss.This
Illustrate that shampoo provided by the invention has the effect of high security performance and good removal dandruff, nourishes hair.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. a kind of anti-dandruff nourishing shampoo of plant essence, which is characterized in that include the component of following parts by weight：
13~15 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, 3.5~4.5 parts of lauric alcohol sodium sulphate, 0.5~1 part of coconut oleoyl amine are adjacent
0.5~1 part of phthalic acid amide, 1.5~2 parts of Cocoamidopropyl betaine, 0.15~0.2 part of titanium dioxide, silicone emulsion 4~
5 parts, 0.08~0.12 part of citric acid, 0.8~1.2 part of sodium chloride, 10~12 parts of Chinese honey locust (fruit) extract liquor, thuja branch extract liquor 4.5
~5.5 parts, 2.8~3.2 parts of mulberry leaf extract fluid, 1.8~2.2 parts of chamomile extract liquor, 0.15~0.3 part of polyhexamethylene guanide and
45~55 parts of water.
2. the anti-dandruff nourishing shampoo of plant essence according to claim 1, which is characterized in that further include ethylene glycol distearyl
1~1.5 part of acid esters.
3. the anti-dandruff nourishing shampoo of plant essence according to claim 2, which is characterized in that further include essence 0.5~0.6
Part.
4. the anti-dandruff nourishing shampoo of plant essence according to claim 3, which is characterized in that include the group of following parts by weight
Point：14.45 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, 4.05 parts of lauric alcohol sodium sulphate, 0.72 part of coconut oleoyl amine, ethylene glycol two are hard
1.28 parts of resin acid ester, 0.76 part of phthalic acid amide, 1.64 parts of Cocoamidopropyl betaine, 0.17 part of titanium dioxide, emulsification
4.45 parts of silicone oil, 0.1 part of citric acid, 1 part of sodium chloride, 10.48 parts of Chinese honey locust (fruit) extract liquor, 5 parts of thuja branch extract liquor, mulberry leaf extraction
50 parts of 3 parts of liquid, 2 parts of chamomile extract liquor, 0.3 part of polyhexamethylene guanide, 0.6 part of essence and water.
5. the anti-dandruff preparation method for nourishing shampoo of any plant essence of Claims 1 to 4, which is characterized in that including
Following steps：
(1) Chinese honey locust (fruit) extract liquor is prepared：200~210 parts by weight of Chinese honey locust (fruit) are taken, 500~600 parts by weight water are added, are heated to 75
It~80 DEG C, is ultrasonically treated, filtering takes filtrate, obtains 550~580 parts by weight extracting solutions, is then 75-80 DEG C in temperature, pressure
For distillation under -1~-0.5MPa Chinese honey locust (fruit) extract liquor is obtained to 150-160 parts by weight；
(2) thuja branch extract liquor is prepared：Arbor-vitae 50-60 parts by weight are taken, the water of 280-320 parts by weight is added, is heated to 72-76
DEG C, it is ultrasonically treated, filtering takes filtrate, obtains the extracting solution of 300-320 parts by weight, is then 72-76 DEG C in temperature, pressure
For distillation under -1~-0.5MPa thuja branch extract liquor is obtained to 105-110 parts by weight；
(3) mulberry leaf extract fluid is prepared：25~35 parts by weight of mulberry leaf are taken, are crushed, the water of 220~300 parts by weight is added, is heated to 65
~75 DEG C, it is ultrasonically treated 60~75min, filtering takes filtrate, is then 65~75 DEG C in temperature, pressure is -1~-0.5MPa
Lower distillation, obtains mulberry leaf extract fluid；
(4) chamomile extract liquor is prepared：18~22 parts by weight of chamomile are taken, the water of 180~220 parts by weight is added, is heated to 85
~95 DEG C, it is ultrasonically treated 50~80min, filtering takes filtrate, is then 85~95 DEG C in temperature, pressure is under -1~-0.5MPa
Distillation, obtains chamomile extract liquor；
(5) raw material is added to the water according to weight ratio, is heated to 40-55 DEG C, stirred evenly, it is cooling, obtain the plant essence
The anti-dandruff nourishing shampoo of China.
6. the anti-dandruff preparation method for nourishing shampoo of plant essence according to claim 4, which is characterized in that step (1)
In, the time of supersound process is 60~75min.
7. the anti-dandruff preparation method for nourishing shampoo of plant essence according to claim 4, which is characterized in that step (2)
In, the time of supersound process is 45-60min.
8. the anti-dandruff preparation method for nourishing shampoo of plant essence according to claim 4, which is characterized in that step (3)
In, the mulberry leaf crushed 20-200 mesh sieve.
9. the anti-dandruff preparation method for nourishing shampoo of plant essence according to claim 4, which is characterized in that step (4)
In, the edible salt of 2-3 parts by weight is added when supersound process into chamomile.
10. the anti-dandruff preparation method for nourishing shampoo of plant essence according to claim 4, which is characterized in that step (5)
In, the rate of stirring is 500-1500r/min, and the time of stirring is 15-30min.
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Application publication date: 20180907 |